CN108889083A - A kind of efficiently removal formaldehyde air purifying preparation - Google Patents
A kind of efficiently removal formaldehyde air purifying preparation Download PDFInfo
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- CN108889083A CN108889083A CN201810809663.6A CN201810809663A CN108889083A CN 108889083 A CN108889083 A CN 108889083A CN 201810809663 A CN201810809663 A CN 201810809663A CN 108889083 A CN108889083 A CN 108889083A
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- extract
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- air purifying
- lemon
- epipremnum aureum
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- QPHXPNUXTNHJOF-UHFFFAOYSA-N quercetin-7-O-beta-L-rhamnopyranoside Natural products OC1C(O)C(O)C(C)OC1OC1=CC(O)=C2C(=O)C(O)=C(C=3C=C(O)C(O)=CC=3)OC2=C1 QPHXPNUXTNHJOF-UHFFFAOYSA-N 0.000 description 1
- OXGUCUVFOIWWQJ-HQBVPOQASA-N quercitrin Chemical compound O[C@@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@H]1OC1=C(C=2C=C(O)C(O)=CC=2)OC2=CC(O)=CC(O)=C2C1=O OXGUCUVFOIWWQJ-HQBVPOQASA-N 0.000 description 1
- 201000010727 rectal prolapse Diseases 0.000 description 1
- 208000023504 respiratory system disease Diseases 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
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- IKGXIBQEEMLURG-BKUODXTLSA-N rutin Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@@H]1OC[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](OC=2C(C3=C(O)C=C(O)C=C3OC=2C=2C=C(O)C(O)=CC=2)=O)O1 IKGXIBQEEMLURG-BKUODXTLSA-N 0.000 description 1
- 235000005493 rutin Nutrition 0.000 description 1
- 229960004555 rutoside Drugs 0.000 description 1
- 239000012488 sample solution Substances 0.000 description 1
- 208000005687 scabies Diseases 0.000 description 1
- 231100000241 scar Toxicity 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 210000000952 spleen Anatomy 0.000 description 1
- 208000000995 spontaneous abortion Diseases 0.000 description 1
- 150000003431 steroids Chemical class 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- ZPHGMBGIFODUMF-UHFFFAOYSA-N thiophen-2-ylmethanol Chemical compound OCC1=CC=CS1 ZPHGMBGIFODUMF-UHFFFAOYSA-N 0.000 description 1
- 150000003648 triterpenes Chemical class 0.000 description 1
- 150000008130 triterpenoid saponins Chemical class 0.000 description 1
- 230000010415 tropism Effects 0.000 description 1
- 208000009852 uremia Diseases 0.000 description 1
- PLSAJKYPRJGMHO-UHFFFAOYSA-N ursolic acid Natural products CC1CCC2(CCC3(C)C(C=CC4C5(C)CCC(O)C(C)(C)C5CCC34C)C2C1C)C(=O)O PLSAJKYPRJGMHO-UHFFFAOYSA-N 0.000 description 1
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- 239000002699 waste material Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/1487—Removing organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/1493—Selection of liquid materials for use as absorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/72—Organic compounds not provided for in groups B01D53/48 - B01D53/70, e.g. hydrocarbons
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/77—Liquid phase processes
- B01D53/78—Liquid phase processes with gas-liquid contact
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
- B01D2252/20—Organic absorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
- B01D2252/50—Combinations of absorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
- B01D2257/708—Volatile organic compounds V.O.C.'s
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Environmental & Geological Engineering (AREA)
- Health & Medical Sciences (AREA)
- Biomedical Technology (AREA)
- Fats And Perfumes (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The present invention provides a kind of efficiently removal formaldehyde air purifying preparation, and the raw material for preparing of the efficient removal formaldehyde air purifying preparation includes at least：Lemon extract, jasmine extract, tea tree extract, Flos Osmanthi Fragrantis extract, Lignum cinnamomi camphorae extract, epipremnum aureum extract, bracketplant extract, eucalyptus extracts, Extractives From Melia Azedarach L, the white palm and epipremnum aureum extract, Fructus Gleditsiae Abnormalis extract, Gotu Kola P.E, Herba Asari extract, Fructus Kochiae extract, cimicifuga foetida extract, second alcohol and water；Efficient removal formaldehyde air purifying preparation source provided by the invention is mainly plant extracts, does not generate secondary pollution.
Description
Technical field
The invention belongs to technical field of air purification, specifically, being related to a kind of efficiently removal formaldehyde air purifying preparation.
Background technique
With the raising of people's awareness of environment protection and health, the requirement to house decorative material is higher and higher, commonly uses decoration material
Material can gradually release the pernicious gases such as formaldehyde during use.Formaldehyde is colourless gas, irritant smell, a large amount of to suck
Formaldehyde can make one to suffer from respiratory disease, nasopharyngeal carcinoma, uremia, and jeopardize pregnant woman's miscarriage, fetal anomaly, children's high probability
Leukaemia etc..State health standards regulation, indoor formaldehyde concentration limit value is 0.1 milligram every cubic metre, indoor at this stage in China
Household is limited by all kinds of ornament materials not environmentally, and especially newly-decorated room causes content of formaldehyde higher.The danger of formaldehyde
The harmful prevention and treatment with formaldehyde also increasingly attracts people's attention.
There are many kinds of the control methods of formaldehyde, general using windowing ventilation for a long time, places green plant, activated carbon adsorption class material
Material, air purifier or all kinds of formaldehyde scavengers of selection, biological enzyme carry out construction processing using certain process.These
Method to a certain extent can the harmful substances such as PARA FORMALDEHYDE PRILLS(91,95) handled, eliminate.
Currently, the major technique for eliminating formaldehyde is using active carbon as adsorbent, such method is relatively simple, but
Purification cycle is long, and active carbon needs to regularly replace.
The measure and method for taking science purify indoor pollution air, reduce air pollution to the danger of human health
Evil has become the task of top priority.
Summary of the invention
The present invention provides a kind of efficiently removal formaldehyde air purifying preparation, the preparation of the efficient removal formaldehyde air purifying preparation
Raw material includes at least：Lemon extract, jasmine extract, tea tree extract, Flos Osmanthi Fragrantis extract, Lignum cinnamomi camphorae extract, epipremnum aureum are extracted
Object, bracketplant extract, eucalyptus extracts, Extractives From Melia Azedarach L, the white palm and epipremnum aureum extract, Fructus Gleditsiae Abnormalis extract, centella are extracted
Object, Herba Asari extract, Fructus Kochiae extract, cimicifuga foetida extract, second alcohol and water.
As one embodiment of the present invention, by weight, the preparation of the efficient removal formaldehyde air purifying preparation
Raw material includes at least：1-5 parts of lemon extract, 1-3 parts of jasmine extract, 0.1-1.5 parts of tea tree extract, Flos Osmanthi Fragrantis extract
5-10 parts, 1-3 parts of Lignum cinnamomi camphorae extract, 1-5 parts of epipremnum aureum extract, 5-15 parts of bracketplant extract, 0.1-0.5 parts of eucalyptus extracts,
1-3 parts of Extractives From Melia Azedarach L, it is white the palm and 5-10 part of epipremnum aureum extract, 1-8 parts of Fructus Gleditsiae Abnormalis extract, 1-3 parts of Gotu Kola P.E, carefully
Pungent extract 0.5-1.5 parts, 1.5-3.5 parts of Fructus Kochiae extract, 3.5-6.5 parts of cimicifuga foetida extract, 0.1-3 parts of ethyl alcohol and water
50-60 parts.
As one embodiment of the present invention, by weight, the preparation of the efficient removal formaldehyde air purifying preparation
Raw material includes at least：3 parts of lemon extract, 2 parts of jasmine extract, 0.8 part of tea tree extract, 6 parts of Flos Osmanthi Fragrantis extract, camphor tree
2 parts of extract, 3 parts of epipremnum aureum extract, 8 parts of bracketplant extract, 0.3 part of eucalyptus extracts, 2 parts of Extractives From Melia Azedarach L, it is white the palm and
8 parts of epipremnum aureum extract, 5 parts of Fructus Gleditsiae Abnormalis extract, 2 parts of Gotu Kola P.E, 1.1 parts of Herba Asari extract, Fructus Kochiae extract 2.0
Part, 4.3 parts of cimicifuga foetida extract, 2.1 parts of ethyl alcohol and 55 parts of water.
As one embodiment of the present invention, the raw material for preparing of the efficient removal formaldehyde air purifying preparation also includes stone
10-15 parts and flaxseed gum 5-10 parts of calamus extract.
As one embodiment of the present invention, the flaxseed gum passes through combined processing, and the combined processing step is such as
Under：
Containing hydrogen silicone oil, divinylbenzene and chloroplatinic acid are 6 by S01 in mass ratio：3：1 hands at 120 DEG C after mixing
After connection reaction 12 hours, solid 1 is obtained；
Solid 1, cellulose and sepiolite powder are 1 by S02 in mass ratio：1：Ball milling 16 hours after 2 mixing；
S03 will obtain mixture and enclose lower high-temperature calcination in Ar atmosphere in S02；
S04 carries out acid etch to the calcined powder of S03 using hydrofluoric acid solution, and flaxseed gum is added after being washed to neutrality
Solution is warming up to 50 DEG C, after mixing evenly, can be prepared.
As one embodiment of the present invention, in the S03, the process of high-temperature calcination is as follows：
Being sintered initial temperature is 60 DEG C, rises to 500 DEG C with the speed of 2.5 DEG C/min, keeps the temperature 60min；Again with 6 DEG C/min's
Speed is warming up to 1200 DEG C and continues furnace cooling after 2 hours again.
As one embodiment of the present invention, in the S04, the flaxseed gum solution be formulated as flaxseed gum and
Water is 7 according to weight ratio：10.
As one embodiment of the present invention, in the S04, the concentration of the hydrofluoric acid solution is 18%, when etching
Between be 5 hours.
As one embodiment of the present invention, the extracting method of the lemon extract is as follows：
(1) Fresh Lemon is squeezed broken, takes clear lemon fluid；
(2) by lemon fluid and formic acid obtained in step (1) according to 20：1 mixing, can be prepared lemon extract.
As one embodiment of the present invention, the preparation method of the Fructus Kochiae extract is as follows：
The extracting method of Fructus Kochiae extract is to clean the fruit of summer cypress, chopping, is impregnated for 24 hours with yellow rice wine, is then dried, and is used
Water decocts 3 times, and using jujube and ginger as medicine efficacy enhancing ingredient, the weight ratio of water and the fruit of summer cypress is 8：1,40min is decocted every time, is merged and is decocted
Boil liquid, vacuum drying to get.
Beneficial effect：
1, efficient removal formaldehyde air purifying preparation source provided by the invention is mainly plant extracts, does not generate secondary dirt
Dye；
2, efficient removal formaldehyde air purifying preparation raw material provided by the invention is simple, and ingredient is cheap, and manufacturing process is simple.
Specific embodiment
For the purpose of following detailed description, it should be understood that the present invention can be used various substitutions variation and step it is suitable
Sequence, unless specifically stated on the contrary.In addition, in the case where in addition in any operational instances or otherwise pointing out, table
All numbers of the amount of example ingredient as used in description and claims should be understood in all cases by term
" about " it modifies.Therefore, unless indicated to the contrary, the numerical parameter otherwise illustrated in the following description and appended dependent claims is
The expected performance to be obtained according to the present invention and the approximation changed.It is at least not intended to the applicable limit of doctrine of equivalents
Within the scope of the claims, each numerical parameter at least according to the number of the effective digital of report and should pass through application to system
Common rounding-off technology is explained.
Although illustrating that broad range of numberical range and parameter of the invention are approximations, listed in specific example
Numerical value is reported as accurately as possible.However, any numerical value inherently includes the standard deviation by finding in its each self-test measurement
The certain errors necessarily led to.
In addition, it should be understood that any numberical range as described herein, which is intended to include, is included into all subranges therein.Example
Such as, the range of " 1 to 10 " is intended to include all sub- models between (and including) described minimum value 1 and the maximum value 10
It encloses, that is, there is the minimum value equal to or more than 1 and the maximum value equal to or less than 10.
The present invention provides a kind of efficiently removal formaldehyde air purifying preparation, the preparation of the efficient removal formaldehyde air purifying preparation
Raw material includes at least：Lemon extract, jasmine extract, tea tree extract, Flos Osmanthi Fragrantis extract, Lignum cinnamomi camphorae extract, epipremnum aureum are extracted
Object, bracketplant extract, eucalyptus extracts, Extractives From Melia Azedarach L, the white palm and epipremnum aureum extract, Fructus Gleditsiae Abnormalis extract, centella are extracted
Object, Herba Asari extract, Fructus Kochiae extract, cimicifuga foetida extract, second alcohol and water.
