CN108706879A - Color material and its manufacture craft of ceramics under furnace transmutation glaze - Google Patents
Color material and its manufacture craft of ceramics under furnace transmutation glaze Download PDFInfo
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- CN108706879A CN108706879A CN201810485711.0A CN201810485711A CN108706879A CN 108706879 A CN108706879 A CN 108706879A CN 201810485711 A CN201810485711 A CN 201810485711A CN 108706879 A CN108706879 A CN 108706879A
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- 239000000463 material Substances 0.000 title claims abstract description 117
- 238000009377 nuclear transmutation Methods 0.000 title claims abstract description 102
- 239000000919 ceramic Substances 0.000 title claims abstract description 72
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 18
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 40
- 239000011707 mineral Substances 0.000 claims abstract description 40
- 238000010304 firing Methods 0.000 claims abstract description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 26
- 238000005034 decoration Methods 0.000 claims abstract description 23
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 13
- DQMUQFUTDWISTM-UHFFFAOYSA-N O.[O-2].[Fe+2].[Fe+2].[O-2] Chemical compound O.[O-2].[Fe+2].[Fe+2].[O-2] DQMUQFUTDWISTM-UHFFFAOYSA-N 0.000 claims abstract description 13
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 13
- 239000010433 feldspar Substances 0.000 claims abstract description 13
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000010453 quartz Substances 0.000 claims abstract description 13
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 13
- 235000015895 biscuits Nutrition 0.000 claims description 25
- 238000010792 warming Methods 0.000 claims description 15
- 238000000498 ball milling Methods 0.000 claims description 12
- 239000003086 colorant Substances 0.000 claims description 12
- 238000001816 cooling Methods 0.000 claims description 5
- 238000007873 sieving Methods 0.000 claims description 5
- 238000010583 slow cooling Methods 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 8
- 238000000034 method Methods 0.000 abstract description 7
- 229910052573 porcelain Inorganic materials 0.000 abstract description 4
- 230000019612 pigmentation Effects 0.000 abstract description 2
- 239000000047 product Substances 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical group [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 238000010422 painting Methods 0.000 description 2
- 238000005282 brightening Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000011265 semifinished product Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Glass Compositions (AREA)
Abstract
The present invention relates to ceramic fabrication technique field, it is specifically related to color material and its manufacture craft of ceramics under a kind of furnace transmutation glaze.Color material under this kind of furnace transmutation glaze, including raw mineral materials and water, wherein raw mineral materials are made of feldspar, quartz, kaolin, titanium dioxide, di-iron trioxide, inorganic color, and the ratio of raw mineral materials and water is 3-4:1.Color material and its manufacture craft of ceramics under furnace transmutation glaze provided by the invention, due to containing in color material under furnace transmutation glaze, there are many pigmentation elements, by the temperature change of kiln when firing, oxidized or reduction, color material generates reaction under furnace transmutation glaze, colorful transmutation effect is formed under transparent glaze layer, seems very unique and marvellous using color material decoration porcelain under this kind of furnace transmutation glaze.This kind of transmutation under-glaze decoration ceramic provides a kind of completely new ceramic kind, to pushing the development of ceramic product with positive meaning and with positive economic benefit.
Description
Technical field
The present invention relates to ceramic fabrication technique field, it is specifically related to color material and its making work of ceramics under a kind of furnace transmutation glaze
Skill.
Background technology
Underglaze colour is one kind of porcelain muffle painting decoration, You Cheng "Kiln kiln ".Underglaze colour is a kind of primary decoration hand of ware
Section, is to draw various decorative patterns on the molded biscuit (i.e. semi-finished product) dried with colorant, then cover with white clear glaze or
Other light overglazes, once-firing.Pattern after firing is covered in below by the glaze film of layer of transparent, and surface-brightening is soft, flat
Cunning is non-bulging, it appears sparkling and crystal-clear bright.
