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CN108821886A - A kind of production technology of organic water-soluble fertilizer - Google Patents

A kind of production technology of organic water-soluble fertilizer Download PDF

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Publication number
CN108821886A
CN108821886A CN201810979427.9A CN201810979427A CN108821886A CN 108821886 A CN108821886 A CN 108821886A CN 201810979427 A CN201810979427 A CN 201810979427A CN 108821886 A CN108821886 A CN 108821886A
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CN
China
Prior art keywords
organic
water
soluble fertilizer
mixed solution
solution
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Pending
Application number
CN201810979427.9A
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Chinese (zh)
Inventor
陈建军
聂廷荣
赵兴伟
南玺章
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Gansu Tianyuan Chemical Industry Co Ltd
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Gansu Tianyuan Chemical Industry Co Ltd
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Priority to CN201810979427.9A priority Critical patent/CN108821886A/en
Publication of CN108821886A publication Critical patent/CN108821886A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D1/00Fertilisers containing potassium

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a kind of production technologies of organic water-soluble fertilizer, include the following steps:S1, progress fragmentation procedure in crusher is added in agricultural organic waste and sieving is collected by filtration, it is spare;S2, organic fertilizer raw material is invested in heating stirring in water, and adds organic active matter in mixed solution to carry out sufficient bioactivation;Suspended matter in S3, elimination mixed solution, and KOH is added into solution to adjust the pH value of organic liquid;S4, moderate-element and microelement are added in the high organic matter mixed solution of activity, are reacted after matching in proportion;S5, it the solution after reaction is placed under ultrasound environments acts on, glue film is carried out by adhesive film machine again, mixed solution is sufficiently heated, sufficiently drying, organic water-soluble fertilizer is made, this convenient production process operation of the present invention utilizes production technology organic water soluble fertilizer produced, the water-insoluble object content contained in raw material is low, greatly improves the economic value of organic water-soluble fertilizer.