As one embodiment of the present invention, by weight, the preparation of the efficient removal formaldehyde air purifying preparation
Raw material includes at least：1-5 parts of lemon extract, 1-3 parts of jasmine extract, 0.1-1.5 parts of tea tree extract, Flos Osmanthi Fragrantis extract
5-10 parts, 1-3 parts of Lignum cinnamomi camphorae extract, 1-5 parts of epipremnum aureum extract, 5-15 parts of bracketplant extract, 0.1-0.5 parts of eucalyptus extracts,
1-3 parts of Extractives From Melia Azedarach L, it is white the palm and 5-10 part of epipremnum aureum extract, 1-8 parts of Fructus Gleditsiae Abnormalis extract, 1-3 parts of Gotu Kola P.E, carefully
Pungent extract 0.5-1.5 parts, 1.5-3.5 parts of Fructus Kochiae extract, 3.5-6.5 parts of cimicifuga foetida extract, 0.1-3 parts of ethyl alcohol and water
50-60 parts.
As one embodiment of the present invention, by weight, the preparation of the efficient removal formaldehyde air purifying preparation
Raw material includes at least：3 parts of lemon extract, 2 parts of jasmine extract, 0.8 part of tea tree extract, 6 parts of Flos Osmanthi Fragrantis extract, camphor tree
2 parts of extract, 3 parts of epipremnum aureum extract, 8 parts of bracketplant extract, 0.3 part of eucalyptus extracts, 2 parts of Extractives From Melia Azedarach L, it is white the palm and
8 parts of epipremnum aureum extract, 5 parts of Fructus Gleditsiae Abnormalis extract, 2 parts of Gotu Kola P.E, 1.1 parts of Herba Asari extract, Fructus Kochiae extract 2.0
Part, 4.3 parts of cimicifuga foetida extract, 2.1 parts of ethyl alcohol and 55 parts of water.
As one embodiment of the present invention, the raw material for preparing of the efficient removal formaldehyde air purifying preparation also includes stone
10-15 parts and flaxseed gum 5-10 parts of calamus extract.
Lemon extract
The extracting method of the lemon extract is as follows：
(1) Fresh Lemon is squeezed broken, takes clear lemon fluid；
(2) by lemon fluid and formic acid obtained in step (1) according to 20：1 mixing, can be prepared lemon extract.
Jasmine extract
The extracting method of heretofore described jasmine extract is as follows：1. four-o'clock herb is dried in the shade, with plant pulverizer
It crushes, crosses 40 meshes, add 2~10 times of 95% ethyl alcohol of amount, be stored at room temperature extraction 1~7 day, centre is stirred often, is filtered, must be soaked
Extract；2~10 times of 95% alcohol steeps of amount are added in filter residue again, so extract three times, merge leaching liquor three times, are steamed with rotation
It sends out instrument to be concentrated under reduced pressure, obtains dark brown stiff paste form up to Radix Mirabilis extract of the present invention；2. four-o'clock herb is dried in the shade, with plant
Object pulverizer crushes, and crosses 40 meshes, adds 2~10 times of 95% ethyl alcohol of amount, refluxing extraction 5~15 hours, filtering obtained refluxing extraction
Liquid is concentrated under reduced pressure with Rotary Evaporators, obtains stiff paste form up to this Radix Mirabilis extract.
Tea tree extract
The extracting method of heretofore described tea tree extract is as follows：The blade of tea tree is chosen, after cleaning, takes 20g leaf,
Without crushing, steam distillation is carried out to complete leaf, distillation time is 18 hours, removes thick slag, obtains oily mater
Afterwards, after -10 DEG C freeze 12 hours, moisture removal is removed in air-distillation, then freezes the grease of acquisition 24 hours at -10 DEG C
Afterwards, grease is removed, thick slag is taken, after thick slag heating melting, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil
Tea tree ethereal oil is prepared.
Flos Osmanthi Fragrantis extract
The Flos Osmanthi Fragrantis extract is bought from Xi'an Jin Di Biotechnology Co., Ltd.
Lignum cinnamomi camphorae extract
Camphor tree alias：Camphor tree material, lignum cinnamomi camphorae, oblongleaf kadsura stem or root；Channel tropism：It is acrid in flavour and warm in nature；Major function：It is sensible to ward off dirty, warm in pain, benefit
Wet desinsection.It vomits and diarrhoea for cold-dampness, stomach abdomen pain；External application controls scabies, tinea, saprodontia and has a pain.Source be Lauraceae cinnamon camphor tree, with root,
Branch, leaf and waste wood are through distilling resulting crystalline particulate.
In the present invention, the Lignum cinnamomi camphorae extract is commercially available.
Epipremnum aureum extract
Epipremnum aureum (scientific name：Epipremnum aureum), belong to kylin leaf platymiscium, large-scale evergreen liana is grown on the torrid zone
Area, for normal climbing growth on the rock and trunk of rainforest, prehensile is strong, and aerial root is flourishing, can be planted with water planting.
There are also extremely strong air-cleaning functions for epipremnum aureum, there is the good name of green clarifier.Epipremnum aureum can be in metabolism by first
Aldehyde converts the substances such as saccharogenesis or amino acid.
Extracting method：The fresh blade obtained from epipremnum aureum plant is ground, and is 50-70 DEG C of ethyl acetate and ethyl alcohol in temperature
Mixed liquor in impregnate 20h, after aqueous citric acid solution is added, stand extraction 1~7 day at room temperature, centre is stirred often, mistake
Filter, obtains leaching liquor；It so extracts three times, merges leaching liquor three times, be concentrated under reduced pressure with Rotary Evaporators to get epipremnum aureum extract.
Bracketplant extract
Bracketplant alias sclerophyll bracketplant, fish orchid, Gui Lan, grape blue, tree any of several broadleaf plants melon, Zhe Helan, folding crane orchid, fragrant thoroughwort, hang upside down orchid,
Native American ginseng, eight aspidistras, feathering bracketplant；Monocotyledonae, Liliaceae, bracketplant category perennial evergreen herbaceous plant, rhizomes are flat
It is raw or tiltedly raw, there is the root of most plumpnesses.Overgrown, linear, leaf is elongated, like orchid.Sometimes intermediate to have green or yellow cord.
Scape is extracted out from leafage, grows up to stolon in top leaf development cluster, grey color, normal 2-4 fasciation lines up total shape of evacuation
Inflorescence or panicle accidentally inside will appear purple petal；Three prismatic oblate spheroid of capsule, is about 5 millimeters, about 8 millimeters wide, often
Room has 3-5, seed.May at florescence, fruiting period August.Plant plays the role of purifying air, and complete stool can be used as medicine.
In the present invention, the bracketplant extract is commercially available.
Eucalyptus extracts
Eucalyptus is also known as You Jiali tree, is the general designation of Myrtaceae cup fruit tree category, umbrella room category and eucalyptus, source area print
The ground such as Buddhist nun and Australia.There are many kinds of classes for eucalyptus, such as have arid sclerophyll high forest type, moisten sclerophyll arbor type, is dilute
Set Types of Grassland, arid sclerophyll arbor type, mesophorbium, coryphile type.
Main ingredient is pentacyclic triterpene compound in eucalyptus barks, for example, malol, betulinic acid, oleanolic acid, ursolic acid,
Betulic acid, birch resin acid, betulonic acid, 3- β-O- are trans- to hydroxy cinnamate acyl group -12- alkene -28- oleanolic acid, 3- β-O-
It is trans- to -2 σ of hydroxy cinnamate acyl group-hydroxyl -12- alkene stamen-ursolic acid.
Eucalyptus leaf volatile oil main component is 1,8- Cineole, firpene, aromadendrene, cumaldehyde, pinocarveol and 1- acetyl -4-
Isopropylidene cyclopentene etc., and contain rutin, quercitrin, Quercetin, homoserine, also separate eucalyptin.In folium eucalypti other at
Point, such as terpene, flavonoids, tannin, phloroglucinol derivatives and glycoside are also with bioactivity abundant.
The preparation method of the eucalyptus extracts is：By the powder of eucalyptus barks, ethyl alcohol is added, uses microwave after impregnating 2-3h
Heating extraction 2-3 times, filtering, filtrate be concentrated under reduced pressure into no ethyl alcohol to get.
Extractives From Melia Azedarach L
In the present invention, the preparation method of the Extractives From Melia Azedarach L is as follows：China tree is shredded, after being soaked with ammonium hydroxide, then with it is clear
After clear limewash mixing, and ethyl alcohol is added, flow back 1-3h, filters, is concentrated while hot to obtain the final product.
The weight ratio for clarifying limewash and ethyl alcohol is 1：3.
The white palm and epipremnum aureum extract
In the present invention, the extracting method of the white palm and epipremnum aureum extract is as follows：The epipremnum aureum of fresh picking is squeezed the juice, is obtained
Epipremnum aureum juice, for use；The white palm is shredded, gallic acid is added and impregnates 2h, then filters, takes filtrate and epipremnum aureum juice to mix, at 65 DEG C
Lower stirring 30min, is cooled to room temperature, filtering, collect filtrate to get.
Fructus Gleditsiae Abnormalis extract
Gleditsia sinensis, also known as Chinese honey locust, Gleditsia officinalis belong to Rosales, pulse family deciduous tree or dungarunga,
Chinese honey locust is containing triterpenoid saponin, tannin, ceryl alcohol, nonacosane, stigmasterol, sitosterol etc..The element of saponin(e contained in Chinese honey locust
It is triterpene alkenes and oligosaccharide.The chemical component of Chinese honey locust is mainly terpene, flavonoids, phenolic acid class, steroid etc..
The pod formula of soap containing triterpene：Gledinin, glucoside glucoside member are gledigenin, gleditschiasaponin.Still contain cerinic acid, nonacosane, just
Heptacosane, stigmasterol, sitosterol, tannin etc..Saponin has gledinin, and glucoside member and gleditschiasaponin are obtained after hydrolysis, glucoside is obtained after hydrolysis
Member and arabinose.In addition, still containing ceryl alcohol, nonacosane, stigmasterol, sitosterol etc..
In the present invention, the method for the Fructus Gleditsiae Abnormalis extract is：Gleditsia sinensis explosion is crushed to 100-200 mesh and threonine is total
It is mixed, with the mixture (volume ratio 1 of second alcohol and water：4) it is extracted as solvent at 50 DEG C, filtrate, concentration.
Gotu Kola P.E
In the present invention, the preparation method of the Gotu Kola P.E is as follows：Centella raw material is taken, 50-60 DEG C dry, pulverize
Machine is ground into coarse powder, by 1：Water is added in (10-15) ratio, and homogenate extraction 3-5min is extracted 2 times.
Herba Asari extract
Asarum is aristolochiaceae plant Herba Asari Asarum heterotropoides Fr.Schmidt
Var.mandshuricum (Maxim.) Kitag., Seoul asarum Asarum sieboldii Miq.var.seoulense
The drying herb of Nakai or asarum sieboldii Asarum sieboldii Miq..The first two kind, which is practised, claims " HERBA ASARI from Liaoning of China ".Summer fruit mature period or
Early autumn excavation, removes silt, dries in the shade.Herba Asari：It often crispaturas agglomerating.Rhizome grows wild in irregular roundness cylindricality, has short branch, length 1
~10cm, 0.2~0.4cm of diameter；Surface taupe brown, it is coarse, there is the section of annular, 0.2~0.3cm of internode length, branch top has
Bowl-shape stem trace.Root is elongated, on dense section, long 10~20cm, diameter 0.1cm；Surface lark, smooth or tool vertical wrinkle, has
Fibrous root and mark of fibrous root.Basal leaf 1~3, has long handle, and surface light green is smooth；Blade is mostly broken, complete person's heart to the kidney shape
Heart, full edge, the anxious point of apex, base portion innermost being shape, long 4~10cm, wide 6~12cm.The visible flower having, more shrinkages are bell, secretly
Purple, perianth Capping piece are affixed by base portion warp and perianth tube almost all.Fruit hemispherical.The pungent perfume (or spice) of gas, acrid flavour is peppery, numb tongue.
Seoul asarum：Rhizome 0.1~0.5cm of diameter, 0.1~1cm of internode length.Basal leaf is mostly 2, and petiole hairiness, blade is thicker, flower
Carried out by sliver.Fruit hemispherical.Asarum sieboldii：Rhizome grows 5~20cm, 0.1~0.2cm of diameter, 0.2~1cm of internode length.Base
Leave 1~2, blade is relatively thin, heart-shaped, and apex is tapering.Perianth sliver is carried out.Fruit is subsphaeroidal.Smell is weaker.
There is a wind-dispelling, cold dispelling, row water, have one's ideas straightened out and other effects.It is usually used in air-cooled headache, nasosinusitis, dentalgia, sip and cough, rheumatism numbness
Pain etc..Asarum can outer dispersing wind and cold and in dispel cold sensation of the genitalia, while relieve pain, antibechic effect it is preferable.
HERBA ASARI from Liaoning of China contains volatile oil about 3%, and the main component of volatile oil is methyleugenol, other have safrole, β-pinane
Alkene, Eucarvone, phenolic substance etc..Asarum sieboldii contain volatile oil 2.75%, 1.9%.Mainly contain methyleugenol in volatile oil
(accounting for about 50%), there are also saishinone, firpene, Eucarvone, safrole, 1, 8-Cineole, l- asarinins etc..
