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CN108863586A - A kind of youth-and-old-age biology base manure and preparation method thereof - Google Patents

A kind of youth-and-old-age biology base manure and preparation method thereof Download PDF

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Publication number
CN108863586A
CN108863586A CN201810914353.0A CN201810914353A CN108863586A CN 108863586 A CN108863586 A CN 108863586A CN 201810914353 A CN201810914353 A CN 201810914353A CN 108863586 A CN108863586 A CN 108863586A
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China
Prior art keywords
added
powder
youth
old
age
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CN201810914353.0A
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Chinese (zh)
Inventor
李理想
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Wuhu March Horticulture Design Co Ltd
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Wuhu March Horticulture Design Co Ltd
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Priority to CN201810914353.0A priority Critical patent/CN108863586A/en
Publication of CN108863586A publication Critical patent/CN108863586A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C3/00Fertilisers containing other salts of ammonia or ammonia itself, e.g. gas liquor
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Biotechnology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Molecular Biology (AREA)
  • Treatment Of Sludge (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a kind of youth-and-old-age biology base manure, it is made of the raw material of following weight parts:Polyglyceryl fatty acid ester 0.7-1, furfural dregs 30-50, polyethylene glycol 2-4, maize cob meal 10-16, D-araboascorbic acid sodium 0.1-0.2, Tea Saponin 0.6-1, magnesium sulfate 4-7, doping scolecite powder 100-110, cotton seed hulls 10-20, tall oil 2-3, base manure of the invention is using biomass as raw material, Safety and Environmental Protection is good, it is full of nutrition, the various nutritional needs that youth-and-old-age growth phase can effectively be met, accelerate its healthy growth.

