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CN108793585A - A kind of waste water treatment process - Google Patents

A kind of waste water treatment process Download PDF

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Publication number
CN108793585A
CN108793585A CN201810463840.XA CN201810463840A CN108793585A CN 108793585 A CN108793585 A CN 108793585A CN 201810463840 A CN201810463840 A CN 201810463840A CN 108793585 A CN108793585 A CN 108793585A
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China
Prior art keywords
waste water
ceramic
film tube
treatment process
treated
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Granted
Application number
CN201810463840.XA
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Chinese (zh)
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CN108793585B (en
Inventor
殷开兵
陆云发
闫师
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Yipute Group Co.,Ltd.
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Anhui Yi Pu Te Group Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00Multistage treatment of water, waste water or sewage
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/38Treatment of water, waste water, or sewage by centrifugal separation
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/44Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/5236Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
    • C02F1/5245Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents using basic salts, e.g. of aluminium and iron
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2209/00Controlling or monitoring parameters in water treatment
    • C02F2209/003Downstream control, i.e. outlet monitoring, e.g. to check the treating agents, such as halogens or ozone, leaving the process
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/005Combined electrochemical biological processes
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/28Anaerobic digestion processes

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  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Water Treatment By Electricity Or Magnetism (AREA)
  • Physical Water Treatments (AREA)

Abstract

The present invention provides a kind of waste water treatment process, the specific steps are:Centrifuging treatment, ceramic membrane filter processing, anaerobic bio-treated, chemical precipitation processing and wastewater recycle processing.Advantage is:In such a way that centrifugal separator and cyclone hydraulic separators are combined, the solid impurity in waste liquid is effectively removed, basis is carried out for subsequent sewage disposal, is conducive to the efficiency of follow-up sewage disposal;Using ceramic-film tube, due to the densely covered micropore of ceramic membrane tube wall, under pressure, waste water flows in membrane tube or on the outside of film, small-molecule substance(Or liquid)Through film, macromolecular substances(Or solid particle, liquid drop)It is rejected by reach separation of solid and liquid, concentration and the purpose of purifying, the little particle impurity in waste water can be effectively removed, in addition, in such a way that ceramic-film tube setting is helically risen, not only increase the time of contact of waste water and ceramic-film tube, and by the effect by gravity, further increase the filter capacity of ceramic-film tube all.