The volatile oil of double leaf asarum containing Eucarvone 6%, borneol or estragole 7%, 1, 8-Cineole 4%, firpene 2%,
It is methyleugenol 15%, safrole 10%, croweacin 10%, elemicine 8%, saishinone 0.2%, linalool, big
Three enol of Mang ox.2- methyl -2- vinyl -3- isopropenyl -5- isopropylidene cyclohexanol etc..
Roundleaf asarum herb contains glycosides displayed, amino acid, carbohydrate and volatile oil.
In the present invention, the Herba Asari extract is commercially available.
Fructus Kochiae extract
The fruit of summer cypress is the dry mature fruit of chenopod summer cypress Kochia scoparia (L.) Schrad..Autumn fruit
Plant is harvested when mature, is dried, fruit is laid, and removes impurity.In oblate spheroid shape pentalpha, 1~3mm of diameter.It is outer to be harbored flower
There are the dotted carpopodium trace of micro-protuberance and radial in quilt, surface celadon or light brown, 5 pieces of film quality winglet of surrounding tool, back center
Vein 5~10；Remove perianth, it is seen that film quality pericarp is translucent.Seed is flat oval, about 1mm, black.Gas is micro-, mildly bitter flavor.
Acrid flavour, hardship, it is cold in nature.Return kidney, bladder meridian.With clearing heat and promoting diuresis, the effect of dispelling wind and arresting itching.Difficulty and pain in micturition is cured mainly, yin
Itch leukorrhagia, rubeola eczema, pruitus.
The extracting method of Fructus Kochiae extract is to clean the fruit of summer cypress, chopping, is impregnated for 24 hours with yellow rice wine, is then dried, and is used
Water decocts 3 times, and using jujube and ginger as medicine efficacy enhancing ingredient, the weight ratio of water and the fruit of summer cypress is 8：1,40min is decocted every time, is merged and is decocted
Boil liquid, vacuum drying to get.
Cimicifuga foetida extract
Cimicifugae foetidae is ranunculaceae plant C.heracleifolia Cimicifuga heracleifolia Kom., Cimicifuga Dahurica
The dry rhizome of Cimicifuga dahurica (Turcz.) Maxim. or cimicifugae foetidae Cimicifuga foetida L..Not advise
Elongated bulk then, multi-branched are in nodositas, long 10~20cm, 2~4cm of diameter.Surface dark brown or sepia, it is coarse not
It is flat, there is hard thin fibrous root residual, there is the stem foot trace in several round cavities above, hole inner wall shows netted rill；Below it is concave-convex not
It is flat, have mark of fibrous root.Body is light, and matter is hard, is not easily broken, and section is uneven, there is crack, fibroid, yellow green or yellowish white.
Gas is micro-, mildly bitter flavor and it is puckery.Pungent, micro-sweet, it is slightly cold.Return lung, spleen, stomach, large intestine channel.With promoting eruption is delivered, clearing heat and detoxicating, liter lifts sun
The effect of gas.For headache due to pathogenic wind-heat, dentalgia, aphtha, abscess of throat, measles without adequate eruption, sun poison macular eruption；Rectal prolapse, uterine prolapse.
Cimicifuga Dahurica rhizome (ferulic acid) containing ferulic acid, isoferulic acid (isoferulic acid), caffeic acid
(caffeic acid), [E] -3- (3'- methyl -2'- butenylidene) -2- indolone ([E] -3- (3'-methyl-2'-
Butenylidene) -2-indokinone), [Z] -3- (3'- methyl -2'- butenylidene) -2- indolone, cimifugin
(cimifugin), visnagin (visnagin) removes first visnagin (norvisnagin), visamminol
(visamminol), rhizoma cimicifugae dahuricae terpene (cimicilen), 12- hydroxyl cimicifugae foetidae epoxy alcohol Arab glucoside (12-
Hydroxycimigenol arabinoside) and with cupreol (β-sitosterol), cimicifugae foetidae epoxy alcohol
(cimigenol), cimicifugae foetidae epoxy alcohol xyloside (cimigenyl xyloside), Cimicifuga Dahurica alcohol (dahurinol) are glucoside member
Glucoside, also contain cimicifugoside (cimigenyl xyloside), Cimicifuga Dahurica alcohol (dahurinol) be glucoside member glucoside, and also
Containing cimicifugoside (cimicifugoside), the new alcohol xyloside of cimicifugae foetidae (shengmanol xyloside), the new alcohol of acetyl cimicifugae foetidae
Xyloside, 24- acetyl group are hydrated the new alcohol xyloside of cimicifugae foetidae (24-acetylhydroshengmanol xyloside).
Heretofore described cimicifuga foetida extract is commercially available.
Rhizoma Acori Graminei extract
Rhizoma acori graminei is the dry rhizome of acorus gramineus araceae plant Acorus tatarinowii Schott.In oblate
Cylindricality, it is be bent more, often there are branch, long 3~20cm, 0.3~1cm of diameter.Surface sepia or taupe brown, it is coarse, there is density not
Even link, 0.2~0.8cm of internode length have thin longitudinal grin, remain fibrous root or round point shape root trace on one side；Leaf scar is triangular in shape, left
The phyllopodium of right interaction arrangement, some hairiness squamous thereon is remaining.Matter is hard, section fibrous, off-white color or blush, endodermis
Ring is obvious, it is seen that most vascular bundle dots and brown eleocyte.Gas fragrance, bitter, micro-pungent.
With dampness elimination appetizing, slit phlegm of having one's ideas straightened out, inducing resuscitation intelligence development.For gastral cavity ruffian is not hungry, apnea, coma epilepsy, amnesia ear
It is deaf.
Heretofore described Rhizoma Acori Graminei extract is commercially available.
Flaxseed gum
In the present invention, the flaxseed gum passes through combined processing, and steps are as follows for the combined processing：
Containing hydrogen silicone oil, divinylbenzene and chloroplatinic acid are 6 by S01 in mass ratio：3：1 hands at 120 DEG C after mixing
After connection reaction 12 hours, solid 1 is obtained；
Solid 1, cellulose and sepiolite powder are 1 by S02 in mass ratio：1：Ball milling 16 hours after 2 mixing；
S03 will obtain mixture and enclose lower high-temperature calcination in Ar atmosphere in S02；
S04 carries out acid etch to the calcined powder of S03 using hydrofluoric acid solution, and flaxseed gum is added after being washed to neutrality
Solution is warming up to 50 DEG C, after mixing evenly, can be prepared.
In the S03, the process of high-temperature calcination is as follows：
Being sintered initial temperature is 60 DEG C, rises to 500 DEG C with the speed of 2.5 DEG C/min, keeps the temperature 60min；Again with 6 DEG C/min's
Speed is warming up to 1200 DEG C and continues furnace cooling after 2 hours again.
In the S04, it is 7 that the flaxseed gum solution, which is formulated as flaxseed gum and water according to weight ratio,：10.
In the S04, the concentration of the hydrofluoric acid solution is 18%, and etch period is 5 hours.
A kind of efficiently removal formaldehyde air purifying preparation of embodiment 1., the preparation of the efficient removal formaldehyde air purifying preparation
Raw material includes at least：Lemon extract, jasmine extract, tea tree extract, Flos Osmanthi Fragrantis extract, Lignum cinnamomi camphorae extract, epipremnum aureum are extracted
Object, bracketplant extract, eucalyptus extracts, Extractives From Melia Azedarach L, the white palm and epipremnum aureum extract, Fructus Gleditsiae Abnormalis extract, centella are extracted
Object, Herba Asari extract, Fructus Kochiae extract, cimicifuga foetida extract, second alcohol and water.
One kind described in 2. embodiment 1 of embodiment efficiently removes formaldehyde air purifying preparation, by weight, the height
The raw material for preparing of effect removal formaldehyde air purifying preparation includes at least：1-5 parts of lemon extract, 1-3 parts of jasmine extract, tea tree
0.1-1.5 parts of extract, 5-10 parts of Flos Osmanthi Fragrantis extract, 1-3 parts of Lignum cinnamomi camphorae extract, 1-5 parts of epipremnum aureum extract, bracketplant extract
5-15 parts, 0.1-0.5 parts of eucalyptus extracts, 1-3 parts of Extractives From Melia Azedarach L, the white palm and 5-10 parts of epipremnum aureum extract, Fructus Gleditsiae Abnormalis extract
1-8 parts, 1-3 parts of Gotu Kola P.E, 0.5-1.5 parts of Herba Asari extract, 1.5-3.5 parts of Fructus Kochiae extract, cimicifuga foetida extract
3.5-6.5 parts, 0.1-3 parts of ethyl alcohol and 50-60 parts of water.
One kind described in 3. embodiment 1 of embodiment efficiently removes formaldehyde air purifying preparation, by weight, the height
The raw material for preparing of effect removal formaldehyde air purifying preparation includes at least：3 parts of lemon extract, 2 parts of jasmine extract, tea tree are extracted
0.8 part of object, 6 parts of Flos Osmanthi Fragrantis extract, 2 parts of Lignum cinnamomi camphorae extract, 3 parts of epipremnum aureum extract, 8 parts of bracketplant extract, eucalyptus extracts
0.3 part, 2 parts of Extractives From Melia Azedarach L, the white palm and 8 parts of epipremnum aureum extract, 5 parts of Fructus Gleditsiae Abnormalis extract, 2 parts of Gotu Kola P.E, asarum mention
Take 1.1 parts of object, 2.0 parts of Fructus Kochiae extract, 4.3 parts of cimicifuga foetida extract, 2.1 parts of ethyl alcohol and 55 parts of water.
One kind described in 4. embodiment 1 of embodiment efficiently removes formaldehyde air purifying preparation, the efficient removal formaldehyde
Air purifying preparation prepares raw material also and includes 10-15 parts and flaxseed gum 5-10 parts of Rhizoma Acori Graminei extract.
Efficiently removal formaldehyde air purifying preparation, the flaxseed gum pass through one kind described in 5. embodiment 4 of embodiment
Combined processing, steps are as follows for the combined processing：
Containing hydrogen silicone oil, divinylbenzene and chloroplatinic acid are 6 by S01 in mass ratio：3：1 hands at 120 DEG C after mixing
After connection reaction 12 hours, solid 1 is obtained；
Solid 1, cellulose and sepiolite powder are 1 by S02 in mass ratio：1：Ball milling 16 hours after 2 mixing；
S03 will obtain mixture and enclose lower high-temperature calcination in Ar atmosphere in S02；
S04 carries out acid etch to the calcined powder of S03 using hydrofluoric acid solution, and flaxseed gum is added after being washed to neutrality
Solution is warming up to 50 DEG C, after mixing evenly, can be prepared.
The efficient removal formaldehyde air purifying preparation of one kind described in 6. embodiment 5 of embodiment, in the S03, high temperature is forged
The process of burning is as follows：
Being sintered initial temperature is 60 DEG C, rises to 500 DEG C with the speed of 2.5 DEG C/min, keeps the temperature 60min；Again with 6 DEG C/min's
Speed is warming up to 1200 DEG C and continues furnace cooling after 2 hours again.
The efficient removal formaldehyde air purifying preparation of one kind described in 7. embodiment 5 of embodiment, in the S04, the Asia
It is 7 that numb seed sol solution, which is formulated as flaxseed gum and water according to weight ratio,：10.
The efficient removal formaldehyde air purifying preparation of one kind described in 8. embodiment 5 of embodiment, in the S04, the hydrogen
The concentration of fluorspar acid solution is 18%, and etch period is 5 hours.
One kind described in 9. embodiment 1 of embodiment efficiently removes formaldehyde air purifying preparation, the lemon extract
Extracting method is as follows：
(1) Fresh Lemon is squeezed broken, takes clear lemon fluid；
(2) by lemon fluid and formic acid obtained in step (1) according to 20：1 mixing, can be prepared lemon extract.
One kind described in 10. embodiment 1 of embodiment efficiently removes formaldehyde air purifying preparation, the Fructus Kochiae extract
Preparation method it is as follows：
The extracting method of Fructus Kochiae extract is to clean the fruit of summer cypress, chopping, is impregnated for 24 hours with yellow rice wine, is then dried, and is used
Water decocts 3 times, and using jujube and ginger as medicine efficacy enhancing ingredient, the weight ratio of water and the fruit of summer cypress is 8：1,40min is decocted every time, is merged and is decocted
Boil liquid, vacuum drying to get.
To one kind provided by the invention, efficiently removal formaldehyde air purifying preparation is carried out specifically combined with specific embodiments below
It is bright.