Description

A kind of production technology of organic water-soluble fertilizer
Technical field
The present invention relates to organic water-soluble fertilizer production technical field more particularly to a kind of production works of organic water-soluble fertilizer Skill.
Background technique
Water soluble fertilizer is a kind of polyelement composite fertilizer that can be completely soluble, it, which can promptly be dissolved in the water, more holds Easily be absorbed by crops, and its absorption rate is relatively high, more crucially it can be applied to be sprayed fill etc. agriculturals set Apply, realize that water-fertilizer integral reaches the efficiency that water-saving saves fertile saving of labor, water soluble organic fertilizer have complete water-soluble, high activity, hypersorption, It is quick, the high feature of water-soluble potassium content.
The production of organic water-soluble fertilizer is the development need of modern agriculture, can greatly improve the efficiency of fertilising, still, existing Have under technology, the production technology of organic or inorganic compound prescription organic water-soluble fertilizer produced often will appear solid sediment or Character instability can be precipitated after being long placed in, this is because in current production technology, the water-insoluble object content that contains in raw material Height, and technique circulation in this substance is not decomposed sufficiently caused by, finally affect the quality of product.
Therefore, we have proposed a kind of production technologies of organic water-soluble fertilizer for solving the above problems.
Summary of the invention
The purpose of the present invention is to solve the water-insoluble object content height contained in raw material existing in the prior art, have The shortcomings that impurity can be precipitated after being long placed in machine water-soluble fertilizer, and a kind of production technology of the organic water-soluble fertilizer proposed.
A kind of production technology of organic water-soluble fertilizer, which is characterized in that include the following steps:
S1, agricultural organic waste be added in crusher carry out fragmentation procedure, the bottom of crusher be equipped with the first filter screen and Second filter screen, the mica raw material for not crossing the first filter screen is transferred back to crusher and carries out second-time breakage, until all passing through second The sieve of filter screen collects sieving, obtains powdered organic fertilizer raw material, spare;
S2, organic fertilizer raw material is invested in water, and is stirred 10min-30min in the environment of heating water bath, by stirring It mixes and is mixed into uniform solution, and add organic active matter in mixed solution to carry out sufficient bioactivation;
Suspended matter in S3, elimination mixed solution, and KOH is added into solution to adjust the pH value of organic liquid;
S4, moderate-element and microelement are added in the high organic matter mixed solution of activity, after matching in proportion 25 DEG C- 100 DEG C, relative humidity 50%-95%, chelatropic reaction 10h-20h is carried out under conditions of reaction pressure 0-5kpa;
S5, it the solution after reaction is placed under ultrasound environments acts on 2h-4h, obtain the dispersion liquid of organic solution, then pass through glue Film machine carries out glue film, allows the more refinement of undecomposed fixed particle breakdown, and mixed solution is sufficiently heated, solid is filtered out, fills Divide drying, organic water-soluble fertilizer is made.
Preferably, the agricultural organic waste includes agricultural crop straw tendril and waste of aquatic.
Preferably, the organic active object includes at least detergent alkylate phenol polyethenoxy ether, sodium lignin sulphate, alkyl One of benzene sulfonate and the ammonium salt of fatty alcohol polyoxyethylene ether
Preferably, the moderate-element is Chelating state moderate-element, and moderate-element includes nitrogen, phosphorus, potassium.
Preferably, the microelement be chelated microelements, the content of microelement be and microelement include copper, Iron, manganese, zinc, boron, molybdenum.
Preferably, the sieve specification of first filter screen is -50 mesh of 30 mesh, and the sieve specification of the second filter screen is 80 - 100 mesh of mesh.
The beneficial effects of the invention are as follows:This convenient production process operation, the organic water-soluble fertilizer purity is high of preparation, utilizes this Production technology organic water soluble fertilizer produced, the water-insoluble object content contained in raw material is low, further improves its suction Utilization rate is received, and its organic water-soluble fertilizer can save steadily in the long term, will not be precipitated, and greatly improve organic water soluble fertilizer Economic value.
Specific embodiment
Combined with specific embodiments below the present invention is made further to explain.
A kind of production technology of organic water-soluble fertilizer, includes the following steps:S1, crusher is added in agricultural organic waste The bottom of middle carry out fragmentation procedure, crusher is equipped with the first filter screen and the second filter screen, and the mica for not crossing the first filter screen is former Material is transferred back to crusher and carries out second-time breakage, until all by the sieve of the second filter screen, collection sieving, obtaining powdered has Machine fertilizer raw material, it is spare;S2, organic fertilizer raw material is invested in water, and is stirred 10min- in the environment of heating water bath 30min mixes by stirring into uniform solution, and adds organic active matter in mixed solution to carry out adequately biology and live Change;Suspended matter in S3, elimination mixed solution, and KOH is added into solution to adjust the pH value of organic liquid;S4, will in Secondary element and microelement are added in the high organic matter mixed solution of activity, after matching in proportion 25 DEG C -100 DEG C, it is opposite Chelatropic reaction 10h-20h is carried out under conditions of humidity 50%-95%, reaction pressure 0-5kpa;S5, the solution after reaction is placed in it is super 2h-4h is acted under acoustic environment, obtains the dispersion liquid of organic solution, then glue film is carried out by adhesive film machine, allows undecomposed fixation Mixed solution is sufficiently heated, filters out solid by the more refinement of particle breakdown, is sufficiently dried, and organic water-soluble fertilizer, agricultural is made Organic waste includes agricultural crop straw tendril and waste of aquatic, and organic active object includes at least dodecyl phenol polyoxy second One of alkene ether, sodium lignin sulphate, alkylbenzene sulfonate and ammonium salt of fatty alcohol polyoxyethylene ether, moderate-element are chelating State moderate-element, and moderate-element includes nitrogen, phosphorus, potassium, microelement are chelated microelements, and microelement include copper, Iron, manganese, zinc, boron, molybdenum, the sieve specification of the first filter screen are -50 mesh of 30 mesh, and the sieve specification of the second filter screen is 80 mesh -100 Mesh.