Traditional underglaze colour includes brown coloured silk, breen coloured silk etc. under three coloured silks, five color painting in the glaze, glaze under blue and white, under-glaze red, glaze.As specially
Profit number is related to ceramics technique for color under glaze in high temp for " ceramics technique for color under glaze in high temp " patent of CN02136786.8, which includes
Molding, biscuiting, polishing, colored drawing, color burn, pour glaze, grand feu, at processing steps such as porcelain, and existing technique for color under glaze in high temp needs
Will be by biscuiting, color be burnt, klining is burnt into could be molded three times, wherein biscuiting temperature is 700-800 DEG C, color burning temperature is 700-
800 DEG C, temperature of glaze firing be 1320-1400 DEG C；The requirement color development of good underglaze colour is bright, and color stable just can guarantee the five colours
The effect of in riotous profusion firing.Constantly change with the aesthetic consciousness of people, transmutation effect gradually obtains liking for people, existing
The transmutation effect of ceramic surface can only realize that is, furnace transmutation glaze can only decorate the whole surface of ceramic body by glaze；
Therefore, if can provide it is a kind of by way of underglaze colour to ceramic surface carry out furnace transmutation decoration, especially part decoration, can carry
For a kind of completely new ceramic decoration method, it can not only meet the aesthetic diversified demand of people, moreover it is possible to provide a kind of completely new pottery
Ceramic products, to pushing the development of ceramic product with positive meaning and with positive economic benefit.
Invention content
In order to solve the deficiencies in the prior art, the present invention provides color material under a kind of furnace transmutation glaze and preparation method thereof and its systems
Make technique.
To achieve the above object, color material under furnace transmutation glaze, which is characterized in that under the furnace transmutation glaze color material include raw mineral materials and
The component of water, wherein raw mineral materials is as follows：32-40 parts of feldspar, 25-32 parts of quartz, 8-10 parts of kaolin, titanium dioxide 8-16
Part, 6-15 parts of di-iron trioxide, 3-5 parts of inorganic color, and the ratio of raw mineral materials and water are 3-4:1.
Further, the component of color material is as follows under furnace transmutation glaze：36 parts of feldspar, 30 parts of quartz, 8 parts of kaolin, titanium dioxide 9
Part, 14 parts of di-iron trioxide, 3 parts of inorganic color, and the ratio of raw mineral materials and water are 3.5:1.
Further,：33 parts of feldspar, 31 parts of quartz, 10 parts of kaolin, 10 parts of titanium dioxide, 11 parts of di-iron trioxide, nothing
5 parts of machine colorant, and the ratio of raw mineral materials and water is 3.8:1.
Further, the component of color material is as follows under furnace transmutation glaze：38 parts of feldspar, 26 parts of quartz, 9 parts of kaolin, titanium dioxide
15 parts, 8 parts of di-iron trioxide, 4 parts of inorganic color, and the ratio of raw mineral materials and water are 3.2:1.
A kind of manufacture craft of transmutation under-glaze decoration ceramic, using color material under the furnace transmutation glaze described in above-mentioned any one, specifically
Steps are as follows：
Step 1, ceramic body is prepared；
Step 2, it according to the material component of color material under furnace transmutation glaze, configures, prepare color material under furnace transmutation glaze；
Step 3, ceramic body made from step 1 is put into biscuiting in kiln, obtains biscuit；
Step 4, color material under furnace transmutation glaze made from step 2 is plotted on biscuit of ceramics；
Step 5, clear frit is applied on biscuit of ceramics；
Step 6, the biscuit of ceramics after glazing is put into kiln and is formed by a firing, firing temperature is 1250 ± 50 DEG C.
Further, ceramic body is light color.
Further, in step 2, under furnace transmutation glaze the preparation of color material be as follows：
S1 weighs mixing according to the raw mineral materials component of color material under furnace transmutation glaze；
S2 will add water for ball milling in raw mineral materials that step 1 configures；
S3, after ball milling sieving be prepared into Freehandhand-drawing colorant under furnace transmutation glaze.
Further, the sieve in S3 is 300 mesh or less.
Further, the thickness of clear frit is 0.5-8mm in step 5.
Further, firing control is divided into five sections of controls in step 6, respectively：
Low-temperature zone, kiln pass through 2-3 hours, and 600 DEG C are warming up to by 250 DEG C；
Middle-temperature section, kiln pass through 1-2 hours, and 1000 DEG C are warming up to by 600 DEG C；
Become temperature section, kiln is cooled to 800 DEG C through 0.5-1 hours, by 1000 DEG C；
High temperature section, kiln pass through 2-3 hours, are warming up to firing temperature by 1000 DEG C, and small in firing temperature heat preservation 0.5-1
When；
Slow cooling section, kiln are cooled to 200 DEG C through 2.5-3 hours, by firing temperature, kiln natural cooling are opened, by 200 DEG C
It is cooled to 20 degrees Celsius.
