CN108836886A - A kind of blueberry formulation of tooth-paste and preparation method thereof - Google Patents
A kind of blueberry formulation of tooth-paste and preparation method thereof Download PDFInfo
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- CN108836886A CN108836886A CN201810966631.7A CN201810966631A CN108836886A CN 108836886 A CN108836886 A CN 108836886A CN 201810966631 A CN201810966631 A CN 201810966631A CN 108836886 A CN108836886 A CN 108836886A
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- 235000003095 Vaccinium corymbosum Nutrition 0.000 title claims abstract description 32
- 235000017537 Vaccinium myrtillus Nutrition 0.000 title claims abstract description 32
- 235000021014 blueberries Nutrition 0.000 title claims abstract description 32
- 239000000606 toothpaste Substances 0.000 title claims abstract description 27
- 229940034610 toothpaste Drugs 0.000 title claims abstract description 27
- 240000000851 Vaccinium corymbosum Species 0.000 title claims abstract description 26
- 239000000203 mixture Substances 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 238000009472 formulation Methods 0.000 title claims abstract description 11
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 55
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 34
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 24
- 238000002156 mixing Methods 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims abstract description 15
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims abstract description 15
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims abstract description 15
- 238000000034 method Methods 0.000 claims abstract description 15
- 239000008213 purified water Substances 0.000 claims abstract description 15
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 235000010208 anthocyanin Nutrition 0.000 claims abstract description 14
- 229930002877 anthocyanin Natural products 0.000 claims abstract description 14
- 239000004410 anthocyanin Substances 0.000 claims abstract description 14
- 150000004636 anthocyanins Chemical class 0.000 claims abstract description 14
- FUFJGUQYACFECW-UHFFFAOYSA-L calcium hydrogenphosphate Chemical compound [Ca+2].OP([O-])([O-])=O FUFJGUQYACFECW-UHFFFAOYSA-L 0.000 claims abstract description 12
- 235000019700 dicalcium phosphate Nutrition 0.000 claims abstract description 12
- 150000003839 salts Chemical class 0.000 claims abstract description 12
- 239000011780 sodium chloride Substances 0.000 claims abstract description 12
- 229920005682 EO-PO block copolymer Polymers 0.000 claims abstract description 11
- MOTZDAYCYVMXPC-UHFFFAOYSA-N dodecyl hydrogen sulfate Chemical compound CCCCCCCCCCCCOS(O)(=O)=O MOTZDAYCYVMXPC-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229940043264 dodecyl sulfate Drugs 0.000 claims abstract description 10
- 229940075614 colloidal silicon dioxide Drugs 0.000 claims abstract description 9
- 238000011049 filling Methods 0.000 claims abstract description 8
- 239000003292 glue Substances 0.000 claims abstract description 8
- 238000000227 grinding Methods 0.000 claims abstract description 7
- 238000007872 degassing Methods 0.000 claims abstract description 6
- 239000000470 constituent Substances 0.000 claims abstract description 4
- 239000006210 lotion Substances 0.000 claims description 11
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 7
- 239000000084 colloidal system Substances 0.000 claims description 7
- 239000011734 sodium Substances 0.000 claims description 7
- 229910052708 sodium Inorganic materials 0.000 claims description 7
- 244000077233 Vaccinium uliginosum Species 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 239000004615 ingredient Substances 0.000 claims description 4
- 238000009849 vacuum degassing Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 3
- 238000004806 packaging method and process Methods 0.000 claims description 3
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 claims description 2
- 238000005429 filling process Methods 0.000 claims description 2
- 239000000377 silicon dioxide Substances 0.000 claims description 2
- 229920002678 cellulose Polymers 0.000 claims 1
- 239000001913 cellulose Substances 0.000 claims 1
- ANRHNWWPFJCPAZ-UHFFFAOYSA-M thionine Chemical compound [Cl-].C1=CC(N)=CC2=[S+]C3=CC(N)=CC=C3N=C21 ANRHNWWPFJCPAZ-UHFFFAOYSA-M 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 9
- 206010020751 Hypersensitivity Diseases 0.000 abstract description 5
- 208000009019 Pericoronitis Diseases 0.000 abstract description 5
- 210000004268 dentin Anatomy 0.000 abstract description 5
- 210000004373 mandible Anatomy 0.000 abstract description 5
- 208000030194 mouth disease Diseases 0.000 abstract description 5
- 201000001245 periodontitis Diseases 0.000 abstract description 5
