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CN108690731A - The resistance to migration candle colorant of one kind and preparation method - Google Patents

The resistance to migration candle colorant of one kind and preparation method Download PDF

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Publication number
CN108690731A
CN108690731A CN201810637488.7A CN201810637488A CN108690731A CN 108690731 A CN108690731 A CN 108690731A CN 201810637488 A CN201810637488 A CN 201810637488A CN 108690731 A CN108690731 A CN 108690731A
Authority
CN
China
Prior art keywords
parts
candle
antioxidant
colorant
migration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810637488.7A
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Chinese (zh)
Inventor
林海松
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fujian Suobang Chemical Co Ltd
Original Assignee
Fujian Suobang Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fujian Suobang Chemical Co Ltd filed Critical Fujian Suobang Chemical Co Ltd
Priority to CN201810637488.7A priority Critical patent/CN108690731A/en
Publication of CN108690731A publication Critical patent/CN108690731A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C5/00Candles
    • C11C5/002Ingredients
    • C11C5/004Ingredients dyes, pigments; products giving a coloured flame
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C5/00Candles
    • C11C5/002Ingredients

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  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

A kind of resistance to migration candle colorant, is made of following components in parts by weight:10 ~ 20 parts of stearic acid, 60 ~ 80 parts of paraffin, 2 ~ 10 parts of beeswax, 5 ~ 20 parts of cottonseed oil, 0.2 ~ 1 part of pigment, 0.2 ~ 1 part of essence, 10 ~ 30 parts of color fixing agent, 10 ~ 30 parts of antioxidant, 5 ~ 20 parts of oil antioxidant;Color fixing agent and antioxidant, oil antioxidant is added in traditional candle formula in the present invention, and 120 °C of maintaining reaction temperature, the repertoire of candle can fully react at this temperature, wax body is put into reheating in reaction kettle simultaneously, each constituent is set more fully to merge, color fixing agent and antioxidant, oil antioxidant can increase the resistance to migration of candle colorant, and color is prevented to be lost in.