Further, step firing temperature is 1265 DEG C.
Color material and its manufacture craft of ceramics under furnace transmutation glaze provided by the invention, it is former to pass through mineral for color material under the furnace transmutation glaze
Material, inorganic color and water match, due in color material under furnace transmutation glaze containing there are many pigmentation element, by the temperature of kiln when firing
Degree changes, oxidized or reduction, and color material generates reaction under furnace transmutation glaze, and colorful transmutation effect is formed under transparent glaze layer,
Seem very unique and marvellous using color material decoration porcelain under this kind of furnace transmutation glaze；In addition, the firing of this kind of transmutation under-glaze decoration ceramic
It only needs to be burnt into twice by biscuiting and glaze firing, firing temperature is low, is conducive to environmental protection and energy-saving and emission-reduction；Under this kind of furnace transmutation glaze
Color ceramic provides a kind of completely new ceramic kind, to pushing the development of ceramic product with positive meaning and with actively
Economic benefit.
Specific implementation mode
Below by way of specific implementation mode, the invention will be further described.
Color material under furnace transmutation glaze, which is characterized in that color material includes raw mineral materials and water, wherein raw mineral materials under the furnace transmutation glaze
Component it is as follows：32-40 parts of feldspar, 25-32 parts of quartz, 8-10 parts of kaolin, 8-16 parts of titanium dioxide, di-iron trioxide 6-15
Part, 3-5 parts of inorganic color, and the ratio of raw mineral materials and water are 3-4:1.
A kind of manufacture craft of transmutation under-glaze decoration ceramic is as follows using color material under above-mentioned furnace transmutation glaze：
Step 1, ceramic body is prepared；
Step 2, it according to the material component of color material under furnace transmutation glaze, configures, prepare color material under furnace transmutation glaze, first according to furnace transmutation glaze
The raw mineral materials component of lower color material is weighed mixing, then water for ball milling will be added in the raw mineral materials of configuration, finally ball milling
300 mesh or less are crossed afterwards to sieve, and are prepared into Freehandhand-drawing colorant under furnace transmutation glaze；
Step 3, ceramic body made from step 1 is put into biscuiting in kiln, obtains biscuit；
Step 4, color material under furnace transmutation glaze made from step 2 is plotted on biscuit of ceramics；
Step 5, clear frit is applied on biscuit of ceramics；
Step 6, the biscuit of ceramics after glazing is put into kiln and is formed by a firing, firing temperature is 1250 ± 50 DEG C.
Specific embodiment one：
Color material under furnace transmutation glaze, color material includes raw mineral materials and water under the furnace transmutation glaze, and the component of wherein raw mineral materials is as follows：
36 parts of feldspar, 30 parts of quartz, 8 parts of kaolin, 9 parts of titanium dioxide, 14 parts of di-iron trioxide, 3 parts of inorganic color, and raw mineral materials
Ratio with water is 3.5:1, wherein inorganic color is red, yellow and green, and the ratio of the red, yellow and green is 1:1：1.
A kind of manufacture craft of transmutation under-glaze decoration ceramic, using color material under the furnace transmutation glaze described in above-mentioned any one, specifically
Steps are as follows：
Step 1, ceramic body is prepared, ceramic body is ecru；
Step 2, it according to the material component of color material under furnace transmutation glaze, configures, prepare color material under furnace transmutation glaze, first according to furnace transmutation glaze
The raw mineral materials component of lower color material is weighed mixing, then water for ball milling will be added in the raw mineral materials of configuration, finally ball milling
Sieving is prepared into Freehandhand-drawing colorant under furnace transmutation glaze afterwards；
Step 3, ceramic body made from step 1 is put into biscuiting in kiln, obtains biscuit；
Step 4, color material under furnace transmutation glaze made from step 2 is plotted in biscuit of ceramics part by writing brush；
Step 5, clear frit is applied on biscuit of ceramics, the thickness of clear frit is 0.55mm；
Step 6, the biscuit of ceramics after glazing is put into kiln and is formed by a firing, firing control is divided into five sections of controls, respectively
For：
Low-temperature zone, kiln pass through 2.5 hours, and 600 DEG C are warming up to by 250 DEG C；
Middle-temperature section, kiln pass through 1.3 hours, and 1000 DEG C are warming up to by 600 DEG C；
Become temperature section, kiln is cooled to 800 DEG C through 0.8 hour, by 1000 DEG C；
High temperature section, kiln pass through 2.1 hours, are warming up to 1255 DEG C by 1000 DEG C, and keep the temperature 1 hour at 1265 DEG C；
Slow cooling section, kiln are cooled to 200 DEG C through 2.5 hours, by firing temperature, open kiln natural cooling, dropped by 200 DEG C
Temperature is to 20 degrees Celsius.