Embodiment 1：The present embodiment provides a kind of raw materials for preparing of efficiently removal formaldehyde air purifying preparation to include at least：Lemon
3 parts of extract, 2 parts of jasmine extract, 0.8 part of tea tree extract, 6 parts of Flos Osmanthi Fragrantis extract, 2 parts of Lignum cinnamomi camphorae extract, epipremnum aureum mention
Take 3 parts of object, 8 parts of bracketplant extract, 0.3 part of eucalyptus extracts, 2 parts of Extractives From Melia Azedarach L, the white palm and 8 parts of epipremnum aureum extract, gleditsia sinensis
5 parts of extract, 2 parts of Gotu Kola P.E, 1.1 parts of Herba Asari extract, 2.0 parts of Fructus Kochiae extract, 4.3 parts of cimicifuga foetida extract,
12 parts of Rhizoma Acori Graminei extract, 8 parts of flaxseed gum, 2.1 parts of ethyl alcohol and 55 parts of water.
Lemon extract：The extracting method of the lemon extract is as follows：
(1) Fresh Lemon is squeezed broken, takes clear lemon fluid；
(2) by lemon fluid and formic acid obtained in step (1) according to 20：1 mixing, can be prepared lemon extract.
Jasmine extract：The extracting method of heretofore described jasmine extract is as follows：1. four-o'clock herb is dried in the shade, use
Plant pulverizer crushes, and crosses 40 meshes, adds 2~10 times of 95% ethyl alcohol of amount, be stored at room temperature extraction 1~7 day, and centre is stirred often,
Filtering, obtains leaching liquor；2~10 times of 95% alcohol steeps of amount are added in filter residue again, so extract three times, merge leaching liquor three times,
It is concentrated under reduced pressure with Rotary Evaporators, obtains dark brown stiff paste form up to Radix Mirabilis extract of the present invention；2. by four-o'clock herb yin
It is dry, it is crushed with plant pulverizer, crosses 40 meshes, add 2~10 times of 95% ethyl alcohol of amount, refluxing extraction 5~15 hours, filtering must return
Extracting solution is flowed, is concentrated under reduced pressure with Rotary Evaporators, obtains stiff paste form up to this Radix Mirabilis extract.
Tea tree extract：The extracting method of the tea tree extract is as follows：The blade of tea tree is chosen, after cleaning, takes 20g tree
Leaf carries out steam distillation to complete leaf without crushing, and distillation time is 18 hours, removes thick slag, obtains grease
After matter, after -10 DEG C freeze 12 hours, moisture removal is removed in air-distillation, then that the grease of acquisition is small in -10 DEG C of freezings 24
Shi Hou removes grease, takes thick slag, and after thick slag heating melting, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil,
Tea tree ethereal oil can be prepared.
Flos Osmanthi Fragrantis extract：The Flos Osmanthi Fragrantis extract is bought from Xi'an Jin Di Biotechnology Co., Ltd.
Lignum cinnamomi camphorae extract：In the present invention, the Lignum cinnamomi camphorae extract is commercially available.
Epipremnum aureum extract：Extracting method：The fresh blade obtained from epipremnum aureum plant is ground, and is 50-70 DEG C of second in temperature
20h is impregnated in the mixed liquor of acetoacetic ester and ethyl alcohol, after aqueous citric acid solution is added, stands extraction 1~7 day at room temperature, it is intermediate
Often it stirs, filters, obtain leaching liquor；So extract three times, merge leaching liquor three times, with Rotary Evaporators be concentrated under reduced pressure to get
Epipremnum aureum extract.
Bracketplant extract：The bracketplant extract is commercially available.
Eucalyptus extracts：The preparation method of the eucalyptus extracts is：By the powder of eucalyptus barks, ethyl alcohol is added, impregnates 2-
After 3h use extracting through microwave heating 2-3 time, filter, filtrate be concentrated under reduced pressure into no ethyl alcohol to get.
Extractives From Melia Azedarach L：The preparation method of the Extractives From Melia Azedarach L is as follows：China tree is shredded, after being soaked with ammonium hydroxide, then and
After clarifying limewash mixing, and ethyl alcohol is added, flow back 1-3h, filters, is concentrated while hot to obtain the final product.
The weight ratio for clarifying limewash and ethyl alcohol is 1：3.
The white palm and epipremnum aureum extract：The extracting method of the white palm and epipremnum aureum extract is as follows：By the epipremnum aureum of fresh picking
Juicing, obtains epipremnum aureum juice, for use；The white palm is shredded, gallic acid is added and impregnates 2h, then filters, takes filtrate and epipremnum aureum juice mixed
Close, stir 30min at 65 DEG C, be cooled to room temperature, filter, collect filtrate to get.
Fructus Gleditsiae Abnormalis extract：The method of the Fructus Gleditsiae Abnormalis extract is：Gleditsia sinensis explosion is crushed to 100-200 mesh and threonine
It is blended, with the mixture (volume ratio 1 of second alcohol and water：4) it is extracted as solvent at 50 DEG C, filtrate, concentration.
Gotu Kola P.E：The preparation method of the Gotu Kola P.E is as follows：Take centella raw material, 50-60 DEG C of drying,
Pulverizer is ground into coarse powder, by 1：Water is added in 13 ratios, and homogenate extraction 3-5min is extracted 2 times.
Herba Asari extract：The Herba Asari extract is commercially available.
Fructus Kochiae extract：The fruit of summer cypress is cleaned, chopping, impregnated for 24 hours with yellow rice wine, then dried, decocted 3 times with water, with
Jujube and ginger are medicine efficacy enhancing ingredient, and the weight ratio of water and the fruit of summer cypress is 8：1,40min is decocted every time, merges decoction liquor, and vacuum is dry
It is dry to get.
Cimicifuga foetida extract：Heretofore described cimicifuga foetida extract is commercially available.
Rhizoma Acori Graminei extract：Heretofore described Rhizoma Acori Graminei extract is commercially available.
Flaxseed gum：The flaxseed gum passes through combined processing, and steps are as follows for the combined processing：
Containing hydrogen silicone oil, divinylbenzene and chloroplatinic acid are 6 by S01 in mass ratio：3：1 hands at 120 DEG C after mixing
After connection reaction 12 hours, solid 1 is obtained；
Solid 1, cellulose and sepiolite powder are 1 by S02 in mass ratio：1：Ball milling 16 hours after 2 mixing；
S03 will obtain mixture and enclose lower high-temperature calcination in Ar atmosphere in S02；
S04 carries out acid etch to the calcined powder of S03 using hydrofluoric acid solution, and flaxseed gum is added after being washed to neutrality
Solution is warming up to 50 DEG C, after mixing evenly, can be prepared.
In the S03, the process of high-temperature calcination is as follows：
Being sintered initial temperature is 60 DEG C, rises to 500 DEG C with the speed of 2.5 DEG C/min, keeps the temperature 60min；Again with 6 DEG C/min's
Speed is warming up to 1200 DEG C and continues furnace cooling after 2 hours again.
In the S04, it is 7 that the flaxseed gum solution, which is formulated as flaxseed gum and water according to weight ratio,：10.
In the S04, the concentration of the hydrofluoric acid solution is 18%, and etch period is 5 hours.
Embodiment 2：The present embodiment provides a kind of raw materials for preparing of efficiently removal formaldehyde air purifying preparation to include at least：Lemon
5 parts of extract, 3 parts of jasmine extract, 1.5 parts of tea tree extract, 10 parts of Flos Osmanthi Fragrantis extract, 3 parts of Lignum cinnamomi camphorae extract, epipremnum aureum mention
Take 5 parts of object, 15 parts of bracketplant extract, 0.5 part of eucalyptus extracts, 3 parts of Extractives From Melia Azedarach L, the white palm and 10 parts of epipremnum aureum extract, soap
8 parts of horn extraction, 3 parts of Gotu Kola P.E, 1.5 parts of Herba Asari extract, 3.5 parts of Fructus Kochiae extract, cimicifuga foetida extract 6.5
Part, 15 parts of Rhizoma Acori Graminei extract, 10 parts of flaxseed gum, 2.1 parts of ethyl alcohol and 55 parts of water.
Lemon extract：The extracting method of the lemon extract is as follows：
(1) Fresh Lemon is squeezed broken, takes clear lemon fluid；
(2) by lemon fluid and formic acid obtained in step (1) according to 20：1 mixing, can be prepared lemon extract.
Jasmine extract：The extracting method of heretofore described jasmine extract is as follows：1. four-o'clock herb is dried in the shade, use
Plant pulverizer crushes, and crosses 40 meshes, adds 2~10 times of 95% ethyl alcohol of amount, be stored at room temperature extraction 1~7 day, and centre is stirred often,
Filtering, obtains leaching liquor；2~10 times of 95% alcohol steeps of amount are added in filter residue again, so extract three times, merge leaching liquor three times,
It is concentrated under reduced pressure with Rotary Evaporators, obtains dark brown stiff paste form up to Radix Mirabilis extract of the present invention；2. by four-o'clock herb yin
It is dry, it is crushed with plant pulverizer, crosses 40 meshes, add 2~10 times of 95% ethyl alcohol of amount, refluxing extraction 5~15 hours, filtering must return
Extracting solution is flowed, is concentrated under reduced pressure with Rotary Evaporators, obtains stiff paste form up to this Radix Mirabilis extract.
Tea tree extract：The extracting method of the tea tree extract is as follows：The blade of tea tree is chosen, after cleaning, takes 20g tree
Leaf carries out steam distillation to complete leaf without crushing, and distillation time is 18 hours, removes thick slag, obtains grease
After matter, after -10 DEG C freeze 12 hours, moisture removal is removed in air-distillation, then that the grease of acquisition is small in -10 DEG C of freezings 24
Shi Hou removes grease, takes thick slag, and after thick slag heating melting, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil,
Tea tree ethereal oil can be prepared.
Flos Osmanthi Fragrantis extract：The Flos Osmanthi Fragrantis extract is bought from Xi'an Jin Di Biotechnology Co., Ltd.
Lignum cinnamomi camphorae extract：In the present invention, the Lignum cinnamomi camphorae extract is commercially available.
Epipremnum aureum extract：Extracting method：The fresh blade obtained from epipremnum aureum plant is ground, and is 50-70 DEG C of second in temperature
20h is impregnated in the mixed liquor of acetoacetic ester and ethyl alcohol, after aqueous citric acid solution is added, stands extraction 1~7 day at room temperature, it is intermediate
Often it stirs, filters, obtain leaching liquor；So extract three times, merge leaching liquor three times, with Rotary Evaporators be concentrated under reduced pressure to get
Epipremnum aureum extract.
Bracketplant extract：The bracketplant extract is commercially available.
Eucalyptus extracts：The preparation method of the eucalyptus extracts is：By the powder of eucalyptus barks, ethyl alcohol is added, impregnates 2-
After 3h use extracting through microwave heating 2-3 time, filter, filtrate be concentrated under reduced pressure into no ethyl alcohol to get.
Extractives From Melia Azedarach L：The preparation method of the Extractives From Melia Azedarach L is as follows：China tree is shredded, after being soaked with ammonium hydroxide, then and
After clarifying limewash mixing, and ethyl alcohol is added, flow back 1-3h, filters, is concentrated while hot to obtain the final product.
The weight ratio for clarifying limewash and ethyl alcohol is 1：3.
The white palm and epipremnum aureum extract：The extracting method of the white palm and epipremnum aureum extract is as follows：By the epipremnum aureum of fresh picking
Juicing, obtains epipremnum aureum juice, for use；The white palm is shredded, gallic acid is added and impregnates 2h, then filters, takes filtrate and epipremnum aureum juice mixed
Close, stir 30min at 65 DEG C, be cooled to room temperature, filter, collect filtrate to get.
Fructus Gleditsiae Abnormalis extract：The method of the Fructus Gleditsiae Abnormalis extract is：Gleditsia sinensis explosion is crushed to 100-200 mesh and threonine
It is blended, with the mixture (volume ratio 1 of second alcohol and water：4) it is extracted as solvent at 50 DEG C, filtrate, concentration.
Gotu Kola P.E：The preparation method of the Gotu Kola P.E is as follows：Take centella raw material, 50-60 DEG C of drying,
Pulverizer is ground into coarse powder, by 1：Water is added in 13 ratios, and homogenate extraction 3-5min is extracted 2 times.
Herba Asari extract：The Herba Asari extract is commercially available.
Fructus Kochiae extract：The fruit of summer cypress is cleaned, chopping, impregnated for 24 hours with yellow rice wine, then dried, decocted 3 times with water, with
Jujube and ginger are medicine efficacy enhancing ingredient, and the weight ratio of water and the fruit of summer cypress is 8：1,40min is decocted every time, merges decoction liquor, and vacuum is dry
It is dry to get.
Cimicifuga foetida extract：Heretofore described cimicifuga foetida extract is commercially available.
Rhizoma Acori Graminei extract：Heretofore described Rhizoma Acori Graminei extract is commercially available.
