A kind of preparation process of green banana tablet
【Technical field】
The present invention relates to the preparation field of tablet, more particularly to a kind of preparation process of green banana tablet.
【Background technology】
Banana is full of nutrition, is known as " king of new fruit ".Began from 2013, Guangxi banana production and cultivated area are
The whole nation second and third are leapt to respectively.Climate influences, and banana is unsalable to be often occurred, and orchard worker is caused largely to be lost.If can incite somebody to action
A part of banana is picked in the immature phase, is processed into food, and banana market can be effectively adjusted.Resistant starch in the full powder of green banana
Content reaches 70.96%, and resistant starch has low in calories, prevention diabetes, reducing blood lipid, weight-reducing and other effects.If making full use of blueness
Resistant starch effect in banana is processed into tablet easy to carry and edible, will bring certain industry application value,
Process parameters can be provided for the further deep processing of banana industry.Green banana powder tablet, process are made using direct tablet compressing technology
Less, the time is short and not contact wetting, can effectively reduce ambient temperature and humidity and microbial contamination.Green banana powder is not easy film-making, tablet
Hardness is low, broken at a touch, can not carry out product packaging and transport;And not easy disintegrating, it does not meet《Chinese Pharmacopoeia》Middle tablet is answered
In the requirement that 15 minutes are all disintegrated.To solve the problems, such as this, by add auxiliary material, but auxiliary material for tablet hardness, disintegration when
Limit has great influence, directly affects product quality problem.On the other hand, green banana pulp mouthfeel itself is bad, if by
During preparing green banana powder, passion fruit pulp (giving off a strong fragrance, acidity height) is added, color, smell and taste and the nutrition of product can be increased
Ingredient.In addition, taro covers the dietary fiber of the title rich in human body " the 7th nutrition ", also contain abundant zinc (2.3mg/kg), dimension life
The nutritional ingredients such as plain B1 (7.42g/100g), B2 (11.6g/100g), but at present taro cover be mainly used for curing food " ganoid konjaku taro stalk salts down
Product and its method for salting " (201410698887.6), there is no be applied in product development in the form of taro illiteracy powder.
【Invention content】
Present invention aims at a kind of preparation process of green banana tablet is provided, green banana pulp is first immersed in low temperature lemon
In lemon acid solution, then after mixing by green banana pulp and passion fruit pulp, after drying and crushing is handled, highly resistance is prepared
Property content of starch green banana compound powder;Then after carrying out dispensing, compression molding is carried out.The present invention prepares green banana tablet hardness
Height, disintegration time are short, have large market promotion prospect.
In order to achieve the above objectives, the technical solution adopted in the present invention is:A kind of preparation process of green banana tablet, including
Following steps:
(1) preparation of green banana compounding powder:Green banana cleaning, cut-out of the maturity at 1 grade or 2 grades are taken, and by green banana
Gained pulp, is placed in that temperature is 5~8 DEG C, mass fraction is to be soaked in 0.1%~0.2% citric acid solution by skin and pulp separation
It is taken out after 15~25min of bubble, is 9 by weight:After 1 ratio mixes green banana pulp and passion fruit pulp, low temperature is carried out
Mashing, then drying temperature is 30~50 DEG C, ultrasonic acoustic density is 1~2W/g and the ultrasonic duration is 0.5~2h's
Under the conditions of carry out vacuum ultrasonic drying, after finally carrying out ultramicro grinding processing, obtain that water content is 5%~8%, resistant starch contains
Amount compounds powder for 69%~71% green banana;
(2) tablet formulations:Count in parts by weight, 20~50 parts of green banana powder of precise, 10~25 portions of taros cover powder, 20~
23 portions of mannitol, 10~15 parts of built-up starch carry out preliminary mixing with vortex mixer, and sieving obtains waiting for tabletting material;
(3) compression molding:It will wait for that tabletting material is placed in constant temperature and humidity fluid bed, addition waits for tabletting quality of material 1.5%
Magnesium stearate, by air flowing so that material is further mixed into fine particle, be then placed in tablet press machine, be pressed into two
While there is the green banana tablet of chamfering.