Description

The resistance to migration candle colorant of one kind and preparation method
Technical field
The present invention relates to candle fields, more particularly to a kind of resistance to migration candle colorant and preparation method.
Background technology
When candle combustion, what is first lighted is the candle wick of candle, and when about 60 DEG C of the temperature of flame, the wax of solid will melt It is melted into liquid;Under candle flame, the wax of liquid is stored, the wax of liquid can climb up to come along match suede, then fiery Heating becomes gas;Candle colorant is readily migrate on packaging product or other contact surface substances and body color are degenerated or become It is shallow, cause the original color of product to be lost in, is unfavorable for the beauty and the new gorgeous degree of color of product itself, to influence sale circulation.
Invention content
In order to solve the above technical problems, first purpose of the present invention is to provide a kind of resistance lighted candle colorant and preparation side Method;Resistance to migration candle colorant provided by the invention and preparation method can make candle combustion time and the more stable property of combustion efficiency.
Technical solution provided by the invention is as follows:
A kind of resistance to migration candle colorant, is made of following components in parts by weight:10 ~ 20 parts of stearic acid, 60 ~ 80 parts of paraffin, beeswax 2 ~ 10 parts, 5 ~ 20 parts of cottonseed oil, 0.2 ~ 1 part of pigment, 0.2 ~ 1 part of essence, 10 ~ 30 parts of color fixing agent, 10 ~ 30 parts of antioxidant, grease 5 ~ 20 parts of antioxidant;
Further, it is made of following components in parts by weight:10 ~ 15 parts of stearic acid, 65 ~ 75 parts of paraffin, 2 ~ 8 parts of beeswax, cottonseed 10 ~ 15 parts of oil, 0.5 ~ 1 part of pigment, 0.2 ~ 0.8 part of essence, 16 ~ 25 parts of color fixing agent, 15 ~ 25 parts of antioxidant, lipid-antioxidant activity 10 ~ 18 parts of agent;
Further, it is made of following components in parts by weight:13 parts of stearic acid, 70 parts of paraffin, 6 parts of beeswax, 11 parts of cottonseed oil, face 0.8 part of material, 0.6 part of essence, 22 parts of color fixing agent, 18 parts of antioxidant, 10 parts of oil antioxidant;
Further, the color fixing agent be dicyandiamide-methanol condensation polymer, diallyl dimethyl ammoniumchloride one kind or more Kind;
Further, the antioxidant be liquid soybean lecithin, microcapsules lecithin it is one or more;
Further, the oil antioxidant be rosemary, tea polyphenols it is one or more;
A kind of preparation method of resistance to migration candle colorant, which is characterized in that include the following steps:
(1)Stearic acid, paraffin, beeswax, cottonseed oil, pigment, essence are put into reaction kettle and are heated to 120 °C, quickly stirring 6min maintains 120 °C of temperature and continues to stir, color fixing agent, antioxidant, oil antioxidant is added, and continues quickly stirring 6min obtains wax liquor;
(2)By step(1)Wax liquor be cooled to 60 °C ~ 80 °C after with tablet press machine carry out tabletting, obtain the wax body of sheet;
(3)By step(2)Wax body pour into reaction kettle and continue to heat, heating temperature is 120 °C, and after heating 8min, wax body is melted Chemical conversion is wax liquor;
(4)By step(3)Wax liquor pour into injection molding machine, be extruded as strip through injection molding machine, be put into pallet, natural cooling, i.e., At.
Further, the quick mixing speed of the reaction kettle is 800 revs/min.
Color fixing agent and antioxidant, oil antioxidant is added in traditional candle formula in the present invention, and maintains to react 120 °C of temperature, the repertoire of candle can fully react at this temperature, while wax body is put into secondary in reaction kettle Heating, makes each constituent more fully merge, color fixing agent and antioxidant, oil antioxidant can increase the resistance to of candle colorant and move Shifting property, prevents color to be lost in.
Specific implementation mode
Embodiment 1
A kind of resistance to migration candle colorant, is made of following components in parts by weight:10 parts of stearic acid, 75 parts of paraffin, 5 parts of beeswax, cotton 13 parts of seed oil, 0.2 part of pigment, 0.5 part of essence, 10 parts of color fixing agent, 15 parts of antioxidant, 5 parts of oil antioxidant.
A kind of preparation method of resistance to migration candle colorant, includes the following steps:
(1)Stearic acid, paraffin, beeswax, cottonseed oil, pigment, essence are put into reaction kettle and are heated to 120 °C, quickly stirring 6min maintains 120 °C of temperature and continues to stir, color fixing agent, antioxidant, oil antioxidant is added, and continues quickly stirring 6min obtains wax liquor, and the quick mixing speed of reaction kettle is 800 revs/min;
(2)By step(1)Wax liquor be cooled to 60 °C after with tablet press machine carry out tabletting, obtain the wax body of sheet;
(3)By step(2)Wax body pour into reaction kettle and continue to heat, heating temperature is 120 °C, and after heating 8min, wax body is melted Chemical conversion is wax liquor;
(4)By step(3)Wax liquor pour into injection molding machine, be extruded as strip through injection molding machine, be put into pallet, natural cooling, i.e., At.
Embodiment 2
A kind of resistance to migration candle colorant, is made of following components in parts by weight:13 parts of stearic acid, 60 parts of paraffin, 10 parts of beeswax, cotton 9 parts of seed oil, 01 part of pigment, 0.2 part of essence, 30 parts of color fixing agent, 25 parts of antioxidant, 20 parts of oil antioxidant.
A kind of preparation method of resistance to migration candle colorant, includes the following steps:
(1)Stearic acid, paraffin, beeswax, cottonseed oil, pigment, essence are put into reaction kettle and are heated to 120 °C, quickly stirring 6min maintains 120 °C of temperature and continues to stir, color fixing agent, antioxidant, oil antioxidant is added, and continues quickly stirring 6min obtains wax liquor, and the quick mixing speed of reaction kettle is 800 revs/min;