Description

A kind of waste water treatment process
Technical field
The present invention relates to technical field of waste water processing more particularly to a kind of waste water treatment process.
Background technology
Waste water of the people discharged in number of storage tanks produced per day, this waste water is mainly by the excreta of life waste material and people institute Pollution, quantity, ingredient and the concentration of pollutant are related with people's lives custom, water consumption.Sanitary sewage is general and does not contain Noxious material, still, it has the condition suitable for microbial reproduction, containing a large amount of bacteriums and pathogen, from the point of view of sanitation point, With certain harmfulness.Wastewater treatment is exactly to be handled waste water using the method for physics, chemistry and biology, keeps waste water net Change, reduce pollution, so that reaching Sewage treatment, multiplexing, makes full use of water resource.
Invention content
To solve the above problems, the invention discloses a kind of waste water treatment process, the effect of processing waste water is effectively played.
In order to reach object above, the present invention provides the following technical solutions:
A kind of waste water treatment process, it is characterised in that:The specific steps are:
S1:Centrifuging treatment:Prepare centrifugal separator first, when frequency converter frequency be 25~30Hz when, by waste water be passed through from The feed inlet of centrifugal separator, subsequent frequency converter frequency rise to 50~60Hz carry out high-speed separation, 6~8min of control time, later The waste water being centrifuged out is passed into cyclone hydraulic separators again, and it is 15000~17000 to control Fr, 5~8min of time;
S2:Ceramic membrane filter processing:By treated in S1, waste water is passed into ceramic-film tube, and the flow velocity for controlling waste liquid is 1.1~1.5m3/ min, ceramic-film tube helically rise shape, and waste water enters from the lower port of ceramic-film tube;
S3:Anaerobic bio-treated:First container bottom install anaerobic reactor, anode and cathode be placed in container and submerge and Among sludge, in addition, the bottom of container is also evenly equipped with ultrasonic transducer, then the bottom of the dirty water from container in S1 is led to Enter, and the DC voltage of 0.5~0.8V is provided simultaneously, cathode directly generates hydrogen or methane gas is expelled directly out;
S4:Chemical precipitation is handled:Pure Fe is added into S3 treated waste water3O4Particle stirs 8~12min, is then added NaOH solution adjusts pH value to 8.5~9.5, adds HCL solution later and adjusts pH value to 6.5~7.5, and it is stirred to react 15~ 20min is separated by solid-liquid separation;
S5:Wastewater recycle processing:By sewage monitoring instrument to carrying out composition detection by S4 treated waste water, if Testing index Waste water is then discharged in qualification, if detection is unqualified, the processing through S1, S2, S3 and S4 successively again, until each finger in waste water Until mark is qualified.
Processing is centrifuged in the present invention first, prepares centrifugal separator, will when frequency converter frequency is 25~30Hz Waste water is passed through the feed inlet of centrifugal separator, and subsequent frequency converter frequency rises to 50~60Hz and carries out high-speed separation, later will centrifugation The waste water gone out is passed into cyclone hydraulic separators again, and it is 15000~17000 to control Fr;Using centrifugal separator and rotary filter press The mode that device is combined effectively removes the solid impurity in waste liquid, carries out basis for subsequent sewage disposal, is conducive to follow-up dirt The efficiency of water process.
It is then handled using ceramic membrane filter, by treated in S1, waste water is passed into ceramic-film tube, and controls waste liquid Flow velocity be 1.1~1.5m3/ min, ceramic-film tube helically rise shape, and waste water enters from the lower port of ceramic-film tube;Using pottery Porcelain membrane tube, due to the densely covered micropore of ceramic membrane tube wall, under pressure, waste water flows in membrane tube or on the outside of film, small molecule object Matter(Or liquid)Through film, macromolecular substances(Or solid particle, liquid drop)It is rejected by reach separation of solid and liquid, concentration With the purpose of purifying, the little particle impurity in waste water can be effectively removed, in addition, by helically rising ceramic-film tube setting Mode, not only increase the time of contact of waste water and ceramic-film tube, and by the effect by gravity, further increase pottery The filter capacity of porcelain membrane tube all.
It uses chemical precipitation to handle later, pure Fe is added into S3 treated waste water3O4Particle stirs 8~12min, with NaOH solution is added afterwards and adjusts pH value to 8.5~9.5, adds HCL solution later and adjusts pH value to 6.5~7.5, and stir anti- 15~20min is answered, is separated by solid-liquid separation;The mode that pH value is gradually adjusted by using two-stage, in removing sewage heavy metal from While sub-, the control of pH value efficient fine is realized.
Wastewater recycle processing is finally carried out, by sewage monitoring instrument to carrying out composition detection by S4 treated waste water, If Testing index is qualified, waste water is discharged, if detection is unqualified, the processing through S1, S2, S3 and S4 successively again, until useless Until each qualified in water.
Further, the ultrasonic transducer in the S3 is connected with supersonic generator.
Further, pure Fe in the S43O4The grain size of particle is 13~15 μm.
Further, the NaOH content in the S4 in NaOH melts is 40~43%.
Further, the HCL contents in the S4 in HCL melts are 38~42%.
Compared with prior art, the beneficial effects of the present invention are:It is combined using centrifugal separator and cyclone hydraulic separators Mode, effectively remove the solid impurity in waste liquid, carry out basis for subsequent sewage disposal, be conducive to follow-up sewage disposal Efficiency;Using ceramic-film tube, due to the densely covered micropore of ceramic membrane tube wall, under pressure, waste water effluent in membrane tube or outside film It is dynamic, small-molecule substance(Or liquid)Through film, macromolecular substances(Or solid particle, liquid drop)It is rejected by reach solid The purpose of liquid separation, concentration and purifying, can effectively remove the little particle impurity in waste water, in addition, by setting ceramic-film tube The mode helically risen is set, not only increases the time of contact of waste water and ceramic-film tube, and by the effect by gravity, Further increase the filter capacity of ceramic-film tube all;The mode that pH value is gradually adjusted by using two-stage, the weight in removing sewage While metal ion, the control of pH value efficient fine is realized.