Flaxseed gum：The flaxseed gum passes through combined processing, and steps are as follows for the combined processing：
Containing hydrogen silicone oil, divinylbenzene and chloroplatinic acid are 6 by S01 in mass ratio：3：1 hands at 120 DEG C after mixing
After connection reaction 12 hours, solid 1 is obtained；
Solid 1, cellulose and sepiolite powder are 1 by S02 in mass ratio：1：Ball milling 16 hours after 2 mixing；
S03 will obtain mixture and enclose lower high-temperature calcination in Ar atmosphere in S02；
S04 carries out acid etch to the calcined powder of S03 using hydrofluoric acid solution, and flaxseed gum is added after being washed to neutrality
Solution is warming up to 50 DEG C, after mixing evenly, can be prepared.
In the S03, the process of high-temperature calcination is as follows：
Being sintered initial temperature is 60 DEG C, rises to 500 DEG C with the speed of 2.5 DEG C/min, keeps the temperature 60min；Again with 6 DEG C/min's
Speed is warming up to 1200 DEG C and continues furnace cooling after 2 hours again.
In the S04, it is 7 that the flaxseed gum solution, which is formulated as flaxseed gum and water according to weight ratio,：10.
In the S04, the concentration of the hydrofluoric acid solution is 18%, and etch period is 5 hours.
Embodiment 3：The present embodiment provides a kind of raw materials for preparing of efficiently removal formaldehyde air purifying preparation to include at least：Lemon
1 part of extract, 1 part of jasmine extract, 0.1 part of tea tree extract, 5 parts of Flos Osmanthi Fragrantis extract, 1 part of Lignum cinnamomi camphorae extract, epipremnum aureum mention
Take 1 part of object, 5 parts of bracketplant extract, 0.1 part of eucalyptus extracts, 1 part of Extractives From Melia Azedarach L, the white palm and 5 parts of epipremnum aureum extract, gleditsia sinensis
1 part of extract, 1 part of Gotu Kola P.E, 0.5 part of Herba Asari extract, 1.5 parts of Fructus Kochiae extract, 3.5 parts of cimicifuga foetida extract,
10 parts of Rhizoma Acori Graminei extract, 5 parts of flaxseed gum, 0.1 part of ethyl alcohol and 50 parts of water.
Lemon extract：The extracting method of the lemon extract is as follows：
(1) Fresh Lemon is squeezed broken, takes clear lemon fluid；
(2) by lemon fluid and formic acid obtained in step (1) according to 20：1 mixing, can be prepared lemon extract.
Jasmine extract：The extracting method of heretofore described jasmine extract is as follows：1. four-o'clock herb is dried in the shade, use
Plant pulverizer crushes, and crosses 40 meshes, adds 2~10 times of 95% ethyl alcohol of amount, be stored at room temperature extraction 1~7 day, and centre is stirred often,
Filtering, obtains leaching liquor；2~10 times of 95% alcohol steeps of amount are added in filter residue again, so extract three times, merge leaching liquor three times,
It is concentrated under reduced pressure with Rotary Evaporators, obtains dark brown stiff paste form up to Radix Mirabilis extract of the present invention；2. by four-o'clock herb yin
It is dry, it is crushed with plant pulverizer, crosses 40 meshes, add 2~10 times of 95% ethyl alcohol of amount, refluxing extraction 5~15 hours, filtering must return
Extracting solution is flowed, is concentrated under reduced pressure with Rotary Evaporators, obtains stiff paste form up to this Radix Mirabilis extract.
Tea tree extract：The extracting method of the tea tree extract is as follows：The blade of tea tree is chosen, after cleaning, takes 20g tree
Leaf carries out steam distillation to complete leaf without crushing, and distillation time is 18 hours, removes thick slag, obtains grease
After matter, after -10 DEG C freeze 12 hours, moisture removal is removed in air-distillation, then that the grease of acquisition is small in -10 DEG C of freezings 24
Shi Hou removes grease, takes thick slag, and after thick slag heating melting, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil,
Tea tree ethereal oil can be prepared.
Flos Osmanthi Fragrantis extract：The Flos Osmanthi Fragrantis extract is bought from Xi'an Jin Di Biotechnology Co., Ltd.
Lignum cinnamomi camphorae extract：In the present invention, the Lignum cinnamomi camphorae extract is commercially available.
Epipremnum aureum extract：Extracting method：The fresh blade obtained from epipremnum aureum plant is ground, and is 50-70 DEG C of second in temperature
20h is impregnated in the mixed liquor of acetoacetic ester and ethyl alcohol, after aqueous citric acid solution is added, stands extraction 1~7 day at room temperature, it is intermediate
Often it stirs, filters, obtain leaching liquor；So extract three times, merge leaching liquor three times, with Rotary Evaporators be concentrated under reduced pressure to get
Epipremnum aureum extract.
Bracketplant extract：The bracketplant extract is commercially available.
Eucalyptus extracts：The preparation method of the eucalyptus extracts is：By the powder of eucalyptus barks, ethyl alcohol is added, impregnates 2-
After 3h use extracting through microwave heating 2-3 time, filter, filtrate be concentrated under reduced pressure into no ethyl alcohol to get.
Extractives From Melia Azedarach L：The preparation method of the Extractives From Melia Azedarach L is as follows：China tree is shredded, after being soaked with ammonium hydroxide, then and
After clarifying limewash mixing, and ethyl alcohol is added, flow back 1-3h, filters, is concentrated while hot to obtain the final product.
The weight ratio for clarifying limewash and ethyl alcohol is 1：3.
The white palm and epipremnum aureum extract：The extracting method of the white palm and epipremnum aureum extract is as follows：By the epipremnum aureum of fresh picking
Juicing, obtains epipremnum aureum juice, for use；The white palm is shredded, gallic acid is added and impregnates 2h, then filters, takes filtrate and epipremnum aureum juice mixed
Close, stir 30min at 65 DEG C, be cooled to room temperature, filter, collect filtrate to get.
Fructus Gleditsiae Abnormalis extract：The method of the Fructus Gleditsiae Abnormalis extract is：Gleditsia sinensis explosion is crushed to 100-200 mesh and threonine
It is blended, with the mixture (volume ratio 1 of second alcohol and water：4) it is extracted as solvent at 50 DEG C, filtrate, concentration.
Gotu Kola P.E：The preparation method of the Gotu Kola P.E is as follows：Take centella raw material, 50-60 DEG C of drying,
Pulverizer is ground into coarse powder, by 1：Water is added in 13 ratios, and homogenate extraction 3-5min is extracted 2 times.
Herba Asari extract：The Herba Asari extract is commercially available.
Fructus Kochiae extract：The fruit of summer cypress is cleaned, chopping, impregnated for 24 hours with yellow rice wine, then dried, decocted 3 times with water, with
Jujube and ginger are medicine efficacy enhancing ingredient, and the weight ratio of water and the fruit of summer cypress is 8：1,40min is decocted every time, merges decoction liquor, and vacuum is dry
It is dry to get.
Cimicifuga foetida extract：Heretofore described cimicifuga foetida extract is commercially available.
Rhizoma Acori Graminei extract：Heretofore described Rhizoma Acori Graminei extract is commercially available.
Flaxseed gum：The flaxseed gum passes through combined processing, and steps are as follows for the combined processing：
Containing hydrogen silicone oil, divinylbenzene and chloroplatinic acid are 6 by S01 in mass ratio：3：1 hands at 120 DEG C after mixing
After connection reaction 12 hours, solid 1 is obtained；
Solid 1, cellulose and sepiolite powder are 1 by S02 in mass ratio：1：Ball milling 16 hours after 2 mixing；
S03 will obtain mixture and enclose lower high-temperature calcination in Ar atmosphere in S02；
S04 carries out acid etch to the calcined powder of S03 using hydrofluoric acid solution, and flaxseed gum is added after being washed to neutrality
Solution is warming up to 50 DEG C, after mixing evenly, can be prepared.
In the S03, the process of high-temperature calcination is as follows：
Being sintered initial temperature is 60 DEG C, rises to 500 DEG C with the speed of 2.5 DEG C/min, keeps the temperature 60min；Again with 6 DEG C/min's
Speed is warming up to 1200 DEG C and continues furnace cooling after 2 hours again.
In the S04, it is 7 that the flaxseed gum solution, which is formulated as flaxseed gum and water according to weight ratio,：10.
In the S04, the concentration of the hydrofluoric acid solution is 18%, and etch period is 5 hours.
Embodiment 4：The present embodiment provides a kind of raw materials for preparing of efficiently removal formaldehyde air purifying preparation to include at least：Lemon
3 parts of extract, 2 parts of jasmine extract, 0.8 part of tea tree extract, 6 parts of Flos Osmanthi Fragrantis extract, 2 parts of Lignum cinnamomi camphorae extract, epipremnum aureum mention
Take 3 parts of object, 8 parts of bracketplant extract, 0.3 part of eucalyptus extracts, 2 parts of Extractives From Melia Azedarach L, the white palm and 8 parts of epipremnum aureum extract, gleditsia sinensis
5 parts of extract, 2 parts of Gotu Kola P.E, 1.1 parts of Herba Asari extract, 2.0 parts of Fructus Kochiae extract, 4.3 parts of cimicifuga foetida extract,
12 parts of Rhizoma Acori Graminei extract, 8 parts of flaxseed gum, 2.1 parts of ethyl alcohol and 55 parts of water.
Lemon extract：The extracting method of the lemon extract is as follows：
Fresh Lemon is squeezed broken, takes clear lemon fluid, lemon extract can be prepared.
Jasmine extract：The extracting method of heretofore described jasmine extract is as follows：1. four-o'clock herb is dried in the shade, use
Plant pulverizer crushes, and crosses 40 meshes, adds 2~10 times of 95% ethyl alcohol of amount, be stored at room temperature extraction 1~7 day, and centre is stirred often,
Filtering, obtains leaching liquor；2~10 times of 95% alcohol steeps of amount are added in filter residue again, so extract three times, merge leaching liquor three times,
It is concentrated under reduced pressure with Rotary Evaporators, obtains dark brown stiff paste form up to Radix Mirabilis extract of the present invention；2. by four-o'clock herb yin
It is dry, it is crushed with plant pulverizer, crosses 40 meshes, add 2~10 times of 95% ethyl alcohol of amount, refluxing extraction 5~15 hours, filtering must return
Extracting solution is flowed, is concentrated under reduced pressure with Rotary Evaporators, obtains stiff paste form up to this Radix Mirabilis extract.
Tea tree extract：The extracting method of the tea tree extract is as follows：The blade of tea tree is chosen, after cleaning, takes 20g tree
Leaf carries out steam distillation to complete leaf without crushing, and distillation time is 18 hours, removes thick slag, obtains grease
After matter, after -10 DEG C freeze 12 hours, moisture removal is removed in air-distillation, then that the grease of acquisition is small in -10 DEG C of freezings 24
Shi Hou removes grease, takes thick slag, and after thick slag heating melting, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil,
Tea tree ethereal oil can be prepared.
Flos Osmanthi Fragrantis extract：The Flos Osmanthi Fragrantis extract is bought from Xi'an Jin Di Biotechnology Co., Ltd.
Lignum cinnamomi camphorae extract：In the present invention, the Lignum cinnamomi camphorae extract is commercially available.
Epipremnum aureum extract：Extracting method：The fresh blade obtained from epipremnum aureum plant is ground, and is 50-70 DEG C of second in temperature
20h is impregnated in the mixed liquor of acetoacetic ester and ethyl alcohol, after aqueous citric acid solution is added, stands extraction 1~7 day at room temperature, it is intermediate
Often it stirs, filters, obtain leaching liquor；So extract three times, merge leaching liquor three times, with Rotary Evaporators be concentrated under reduced pressure to get
Epipremnum aureum extract.
Bracketplant extract：The bracketplant extract is commercially available.
Eucalyptus extracts：The preparation method of the eucalyptus extracts is：By the powder of eucalyptus barks, ethyl alcohol is added, impregnates 2-
After 3h use extracting through microwave heating 2-3 time, filter, filtrate be concentrated under reduced pressure into no ethyl alcohol to get.
Extractives From Melia Azedarach L：The preparation method of the Extractives From Melia Azedarach L is as follows：China tree is shredded, after being soaked with ammonium hydroxide, then and
After clarifying limewash mixing, and ethyl alcohol is added, flow back 1-3h, filters, is concentrated while hot to obtain the final product.
The weight ratio for clarifying limewash and ethyl alcohol is 1：3.
The white palm and epipremnum aureum extract：The extracting method of the white palm and epipremnum aureum extract is as follows：By the epipremnum aureum of fresh picking
Juicing, obtains epipremnum aureum juice, for use；The white palm is shredded, gallic acid is added and impregnates 2h, then filters, takes filtrate and epipremnum aureum juice mixed
Close, stir 30min at 65 DEG C, be cooled to room temperature, filter, collect filtrate to get.
Fructus Gleditsiae Abnormalis extract：The method of the Fructus Gleditsiae Abnormalis extract is：Gleditsia sinensis explosion is crushed to 100-200 mesh and threonine
It is blended, with the mixture (volume ratio 1 of second alcohol and water：4) it is extracted as solvent at 50 DEG C, filtrate, concentration.