(2)By step(1)Wax liquor be cooled to 70 °C after with tablet press machine carry out tabletting, obtain the wax body of sheet;
(3)By step(2)Wax body pour into reaction kettle and continue to heat, heating temperature is 120 °C, and after heating 8min, wax body is melted Chemical conversion is wax liquor;
(4)By step(3)Wax liquor pour into injection molding machine, be extruded as strip through injection molding machine, be put into pallet, natural cooling, i.e., At.
Embodiment 3
A kind of resistance to migration candle colorant, is made of following components in parts by weight:15 parts of stearic acid, 65 parts of paraffin, 2 parts of beeswax, cotton 5 parts of seed oil, 0.7 part of pigment, 1 part of essence, 25 parts of color fixing agent, 10 parts of antioxidant, 8 parts of oil antioxidant.
A kind of preparation method of resistance to migration candle colorant, includes the following steps:
(1)Stearic acid, paraffin, beeswax, cottonseed oil, pigment, essence are put into reaction kettle and are heated to 120 °C, quickly stirring 6min maintains 120 °C of temperature and continues to stir, color fixing agent, antioxidant, oil antioxidant is added, and continues quickly stirring 6min obtains wax liquor, and the quick mixing speed of reaction kettle is 800 revs/min;
(2)By step(1)Wax liquor be cooled to 80 °C after with tablet press machine carry out tabletting, obtain the wax body of sheet;
(3)By step(2)Wax body pour into reaction kettle and continue to heat, heating temperature is 120 °C, and after heating 8min, wax body is melted Chemical conversion is wax liquor;
(4)By step(3)Wax liquor pour into injection molding machine, be extruded as strip through injection molding machine, be put into pallet, natural cooling, i.e., At.
Embodiment 4
A kind of resistance to migration candle colorant, is made of following components in parts by weight:20 parts of stearic acid, 80 parts of paraffin, 8 parts of beeswax, cotton 20 parts of seed oil, 0.5 part of pigment, 0.8 part of essence, 16 parts of color fixing agent, 30 parts of antioxidant, 16 parts of oil antioxidant.
A kind of preparation method of resistance to migration candle colorant, includes the following steps:
(1)Stearic acid, paraffin, beeswax, cottonseed oil, pigment, essence are put into reaction kettle and are heated to 120 °C, quickly stirring 6min maintains 120 °C of temperature and continues to stir, color fixing agent, antioxidant, oil antioxidant is added, and continues quickly stirring 6min obtains wax liquor, and the quick mixing speed of reaction kettle is 800 revs/min;
(2)By step(1)Wax liquor be cooled to 70 °C after with tablet press machine carry out tabletting, obtain the wax body of sheet;
(3)By step(2)Wax body pour into reaction kettle and continue to heat, heating temperature is 120 °C, and after heating 8min, wax body is melted Chemical conversion is wax liquor;
(4)By step(3)Wax liquor pour into injection molding machine, be extruded as strip through injection molding machine, be put into pallet, natural cooling, i.e., At.
Embodiment 5
A kind of resistance to migration candle colorant, is made of following components in parts by weight:13 parts of stearic acid, 70 parts of paraffin, 6 parts of beeswax, cotton 11 parts of seed oil, 0.8 part of pigment, 0.6 part of essence, 22 parts of color fixing agent, 18 parts of antioxidant, 10 parts of oil antioxidant.
A kind of preparation method of resistance to migration candle colorant, includes the following steps:
(1)Stearic acid, paraffin, beeswax, cottonseed oil, pigment, essence are put into reaction kettle and are heated to 120 °C, quickly stirring 6min maintains 120 °C of temperature and continues to stir, color fixing agent, antioxidant, oil antioxidant is added, and continues quickly stirring 6min obtains wax liquor, and the quick mixing speed of reaction kettle is 800 revs/min;
(2)By step(1)Wax liquor be cooled to 65 °C after with tablet press machine carry out tabletting, obtain the wax body of sheet;
(3)By step(2)Wax body pour into reaction kettle and continue to heat, heating temperature is 120 °C, and after heating 8min, wax body is melted Chemical conversion is wax liquor;
(4)By step(3)Wax liquor pour into injection molding machine, be extruded as strip through injection molding machine, be put into pallet, natural cooling, i.e., At.
Comparative example
A kind of resistance to migration candle colorant, is made of following components in parts by weight:13 parts of stearic acid, 70 parts of paraffin, 6 parts of beeswax, cotton 11 parts of seed oil, 0.8 part of pigment, 0.6 part of essence.
A kind of preparation method of resistance to migration candle colorant, includes the following steps:
(1) stearic acid, paraffin, beeswax, cottonseed oil, pigment, essence are put into reaction kettle and are heated to 120 °C, quickly stirring 6min maintains 120 °C of temperature and continues to stir 6min, obtains wax liquor, the quick mixing speed of reaction kettle is 800 revs/min;
(2) by step(1)Wax liquor be cooled to 65 °C after with tablet press machine carry out tabletting, obtain the wax body of sheet;
(3) by step(2)Wax body pour into reaction kettle and continue to heat, heating temperature is 120 °C, and after heating 8min, wax body is melted Chemical conversion is wax liquor;
(4) by step(3)Wax liquor pour into injection molding machine, be extruded as strip through injection molding machine, be put into pallet, natural cooling, i.e., At.
The candle colorant of embodiment 1-5 and comparative example is fabricated to candle with same process, candle is in natural lighting Under the conditions of, showing whether color changes through naked eyes viewing after storage after a period of time, experimental result is as shown in table 1 below, The candle of the resistance to migration colorant of the present invention is non-discolouring.
Embodiment Experimental period Discoloration Condition
Embodiment 1 18 months It is non-discolouring Natural lighting
Embodiment 2 18 months It is non-discolouring Natural lighting
Embodiment 3 18 months It is non-discolouring Natural lighting
Embodiment 4 18 months It is non-discolouring Natural lighting
Embodiment 5 18 months It is non-discolouring Natural lighting
Comparative example 18 months Color change Natural lighting
Table 1