In the present invention, as further explanation, the technological parameter of the ultramicro grinding processing described in step (1) is:It crushes
Rotating speed is 3000~5000r/min, grinding time is 3~5min, crosses 100~140 mesh sieve.
In the present invention, as further explanation, the low temperature described in step (1) is beaten by liquid nitrogen environment or ice bath ring
Mashing processing is carried out in border.
In the present invention, as further explanation, built-up starch described in step (2) is by by weight being 3~5:1:1
The mixing starch that cornstarch, tapioca and chestnut starch are composed.
In the present invention, as further explanation, it is that fresh taro illiteracy stem is peelled off extexine that the taro described in step (2), which covers powder,
Pi Hou, the powder cleaned, cut off, obtained after vacuum freeze drying and ultramicro grinding.
In the present invention, as further explanation, content that the taro described in step (2) covers dietary fiber in powder is 10%~
17%.
In the present invention, as further explanation, the taro described in step (2) covers fineness≤5 μm of powder.
The function introduction of part material is as follows:
Citric acid is used as antioxidant, in order to reduce the brown stain of green banana in the present invention.
Mannitol is used as excipient in the present invention.
Cornstarch, tapioca and chestnut starch, in the present invention be used as filler, to make up single starch nutrition at
Divide the drawback single, filling effect is undesirable.
Taro covers powder, containing abundant dietary fiber, but also rich in zinc, vitamin B1, B2, is used in the present invention and green
The nutritional ingredient of banaina is complementary, increases dietary fiber content in green banana compounding powder, solves to lack zinc, vitamin B1, B2
Problem, while dietary fiber promotes the wriggling of stomach, can accelerate absorption of the stomach to green banana tablet.
Magnesium stearate is used as lubricant in the present invention.
The invention has the advantages that:
1, the preparation method for the green banana powder that the present invention uses, can efficiently retain the resistant starch in green banana.This hair
Green banana pulp is immersed in citric acid solution by bright first use under 5~8 DEG C of cryogenic conditions, to reduce the brown of green banana
Become;Then using the technological means for green banana pulp and passion fruit pulp being mixed, being carried out low temperature mashing, the color for increasing product is fragrant
While taste and nutritional ingredient, using the acidic materials in passion fruit pulp, and then the inoxidizability of green banana is improved;Finally lead to
The technological means for crossing vacuum ultrasonic drying, further reduces the brown stain of nutriment in green banana, improves resistant starch
Reserving degree.
2, the present invention can utilize constant temperature and humidity condition to keep nutrition using compression molding is carried out under the conditions of constant temperature and humidity
The stabilization of substance can also preserve the activity of resistant starch in material.
3, the present invention prepares green banana tablet using direct tablet compressing technique, makes simply, farthest remains green perfume
The resistance starch content of any of several broadleaf plants fruit, the tablet were not only easy for carrying and eating but also nutritious.
4, mannitol of the present invention more common pregelatinized starch or microcrystalline cellulose, the hardness of detection can be from
The 102g of pregelatinized starch, the 544g of microcrystalline cellulose promote the 899g to mannitol, realize and significantly promote tablet hardness
Effect.
5, magnesium stearate of the present invention more common superfine silica gel powder or talcum powder, can be from the 39.7 of superfine silica gel powder
39.1 degree of be reduced to magnesium stearate 36.3 degree of degree and talcum powder, realize the angle of repose that material is greatly lowered, Jin Erti
The mobility of high material promotes the compression moulding of tablet.
6, (cornstarch, tapioca and chestnut starch weight ratio are 5 to built-up starch of the present invention:1:1) compared with
Common sodium carboxymethyl starch or low-substituted hydroxypropyl cellulose, disintegration time can be from the 2.03min of sodium carboxymethyl starch, low
The 1.30min of substitution hydroxypropyl cellulose is reduced to the 22s of built-up starch, realizes the effect for quickly reducing tablet disintegration times
Fruit.