In the present embodiment, use KOH as the regulator for adjusting organic liquid pH value, K element is also raw as crop simultaneously Long Quality Element improves crop product and quality, also avoids bringing into fertilizer for the harmful substances such as sodium ion, and by special Rubber mill allows not sufficiently reactive solid material more fully to react and refine in organic liquid, improves liquid Stability, glue film fineness is small, and visibly homogeneous.
The present embodiment one
A kind of production technology of organic water-soluble fertilizer, includes the following steps:
S1, agricultural organic waste be added in crusher carry out fragmentation procedure, the bottom of crusher be equipped with the first filter screen and Second filter screen, the mica raw material for not crossing the first filter screen is transferred back to crusher and carries out second-time breakage, until all passing through second The sieve of filter screen collects sieving, obtains powdered organic fertilizer raw material, spare;
S2, organic fertilizer raw material is invested in water, and is stirred 30min in the environment of heating water bath, mixed by stirring Organic active matter is added at uniform solution, and in mixed solution to carry out sufficient bioactivation;
Suspended matter in S3, elimination mixed solution, and KOH is added into solution to adjust the pH value of organic liquid;
S4, moderate-element and microelement are added in the high organic matter mixed solution of activity, after matching in proportion 50 DEG C, Chelatropic reaction 14h is carried out under conditions of relative humidity 70%, reaction pressure 2kpa;
S5, it the solution after reaction is placed under ultrasound environments acts on 2h, obtain the dispersion liquid of organic solution, then pass through adhesive film machine Glue film is carried out, allows the more refinement of undecomposed fixed particle breakdown, mixed solution is sufficiently heated, solid is filtered out, is sufficiently dried It is dry, organic water-soluble fertilizer is made.
In the present embodiment one, organic active object selection detergent alkylate phenol polyethenoxy ether, and the sieve of the first filter screen Specification is 40 mesh, and the sieve specification of the second filter screen is 90 mesh.
The present embodiment two
S1, agricultural organic waste be added in crusher carry out fragmentation procedure, the bottom of crusher be equipped with the first filter screen and Second filter screen, the mica raw material for not crossing the first filter screen is transferred back to crusher and carries out second-time breakage, until all passing through second The sieve of filter screen collects sieving, obtains powdered organic fertilizer raw material, spare;
S2, organic fertilizer raw material is invested in water, and is stirred 30min in the environment of heating water bath, mixed by stirring Organic active matter is added at uniform solution, and in mixed solution to carry out sufficient bioactivation;
Suspended matter in S3, elimination mixed solution, and KOH is added into solution to adjust the pH value of organic liquid;
S4, moderate-element and microelement are added in the high organic matter mixed solution of activity, after matching in proportion 90 DEG C, Chelatropic reaction 20h is carried out under conditions of relative humidity 90%, reaction pressure 4kpa;
S5, it the solution after reaction is placed under ultrasound environments acts on 2h, obtain the dispersion liquid of organic solution, then pass through adhesive film machine Glue film is carried out, allows the more refinement of undecomposed fixed particle breakdown, mixed solution is sufficiently heated, solid is filtered out, is sufficiently dried It is dry, organic water-soluble fertilizer is made.
In the present embodiment two, organic active object selection detergent alkylate phenol polyethenoxy ether, and the sieve of the first filter screen Specification is 40 mesh, and the sieve specification of the second filter screen is 90 mesh.
The present embodiment three
S1, agricultural organic waste be added in crusher carry out fragmentation procedure, the bottom of crusher be equipped with the first filter screen and Second filter screen, the mica raw material for not crossing the first filter screen is transferred back to crusher and carries out second-time breakage, until all passing through second The sieve of filter screen collects sieving, obtains powdered organic fertilizer raw material, spare;
S2, organic fertilizer raw material is invested in water, and is stirred 30min in the environment of heating water bath, mixed by stirring Organic active matter is added at uniform solution, and in mixed solution to carry out sufficient bioactivation;
Suspended matter in S3, elimination mixed solution, and KOH is added into solution to adjust the pH value of organic liquid;
S4, moderate-element and microelement are added in the high organic matter mixed solution of activity, after matching in proportion 50 DEG C, Chelatropic reaction 14h is carried out under conditions of relative humidity 70%, reaction pressure 2kpa;
S5, it the solution after reaction is placed under ultrasound environments acts on 4h, obtain the dispersion liquid of organic solution, then pass through adhesive film machine Glue film is carried out, allows the more refinement of undecomposed fixed particle breakdown, mixed solution is sufficiently heated, solid is filtered out, is sufficiently dried It is dry, organic water-soluble fertilizer is made.
In the present embodiment three, organic active object selects sodium lignin sulphate, and the sieve specification of the first filter screen is 50 mesh, The sieve specification of second filter screen is 100 mesh.
In above-described embodiment one and embodiment two, only change the chelatropic reaction condition of organic water-soluble fertilizer, remaining technique It is required that not changing, in above-described embodiment one and embodiment three, only in the effect of ultrasonic wave after change organic solution chelatropic reaction Condition, remaining technique requires not change, and the organic fertilizer prepared under three kinds of processes is soluble in water, when standing identical Between, and its purity is detected, detection structure is as follows:
Embodiment one Embodiment two Embodiment three
Purity % 92 94.6 97.8
Comparison discovery, organic water-soluble fertilizer chelate that the time is longer, the ultrasonication time is longer, the impurity particle in organic fertilizer Smaller, water insoluble matter content is fewer, and impurity is precipitated fewer.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (6)