Gotu Kola P.E：The preparation method of the Gotu Kola P.E is as follows：Take centella raw material, 50-60 DEG C of drying,
Pulverizer is ground into coarse powder, by 1：Water is added in 13 ratios, and homogenate extraction 3-5min is extracted 2 times.
Herba Asari extract：The Herba Asari extract is commercially available.
Fructus Kochiae extract：The fruit of summer cypress is cleaned, chopping, impregnated for 24 hours with yellow rice wine, then dried, decocted 3 times with water, with
Jujube and ginger are medicine efficacy enhancing ingredient, and the weight ratio of water and the fruit of summer cypress is 8：1,40min is decocted every time, merges decoction liquor, and vacuum is dry
It is dry to get.
Cimicifuga foetida extract：Heretofore described cimicifuga foetida extract is commercially available.
Rhizoma Acori Graminei extract：Heretofore described Rhizoma Acori Graminei extract is commercially available.
Flaxseed gum：The flaxseed gum passes through combined processing, and steps are as follows for the combined processing：
Containing hydrogen silicone oil, divinylbenzene and chloroplatinic acid are 6 by S01 in mass ratio：3：1 hands at 120 DEG C after mixing
After connection reaction 12 hours, solid 1 is obtained；
Solid 1, cellulose and sepiolite powder are 1 by S02 in mass ratio：1：Ball milling 16 hours after 2 mixing；
S03 will obtain mixture and enclose lower high-temperature calcination in Ar atmosphere in S02；
S04 carries out acid etch to the calcined powder of S03 using hydrofluoric acid solution, and flaxseed gum is added after being washed to neutrality
Solution is warming up to 50 DEG C, after mixing evenly, can be prepared.
In the S03, the process of high-temperature calcination is as follows：
Being sintered initial temperature is 60 DEG C, rises to 500 DEG C with the speed of 2.5 DEG C/min, keeps the temperature 60min；Again with 6 DEG C/min's
Speed is warming up to 1200 DEG C and continues furnace cooling after 2 hours again.
In the S04, it is 7 that the flaxseed gum solution, which is formulated as flaxseed gum and water according to weight ratio,：10.
In the S04, the concentration of the hydrofluoric acid solution is 18%, and etch period is 5 hours.
Embodiment 5：The present embodiment provides a kind of raw materials for preparing of efficiently removal formaldehyde air purifying preparation to include at least：Lemon
3 parts of extract, 2 parts of jasmine extract, 0.8 part of tea tree extract, 6 parts of Flos Osmanthi Fragrantis extract, 2 parts of Lignum cinnamomi camphorae extract, epipremnum aureum mention
Take 3 parts of object, 8 parts of bracketplant extract, 0.3 part of eucalyptus extracts, 2 parts of Extractives From Melia Azedarach L, the white palm and 8 parts of epipremnum aureum extract, gleditsia sinensis
5 parts of extract, 2 parts of Gotu Kola P.E, 1.1 parts of Herba Asari extract, 2.0 parts of Fructus Kochiae extract, 4.3 parts of cimicifuga foetida extract,
12 parts of Rhizoma Acori Graminei extract, 8 parts of flaxseed gum, 2.1 parts of ethyl alcohol and 55 parts of water.
Lemon extract：The extracting method of the lemon extract is as follows：
(1) Fresh Lemon is squeezed broken, takes clear lemon fluid；
(2) by lemon fluid and formic acid obtained in step (1) according to 20：1 mixing, can be prepared lemon extract.
Jasmine extract：The extracting method of heretofore described jasmine extract is as follows：1. four-o'clock herb is dried in the shade, use
Plant pulverizer crushes, and crosses 40 meshes, adds 2~10 times of 95% ethyl alcohol of amount, be stored at room temperature extraction 1~7 day, and centre is stirred often,
Filtering, obtains leaching liquor；2~10 times of 95% alcohol steeps of amount are added in filter residue again, so extract three times, merge leaching liquor three times,
It is concentrated under reduced pressure with Rotary Evaporators, obtains dark brown stiff paste form up to Radix Mirabilis extract of the present invention；2. by four-o'clock herb yin
It is dry, it is crushed with plant pulverizer, crosses 40 meshes, add 2~10 times of 95% ethyl alcohol of amount, refluxing extraction 5~15 hours, filtering must return
Extracting solution is flowed, is concentrated under reduced pressure with Rotary Evaporators, obtains stiff paste form up to this Radix Mirabilis extract.
Tea tree extract：The extracting method of the tea tree extract is as follows：The blade of tea tree is chosen, after cleaning, takes 20g tree
Leaf carries out steam distillation to complete leaf without crushing, and distillation time is 18 hours, removes thick slag, obtains grease
After matter, after -10 DEG C freeze 12 hours, moisture removal is removed in air-distillation, then that the grease of acquisition is small in -10 DEG C of freezings 24
Shi Hou removes grease, takes thick slag, and after thick slag heating melting, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil,
Tea tree ethereal oil can be prepared.
Flos Osmanthi Fragrantis extract：The Flos Osmanthi Fragrantis extract is bought from Xi'an Jin Di Biotechnology Co., Ltd.
Lignum cinnamomi camphorae extract：In the present invention, the Lignum cinnamomi camphorae extract is commercially available.
Epipremnum aureum extract：Extracting method：The fresh blade obtained from epipremnum aureum plant is ground, and is 50-70 DEG C of second in temperature
20h is impregnated in the mixed liquor of acetoacetic ester and ethyl alcohol, stands extraction 1~7 day at room temperature, centre is stirred often, is filtered, must be soaked
Extract；It so extracts three times, merges leaching liquor three times, be concentrated under reduced pressure with Rotary Evaporators to get epipremnum aureum extract.
Bracketplant extract：The bracketplant extract is commercially available.
Eucalyptus extracts：The preparation method of the eucalyptus extracts is：By the powder of eucalyptus barks, ethyl alcohol is added, impregnates 2-
After 3h use extracting through microwave heating 2-3 time, filter, filtrate be concentrated under reduced pressure into no ethyl alcohol to get.
Extractives From Melia Azedarach L：The preparation method of the Extractives From Melia Azedarach L is as follows：China tree is shredded, after being soaked with ammonium hydroxide, then and
After clarifying limewash mixing, and ethyl alcohol is added, flow back 1-3h, filters, is concentrated while hot to obtain the final product.
The weight ratio for clarifying limewash and ethyl alcohol is 1：3.
The white palm and epipremnum aureum extract：The extracting method of the white palm and epipremnum aureum extract is as follows：By the epipremnum aureum of fresh picking
Juicing, obtains epipremnum aureum juice, for use；The white palm is shredded, gallic acid is added and impregnates 2h, then filters, takes filtrate and epipremnum aureum juice mixed
Close, stir 30min at 65 DEG C, be cooled to room temperature, filter, collect filtrate to get.
Fructus Gleditsiae Abnormalis extract：The method of the Fructus Gleditsiae Abnormalis extract is：Gleditsia sinensis explosion is crushed to 100-200 mesh and threonine
It is blended, with the mixture (volume ratio 1 of second alcohol and water：4) it is extracted as solvent at 50 DEG C, filtrate, concentration.
Gotu Kola P.E：The preparation method of the Gotu Kola P.E is as follows：Take centella raw material, 50-60 DEG C of drying,
Pulverizer is ground into coarse powder, by 1：Water is added in 13 ratios, and homogenate extraction 3-5min is extracted 2 times.
Herba Asari extract：The Herba Asari extract is commercially available.
Fructus Kochiae extract：The fruit of summer cypress is cleaned, chopping, impregnated for 24 hours with yellow rice wine, then dried, decocted 3 times with water, with
Jujube and ginger are medicine efficacy enhancing ingredient, and the weight ratio of water and the fruit of summer cypress is 8：1,40min is decocted every time, merges decoction liquor, and vacuum is dry
It is dry to get.
Cimicifuga foetida extract：Heretofore described cimicifuga foetida extract is commercially available.
Rhizoma Acori Graminei extract：Heretofore described Rhizoma Acori Graminei extract is commercially available.
Flaxseed gum：The flaxseed gum passes through combined processing, and steps are as follows for the combined processing：
Containing hydrogen silicone oil, divinylbenzene and chloroplatinic acid are 6 by S01 in mass ratio：3：1 hands at 120 DEG C after mixing
After connection reaction 12 hours, solid 1 is obtained；
Solid 1, cellulose and sepiolite powder are 1 by S02 in mass ratio：1：Ball milling 16 hours after 2 mixing；
S03 will obtain mixture and enclose lower high-temperature calcination in Ar atmosphere in S02；
S04 carries out acid etch to the calcined powder of S03 using hydrofluoric acid solution, and flaxseed gum is added after being washed to neutrality
Solution is warming up to 50 DEG C, after mixing evenly, can be prepared.
In the S03, the process of high-temperature calcination is as follows：
Being sintered initial temperature is 60 DEG C, rises to 500 DEG C with the speed of 2.5 DEG C/min, keeps the temperature 60min；Again with 6 DEG C/min's
Speed is warming up to 1200 DEG C and continues furnace cooling after 2 hours again.
In the S04, it is 7 that the flaxseed gum solution, which is formulated as flaxseed gum and water according to weight ratio,：10.
In the S04, the concentration of the hydrofluoric acid solution is 18%, and etch period is 5 hours.
Embodiment 6：The present embodiment provides a kind of raw materials for preparing of efficiently removal formaldehyde air purifying preparation to include at least：Lemon
3 parts of extract, 2 parts of jasmine extract, 0.8 part of tea tree extract, 6 parts of Flos Osmanthi Fragrantis extract, 2 parts of Lignum cinnamomi camphorae extract, epipremnum aureum mention
Take 3 parts of object, 8 parts of bracketplant extract, 0.3 part of eucalyptus extracts, 2 parts of Extractives From Melia Azedarach L, the white palm and 8 parts of epipremnum aureum extract, gleditsia sinensis
5 parts of extract, 2 parts of Gotu Kola P.E, 1.1 parts of Herba Asari extract, 2.0 parts of Fructus Kochiae extract, 4.3 parts of cimicifuga foetida extract,
12 parts of Rhizoma Acori Graminei extract, 8 parts of flaxseed gum, 2.1 parts of ethyl alcohol and 55 parts of water.
Lemon extract：The extracting method of the lemon extract is as follows：
(1) Fresh Lemon is squeezed broken, takes clear lemon fluid；
(2) by lemon fluid and formic acid obtained in step (1) according to 20：1 mixing, can be prepared lemon extract.
Jasmine extract：The extracting method of heretofore described jasmine extract is as follows：1. four-o'clock herb is dried in the shade, use
Plant pulverizer crushes, and crosses 40 meshes, adds 2~10 times of 95% ethyl alcohol of amount, be stored at room temperature extraction 1~7 day, and centre is stirred often,
Filtering, obtains leaching liquor；2~10 times of 95% alcohol steeps of amount are added in filter residue again, so extract three times, merge leaching liquor three times,
It is concentrated under reduced pressure with Rotary Evaporators, obtains dark brown stiff paste form up to Radix Mirabilis extract of the present invention；2. by four-o'clock herb yin
It is dry, it is crushed with plant pulverizer, crosses 40 meshes, add 2~10 times of 95% ethyl alcohol of amount, refluxing extraction 5~15 hours, filtering must return
Extracting solution is flowed, is concentrated under reduced pressure with Rotary Evaporators, obtains stiff paste form up to this Radix Mirabilis extract.
Tea tree extract：The extracting method of the tea tree extract is as follows：The blade of tea tree is chosen, after cleaning, takes 20g tree
Leaf carries out steam distillation to complete leaf without crushing, and distillation time is 18 hours, removes thick slag, obtains grease
After matter, after -10 DEG C freeze 12 hours, moisture removal is removed in air-distillation, then that the grease of acquisition is small in -10 DEG C of freezings 24
Shi Hou removes grease, takes thick slag, and after thick slag heating melting, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil,
Tea tree ethereal oil can be prepared.
Flos Osmanthi Fragrantis extract：The Flos Osmanthi Fragrantis extract is bought from Xi'an Jin Di Biotechnology Co., Ltd.
Lignum cinnamomi camphorae extract：In the present invention, the Lignum cinnamomi camphorae extract is commercially available.
Epipremnum aureum extract：Extracting method：The fresh blade obtained from epipremnum aureum plant is ground, and is 50-70 DEG C of second in temperature
20h is impregnated in the mixed liquor of acetoacetic ester and ethyl alcohol, after aqueous citric acid solution is added, stands extraction 1~7 day at room temperature, it is intermediate
Often it stirs, filters, obtain leaching liquor；So extract three times, merge leaching liquor three times, with Rotary Evaporators be concentrated under reduced pressure to get
Epipremnum aureum extract.
Bracketplant extract：The bracketplant extract is commercially available.