This kind of transmutation under-glaze decoration ceramic has smooth, bright glazed surface, and under clear frit, transmutation color material forms colorful
Transmutation effect staggeredly.
Specific embodiment two：
Color material under furnace transmutation glaze, color material includes raw mineral materials and water under the furnace transmutation glaze, and the component of wherein raw mineral materials is as follows：
The component for stating color material under furnace transmutation glaze is as follows：33 parts of feldspar, 31 parts of quartz, 10 parts of kaolin, 10 parts of titanium dioxide, di-iron trioxide
11 parts, 5 parts of inorganic color, and the ratio of raw mineral materials and water is 3.8:1, wherein inorganic color is copper red color colorant.
A kind of manufacture craft of transmutation under-glaze decoration ceramic, using color material under the furnace transmutation glaze described in above-mentioned any one, specifically
Steps are as follows：
Step 1, ceramic body is prepared, ceramic body is white；
Step 2, it according to the material component of color material under furnace transmutation glaze, configures, prepare color material under furnace transmutation glaze, first according to furnace transmutation glaze
The raw mineral materials component of lower color material is weighed mixing, then water for ball milling will be added in the raw mineral materials of configuration, finally ball milling
Sieving is prepared into Freehandhand-drawing colorant under furnace transmutation glaze afterwards；
Step 3, ceramic body made from step 1 is put into biscuiting in kiln, obtains biscuit；
Step 4, color material under furnace transmutation glaze made from step 2 is plotted in block-like on biscuit of ceramics using brush；
Step 5, clear frit is applied on biscuit of ceramics, the thickness of clear frit is 0.7mm；
Step 6, the biscuit of ceramics after glazing is put into kiln and is formed by a firing, firing control is divided into five sections of controls, respectively
For：
Low-temperature zone, kiln pass through 2.8 hours, and 600 DEG C are warming up to by 250 DEG C；
Middle-temperature section, kiln pass through 1.8 hours, and 1000 DEG C are warming up to by 600 DEG C；
Become temperature section, kiln is cooled to 800 DEG C through 0.6 hour, by 1000 DEG C；
High temperature section, kiln pass through 2.6 hours, are warming up to 1277 DEG C by 1000 DEG C, and keep the temperature 1 hour at 1265 DEG C；
Slow cooling section, kiln are cooled to 200 DEG C through 3 hours, by firing temperature, open kiln natural cooling, cooled down by 200 DEG C
To 20 degrees Celsius.
This kind of transmutation under-glaze decoration ceramic has smooth, bright glazed surface, and under clear frit, transmutation color material forms gradual change
Copper red color effect.