【Specific implementation mode】
Embodiment 1:
A kind of preparation process of green banana tablet, includes the following steps:
(1) preparation of green banana compounding powder:Green banana cleaning, cut-out of the maturity at 1 grade are taken, and by green banana skin and fruit
Meat detach, by gained pulp be placed in temperature be 5 DEG C, mass fraction be in 0.1% citric acid solution impregnate 15min after take out, press
Weight ratio is 9:After 1 ratio mixes green banana pulp and passion fruit pulp, by liquid nitrogen environment or ice bath environment into
Row mashing is handled, then in the condition that drying temperature is 30 DEG C, ultrasonic acoustic density is 1W/g and the ultrasonic duration is 0.5h
Lower progress vacuum ultrasonic drying, finally carry out ultramicro grinding processing after, obtain water content be 5%, resistance starch content 69%
Green banana compound powder;
The technological parameter of the described ultramicro grinding processing is:Crush rotating speed be 3000r/min, grinding time 3min, mistake
100 mesh sieve;
(2) tablet formulations:Count in parts by weight, 20 parts of green banana powder of precise, 10 portions of taros cover powder, 20 portions of mannitol,
10 parts of built-up starch carry out preliminary mixing with vortex mixer, and sieving obtains waiting for tabletting material;
It is after fresh taro illiteracy stem is peelled off extexine skin that the taro, which covers powder, cleaned, cut off, vacuum freeze drying and
The powder obtained after ultramicro grinding;The content that the taro covers dietary fiber in powder is 10%;The taro covers fineness≤5 of powder
μm;
The built-up starch is by being 3 by weight:1:1 cornstarch, tapioca and chestnut starch is composed
Mixing starch;
(3) compression molding:It will wait for that tabletting material is placed in constant temperature and humidity fluid bed, addition waits for tabletting quality of material 1.5%
Magnesium stearate, by air flowing so that material is further mixed into fine particle, be then placed in tablet press machine, be pressed into two
While there is the green banana tablet of chamfering.
Embodiment 2:
A kind of preparation process of green banana tablet, includes the following steps:
(1) preparation of green banana compounding powder:Green banana cleaning, cut-out of the maturity at 2 grades are taken, and by green banana skin and fruit
Meat detach, by gained pulp be placed in temperature be 6 DEG C, mass fraction be in 0.12% citric acid solution impregnate 18min after take out, press
Weight ratio is 9:After 1 ratio mixes green banana pulp and passion fruit pulp, by liquid nitrogen environment or ice bath environment into
Row mashing is handled, then in the condition that drying temperature is 34 DEG C, ultrasonic acoustic density is 1.3W/g and the ultrasonic duration is 1h
Lower progress vacuum ultrasonic drying, finally carry out ultramicro grinding processing after, obtain water content be 6%, resistance starch content 70%
Green banana compound powder;
The technological parameter of the described ultramicro grinding processing is:Crush rotating speed be 3500r/min, grinding time 3.5min,
Cross 110 mesh sieve;
(2) tablet formulations:Count in parts by weight, 30 parts of green banana powder of precise, 17 portions of taros cover powder, 21 portions of mannitol,
14 parts of built-up starch carry out preliminary mixing with vortex mixer, and sieving obtains waiting for tabletting material;
It is after fresh taro illiteracy stem is peelled off extexine skin that the taro, which covers powder, cleaned, cut off, vacuum freeze drying and
The powder obtained after ultramicro grinding;The content that the taro covers dietary fiber in powder is 16%;The taro covers fineness≤5 of powder
μm;
The built-up starch is by being 4 by weight:1:1 cornstarch, tapioca and chestnut starch is composed
Mixing starch;
(3) compression molding:It will wait for that tabletting material is placed in constant temperature and humidity fluid bed, addition waits for tabletting quality of material 1.5%
Magnesium stearate, by air flowing so that material is further mixed into fine particle, be then placed in tablet press machine, be pressed into two
While there is the green banana tablet of chamfering.