Description

A kind of youth-and-old-age biology base manure and preparation method thereof
Technical field
The invention belongs to fertilizer fields, and in particular to a kind of youth-and-old-age biology base manure and preparation method thereof.
Background technique
Youth-and-old-age is annual herb, and stem is upright, 30-100 centimetres high, by rough hair or long bristle.Leaf width oval or length Round shape ellipse, two sides is coarse, and below by close short rough hair, base goes out three arteries and veins.The end capitulum Dan Shengzhi, the wide mitriform of involucre;Always Bract multilayer, width egg shape or ovate-elliptic.Ligulate flower peony, rosiness, violet or white, tongue piece fall oval, first Hold 2-3 fissure or full edge, above by undercoat, below villosity.Tubular flower yellow is orange, apex sliver ovum shape lanceolar, Above by the close fine hair of yellowish-brown.Female flower achene falls oval, the tubular flower achene wedge shape of falling ovate, the month at florescence 6-9, fruiting period 7-10 Month;It grows mainly based on compound fertilizer, however, traditional compound fertilizer's specific aim is poor, and is used for a long time high chemical fertilizer, to plant Growth and ambient enviroment be easy to cause certain harm.
Summary of the invention
In view of the defects and deficiencies of the prior art, the present invention intends to provide a kind of youth-and-old-age biology base manure and its systems Preparation Method.
To achieve the above object, the present invention uses following technical scheme:
A kind of youth-and-old-age biology base manure, it is made of the raw material of following weight parts:Polyglyceryl fatty acid ester 0.7-1, furfural Slag 30-50, polyethylene glycol 2-4, maize cob meal 10-16, D-araboascorbic acid sodium 0.1-0.2, Tea Saponin 0.6-1, magnesium sulfate 4- 7, scolecite powder 100-110, cotton seed hulls 10-20, tall oil 2-3 are adulterated.
What the doping scolecite powder was made of the raw material of following weight parts:Chitosan 3-5, scolecite powder 30-40, Carboxymethyl cellulose 1-2, urea 10-13, ammonium persulfate 0.7-1, ammonium acrylate 30-40.
The preparation method of the doping scolecite powder, includes the following steps:
(1)Ammonium persulfate is taken, is added in the deionized water of 17-20 times of its weight, stirs evenly;
(2)Scolecite powder is taken, is calcined 1-2 hours at 700-750 DEG C, fine powder is worn into after cooling, mixes, be added to chitosan It is 5-10 minutes ultrasonic in the deionized water of 10-15 times of mixture weight, obtain mountain flour dispersion liquid;
(3)Urea, ammonium acrylate mixing are taken, is added in above-mentioned mountain flour dispersion liquid, stirs evenly, be sent in reaction kettle, lead to Enter nitrogen, adjusting temperature of reaction kettle is 60-75 DEG C, and above-mentioned ammonium persulfate aqueous solution, carboxymethyl cellulose, insulated and stirred 4- is added It 5 hours, discharges, filters, filter cake is washed, air drying is to get the doping scolecite powder.
A kind of preparation method of youth-and-old-age biology base manure, includes the following steps:
(1)D-araboascorbic acid sodium, Tea Saponin mixing are taken, is added in the deionized water of 10-17 times of mixture weight, stirring is equal It is even, polyglyceryl fatty acid ester is added, increasing temperature is 50-60 DEG C, insulated and stirred 20-30 minutes, obtains aqueous dispersions;
(2)Cotton seed hulls is taken, is added in the dehydrated alcohol of 3-5 times of its weight, stirs evenly, obtain alcoholic solution;
(3)Maize cob meal is taken, is added in above-mentioned aqueous dispersions, stirs evenly, furfural dregs are added, stir evenly, it is molten that alcohol is added Liquid stirs evenly, and seals 10-20 days, discharging, and doping scolecite powder is added, filters, filter cake is washed, air drying, is milled, Obtain powder;
(4)Above-mentioned powder is taken, is mixed with polyethylene glycol, insulated and stirred 10-20 minutes at 70-80 DEG C, remaining each raw material is added, It stirs evenly to get the youth-and-old-age biology base manure.
Advantages of the present invention:
The present invention is using ammonium acrylate as monomer, using urea as dopant, disperses in scolecite amidin, acts in initiator Lower polymerization obtains urea doping scolecite powder and improves adhesive force of the urea between scolecite powder by the reaction, improve Nutrient stabilizing, the present invention are blended using maize cob meal, cotton seed hulls as raw material with furfural dregs, are sealed by fermentation, to improve finished product The trophism and storage stability of fertilizer, for base manure of the invention using biomass as raw material, Safety and Environmental Protection is good, full of nutrition, energy Enough various nutritional needs for effectively meeting youth-and-old-age growth phase, accelerate its healthy growth.
Specific embodiment
Embodiment 1