Claims (8)

1. a kind of resistance to migration candle colorant, which is characterized in that be made of following components in parts by weight:10 ~ 20 parts of stearic acid, paraffin 60 ~ 80 parts, 2 ~ 10 parts of beeswax, 5 ~ 20 parts of cottonseed oil, 0.2 ~ 1 part of pigment, 0.2 ~ 1 part of essence, 10 ~ 30 parts of color fixing agent is anti-oxidant 10 ~ 30 parts of agent, 5 ~ 20 parts of oil antioxidant.
2. the resistance to migration candle colorant of one kind according to claim 1, which is characterized in that by following components in parts by weight group At:10 ~ 15 parts of stearic acid, 65 ~ 75 parts of paraffin, 2 ~ 8 parts of beeswax, 10 ~ 15 parts of cottonseed oil, 0.5 ~ 1 part of pigment, essence 0.2 ~ 0.8 Part, 16 ~ 25 parts of color fixing agent, 15 ~ 25 parts of antioxidant, 10 ~ 18 parts of oil antioxidant.
3. the resistance to migration candle colorant of one kind according to claim 1, which is characterized in that by following components in parts by weight group At:13 parts of stearic acid, 70 parts of paraffin, 6 parts of beeswax, 11 parts of cottonseed oil, 0.8 part of pigment, 0.6 part of essence, 22 parts of color fixing agent, antioxygen 18 parts of agent, 10 parts of oil antioxidant.
4. according to any resistance to migration candle colorant of one kind of claim 1 ~ 3, which is characterized in that the color fixing agent is double cyanogen Amine-methanol condensation polymer, diallyl dimethyl ammoniumchloride it is one or more.
5. according to any resistance to migration candle colorant of one kind of claim 1 ~ 3, which is characterized in that the antioxidant is liquid State soybean lecithin, microcapsules lecithin it is one or more.
6. according to any resistance to migration candle colorant of one kind of claim 1 ~ 3, which is characterized in that the oil antioxidant For rosemary, tea polyphenols it is one or more.
7. a kind of preparation method of resistance to migration candle colorant, which is characterized in that include the following steps:
Stearic acid, paraffin, beeswax, cottonseed oil, pigment, essence are put into reaction kettle and are heated to 120 °C, quickly stirs 6min, It maintains 120 °C of temperature and continues to stir, color fixing agent, antioxidant, oil antioxidant is added, continue quickly stirring 6min, Obtain wax liquor;
By step(1)Wax liquor be cooled to 60 °C ~ 80 °C after with tablet press machine carry out tabletting, obtain the wax body of sheet;
By step(2)Wax body pour into reaction kettle and continue to heat, heating temperature is 120 °C, and after heating 8min, wax body is melted into For wax liquor;
By step(3)Wax liquor pour into injection molding machine, be extruded as strip through injection molding machine, be put into pallet, natural cooling,.
8. a kind of preparation method of resistance to migration candle colorant according to claim 7, which is characterized in that the reaction kettle Quick mixing speed is 800 revs/min.
CN201810637488.7A 2018-06-20 2018-06-20 The resistance to migration candle colorant of one kind and preparation method Pending CN108690731A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810637488.7A CN108690731A (en) 2018-06-20 2018-06-20 The resistance to migration candle colorant of one kind and preparation method