Embodiment 3:
A kind of preparation process of green banana tablet, includes the following steps:
(1) preparation of green banana compounding powder:Green banana cleaning, cut-out of the maturity at 1 grade are taken, and by green banana skin and fruit
Meat detach, by gained pulp be placed in temperature be 7 DEG C, mass fraction be in 0.15% citric acid solution impregnate 20min after take out, press
Weight ratio is 9:After 1 ratio mixes green banana pulp and passion fruit pulp, by liquid nitrogen environment or ice bath environment into
Row mashing is handled, then in the item that drying temperature is 40 DEG C, ultrasonic acoustic density is 1.5W/g and the ultrasonic duration is 1.5h
Vacuum ultrasonic drying is carried out under part, after finally carrying out ultramicro grinding processing, obtains that water content is 6%, resistance starch content is
70% green banana compounds powder;
The technological parameter of the described ultramicro grinding processing is:Crush rotating speed be 3900r/min, grinding time 4min, mistake
120 mesh sieve;
(2) tablet formulations:Count in parts by weight, 40 parts of green banana powder of precise, 19 portions of taros cover powder, 22 portions of mannitol,
13 parts of built-up starch carry out preliminary mixing with vortex mixer, and sieving obtains waiting for tabletting material;
It is after fresh taro illiteracy stem is peelled off extexine skin that the taro, which covers powder, cleaned, cut off, vacuum freeze drying and
The powder obtained after ultramicro grinding;The content that the taro covers dietary fiber in powder is 14%;The taro covers fineness≤5 of powder
μm;
The built-up starch is by being 5 by weight:1:1 cornstarch, tapioca and chestnut starch is composed
Mixing starch;
(3) compression molding:It will wait for that tabletting material is placed in constant temperature and humidity fluid bed, addition waits for tabletting quality of material 1.5%
Magnesium stearate, by air flowing so that material is further mixed into fine particle, be then placed in tablet press machine, be pressed into two
While there is the green banana tablet of chamfering.
Embodiment 4:
A kind of preparation process of green banana tablet, includes the following steps:
(1) preparation of green banana compounding powder:Green banana cleaning, cut-out of the maturity at 2 grades are taken, and by green banana skin and fruit
Meat detach, by gained pulp be placed in temperature be 7 DEG C, mass fraction be in 0.13% citric acid solution impregnate 22min after take out, press
Weight ratio is 9:After 1 ratio mixes green banana pulp and passion fruit pulp, by liquid nitrogen environment or ice bath environment into
Row mashing is handled, then in the item that drying temperature is 44 DEG C, ultrasonic acoustic density is 1.6W/g and the ultrasonic duration is 1.5h
Vacuum ultrasonic drying is carried out under part, after finally carrying out ultramicro grinding processing, obtains that water content is 7%, resistance starch content is
71% green banana compounds powder;
The technological parameter of the described ultramicro grinding processing is:Crush rotating speed be 4500r/min, grinding time 4.5min,
Cross 130 mesh sieve;
(2) tablet formulations:Count in parts by weight, 30 parts of green banana powder of precise, 21 portions of taros cover powder, 22 portions of mannitol,
14 parts of built-up starch carry out preliminary mixing with vortex mixer, and sieving obtains waiting for tabletting material;
It is after fresh taro illiteracy stem is peelled off extexine skin that the taro, which covers powder, cleaned, cut off, vacuum freeze drying and
The powder obtained after ultramicro grinding;The content that the taro covers dietary fiber in powder is 13%;The taro covers fineness≤5 of powder
μm;
The built-up starch is by being 5 by weight:1:1 cornstarch, tapioca and chestnut starch is composed
Mixing starch;
(3) compression molding:It will wait for that tabletting material is placed in constant temperature and humidity fluid bed, addition waits for tabletting quality of material 1.5%
Magnesium stearate, by air flowing so that material is further mixed into fine particle, be then placed in tablet press machine, be pressed into two
While there is the green banana tablet of chamfering.