Eucalyptus extracts：The preparation method of the eucalyptus extracts is：By the powder of eucalyptus barks, ethyl alcohol is added, impregnates 2-
After 3h use extracting through microwave heating 2-3 time, filter, filtrate be concentrated under reduced pressure into no ethyl alcohol to get.
Extractives From Melia Azedarach L：The preparation method of the Extractives From Melia Azedarach L is as follows：China tree is shredded, after being soaked with ammonium hydroxide, then and
Ethyl alcohol mixing, flow back 1-3h, filters, is concentrated while hot to obtain the final product.
The white palm and epipremnum aureum extract：The extracting method of the white palm and epipremnum aureum extract is as follows：By the epipremnum aureum of fresh picking
Juicing, obtains epipremnum aureum juice, for use；The white palm is shredded, gallic acid is added and impregnates 2h, then filters, takes filtrate and epipremnum aureum juice mixed
Close, stir 30min at 65 DEG C, be cooled to room temperature, filter, collect filtrate to get.
Fructus Gleditsiae Abnormalis extract：The method of the Fructus Gleditsiae Abnormalis extract is：Gleditsia sinensis explosion is crushed to 100-200 mesh and threonine
It is blended, with the mixture (volume ratio 1 of second alcohol and water：4) it is extracted as solvent at 50 DEG C, filtrate, concentration.
Gotu Kola P.E：The preparation method of the Gotu Kola P.E is as follows：Take centella raw material, 50-60 DEG C of drying,
Pulverizer is ground into coarse powder, by 1：Water is added in 13 ratios, and homogenate extraction 3-5min is extracted 2 times.
Herba Asari extract：The Herba Asari extract is commercially available.
Fructus Kochiae extract：The fruit of summer cypress is cleaned, chopping, impregnated for 24 hours with yellow rice wine, then dried, decocted 3 times with water, with
Jujube and ginger are medicine efficacy enhancing ingredient, and the weight ratio of water and the fruit of summer cypress is 8：1,40min is decocted every time, merges decoction liquor, and vacuum is dry
It is dry to get.
Cimicifuga foetida extract：Heretofore described cimicifuga foetida extract is commercially available.
Rhizoma Acori Graminei extract：Heretofore described Rhizoma Acori Graminei extract is commercially available.
Flaxseed gum：The flaxseed gum passes through combined processing, and steps are as follows for the combined processing：
Containing hydrogen silicone oil, divinylbenzene and chloroplatinic acid are 6 by S01 in mass ratio：3：1 hands at 120 DEG C after mixing
After connection reaction 12 hours, solid 1 is obtained；
Solid 1, cellulose and sepiolite powder are 1 by S02 in mass ratio：1：Ball milling 16 hours after 2 mixing；
S03 will obtain mixture and enclose lower high-temperature calcination in Ar atmosphere in S02；
S04 carries out acid etch to the calcined powder of S03 using hydrofluoric acid solution, and flaxseed gum is added after being washed to neutrality
Solution is warming up to 50 DEG C, after mixing evenly, can be prepared.
In the S03, the process of high-temperature calcination is as follows：
Being sintered initial temperature is 60 DEG C, rises to 500 DEG C with the speed of 2.5 DEG C/min, keeps the temperature 60min；Again with 6 DEG C/min's
Speed is warming up to 1200 DEG C and continues furnace cooling after 2 hours again.
In the S04, it is 7 that the flaxseed gum solution, which is formulated as flaxseed gum and water according to weight ratio,：10.
In the S04, the concentration of the hydrofluoric acid solution is 18%, and etch period is 5 hours.
Embodiment 7：The present embodiment provides a kind of raw materials for preparing of efficiently removal formaldehyde air purifying preparation to include at least：Lemon
3 parts of extract, 2 parts of jasmine extract, 0.8 part of tea tree extract, 6 parts of Flos Osmanthi Fragrantis extract, 2 parts of Lignum cinnamomi camphorae extract, epipremnum aureum mention
Take 3 parts of object, 8 parts of bracketplant extract, 0.3 part of eucalyptus extracts, 2 parts of Extractives From Melia Azedarach L, the white palm and 8 parts of epipremnum aureum extract, gleditsia sinensis
5 parts of extract, 2 parts of Gotu Kola P.E, 1.1 parts of Herba Asari extract, 2.0 parts of Fructus Kochiae extract, 4.3 parts of cimicifuga foetida extract,
12 parts of Rhizoma Acori Graminei extract, 8 parts of flaxseed gum, 2.1 parts of ethyl alcohol and 55 parts of water.
Lemon extract：The extracting method of the lemon extract is as follows：
(1) Fresh Lemon is squeezed broken, takes clear lemon fluid；
(2) by lemon fluid and formic acid obtained in step (1) according to 20：1 mixing, can be prepared lemon extract.
Jasmine extract：The extracting method of heretofore described jasmine extract is as follows：1. four-o'clock herb is dried in the shade, use
Plant pulverizer crushes, and crosses 40 meshes, adds 2~10 times of 95% ethyl alcohol of amount, be stored at room temperature extraction 1~7 day, and centre is stirred often,
Filtering, obtains leaching liquor；2~10 times of 95% alcohol steeps of amount are added in filter residue again, so extract three times, merge leaching liquor three times,
It is concentrated under reduced pressure with Rotary Evaporators, obtains dark brown stiff paste form up to Radix Mirabilis extract of the present invention；2. by four-o'clock herb yin
It is dry, it is crushed with plant pulverizer, crosses 40 meshes, add 2~10 times of 95% ethyl alcohol of amount, refluxing extraction 5~15 hours, filtering must return
Extracting solution is flowed, is concentrated under reduced pressure with Rotary Evaporators, obtains stiff paste form up to this Radix Mirabilis extract.
Tea tree extract：The extracting method of the tea tree extract is as follows：The blade of tea tree is chosen, after cleaning, takes 20g tree
Leaf carries out steam distillation to complete leaf without crushing, and distillation time is 18 hours, removes thick slag, obtains grease
After matter, after -10 DEG C freeze 12 hours, moisture removal is removed in air-distillation, then that the grease of acquisition is small in -10 DEG C of freezings 24
Shi Hou removes grease, takes thick slag, and after thick slag heating melting, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil,
Tea tree ethereal oil can be prepared.
Flos Osmanthi Fragrantis extract：The Flos Osmanthi Fragrantis extract is bought from Xi'an Jin Di Biotechnology Co., Ltd.
Lignum cinnamomi camphorae extract：In the present invention, the Lignum cinnamomi camphorae extract is commercially available.
Epipremnum aureum extract：Extracting method：The fresh blade obtained from epipremnum aureum plant is ground, and is 50-70 DEG C of second in temperature
20h is impregnated in the mixed liquor of acetoacetic ester and ethyl alcohol, after aqueous citric acid solution is added, stands extraction 1~7 day at room temperature, it is intermediate
Often it stirs, filters, obtain leaching liquor；So extract three times, merge leaching liquor three times, with Rotary Evaporators be concentrated under reduced pressure to get
Epipremnum aureum extract.
Bracketplant extract：The bracketplant extract is commercially available.
Eucalyptus extracts：The preparation method of the eucalyptus extracts is：By the powder of eucalyptus barks, ethyl alcohol is added, impregnates 2-
After 3h use extracting through microwave heating 2-3 time, filter, filtrate be concentrated under reduced pressure into no ethyl alcohol to get.
Extractives From Melia Azedarach L：The preparation method of the Extractives From Melia Azedarach L is as follows：China tree is shredded, after being soaked with ammonium hydroxide, then and
After clarifying limewash mixing, and ethyl alcohol is added, flow back 1-3h, filters, is concentrated while hot to obtain the final product.
The weight ratio for clarifying limewash and ethyl alcohol is 1：3.
The white palm and epipremnum aureum extract：The extracting method of the white palm and epipremnum aureum extract is as follows：By the epipremnum aureum of fresh picking
Juicing, obtains epipremnum aureum juice, for use；The white palm is shredded, gallic acid is added and impregnates 2h, then filters, takes filtrate and epipremnum aureum juice mixed
Close, stir 30min at 65 DEG C, be cooled to room temperature, filter, collect filtrate to get.
Fructus Gleditsiae Abnormalis extract：The method of the Fructus Gleditsiae Abnormalis extract is：Gleditsia sinensis explosion is crushed to 100-200 mesh, with ethyl alcohol and
Mixture (the volume ratio 1 of water：4) it is extracted as solvent at 50 DEG C, filtrate, concentration.
Gotu Kola P.E：The preparation method of the Gotu Kola P.E is as follows：Take centella raw material, 50-60 DEG C of drying,
Pulverizer is ground into coarse powder, by 1：Water is added in 13 ratios, and homogenate extraction 3-5min is extracted 2 times.
Herba Asari extract：The Herba Asari extract is commercially available.
Fructus Kochiae extract：The fruit of summer cypress is cleaned, chopping, impregnated for 24 hours with yellow rice wine, then dried, decocted 3 times with water, with
Jujube and ginger are medicine efficacy enhancing ingredient, and the weight ratio of water and the fruit of summer cypress is 8：1,40min is decocted every time, merges decoction liquor, and vacuum is dry
It is dry to get.
Cimicifuga foetida extract：Heretofore described cimicifuga foetida extract is commercially available.
Rhizoma Acori Graminei extract：Heretofore described Rhizoma Acori Graminei extract is commercially available.
Flaxseed gum：The flaxseed gum passes through combined processing, and steps are as follows for the combined processing：
Containing hydrogen silicone oil, divinylbenzene and chloroplatinic acid are 6 by S01 in mass ratio：3：1 hands at 120 DEG C after mixing
After connection reaction 12 hours, solid 1 is obtained；
Solid 1, cellulose and sepiolite powder are 1 by S02 in mass ratio：1：Ball milling 16 hours after 2 mixing；
S03 will obtain mixture and enclose lower high-temperature calcination in Ar atmosphere in S02；
S04 carries out acid etch to the calcined powder of S03 using hydrofluoric acid solution, and flaxseed gum is added after being washed to neutrality
Solution is warming up to 50 DEG C, after mixing evenly, can be prepared.
In the S03, the process of high-temperature calcination is as follows：
Being sintered initial temperature is 60 DEG C, rises to 500 DEG C with the speed of 2.5 DEG C/min, keeps the temperature 60min；Again with 6 DEG C/min's
Speed is warming up to 1200 DEG C and continues furnace cooling after 2 hours again.
In the S04, it is 7 that the flaxseed gum solution, which is formulated as flaxseed gum and water according to weight ratio,：10.
In the S04, the concentration of the hydrofluoric acid solution is 18%, and etch period is 5 hours.
Embodiment 8：The present embodiment provides a kind of raw materials for preparing of efficiently removal formaldehyde air purifying preparation to include at least：Lemon
3 parts of extract, 2 parts of jasmine extract, 0.8 part of tea tree extract, 6 parts of Flos Osmanthi Fragrantis extract, 2 parts of Lignum cinnamomi camphorae extract, epipremnum aureum mention
Take 3 parts of object, 8 parts of bracketplant extract, 0.3 part of eucalyptus extracts, 2 parts of Extractives From Melia Azedarach L, the white palm and 8 parts of epipremnum aureum extract, gleditsia sinensis
5 parts of extract, 2 parts of Gotu Kola P.E, 1.1 parts of Herba Asari extract, 2.0 parts of Fructus Kochiae extract, 4.3 parts of cimicifuga foetida extract,
12 parts of Rhizoma Acori Graminei extract, 8 parts of flaxseed gum, 2.1 parts of ethyl alcohol and 55 parts of water.
Lemon extract：The extracting method of the lemon extract is as follows：
(1) Fresh Lemon is squeezed broken, takes clear lemon fluid；
(2) by lemon fluid and formic acid obtained in step (1) according to 20：1 mixing, can be prepared lemon extract.
Jasmine extract：The extracting method of heretofore described jasmine extract is as follows：1. four-o'clock herb is dried in the shade, use
Plant pulverizer crushes, and crosses 40 meshes, adds 2~10 times of 95% ethyl alcohol of amount, be stored at room temperature extraction 1~7 day, and centre is stirred often,
Filtering, obtains leaching liquor；2~10 times of 95% alcohol steeps of amount are added in filter residue again, so extract three times, merge leaching liquor three times,
It is concentrated under reduced pressure with Rotary Evaporators, obtains dark brown stiff paste form up to Radix Mirabilis extract of the present invention；2. by four-o'clock herb yin
It is dry, it is crushed with plant pulverizer, crosses 40 meshes, add 2~10 times of 95% ethyl alcohol of amount, refluxing extraction 5~15 hours, filtering must return
Extracting solution is flowed, is concentrated under reduced pressure with Rotary Evaporators, obtains stiff paste form up to this Radix Mirabilis extract.
Tea tree extract：The extracting method of the tea tree extract is as follows：The blade of tea tree is chosen, after cleaning, takes 20g tree
Leaf carries out steam distillation to complete leaf without crushing, and distillation time is 18 hours, removes thick slag, obtains grease
After matter, after -10 DEG C freeze 12 hours, moisture removal is removed in air-distillation, then that the grease of acquisition is small in -10 DEG C of freezings 24
Shi Hou removes grease, takes thick slag, and after thick slag heating melting, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil,
Tea tree ethereal oil can be prepared.