1. a kind of production technology of organic water-soluble fertilizer, which is characterized in that include the following steps:
S1, agricultural organic waste be added in crusher carry out fragmentation procedure, the bottom of crusher be equipped with the first filter screen and Second filter screen, the mica raw material for not crossing the first filter screen is transferred back to crusher and carries out second-time breakage, until all passing through second The sieve of filter screen collects sieving, obtains powdered organic fertilizer raw material, spare;
S2, organic fertilizer raw material is invested in water, and is stirred 10min-30min in the environment of heating water bath, by stirring It mixes and is mixed into uniform solution, and add organic active matter in mixed solution to carry out sufficient bioactivation;
Suspended matter in S3, elimination mixed solution, and KOH is added into solution to adjust the pH value of organic liquid;
S4, moderate-element and microelement are added in the high organic matter mixed solution of activity, after matching in proportion 25 DEG C- 100 DEG C, relative humidity 50%-95%, chelatropic reaction 10h-20h is carried out under conditions of reaction pressure 0-5kpa;
S5, it the solution after reaction is placed under ultrasound environments acts on 2h-4h, obtain the dispersion liquid of organic solution, then pass through glue Film machine carries out glue film, allows the more refinement of undecomposed fixed particle breakdown, and mixed solution is sufficiently heated, solid is filtered out, fills Divide drying, organic water-soluble fertilizer is made.
2. a kind of production technology of organic water-soluble fertilizer according to claim 1, which is characterized in that the agricultural organic waste Gurry includes agricultural crop straw tendril and waste of aquatic.
3. a kind of production technology of organic water-soluble fertilizer according to claim 1, which is characterized in that the organic active object Including at least detergent alkylate phenol polyethenoxy ether, sodium lignin sulphate, alkylbenzene sulfonate and fatty alcohol polyoxyethylene ether One of ammonium salt.
4. a kind of production technology of organic water-soluble fertilizer according to claim 1, which is characterized in that the moderate-element is Chelating state moderate-element, and moderate-element includes nitrogen, phosphorus, potassium.
5. a kind of production technology of organic water-soluble fertilizer according to claim 1, which is characterized in that the microelement is Chelated microelements, and microelement includes copper, iron, manganese, zinc, boron, molybdenum.
6. a kind of production technology of organic water-soluble fertilizer according to claim 1, which is characterized in that first filter screen Sieve specification be -50 mesh of 30 mesh, the sieve specification of the second filter screen is -100 mesh of 80 mesh.
CN201810979427.9A 2018-08-27 2018-08-27 A kind of production technology of organic water-soluble fertilizer Pending CN108821886A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111018581A (en) * 2019-12-30 2020-04-17 滁州联润生态农业发展有限公司 Organic fertilizer for vegetable planting and preparation process thereof
CN112159272A (en) * 2020-09-27 2021-01-01 深圳市腾浪再生资源发展有限公司 Production process for preparing organic water-soluble fertilizer from kitchen residues
CN112794757A (en) * 2021-03-26 2021-05-14 山东高晟联合农业科技有限公司 Production process of suspended organic water-soluble fertilizer
CN114426440A (en) * 2021-05-06 2022-05-03 内蒙古朵日纳硒科生物技术有限公司 Production process of water-soluble fertilizer for cultivating potatoes
CN116854523A (en) * 2023-06-01 2023-10-10 播乐(海南)生态科技院(有限合伙) Preparation method, product and application of small molecular organic water-soluble fertilizer