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Application Number Priority Date Filing Date Title
CN201810637488.7A CN108690731A (en) 2018-06-20 2018-06-20 The resistance to migration candle colorant of one kind and preparation method

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CN108690731A true CN108690731A (en) 2018-10-23

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110923071A (en) * 2019-12-25 2020-03-27 石家庄市藁城区燃亮烛业有限公司 Fragrant candle and preparation method thereof
CN114591786A (en) * 2022-02-15 2022-06-07 林莹莹 High-color-fastness candle pigment and preparation method thereof
WO2023192493A1 (en) * 2022-03-30 2023-10-05 Cargill, Incorporated Candle wax compositions

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1343246A (en) * 1999-03-11 2002-04-03 雷克特本克斯尔(英国)有限公司 Candle composition
CN1688681A (en) * 2002-08-13 2005-10-26 贝尔美公司 Protection of fragrance in a wax candle using an antioxidant
CN101050400A (en) * 2007-05-21 2007-10-10 申雨林 Wax candle with color flame
CN105008506A (en) * 2013-02-17 2015-10-28 埃莱万斯可再生能源科学股份有限公司 Wax compositions and the effect of metals on burn rates
CN106867313A (en) * 2017-03-29 2017-06-20 南宁市青秀区嘉利林化有限公司 A kind of fixation rosin ink
CN107674766A (en) * 2017-09-28 2018-02-09 山东巧妻食品科技有限公司 It is a kind of using cottonseed oil as edible birthday candle of primary raw material and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1343246A (en) * 1999-03-11 2002-04-03 雷克特本克斯尔(英国)有限公司 Candle composition
CN1688681A (en) * 2002-08-13 2005-10-26 贝尔美公司 Protection of fragrance in a wax candle using an antioxidant
CN101050400A (en) * 2007-05-21 2007-10-10 申雨林 Wax candle with color flame
CN105008506A (en) * 2013-02-17 2015-10-28 埃莱万斯可再生能源科学股份有限公司 Wax compositions and the effect of metals on burn rates
CN106867313A (en) * 2017-03-29 2017-06-20 南宁市青秀区嘉利林化有限公司 A kind of fixation rosin ink
CN107674766A (en) * 2017-09-28 2018-02-09 山东巧妻食品科技有限公司 It is a kind of using cottonseed oil as edible birthday candle of primary raw material and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110923071A (en) * 2019-12-25 2020-03-27 石家庄市藁城区燃亮烛业有限公司 Fragrant candle and preparation method thereof
CN114591786A (en) * 2022-02-15 2022-06-07 林莹莹 High-color-fastness candle pigment and preparation method thereof
WO2023192493A1 (en) * 2022-03-30 2023-10-05 Cargill, Incorporated Candle wax compositions

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Application publication date: 20181023

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