Specific implementation mode
With reference to embodiment, the present invention is furture elucidated, it should be understood that following specific implementation modes are only used for It is bright the present invention rather than limit the scope of the invention.
Embodiment 1
A kind of waste water treatment process, the specific steps are:
S1:Centrifuging treatment:Prepare centrifugal separator first, when frequency converter frequency is 25Hz, waste water is passed through centrifugation point The feed inlet disembarked, subsequent frequency converter frequency rise to 60Hz and carry out high-speed separation, and control time 6min is useless by what is be centrifuged out later Water is passed into cyclone hydraulic separators again, and it is 17000 to control Fr, time 5min;
S2:Ceramic membrane filter processing:By treated in S1, waste water is passed into ceramic-film tube, and the flow velocity for controlling waste liquid is 1.5m3/ min, ceramic-film tube helically rise shape, and waste water enters from the lower port of ceramic-film tube;
S3:Anaerobic bio-treated:First container bottom install anaerobic reactor, anode and cathode be placed in container and submerge and Among sludge, in addition, the bottom of container is also evenly equipped with ultrasonic transducer, then the bottom of the dirty water from container in S1 is led to Enter, and the DC voltage of 0.5V is provided simultaneously, cathode directly generates hydrogen or methane gas is expelled directly out;Wherein, ultrasonic waves Energy device is connected with supersonic generator;
S4:Chemical precipitation is handled:Pure Fe is added into S3 treated waste water3O4Particle stirs 12min, NaOH is then added Solution adjusts pH value to 8.5, adds HCL solution later and adjusts pH value to 7.5, and be stirred to react 15min, carries out solid-liquid point From;Wherein, pure Fe3O4The grain size of particle is 15 μm, and the NaOH content in middle NaOH melts is the HCL contents in 40%, HCL melts It is 42%;
S5:Wastewater recycle processing:By sewage monitoring instrument to carrying out composition detection by S4 treated waste water, if Testing index Waste water is then discharged in qualification, if detection is unqualified, the processing through S1, S2, S3 and S4 successively again, until each finger in waste water Until mark is qualified.
Embodiment 2
A kind of waste water treatment process, the specific steps are:
S1:Centrifuging treatment:Prepare centrifugal separator first, when frequency converter frequency is 30Hz, waste water is passed through centrifugation point The feed inlet disembarked, subsequent frequency converter frequency rise to 50Hz and carry out high-speed separation, and control time 8min is useless by what is be centrifuged out later Water is passed into cyclone hydraulic separators again, and it is 15000 to control Fr, time 8min;
S2:Ceramic membrane filter processing:By treated in S1, waste water is passed into ceramic-film tube, and the flow velocity for controlling waste liquid is 1.1m3/ min, ceramic-film tube helically rise shape, and waste water enters from the lower port of ceramic-film tube;
S3:Anaerobic bio-treated:First container bottom install anaerobic reactor, anode and cathode be placed in container and submerge and Among sludge, in addition, the bottom of container is also evenly equipped with ultrasonic transducer, then the bottom of the dirty water from container in S1 is led to Enter, and the DC voltage of 0.8V is provided simultaneously, cathode directly generates hydrogen or methane gas is expelled directly out;Wherein, ultrasonic waves Energy device is connected with supersonic generator;
S4:Chemical precipitation is handled:Pure Fe is added into S3 treated waste water3O4Particle, stirs 8min, and it is molten that NaOH is then added Liquid adjusts pH value to 9.5, adds HCL solution later and adjusts pH value to 6.5, and be stirred to react 20min, is separated by solid-liquid separation; Wherein, pure Fe3O4The grain size of particle is 13 μm, and the NaOH content in middle NaOH melts is that the HCL contents in 43%, HCL melts are 38%;
S5:Wastewater recycle processing:By sewage monitoring instrument to carrying out composition detection by S4 treated waste water, if Testing index Waste water is then discharged in qualification, if detection is unqualified, the processing through S1, S2, S3 and S4 successively again, until each finger in waste water Until mark is qualified.
Embodiment 3
A kind of waste water treatment process, the specific steps are:
S1:Centrifuging treatment:Prepare centrifugal separator first, when frequency converter frequency is 28Hz, waste water is passed through centrifugation point The feed inlet disembarked, subsequent frequency converter frequency rise to 55Hz and carry out high-speed separation, and control time 7min is useless by what is be centrifuged out later Water is passed into cyclone hydraulic separators again, and it is 16000 to control Fr, time 7min;
S2:Ceramic membrane filter processing:By treated in S1, waste water is passed into ceramic-film tube, and the flow velocity for controlling waste liquid is 1.3m3/ min, ceramic-film tube helically rise shape, and waste water enters from the lower port of ceramic-film tube;
S3:Anaerobic bio-treated:First container bottom install anaerobic reactor, anode and cathode be placed in container and submerge and Among sludge, in addition, the bottom of container is also evenly equipped with ultrasonic transducer, then the bottom of the dirty water from container in S1 is led to Enter, and the DC voltage of 0.7V is provided simultaneously, cathode directly generates hydrogen or methane gas is expelled directly out;Wherein, ultrasonic waves Energy device is connected with supersonic generator;
S4:Chemical precipitation is handled:Pure Fe is added into S3 treated waste water3O4Particle stirs 10min, NaOH is then added Solution adjusts pH value to 8.9, adds HCL solution later and adjusts pH value to 6.9 and be stirred to react 17min, is separated by solid-liquid separation; Wherein, pure Fe3O4The grain size of particle is 14 μm, and the NaOH content in middle NaOH melts is that the HCL contents in 41%, HCL melts are 39%;
S5:Wastewater recycle processing:By sewage monitoring instrument to carrying out composition detection by S4 treated waste water, if Testing index Waste water is then discharged in qualification, if detection is unqualified, the processing through S1, S2, S3 and S4 successively again, until each finger in waste water Until mark is qualified.