Specific embodiment three：
Color material under furnace transmutation glaze, color material includes raw mineral materials and water under the furnace transmutation glaze, and the component of wherein raw mineral materials is as follows：
38 parts of feldspar, 26 parts of quartz, 9 parts of kaolin, 15 parts of titanium dioxide, 8 parts of di-iron trioxide, 4 parts of inorganic color, and raw mineral materials
Ratio with water is 3.2:1, wherein its inorganic color is black, golden colorant, and the wherein ratio of black pigment and golden colorant is 7:
1。
A kind of manufacture craft of transmutation under-glaze decoration ceramic, using color material under the furnace transmutation glaze described in above-mentioned any one, specifically
Steps are as follows：
Step 1, ceramic body is prepared, ceramic body is ivory buff；
Step 2, it according to the material component of color material under furnace transmutation glaze, configures, prepare color material under furnace transmutation glaze, first according to furnace transmutation glaze
The raw mineral materials component of lower color material is weighed mixing, then water for ball milling will be added in the raw mineral materials of configuration, finally ball milling
Sieving is prepared into Freehandhand-drawing colorant under furnace transmutation glaze afterwards；
Step 3, ceramic body made from step 1 is put into biscuiting in kiln, obtains biscuit；
Step 4, color material under furnace transmutation glaze made from step 2 is sprayed on by spray gun on biscuit of ceramics；
Step 5, clear frit is applied on biscuit of ceramics, the thickness of clear frit is 0.6mm；
Step 6, the biscuit of ceramics after glazing is put into kiln and is formed by a firing, firing control is divided into five sections of controls, respectively
For：
Low-temperature zone, kiln pass through 2-3 hours, and 600 DEG C are warming up to by 250 DEG C；
Middle-temperature section, kiln pass through 1-2 hours, and 1000 DEG C are warming up to by 600 DEG C；
Become temperature section, kiln is cooled to 800 DEG C through 0.5-1 hours, by 1000 DEG C；
High temperature section, kiln pass through 2-3 hours, are warming up to 1265 DEG C by 1000 DEG C, and keep the temperature 0.5-1 hours at 1265 DEG C；
Slow cooling section, kiln are cooled to 200 DEG C through 2.5-3 hours, by firing temperature, kiln natural cooling are opened, by 200 DEG C
It is cooled to 20 degrees Celsius.
This kind of transmutation under-glaze decoration ceramic has smooth, bright glazed surface, and under clear frit, transmutation color material has black
Background color, show on black background color golden transmutation speckle, effect is unique.
The specific embodiment of the present invention is above are only, but the design concept of the present invention is not limited thereto, all profits
The change for carrying out unsubstantiality to the present invention with this design, should all belong to the behavior for invading the scope of the present invention.
Claims (10)
1. color material under furnace transmutation glaze, which is characterized in that under the furnace transmutation glaze color material includes raw mineral materials and water, wherein raw mineral materials
Component is as follows：32-40 parts of feldspar, 25-32 parts of quartz, 8-10 parts of kaolin, 8-16 parts of titanium dioxide, di-iron trioxide 6-15
Part, 3-5 parts of inorganic color, and the ratio of raw mineral materials and water are 3-4:1.
2. color material under furnace transmutation glaze according to claim 1, which is characterized in that the component of color material is as follows under the furnace transmutation glaze：
36 parts of feldspar, 30 parts of quartz, 8 parts of kaolin, 9 parts of titanium dioxide, 14 parts of di-iron trioxide, 3 parts of inorganic color, and raw mineral materials
Ratio with water is 3.5:1.
3. color material under furnace transmutation glaze according to claim 1, which is characterized in that the component of color material is as follows under the furnace transmutation glaze：
33 parts of feldspar, 31 parts of quartz, 10 parts of kaolin, 10 parts of titanium dioxide, 11 parts of di-iron trioxide, 5 parts of inorganic color, and mineral are former
The ratio of material and water is 3.8:1.
4. color material under furnace transmutation glaze according to claim 1, which is characterized in that the component of color material is as follows under the furnace transmutation glaze：
38 parts of feldspar, 26 parts of quartz, 9 parts of kaolin, 15 parts of titanium dioxide, 8 parts of di-iron trioxide, 4 parts of inorganic color, and raw mineral materials
Ratio with water is 3.2:1.
5. a kind of manufacture craft of transmutation under-glaze decoration ceramic, using color material under the furnace transmutation glaze described in claim 1-4 any one,
It is as follows：
Step 1, ceramic body is prepared；
Step 2, it according to the material component of color material under furnace transmutation glaze, configures, prepare color material under furnace transmutation glaze；
Step 3, ceramic body made from step 1 is put into biscuiting in kiln, obtains biscuit；
Step 4, color material under furnace transmutation glaze made from step 2 is plotted on biscuit of ceramics；
Step 5, clear frit is applied on biscuit of ceramics；
Step 6, the biscuit of ceramics after glazing is put into kiln and is formed by a firing, firing temperature is 1250 ± 50 DEG C.
6. the manufacture craft of transmutation under-glaze decoration ceramic according to claim 5, which is characterized in that the ceramic body is shallow
Colour system.