A kind of youth-and-old-age biology base manure, it is made of the raw material of following weight parts:
Polyglyceryl fatty acid ester 0.7, furfural dregs 30, polyethylene glycol 2, maize cob meal 10, D-araboascorbic acid sodium 0.1, Tea Saponin 0.6, magnesium sulfate 4, doping scolecite powder 100, cotton seed hulls 10, tall oil 2.
What the doping scolecite powder was made of the raw material of following weight parts:
Chitosan 3, scolecite powder 30, carboxymethyl cellulose 1, urea 10, ammonium persulfate 0.7, ammonium acrylate 30.
The preparation method of the doping scolecite powder, includes the following steps:
(1)Ammonium persulfate is taken, is added in the deionized water of 17 times of its weight, stirs evenly;
(2)Scolecite powder is taken, is calcined 1 hour at 700 DEG C, fine powder is worn into after cooling, is mixed with chitosan, be added to mixture In the deionized water that 10 times of weight, ultrasound 5 minutes obtains mountain flour dispersion liquid;
(3)Urea, ammonium acrylate mixing are taken, is added in above-mentioned mountain flour dispersion liquid, stirs evenly, be sent in reaction kettle, lead to Enter nitrogen, adjusting temperature of reaction kettle is 60 DEG C, above-mentioned ammonium persulfate aqueous solution, carboxymethyl cellulose is added, insulated and stirred 4 is small When, it discharges, filters, filter cake is washed, air drying is to get the doping scolecite powder.
A kind of preparation method of youth-and-old-age biology base manure, includes the following steps:
(1)D-araboascorbic acid sodium, Tea Saponin mixing are taken, is added in 10 times of mixture weight of deionized water, stirs evenly, Polyglyceryl fatty acid ester is added, increasing temperature is 50 DEG C, insulated and stirred 20 minutes, obtains aqueous dispersions;
(2)Cotton seed hulls is taken, is added in the dehydrated alcohol of 3 times of its weight, is stirred evenly, obtain alcoholic solution;
(3)Maize cob meal is taken, is added in above-mentioned aqueous dispersions, stirs evenly, furfural dregs are added, stir evenly, it is molten that alcohol is added Liquid stirs evenly, and seals 10 days, discharging, and doping scolecite powder is added, filters, filter cake is washed, air drying, is milled, obtains powder Material;
(4)Above-mentioned powder is taken, is mixed with polyethylene glycol, remaining each raw material is added in insulated and stirred 10 minutes at 70 DEG C, and stirring is equal It is even to get the youth-and-old-age biology base manure.
Embodiment 2
A kind of youth-and-old-age biology base manure, it is made of the raw material of following weight parts:
Polyglyceryl fatty acid ester 1, furfural dregs 50, polyethylene glycol 4, maize cob meal 16, D-araboascorbic acid sodium 0.2, Tea Saponin 0.6-1, magnesium sulfate 7, doping scolecite powder 110, cotton seed hulls 20, tall oil 3.
What the doping scolecite powder was made of the raw material of following weight parts:
Shell is poly- 5, scolecite powder 40, carboxymethyl cellulose 2, urea 13, ammonium persulfate 1, ammonium acrylate 40.
The preparation method of the doping scolecite powder, includes the following steps:
(1)Ammonium persulfate is taken, is added in the deionized water of 20 times of its weight, stirs evenly;
(2)Scolecite powder is taken, is calcined 2 hours at 750 DEG C, fine powder is worn into after cooling, is mixed with chitosan, be added to mixture In the deionized water that 15 times of weight, ultrasound 10 minutes obtains mountain flour dispersion liquid;
(3)Urea, ammonium acrylate mixing are taken, is added in above-mentioned mountain flour dispersion liquid, stirs evenly, be sent in reaction kettle, lead to Enter nitrogen, adjusting temperature of reaction kettle is 75 DEG C, above-mentioned ammonium persulfate aqueous solution, carboxymethyl cellulose is added, insulated and stirred 5 is small When, it discharges, filters, filter cake is washed, air drying is to get the doping scolecite powder.
A kind of preparation method of youth-and-old-age biology base manure, includes the following steps:
(1)D-araboascorbic acid sodium, Tea Saponin mixing are taken, is added in 17 times of mixture weight of deionized water, stirs evenly, Polyglyceryl fatty acid ester is added, increasing temperature is 60 DEG C, insulated and stirred 30 minutes, obtains aqueous dispersions;
(2)Cotton seed hulls is taken, is added in the dehydrated alcohol of 5 times of its weight, is stirred evenly, obtain alcoholic solution;
(3)Maize cob meal is taken, is added in above-mentioned aqueous dispersions, stirs evenly, furfural dregs are added, stir evenly, it is molten that alcohol is added Liquid stirs evenly, and seals 20 days, discharging, and doping scolecite powder is added, filters, filter cake is washed, air drying, is milled, obtains powder Material;
(4)Above-mentioned powder is taken, is mixed with polyethylene glycol, remaining each raw material is added in insulated and stirred 20 minutes at 80 DEG C, and stirring is equal It is even to get the youth-and-old-age biology base manure.