- 210000004357 third molar Anatomy 0.000 abstract description 5
- 238000004140 cleaning Methods 0.000 abstract description 4
- 208000014674 injury Diseases 0.000 abstract description 3
- 230000008733 trauma Effects 0.000 abstract description 3
- 238000005303 weighing Methods 0.000 abstract description 3
- 230000003712 anti-aging effect Effects 0.000 description 5
- 230000003110 anti-inflammatory effect Effects 0.000 description 5
- 239000003963 antioxidant agent Substances 0.000 description 5
- 230000003078 antioxidant effect Effects 0.000 description 5
- 235000006708 antioxidants Nutrition 0.000 description 5
- 230000036039 immunity Effects 0.000 description 5
- 210000000214 mouth Anatomy 0.000 description 5
- 206010006326 Breath odour Diseases 0.000 description 4
- 208000032139 Halitosis Diseases 0.000 description 4
- 208000020670 canker sore Diseases 0.000 description 4
- 230000007547 defect Effects 0.000 description 4
- 201000010099 disease Diseases 0.000 description 4
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 4
- 229940055416 blueberry extract Drugs 0.000 description 3
- 235000019216 blueberry extract Nutrition 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 244000283207 Indigofera tinctoria Species 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 208000027418 Wounds and injury Diseases 0.000 description 2
- 235000021028 berry Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000004593 Epoxy Substances 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000001856 Ethyl cellulose Substances 0.000 description 1
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- 244000147568 Laurus nobilis Species 0.000 description 1
- 235000017858 Laurus nobilis Nutrition 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 235000005212 Terminalia tomentosa Nutrition 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 229930014669 anthocyanidin Natural products 0.000 description 1
- 150000001453 anthocyanidins Chemical class 0.000 description 1
- 235000008758 anthocyanidins Nutrition 0.000 description 1
- 229920001400 block copolymer Polymers 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000008119 colloidal silica Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229920001249 ethyl cellulose Polymers 0.000 description 1
- 235000019325 ethyl cellulose Nutrition 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000002262 irrigation Effects 0.000 description 1
- 238000003973 irrigation Methods 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/02—Stomatological preparations, e.g. drugs for caries, aphtae, periodontitis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/522—Antioxidants; Radical scavengers
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Organic Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Medicinal Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
Abstract
A kind of blueberry formulation of tooth-paste, using blueberry anthocyanin, sodium chloride, two water salt of calcium monohydrogen phosphate, glycerol, colloidal silicon dioxide, sldium lauryl sulfate, hydroxyethyl cellulose, ethylene oxide-propylene oxide block copolymer, purified water as primary raw material, constituent ratio is as follows：1-10 parts of blueberry anthocyanin, 10-15 parts of sodium chloride, 25-35 parts of two water salt of calcium monohydrogen phosphate, 15-25 parts of glycerol, 2-3 parts of colloidal silicon dioxide, 1-3 parts of sldium lauryl sulfate, 0.5-2 parts of hydroxyethyl cellulose, 0.1-1 parts of ethylene oxide-propylene oxide block copolymer, 10-30 parts of purified water.A kind of preparation method of blueberry formulation of tooth-paste, process is as follows, A:Each composition batch weighing is spare；B:Glue water；C:Mixing in mixing machine is added in all raw materials；D:Grinding, degassing；E：It is filling.The present invention not only has the effect of oral cleaning, moreover it is possible to effectively prevent including the odontopathy such as periapicalitis, pericoronitis of the third molar of the mandible, periodontitis, hypersensitive dentin, tooth trauma and mouth disease, and improve the market competitiveness.
Description
Technical field
The present invention relates to personal hygiene article and preparation method thereof field, especially a kind of blueberry formulation of tooth-paste and its preparation
Method.
Background technique
Toothpaste is a kind of using extensive personal hygiene article, and general toothpaste is since its formula composition limits, to oral cavity
The odontopathy such as disease, such as periapicalitis, pericoronitis of the third molar of the mandible, periodontitis, hypersensitive dentin, tooth trauma and dry, halitosis,
The preventive and therapeutic effect that canker sore etc. cannot play, therefore have the defects that in practical application certain.