Embodiment 5:
A kind of preparation process of green banana tablet, includes the following steps:
(1) preparation of green banana compounding powder:Green banana cleaning, cut-out of the maturity at 1 grade are taken, and by green banana skin and fruit
Meat detach, by gained pulp be placed in temperature be 6 DEG C, mass fraction be in 0.16% citric acid solution impregnate 24min after take out, press
Weight ratio is 9:After 1 ratio mixes green banana pulp and passion fruit pulp, by liquid nitrogen environment or ice bath environment into
Row mashing is handled, then in the condition that drying temperature is 41 DEG C, ultrasonic acoustic density is 1.7W/g and the ultrasonic duration is 1h
Lower progress vacuum ultrasonic drying, finally carry out ultramicro grinding processing after, obtain water content be 7%, resistance starch content 70%
Green banana compound powder;
The technological parameter of the described ultramicro grinding processing is:Crush rotating speed be 3700r/min, grinding time 3.5min,
Cross 110 mesh sieve;
(2) tablet formulations:Count in parts by weight, 36 parts of green banana powder of precise, 16 portions of taros cover powder, 21 portions of mannitol,
12 parts of built-up starch carry out preliminary mixing with vortex mixer, and sieving obtains waiting for tabletting material;
It is after fresh taro illiteracy stem is peelled off extexine skin that the taro, which covers powder, cleaned, cut off, vacuum freeze drying and
The powder obtained after ultramicro grinding;The content that the taro covers dietary fiber in powder is 16%;The taro covers fineness≤5 of powder
μm;
The built-up starch is by being 3.5 by weight:1:1 cornstarch, tapioca and chestnut starch combination and
At mixing starch;
(3) compression molding:It will wait for that tabletting material is placed in constant temperature and humidity fluid bed, addition waits for tabletting quality of material 1.5%
Magnesium stearate, by air flowing so that material is further mixed into fine particle, be then placed in tablet press machine, be pressed into two
While there is the green banana tablet of chamfering.
Embodiment 6:
A kind of preparation process of green banana tablet, includes the following steps:
(1) preparation of green banana compounding powder:Green banana cleaning, cut-out of the maturity at 2 grades are taken, and by green banana skin and fruit
Meat detach, by gained pulp be placed in temperature be 8 DEG C, mass fraction be in 0.2% citric acid solution impregnate 25min after take out, press
Weight ratio is 9:After 1 ratio mixes green banana pulp and passion fruit pulp, by liquid nitrogen environment or ice bath environment into
Row mashing is handled, then under conditions of drying temperature is 50 DEG C, ultrasonic acoustic density is 2W/g and the ultrasonic duration is 2h
Vacuum ultrasonic drying is carried out, after finally carrying out ultramicro grinding processing, obtains that water content is 8%, resistance starch content is 71%
Green banana compounds powder;
The technological parameter of the described ultramicro grinding processing is:Crush rotating speed be 5000r/min, grinding time 5min, mistake
140 mesh sieve;
(2) tablet formulations:Count in parts by weight, 50 parts of green banana powder of precise, 25 portions of taros cover powder, 23 portions of mannitol,
15 parts of built-up starch carry out preliminary mixing with vortex mixer, and sieving obtains waiting for tabletting material;
It is after fresh taro illiteracy stem is peelled off extexine skin that the taro, which covers powder, cleaned, cut off, vacuum freeze drying and
The powder obtained after ultramicro grinding;The content that the taro covers dietary fiber in powder is 17%;The taro covers fineness≤5 of powder
μm;
The built-up starch is by being 5 by weight:1:1 cornstarch, tapioca and chestnut starch is composed
Mixing starch;
(3) compression molding:It will wait for that tabletting material is placed in constant temperature and humidity fluid bed, addition waits for tabletting quality of material 1.5%
Magnesium stearate, by air flowing so that material is further mixed into fine particle, be then placed in tablet press machine, be pressed into two
While there is the green banana tablet of chamfering.