Claims (5)

1. a kind of waste water treatment process, it is characterised in that:The specific steps are:
S1:Centrifuging treatment:Prepare centrifugal separator first, when frequency converter frequency be 25~30Hz when, by waste water be passed through from The feed inlet of centrifugal separator, subsequent frequency converter frequency rise to 50~60Hz carry out high-speed separation, 6~8min of control time, later The waste water being centrifuged out is passed into cyclone hydraulic separators again, and it is 15000~17000 to control Fr, 5~8min of time;
S2:Ceramic membrane filter processing:By treated in S1, waste water is passed into ceramic-film tube, and the flow velocity for controlling waste liquid is 1.1~1.5m3/ min, ceramic-film tube helically rise shape, and waste water enters from the lower port of ceramic-film tube;
S3:Anaerobic bio-treated:First container bottom install anaerobic reactor, anode and cathode be placed in container and submerge and Among sludge, in addition, the bottom of container is also evenly equipped with ultrasonic transducer, then the bottom of the dirty water from container in S1 is led to Enter, and the DC voltage of 0.5~0.8V is provided simultaneously, cathode directly generates hydrogen or methane gas is expelled directly out;
S4:Chemical precipitation is handled:Pure Fe is added into S3 treated waste water3O4Particle stirs 8~12min, is then added NaOH solution adjusts pH value to 8.5~9.5, adds HCL solution later and adjusts pH value to 6.5~7.5, and it is stirred to react 15~ 20min is separated by solid-liquid separation;
S5:Wastewater recycle processing:By sewage monitoring instrument to carrying out composition detection by S4 treated waste water, if Testing index Waste water is then discharged in qualification, if detection is unqualified, the processing through S1, S2, S3 and S4 successively again, until each finger in waste water Until mark is qualified.
2. a kind of waste water treatment process according to claim 1, it is characterised in that:Ultrasonic transducer in the S3 connects It is connected to supersonic generator.
3. a kind of waste water treatment process according to claim 1, it is characterised in that:Pure Fe in the S43O4The grain size of particle It is 13~15 μm.
4. a kind of waste water treatment process according to claim 1, it is characterised in that:NaOH in the S4 in NaOH melts Content is 40~43%.
5. a kind of waste water treatment process according to claim 4, it is characterised in that:HCL in the S4 in HCL melts contains Amount is 38~42%.
CN201810463840.XA 2018-05-15 2018-05-15 Wastewater treatment process Active CN108793585B (en)

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CN108793585B CN108793585B (en) 2021-03-23

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114084974A (en) * 2021-11-23 2022-02-25 上海赛奥分离技术工程有限公司 Treatment method of glass grinding fluid

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014034827A1 (en) * 2012-08-31 2014-03-06 東レ株式会社 Fresh water generation method
CN104276725A (en) * 2014-09-22 2015-01-14 上海安赐机械设备有限公司 Device and method for treating chemical wastewater
WO2016072960A1 (en) * 2014-11-06 2016-05-12 Young Thomas Benton Municipal waste water treatment plant design to produce byproducts and recycle water of drinking water quality
CN207159025U (en) * 2017-07-22 2018-03-30 韩元元 A kind of sewage disposal purification pot

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014034827A1 (en) * 2012-08-31 2014-03-06 東レ株式会社 Fresh water generation method
CN104276725A (en) * 2014-09-22 2015-01-14 上海安赐机械设备有限公司 Device and method for treating chemical wastewater
WO2016072960A1 (en) * 2014-11-06 2016-05-12 Young Thomas Benton Municipal waste water treatment plant design to produce byproducts and recycle water of drinking water quality
CN207159025U (en) * 2017-07-22 2018-03-30 韩元元 A kind of sewage disposal purification pot

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114084974A (en) * 2021-11-23 2022-02-25 上海赛奥分离技术工程有限公司 Treatment method of glass grinding fluid

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Address after: 239300 No.28 Chuangye Road, Yongfeng Industrial Park, Tianchang City, Chuzhou City, Anhui Province

Patentee after: Yipute Group Co.,Ltd.

Address before: 239300 No.28 Chuangye Road, Yongfeng Industrial Park, Tianchang City, Chuzhou City, Anhui Province

Patentee before: ANHUI YIPUTE GROUP Co.,Ltd.