Blueberry anthocyanin is one of Blueberry extract, in addition to high nutritive value, also have it is anti-inflammatory,
Anti-oxidant, anti-aging improves the functions such as immunity.With the development of industrial technology, the market competition of product is increasing, to the greatest extent may be used
The function that product can be improved is the key factor place for guaranteeing product and winning the market.
Based on above-mentioned, provide a kind of using the indigo plant that there is anti-inflammatory, anti-oxidant, anti-aging to human body, improve immunity
Certain kind of berries anthocyanidin is as auxiliary material, the finished product in conjunction with made of existing toothpaste manufacture craft, while bringing oral cleaning,
Mouth disease can also be effectively prevented, and the toothpaste that can improve product competitiveness seems particularly necessary.
Summary of the invention
It is weak to the various disease effects in the oral cavity of human body in order to overcome existing toothpaste because compositing formula is limited, it is deposited in practical application
The certain defect the drawbacks of, the present invention provides using having anti-inflammatory, anti-oxidant, anti-aging, can improve immunity, green natural
Blueberry extract blueberry anthocyanin as principal ingredients, the finished product in conjunction with made from manufacture toothpaste technique not only has mouth
The clean effect of chamber, moreover it is possible to effectively prevent including periapicalitis, pericoronitis of the third molar of the mandible, periodontitis, hypersensitive dentin, tooth trauma etc.
The mouth diseases such as odontopathy and dry, halitosis and canker sore, and the one kind for increasing product function, improving the market competitiveness
Blueberry formulation of tooth-paste and preparation method thereof.
The technical solution adopted by the present invention to solve the technical problems is：
A kind of blueberry formulation of tooth-paste, it is characterised in that use blueberry anthocyanin, sodium chloride, two water salt of calcium monohydrogen phosphate, glycerol, colloid
Silica, sldium lauryl sulfate, hydroxyethyl cellulose, ethylene oxide-propylene oxide block copolymer, purified water are as main
Raw material, blueberry anthocyanin, sodium chloride, two water salt of calcium monohydrogen phosphate, glycerol, colloidal silicon dioxide, sldium lauryl sulfate, ethoxy are fine
Tie up element, ethylene oxide-propylene oxide block copolymer, purified water materials in, constituent ratio is as follows：Blueberry anthocyanin
1-10 parts, 10-15 parts of sodium chloride, 25-35 parts of two water salt of calcium monohydrogen phosphate, 15-25 parts of glycerol, 2-3 parts of colloidal silicon dioxide, laurel
1-3 parts of alcohol sodium sulphate, 0.5-2 parts of hydroxyethyl cellulose, 0.1-1 parts of ethylene oxide-propylene oxide block copolymer, purified water
10-30 parts.
A kind of preparation method of blueberry formulation of tooth-paste, it is characterised in that process is as follows, A:Each composition batch weighing is spare；B:
Glue water；C:Mixing in mixing machine is added in all raw materials；D:Grinding, degassing；E：It is filling.
In the step B, when carrying out glue water conservancy project sequence, glycerol is added in blender with sodium hydroxyethyl cellulose first and is stirred
It mixes, adds purified water, be uniformly mixed, to after in viscous shape translucent liquid, unloading makes glycerol and hydroxyl in container for stirring
Ethyl cellulose sodium dissolve fully expansion after it is spare.
In the step C, when carrying out all raw materials mixed processes in mixing machine are added, all raw materials are added to the mixer
After mixing, the lotion with certain viscosity can be obtained in mixing 30 minutes, raw material.
In the step D, ground, degassing process when, first step C lotion first with colloid mill for the first time grind after store
It deposits, after certain interval of time, then carries out second with colloid mill and grind, be then de-gassed with vacuum degassing machine, vacuum
Degasser work when, vacuum degree, which is maintained at -0.096Mpa, to be advisable, the vacuum outgas time at 50 minutes or so, by grinding twice
Afterwards, lotion can be made to be in fine and smooth, uniform, stable state.
In the step E, when carrying out filling process, after lotion after step D processing is stood a period of time, with filling mechanical irrigation
Loaded in packaging shell i.e. complete all process steps.