Experiment 1:
The influence of mannitol dosage:It is 10% in built-up starch dosage, it is 20% that taro, which covers powder dosage, and magnesium stearate dosage is
When 1.5%, design mannitol dosage is that 10%, 20%, 30%, 40%, 50% 5 additive amount carries out tabletting, hard with tablet
Degree, disintegration time limited are inspection target, investigate the influence of mannitol dosage.Testing result is shown in Table 1.
Table 1:
As shown in Table 1:When the dosage of mannitol is 20%, the hardness of green banana tablet is highest, and disintegration time compared with
It is moderate.
Experiment 2:
The influence of built-up starch dosage:It is 20% to cover powder dosage in mannitol dosage 20%, taro, magnesium stearate dosage
When 1.5%, the dosage of built-up starch is 5%, 10%, 15%, 20%, 25% progress tabletting, is with tablet hardness, disintegration time limited
Inspection target investigates influence of the built-up starch dosage to tablet.Testing result is shown in Table 2:.
Table 2:
As shown in Table 2:When built-up starch dosage is 10%, the hardness of green banana tablet is highest, and disintegration time compared with
It is moderate.
Experiment 3:
The influence of magnesium stearate dosage:It is 20% to cover powder dosage in mannitol dosage 20%, taro, built-up starch dosage 10%
When, design magnesium stearate dosage is 0.5%, 1%, 1.5%, 2%, 2.5% progress tabletting, and tablet hardness, disintegration time limited are to examine
Index is examined, influence of the magnesium stearate to tablet is investigated.Testing result is shown in Table 3.
Table 3:
As shown in Table 3:When magnesium stearate dosage is 1.5%, the hardness of green banana tablet is highest, and disintegration time compared with
It is moderate.
In conclusion when green banana compounding powder is 50%, mannitol dosage is 20% or so, taro cover powder dosage be 20%,
When built-up starch dosage is 10% or so, magnesium stearate dosage is 1.5% or so, the hardness of green banana tablet is preferable, and
Disintegration time is shorter.
Comparative example 1:Specific preparation method is substantially the same manner as Example 1, and difference is:The preparation process of green banana powder
Middle green banana pulp is to be immersed in citric acid solution at normal temperatures;
Comparative example 2:Specific preparation method is substantially the same manner as Example 1, and difference is:Using normal pressure, normal temperature condition
Lower carry out compression molding.
Contrast test 1:
Hardness determination is tested:100g green banana tablets are prepared according to the method for comparative example 1-2 and embodiment 1-6, with green fragrant
Any of several broadleaf plants tablet hardness, disintegration time limited are inspection target, and specific testing result is shown in Table 4.
Table 4:
|
Hardness/g |
Disintegration time limited/min |
Comparative example 1 |
2421±108.475 |
13.39±0.186 |
Comparative example 2 |
3589±175.237 |
10.52±0.107 |
Embodiment 1 |
5218±129.186 |
9.46±0.156 |
Embodiment 2 |
5178±130.264 |
9.51±0.213 |
Embodiment 3 |
5210±122.295 |
9.52±0.316 |
Embodiment 4 |
5206±125.314 |
9.49±0.304 |
Embodiment 5 |
5213±121.175 |
9.50±0.285 |
Embodiment 6 |
5214±120.457 |
9.51±0.281 |
Table 4 the result shows that:The hardness of green banana tablet is bigger, is more conducive to storage and transport.1 tablet of comparative example it is hard
Degree is minimum, and the hardness of 1 tablet of embodiment is maximum, illustrates that, by being immersed in citric acid at low temperature, it is hard raising tablet can be reached
The effect of degree;
The disintegration time of green banana tablet is shorter, is more conducive to make tablet dissolved in aqueous solution.1 tablet of comparative example collapses
Time longest is solved, the disintegration time of 1 tablet of embodiment is most short, illustrates that, by being immersed in citric acid at low temperature, drop can be reached
The effect of low tablet disintegration times.
Above description is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair
Bright patent claim, it is all the present invention suggested by technical spirit under completed same changes or modifications change, should all belong to
In the covered the scope of the claims of the present invention.