Claims (4)

1. a kind of youth-and-old-age biology base manure, which is characterized in that it is made of the raw material of following weight parts:
Polyglyceryl fatty acid ester 0.7-1, furfural dregs 30-50, polyethylene glycol 2-4, maize cob meal 10-16, D-araboascorbic acid sodium 0.1-0.2, Tea Saponin 0.6-1, magnesium sulfate 4-7, doping scolecite powder 100-110, cotton seed hulls 10-20, tall oil 2-3.
2. a kind of youth-and-old-age biology base manure according to claim 1, which is characterized in that the doping scolecite powder be by The raw material composition of following weight parts:
Chitosan 3-5, scolecite powder 30-40, carboxymethyl cellulose 1-2, urea 10-13, ammonium persulfate 0.7-1, ammonium acrylate 30-40。
3. a kind of youth-and-old-age biology base manure according to claim 2, which is characterized in that the system of the doping scolecite powder Preparation Method includes the following steps:
(1)Ammonium persulfate is taken, is added in the deionized water of 17-20 times of its weight, stirs evenly;
(2)Scolecite powder is taken, is calcined 1-2 hours at 700-750 DEG C, fine powder is worn into after cooling, mixes, be added to chitosan It is 5-10 minutes ultrasonic in the deionized water of 10-15 times of mixture weight, obtain mountain flour dispersion liquid;
(3)Urea, ammonium acrylate mixing are taken, is added in above-mentioned mountain flour dispersion liquid, stirs evenly, be sent in reaction kettle, lead to Enter nitrogen, adjusting temperature of reaction kettle is 60-75 DEG C, and above-mentioned ammonium persulfate aqueous solution, carboxymethyl cellulose, insulated and stirred 4- is added It 5 hours, discharges, filters, filter cake is washed, air drying is to get the doping scolecite powder.
4. a kind of preparation method of youth-and-old-age biology base manure as described in claim 1, which is characterized in that include the following steps:
(1)D-araboascorbic acid sodium, Tea Saponin mixing are taken, is added in the deionized water of 10-17 times of mixture weight, stirring is equal It is even, polyglyceryl fatty acid ester is added, increasing temperature is 50-60 DEG C, insulated and stirred 20-30 minutes, obtains aqueous dispersions;
(2)Cotton seed hulls is taken, is added in the dehydrated alcohol of 3-5 times of its weight, stirs evenly, obtain alcoholic solution;
(3)Maize cob meal is taken, is added in above-mentioned aqueous dispersions, stirs evenly, furfural dregs are added, stir evenly, it is molten that alcohol is added Liquid stirs evenly, and seals 10-20 days, discharging, and doping scolecite powder is added, filters, filter cake is washed, air drying, is milled, Obtain powder;
(4)Above-mentioned powder is taken, is mixed with polyethylene glycol, insulated and stirred 10-20 minutes at 70-80 DEG C, remaining each raw material is added, It stirs evenly to get the youth-and-old-age biology base manure.
CN201810914353.0A 2018-08-12 2018-08-12 A kind of youth-and-old-age biology base manure and preparation method thereof Withdrawn CN108863586A (en)

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CN201810914353.0A CN108863586A (en) 2018-08-12 2018-08-12 A kind of youth-and-old-age biology base manure and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201810914353.0A CN108863586A (en) 2018-08-12 2018-08-12 A kind of youth-and-old-age biology base manure and preparation method thereof

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012020420A2 (en) * 2010-08-12 2012-02-16 Maniyam Anuradha Enhancing secondary phytochemical and nutrients in plants and plant parts
CN106431645A (en) * 2016-09-12 2017-02-22 巢湖春友种业科技有限公司 Fermentation fertilizer for rice planting and preparation method thereof
CN106431640A (en) * 2016-09-12 2017-02-22 巢湖春友种业科技有限公司 Compound water retention urea formaldehyde slow release rice fertilizer and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012020420A2 (en) * 2010-08-12 2012-02-16 Maniyam Anuradha Enhancing secondary phytochemical and nutrients in plants and plant parts
CN106431645A (en) * 2016-09-12 2017-02-22 巢湖春友种业科技有限公司 Fermentation fertilizer for rice planting and preparation method thereof
CN106431640A (en) * 2016-09-12 2017-02-22 巢湖春友种业科技有限公司 Compound water retention urea formaldehyde slow release rice fertilizer and preparation method thereof

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