Present invention has the advantages that：The present invention uses with anti-inflammatory, anti-oxidant, anti-aging, can improve immunity, green day
Right Blueberry extract blueberry anthocyanin is as principal ingredients, the finished product in conjunction with made from conventionally manufactured toothpaste technique, not only
Has the effect of oral cleaning, moreover it is possible to effectively prevent including periapicalitis, pericoronitis of the third molar of the mandible, periodontitis, hypersensitive dentin, tooth
The mouth diseases such as the odontopathy such as wound and dry, halitosis and canker sore, and increase product function, improve market competition
Power.Existing toothpaste is overcome because compositing formula is limited, the various diseases in the oral cavity of human body are acted on weak, existed in practical application certain
The shortcomings that defect.Based on above-mentioned, so the application prospect that the present invention has had.
Detailed description of the invention
The present invention is described further below in conjunction with drawings and examples.
Fig. 1 is a kind of flow diagram of blueberry toothpaste preparation method of the present invention.
Specific embodiment
A kind of blueberry formulation of tooth-paste, using blueberry anthocyanin, sodium chloride, two water salt of calcium monohydrogen phosphate, glycerol, colloidal silica
Silicon, sldium lauryl sulfate, hydroxyethyl cellulose, ethylene oxide-propylene oxide block copolymer, purified water as primary raw material,
Blueberry anthocyanin, sodium chloride, two water salt of calcium monohydrogen phosphate, glycerol, colloidal silicon dioxide, sldium lauryl sulfate, hydroxyethyl cellulose,
Ethylene oxide-propylene oxide block copolymer, purified water materials in, constituent ratio is as follows：Blueberry anthocyanin 1-10
Part, 10-15 parts of sodium chloride, 25-35 parts of two water salt of calcium monohydrogen phosphate, 15-25 parts of glycerol, 2-3 parts of colloidal silicon dioxide, laruyl alcohol sulphur
Sour sodium 1-3 parts, 0.5-2 parts of hydroxyethyl cellulose, 0.1-1 parts of ethylene oxide-propylene oxide block copolymer, purified water 10-30
Part.
Shown in Fig. 1, a kind of preparation method process of blueberry formulation of tooth-paste is as follows, A:Each composition batch weighing is spare；B:
Glue water；C:Mixing in mixing machine is added in all raw materials；D:Grinding, degassing；E：It is filling.In step B, glue water conservancy project sequence is carried out
When, glycerol is added in blender with sodium hydroxyethyl cellulose first and is stirred, purified water is added, is uniformly mixed, stirring is extremely
After viscous shape translucent liquid, unloading is spare after so that glycerol and sodium hydroxyethyl cellulose is dissolved fully expansion in container.Step
In C, when carrying out all raw materials mixed processes in mixing machine are added, all raw materials are added to the mixer mixing 30 minutes, raw material
After mixing, the lotion with certain viscosity can be obtained.In step D, ground, degassing process when, first step C cream
Body is stored after being ground for the first time with colloid mill, after certain interval of time, then is carried out second with colloid mill and is ground, then uses vacuum
Degasser is de-gassed, and when vacuum degassing machine works, vacuum degree, which is maintained at -0.096Mpa, to be advisable, and the vacuum outgas time exists
50 minutes or so, after grinding twice, lotion can be made to be in fine and smooth, uniform, stable state.In step E, filling work is carried out
When sequence, by step D processing after lotion stand a period of time after, with bottle placer it is filling in packaging shell i.e. complete all process steps.
Shown in Fig. 1, the present invention uses with anti-inflammatory, anti-oxidant, anti-aging, can improve immunity, the indigo plant of green natural
For certain kind of berries fruit extract blueberry anthocyanin as principal ingredients, sodium chloride can play solidification effect, two water salt of calcium monohydrogen phosphate to tooth
The clean effect that can play to tooth as rubbing agent, glycerol play moisture-keeping function, colloidal silicon dioxide and can play to tooth
Despeckle effect, sldium lauryl sulfate play the role of foaming effect, hydroxyethyl cellulose plays thickening, ethylene oxide-epoxy third
Alkane block copolymer plays the role of bonding, purified water as auxiliary material, the finished product in conjunction with made from conventionally manufactured toothpaste technique, not only
Has the effect of oral cleaning, moreover it is possible to effectively prevent including periapicalitis, pericoronitis of the third molar of the mandible, periodontitis, hypersensitive dentin, tooth
The mouth diseases such as the odontopathy such as wound and dry, halitosis and canker sore, and increase product function, improve market competition
Power.Existing toothpaste is overcome because compositing formula is limited, the various diseases in the oral cavity of human body are acted on weak, existed in practical application certain
The shortcomings that defect.Based on above-mentioned, so the application prospect that the present invention has had.