7. the manufacture craft of transmutation under-glaze decoration ceramic according to claim 5, which is characterized in that in the step 2, transmutation
The preparation of underglaze colour material is as follows：
S1 weighs mixing according to the raw mineral materials component of color material under furnace transmutation glaze；
S2 will add water for ball milling in raw mineral materials that step 1 configures；
S3, after ball milling sieving be prepared into Freehandhand-drawing colorant under furnace transmutation glaze.
8. the manufacture craft of transmutation under-glaze decoration ceramic according to claim 5, which is characterized in that transparent in the step 5
The thickness of glaze is 0.5-8mm.
9. the manufacture craft of transmutation under-glaze decoration ceramic according to claim 5, which is characterized in that be burnt into the step 6
Control is divided into five sections of controls, respectively：
Low-temperature zone, kiln pass through 2-3 hours, and 600 DEG C are warming up to by 250 DEG C；
Middle-temperature section, kiln pass through 1-2 hours, and 1000 DEG C are warming up to by 600 DEG C；
Become temperature section, kiln is cooled to 800 DEG C through 0.5-1 hours, by 1000 DEG C；
High temperature section, kiln pass through 2-3 hours, are warming up to firing temperature by 1000 DEG C, and keep the temperature 0.5-1 hours in firing temperature；
Slow cooling section, kiln are cooled to 200 DEG C through 2.5-3 hours, by firing temperature, open kiln natural cooling, cooled down by 200 DEG C
To 20 degrees Celsius.
10. the manufacture craft of the transmutation under-glaze decoration ceramic according to claim 5 or 8, which is characterized in that the step firing
Temperature is 1265 DEG C.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711031388 | 2017-10-30 | ||
| CN2017110313881 | 2017-10-30 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108706879A true CN108706879A (en) | 2018-10-26 |
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| CN109879596A (en) * | 2019-04-23 | 2019-06-14 | 福建省德化云水窑陶瓷有限公司 | Furnace transmutation glaze colorant and the method for preparing furnace transmutation glaze ceramic under glaze with it under glaze |
| CN110066178A (en) * | 2019-04-12 | 2019-07-30 | 佛山市乐陶工艺陶瓷有限公司 | The manufacture craft of transmutation background ceramic board pictures |
| CN110407469A (en) * | 2019-08-26 | 2019-11-05 | 福建省德化县天俊陶瓷有限公司 | A kind of transparent glase fired at lower temperature, ceramic and preparation method with the glaze |
| CN111454079A (en) * | 2020-04-09 | 2020-07-28 | 广东皓明陶瓷科技有限公司 | Method for forming black substrate golden wafer ceramic product in glaze firing process |
| CN111548012A (en) * | 2020-05-20 | 2020-08-18 | 福建省德化县瓷言坊陶瓷工艺有限公司 | Low-temperature environment-friendly shallow brown white furnace transmutation glazed porcelain and preparation process thereof |
| CN112759355A (en) * | 2019-11-01 | 2021-05-07 | 江苏新嘉理生态环境材料股份有限公司 | Argil plate with reduction and oxidation sintering combined transmutation effect and preparation method and application thereof |
| CN114656289A (en) * | 2022-04-19 | 2022-06-24 | 德化县厚德陶瓷厂 | Under-glaze transmutation glaze ceramic with rust-controllable lines and preparation method thereof |
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| CN109879596B (en) * | 2019-04-23 | 2021-07-20 | 福建省德化云水窑陶瓷有限公司 | Underglaze transmutation glaze pigment and method for preparing underglaze transmutation glaze ceramic product by using same |
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| CN112759355A (en) * | 2019-11-01 | 2021-05-07 | 江苏新嘉理生态环境材料股份有限公司 | Argil plate with reduction and oxidation sintering combined transmutation effect and preparation method and application thereof |
| CN111454079A (en) * | 2020-04-09 | 2020-07-28 | 广东皓明陶瓷科技有限公司 | Method for forming black substrate golden wafer ceramic product in glaze firing process |
| CN111548012A (en) * | 2020-05-20 | 2020-08-18 | 福建省德化县瓷言坊陶瓷工艺有限公司 | Low-temperature environment-friendly shallow brown white furnace transmutation glazed porcelain and preparation process thereof |
| CN114656289A (en) * | 2022-04-19 | 2022-06-24 | 德化县厚德陶瓷厂 | Under-glaze transmutation glaze ceramic with rust-controllable lines and preparation method thereof |
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