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101870611A (en) * 2010-06-25 2010-10-27 汉枫缓释肥料(江苏)有限公司 Amino acid-containing water-soluble fertilizer with novel biological agent and preparation method thereof
CN102503646A (en) * 2011-11-04 2012-06-20 江门市杰士植物营养有限公司 Production technique for effectively producing organic water-soluble fertilizer
CN105481560A (en) * 2015-12-23 2016-04-13 成都新柯力化工科技有限公司 Multifunctional organic water soluble fertilizer resisting plant diseases and insect pests and preparation method thereof
CN106396795A (en) * 2016-08-29 2017-02-15 潘爱华 Medium and trace element-containing organic water-soluble fertilizer produced from tobacco wastes
CN109179442A (en) * 2018-10-30 2019-01-11 安徽恒昊科技有限公司 A kind of preparation method of Conductive mica

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101870611A (en) * 2010-06-25 2010-10-27 汉枫缓释肥料(江苏)有限公司 Amino acid-containing water-soluble fertilizer with novel biological agent and preparation method thereof
CN102503646A (en) * 2011-11-04 2012-06-20 江门市杰士植物营养有限公司 Production technique for effectively producing organic water-soluble fertilizer
CN105481560A (en) * 2015-12-23 2016-04-13 成都新柯力化工科技有限公司 Multifunctional organic water soluble fertilizer resisting plant diseases and insect pests and preparation method thereof
CN106396795A (en) * 2016-08-29 2017-02-15 潘爱华 Medium and trace element-containing organic water-soluble fertilizer produced from tobacco wastes
CN109179442A (en) * 2018-10-30 2019-01-11 安徽恒昊科技有限公司 A kind of preparation method of Conductive mica

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111018581A (en) * 2019-12-30 2020-04-17 滁州联润生态农业发展有限公司 Organic fertilizer for vegetable planting and preparation process thereof
CN112159272A (en) * 2020-09-27 2021-01-01 深圳市腾浪再生资源发展有限公司 Production process for preparing organic water-soluble fertilizer from kitchen residues
CN112794757A (en) * 2021-03-26 2021-05-14 山东高晟联合农业科技有限公司 Production process of suspended organic water-soluble fertilizer
CN114426440A (en) * 2021-05-06 2022-05-03 内蒙古朵日纳硒科生物技术有限公司 Production process of water-soluble fertilizer for cultivating potatoes
CN116854523A (en) * 2023-06-01 2023-10-10 播乐(海南)生态科技院(有限合伙) Preparation method, product and application of small molecular organic water-soluble fertilizer
CN116854523B (en) * 2023-06-01 2024-11-08 播乐(海南)生态科技院(有限合伙) A method for preparing small molecule organic water-soluble fertilizer, and its products and applications
WO2024245130A1 (en) * 2023-06-01 2024-12-05 贺敏 Method for preparing small-molecule organic water-soluble fertilizer using biomass and waste thereof, and product and application

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Application publication date: 20181116