Main feature and advantages of the present invention of the invention has been shown and described above, for those skilled in the art
Speech, it is clear that the present invention is limited to the details of above-mentioned exemplary embodiment, and without departing substantially from spirit or essential attributes of the invention
In the case of, the present invention can be realized in other specific forms.Therefore, in all respects, embodiment should all be regarded as
It is exemplary, and is non-limiting, the scope of the invention being indicated by the appended claims rather than by the foregoing description, therefore
It is intended to include all changes that fall within the meaning and scope of the equivalent elements of the claims in the present invention.It should not be by right
Any appended drawing reference in it is required that is construed as limiting the claims involved.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (6)
1. a kind of blueberry formulation of tooth-paste, it is characterised in that use blueberry anthocyanin, sodium chloride, two water salt of calcium monohydrogen phosphate, glycerol, glue
Body silica, sldium lauryl sulfate, hydroxyethyl cellulose, ethylene oxide-propylene oxide block copolymer, purified water are as master
Want raw material, blueberry anthocyanin, sodium chloride, two water salt of calcium monohydrogen phosphate, glycerol, colloidal silicon dioxide, sldium lauryl sulfate, ethoxy
Cellulose, ethylene oxide-propylene oxide block copolymer, purified water materials in, constituent ratio is as follows：Blueberry cyanine
1-10 parts plain, 10-15 parts of sodium chloride, 25-35 parts of two water salt of calcium monohydrogen phosphate, 15-25 parts of glycerol, 2-3 parts of colloidal silicon dioxide, the moon
1-3 parts of lauryl sulfate, 0.5-2 parts of hydroxyethyl cellulose, 0.1-1 parts of ethylene oxide-propylene oxide block copolymer, purified water
10-30 parts.
2. a kind of blueberry toothpaste preparation method according to claim 1, it is characterised in that process is as follows, A:Each composition ingredient
It weighs spare；B:Glue water；C:Mixing in mixing machine is added in all raw materials；D:Grinding, degassing；E：It is filling.
3. a kind of blueberry toothpaste preparation method according to claim 2, it is characterised in that in step B, carry out glue water conservancy project
When sequence, glycerol is added in blender with sodium hydroxyethyl cellulose first and is stirred, purified water is added, is uniformly mixed, stirred
To after in viscous shape translucent liquid, unloading in container, make glycerol and sodium hydroxyethyl cellulose dissolve fully expand after it is spare.
4. a kind of blueberry toothpaste preparation method according to claim 2, it is characterised in that in step C, carry out all originals
When mixed processes in mixing machine are added in material, all raw materials are added to the mixer mixing 30 minutes, and raw material after mixing, can obtain
To the lotion with certain viscosity.
5. a kind of blueberry toothpaste preparation method according to claim 2, it is characterised in that in step D, ground, deaerated
It when process, stores after first step C lotion is first ground with colloid mill for the first time, after certain interval of time, then is carried out with colloid mill
Second grinds, and is then de-gassed with vacuum degassing machine, and when vacuum degassing machine works, vacuum degree is maintained at-
0.096Mpa is advisable, and the vacuum outgas time at 50 minutes or so, after grinding twice, can make lotion be in fine and smooth, uniform, steady
Determine state.
6. a kind of blueberry toothpaste preparation method according to claim 2, it is characterised in that in step E, carry out filling process
When, by step D processing after lotion stand a period of time after, with bottle placer it is filling in packaging shell i.e. complete all process steps.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810966631.7A CN108836886A (en) | 2018-08-23 | 2018-08-23 | A kind of blueberry formulation of tooth-paste and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810966631.7A CN108836886A (en) | 2018-08-23 | 2018-08-23 | A kind of blueberry formulation of tooth-paste and preparation method thereof |
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| CN108836886A true CN108836886A (en) | 2018-11-20 |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2012219049A (en) * | 2011-04-07 | 2012-11-12 | Lion Corp | Dentifrice composition |
| CN103421610A (en) * | 2013-08-16 | 2013-12-04 | 德利宝(广州)香料有限公司 | Preparation method of essence containing natural blueberry extract and toothpaste containing essence |
| CN105012172A (en) * | 2014-07-31 | 2015-11-04 | 耿福能 | Method for preparing toothpaste containing anthocyanin and application thereof |
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2018
- 2018-08-23 CN CN201810966631.7A patent/CN108836886A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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