Flos Osmanthi Fragrantis extract：The Flos Osmanthi Fragrantis extract is bought from Xi'an Jin Di Biotechnology Co., Ltd.
Lignum cinnamomi camphorae extract：In the present invention, the Lignum cinnamomi camphorae extract is commercially available.
Epipremnum aureum extract：Extracting method：The fresh blade obtained from epipremnum aureum plant is ground, and is 50-70 DEG C of second in temperature
20h is impregnated in the mixed liquor of acetoacetic ester and ethyl alcohol, after aqueous citric acid solution is added, stands extraction 1~7 day at room temperature, it is intermediate
Often it stirs, filters, obtain leaching liquor；So extract three times, merge leaching liquor three times, with Rotary Evaporators be concentrated under reduced pressure to get
Epipremnum aureum extract.
Bracketplant extract：The bracketplant extract is commercially available.
Eucalyptus extracts：The preparation method of the eucalyptus extracts is：By the powder of eucalyptus barks, ethyl alcohol is added, impregnates 2-
After 3h use extracting through microwave heating 2-3 time, filter, filtrate be concentrated under reduced pressure into no ethyl alcohol to get.
Extractives From Melia Azedarach L：The preparation method of the Extractives From Melia Azedarach L is as follows：China tree is shredded, after being soaked with ammonium hydroxide, then and
After clarifying limewash mixing, and ethyl alcohol is added, flow back 1-3h, filters, is concentrated while hot to obtain the final product.
The weight ratio for clarifying limewash and ethyl alcohol is 1：3.
The white palm and epipremnum aureum extract：The extracting method of the white palm and epipremnum aureum extract is as follows：By the epipremnum aureum of fresh picking
Juicing, obtains epipremnum aureum juice, for use；The white palm is shredded, gallic acid is added and impregnates 2h, then filters, takes filtrate and epipremnum aureum juice mixed
Close, stir 30min at 65 DEG C, be cooled to room temperature, filter, collect filtrate to get.
Fructus Gleditsiae Abnormalis extract：The method of the Fructus Gleditsiae Abnormalis extract is：Gleditsia sinensis explosion is crushed to 100-200 mesh and threonine
It is blended, with the mixture (volume ratio 1 of second alcohol and water：4) it is extracted as solvent at 50 DEG C, filtrate, concentration.
Gotu Kola P.E：The preparation method of the Gotu Kola P.E is as follows：Take centella raw material, 50-60 DEG C of drying,
Pulverizer is ground into coarse powder, by 1：Water is added in 13 ratios, and homogenate extraction 3-5min is extracted 2 times.
Herba Asari extract：The Herba Asari extract is commercially available.
Fructus Kochiae extract：The fruit of summer cypress is cleaned, chopping, impregnated for 24 hours with yellow rice wine, then dried, decocted 3 times with water, with
Jujube and ginger are medicine efficacy enhancing ingredient, and the weight ratio of water and the fruit of summer cypress is 8：1,40min is decocted every time, merges decoction liquor, and vacuum is dry
It is dry to get.
Cimicifuga foetida extract：Heretofore described cimicifuga foetida extract is commercially available.
Rhizoma Acori Graminei extract：Heretofore described Rhizoma Acori Graminei extract is commercially available.
The preparation process of embodiment 1-8 is as follows：
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
S02 is cooled to 45 DEG C, with interval 20 minutes for standard, sequentially adds and prepares raw material (except ethyl alcohol), after mixing evenly；
After S03 is cooled to room temperature, ethyl alcohol is added, it is after mixing evenly, filling.
Performance test：
1, physicochemical property is tested
Resistance to Thermal test：Sample is put into the electro-heating standing-temperature cultivator of (40 ± 1) DEG C for 24 hours, is seen whether after restoring room temperature
There is phenomena such as thinning, discoloration, layering and firmness change, with the heat resistance of judgement sample；
Low temperature resistant test：Sample is put into the refrigerator of (- 5~-10) DEG C ± 1 DEG C for 24 hours, has been seen whether after restoring room temperature
Phenomena such as thinning, discoloration, layering and firmness change, with the cold tolerance of judgement sample；
It the results are shown in Table 1
Table 1
| Embodiment | Resistance to Thermal test | Low temperature resistant test |
| Embodiment 1 | Stablize | Stablize |
| Embodiment 2 | Stablize | Stablize |
| Embodiment 3 | Stablize | Stablize |
| Embodiment 4 | Discoloration | Layering |
| Embodiment 5 | Discoloration | Stablize |
| Embodiment 6 | Discoloration | Layering |
| Embodiment 7 | Stablize | Layering |
| Embodiment 8 | Discoloration | Layering |
2, formaldehyde performance test is removed：
1), room temperature removes formaldehyde performance test (25 DEG C)
According to national standard QB-T2761-2006《Indoor air purification product clean-up effect measuring method》Experimental provision is built,
Carry out experiment test.Will 1 square metre of floor of release formaldehyde be placed in 10 square metres of blank cabins, after placing for 24 hours,
It detects in blank cabin, the concentration of formaldehyde is 10 milligrams/cubic metre, is respectively individually positioned in the product of 5g Examples 1 to 8 often
In a blank cabin, and the light source that power is 1W is placed in blank cabin, after 12 hours, detect the concentration of blank cabin formaldehyde.First
The removal rate of aldehyde=(initial concentration-sample solution concentration) × 100/ initial concentration, test result are shown in Table.
2), high temperature removes formaldehyde performance test (100 DEG C)
The temperature in blank cabin is increased to 100 DEG C, repeats above-mentioned test.
Table 2 removes formaldehyde test result
The foregoing is merely presently preferred embodiments of the present invention, is not intended to limit the invention, it is all in spirit of the invention and
Within principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of efficiently removal formaldehyde air purifying preparation, which is characterized in that the preparation of the efficient removal formaldehyde air purifying preparation
Raw material includes at least：Lemon extract, jasmine extract, tea tree extract, Flos Osmanthi Fragrantis extract, Lignum cinnamomi camphorae extract, epipremnum aureum are extracted
Object, bracketplant extract, eucalyptus extracts, Extractives From Melia Azedarach L, it is white the palm and epipremnum aureum extract, Fructus Gleditsiae Abnormalis extract, Gotu Kola P.E,
Herba Asari extract, Fructus Kochiae extract, cimicifuga foetida extract, second alcohol and water.
2. a kind of efficiently removal formaldehyde air purifying preparation described in claim 1, which is characterized in that by weight, the height
The raw material for preparing of effect removal formaldehyde air purifying preparation includes at least：1-5 parts of lemon extract, 1-3 parts of jasmine extract, tea tree mention
Take 0.1-1.5 parts of object, 5-10 parts of Flos Osmanthi Fragrantis extract, 1-3 parts of Lignum cinnamomi camphorae extract, 1-5 parts of epipremnum aureum extract, bracketplant extract 5-15
Part, 0.1-0.5 parts of eucalyptus extracts, 1-3 parts of Extractives From Melia Azedarach L, the white palm and 5-10 parts of epipremnum aureum extract, Fructus Gleditsiae Abnormalis extract 1-8
Part, 1-3 parts of Gotu Kola P.E, 0.5-1.5 parts of Herba Asari extract, 1.5-3.5 parts of Fructus Kochiae extract, cimicifuga foetida extract 3.5-
6.5 parts, 0.1-3 parts of ethyl alcohol and 50-60 parts of water.
3. a kind of efficiently removal formaldehyde air purifying preparation described in claim 1, which is characterized in that by weight, the height
The raw material for preparing of effect removal formaldehyde air purifying preparation includes at least：3 parts of lemon extract, 2 parts of jasmine extract, tea tree extract
0.8 part, 6 parts of Flos Osmanthi Fragrantis extract, 2 parts of Lignum cinnamomi camphorae extract, 3 parts of epipremnum aureum extract, 8 parts of bracketplant extract, eucalyptus extracts 0.3
Part, 2 parts of Extractives From Melia Azedarach L, the white palm and 8 parts of epipremnum aureum extract, 5 parts of Fructus Gleditsiae Abnormalis extract, 2 parts of Gotu Kola P.E, Herba Asari extract
1.1 parts, 2.0 parts of Fructus Kochiae extract, 4.3 parts of cimicifuga foetida extract, 2.1 parts of ethyl alcohol and 55 parts of water.
4. a kind of efficiently removal formaldehyde air purifying preparation described in claim 1, which is characterized in that the efficient removal formaldehyde is empty
Gas cleanser prepares raw material also and includes 10-15 parts and flaxseed gum 5-10 parts of Rhizoma Acori Graminei extract.
5. a kind of efficiently removal formaldehyde air purifying preparation as claimed in claim 4, which is characterized in that the flaxseed gum is by multiple
Conjunction processing, steps are as follows for the combined processing：
Containing hydrogen silicone oil, divinylbenzene and chloroplatinic acid are 6 by S01 in mass ratio：3：1 is crosslinked instead at 120 DEG C after mixing
After answering 12 hours, solid 1 is obtained；
Solid 1, cellulose and sepiolite powder are 1 by S02 in mass ratio：1：Ball milling 16 hours after 2 mixing；
S03 will obtain mixture and enclose lower high-temperature calcination in Ar atmosphere in S02；
S04 carries out acid etch to the calcined powder of S03 using hydrofluoric acid solution, and linseed peptization is added after being washed to neutrality
Liquid is warming up to 50 DEG C, after mixing evenly, can be prepared.
6. one kind described in claim 5 efficiently removes formaldehyde air purifying preparation, which is characterized in that in the S03, high-temperature calcination
Process it is as follows：
Being sintered initial temperature is 60 DEG C, rises to 500 DEG C with the speed of 2.5 DEG C/min, keeps the temperature 60min；Again with the speed of 6 DEG C/min
It is warming up to 1200 DEG C and continues furnace cooling after 2 hours again.
7. one kind described in claim 5 efficiently removes formaldehyde air purifying preparation, which is characterized in that in the S04, described flax
It is 7 that seed sol solution, which is formulated as flaxseed gum and water according to weight ratio,：10.
8. one kind described in claim 5 efficiently removes formaldehyde air purifying preparation, which is characterized in that in the S04, the hydrogen fluorine
The concentration of acid solution is 18%, and etch period is 5 hours.
9. a kind of efficiently removal formaldehyde air purifying preparation described in claim 1, which is characterized in that the lemon extract mentions
Take method as follows：
(1) Fresh Lemon is squeezed broken, takes clear lemon fluid；
(2) by lemon fluid and formic acid obtained in step (1) according to 20：1 mixing, can be prepared lemon extract.
10. a kind of efficiently removal formaldehyde air purifying preparation described in claim 1, which is characterized in that the Fructus Kochiae extract
Preparation method it is as follows：
The extracting method of Fructus Kochiae extract is to clean the fruit of summer cypress, chopping, is impregnated for 24 hours with yellow rice wine, then dries, use decocting
It boils 3 times, using jujube and ginger as medicine efficacy enhancing ingredient, the weight ratio of water and the fruit of summer cypress is 8：1,40min is decocted every time, merges decoction liquor,
Vacuum drying to get.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109621668A (en) * | 2018-12-07 | 2019-04-16 | 杭州合辰环境有限公司 | A kind of plant source reagent and preparation method thereof with function of removing formaldehyde |
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| CN101461954A (en) * | 2007-12-18 | 2009-06-24 | 施忠菊 | Plant composition for air purification agent |
| CN103007325A (en) * | 2012-12-07 | 2013-04-03 | 常州大学 | Air purifying agent containing plant essential oil |
| CN104958774A (en) * | 2015-06-11 | 2015-10-07 | 北京清科慧谷科技发展有限公司 | Air purification plant composition and making method thereof |
| CN107670463A (en) * | 2017-09-28 | 2018-02-09 | 安徽省银锂子生物科技发展有限公司 | It can sterilize, absorb formaldehyde and absorb the automobile air purifying agent of haze |
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| CN101461954A (en) * | 2007-12-18 | 2009-06-24 | 施忠菊 | Plant composition for air purification agent |
| CN103007325A (en) * | 2012-12-07 | 2013-04-03 | 常州大学 | Air purifying agent containing plant essential oil |
| CN104958774A (en) * | 2015-06-11 | 2015-10-07 | 北京清科慧谷科技发展有限公司 | Air purification plant composition and making method thereof |
| CN107670463A (en) * | 2017-09-28 | 2018-02-09 | 安徽省银锂子生物科技发展有限公司 | It can sterilize, absorb formaldehyde and absorb the automobile air purifying agent of haze |
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| CN109621668A (en) * | 2018-12-07 | 2019-04-16 | 杭州合辰环境有限公司 | A kind of plant source reagent and preparation method thereof with function of removing formaldehyde |
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