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CN108580547A - A kind of isometric helix milling method of large-scale titanium alloy ultra fine grained steel bar - Google Patents

A kind of isometric helix milling method of large-scale titanium alloy ultra fine grained steel bar Download PDF

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CN108580547A
CN108580547A CN201810172305.9A CN201810172305A CN108580547A CN 108580547 A CN108580547 A CN 108580547A CN 201810172305 A CN201810172305 A CN 201810172305A CN 108580547 A CN108580547 A CN 108580547A
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titanium alloy
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roll
alloy blank
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CN108580547B (en
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庞玉华
罗远
林鹏程
康荻娜
何威威
陈益哲
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Anhui Dongyun Intelligent Equipment Manufacturing Co ltd
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Xian University of Architecture and Technology
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B1/00Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
    • B21B1/16Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling wire rods, bars, merchant bars, rounds wire or material of like small cross-section
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B27/00Rolls, roll alloys or roll fabrication; Lubricating, cooling or heating rolls while in use
    • B21B27/02Shape or construction of rolls
    • B21B27/024Rolls for bars, rods, rounds, tubes, wire or the like
    • B21B27/025Skew rolls
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B27/00Rolls, roll alloys or roll fabrication; Lubricating, cooling or heating rolls while in use
    • B21B27/02Shape or construction of rolls
    • B21B27/028Variable-width rolls
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B3/00Rolling materials of special alloys so far as the composition of the alloy requires or permits special rolling methods or sequences ; Rolling of aluminium, copper, zinc or other non-ferrous metals
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/06Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of rods or wires

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
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  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Metal Rolling (AREA)
  • Forging (AREA)

Abstract

本发明一种大尺寸钛合金超细晶棒材的等距螺旋轧制方法,涉及机械加工技术领域,具体涉及一种大尺寸钛合金超细晶棒材的等距螺旋轧制方法,包括以下步骤:S1:选取直径尺寸D为40‑150mm,长度为300‑5000mm的钛合金坯料;S2:将上述钛合金坯料放置加热炉内加热至840‑1025℃;S3:将加热后的钛合金坯料从加热炉转运至斜轧机导料槽内,转运时间为5‑20s;S4:在斜轧机的导料槽内进行送料,将钛合金坯料送入斜轧机入口和出口之间的变形区,钛合金坯料在变形区内螺旋运动直至变形结束;S5:重复上述S2‑S4步骤,对钛合金坯料进行2‑6次螺旋轧制得到TC18钛合金整体超细晶棒材;本发明的有益效果是:变形区穿深大,可往复进行多道次轧制。连续稳定局部变形,压‑扭复合三维剧烈变形,能够获得理想的晶粒细化效果。

The invention relates to a method for equidistant spiral rolling of large-sized titanium alloy ultra-fine-grained rods, which relates to the technical field of mechanical processing, and in particular to a method for equidistant spiral rolling of large-sized titanium alloy ultra-fine-grained rods, comprising the following Steps: S1: Select a titanium alloy blank with a diameter D of 40-150mm and a length of 300-5000mm; S2: place the above-mentioned titanium alloy blank in a heating furnace and heat it to 840-1025°C; S3: heat the heated titanium alloy blank Transfer from the heating furnace to the guide trough of the skew rolling mill, the transfer time is 5-20s; S4: Feed in the guide trough of the skew rolling mill, and send the titanium alloy billet into the deformation zone between the entrance and exit of the skew rolling mill, titanium The alloy blank moves spirally in the deformation zone until the deformation ends; S5: repeat the above S2-S4 steps, and carry out 2-6 times of spiral rolling on the titanium alloy blank to obtain the TC18 titanium alloy overall ultra-fine-grained rod; the beneficial effect of the present invention is : The deformation zone has a large penetration depth and can be reciprocated for multi-pass rolling. Continuous and stable local deformation, combined with compression-torsion three-dimensional severe deformation, can obtain ideal grain refinement effect.

Description

一种大尺寸钛合金超细晶棒材的等距螺旋轧制方法A method for equidistant spiral rolling of large-size titanium alloy ultra-fine-grained rods

技术领域technical field

本发明涉及机械加工技术领域,具体涉及一种大尺寸钛合金超细晶棒材的等距螺旋轧制方法。The invention relates to the technical field of mechanical processing, in particular to an equidistant spiral rolling method for large-scale titanium alloy ultra-fine-grained rods.

背景技术Background technique

超细晶/纳米晶材料是当前材料科学研究的热点课题之一。与传统的粗晶金属材料相比,超细晶/纳米材料在某些方面显示出更加优异或独特的性能,如具有更高的强度和硬度,更优的疲劳性能和超塑性,更好的耐蚀性、耐磨性以及生物特性等。这些优良特性使得超细晶材料在航空、航天、汽车、海洋、生物等工程领域有着广泛的应用前景,也使人们更加关注超细晶/纳米制备技术的发展。与传统的粗晶金属材料相比,超细晶/纳米材料在某些方面显示出更加优异或独特的性能。从力学性能角度来说,对于纯钛而言,晶粒尺寸由45um细化至0.4um,屈服强度可由354Mpa增加至582Mpa,抗拉强度可由487Mpa增加至645Mpa。对于某些钛合金而言,在晶粒尺寸达到1.2um左右,其室温拉伸可达到1300Mpa以上,相比原坯料的室温拉伸性能提高60%。超细晶材料在疲劳性能的提高上非常显著,其中平均晶粒尺寸为0.25um的超细晶钛与20um的粗晶钛相比,疲劳极限从252Mpa提高至403Mpa,且循环应力由4.211N提升至34.504N。由上可知,大尺寸钛合金超细晶棒材在工业应用领域有非常大的潜质。Ultrafine crystal/nanocrystalline materials are one of the hot topics in current material science research. Compared with traditional coarse-grained metal materials, ultra-fine-grained/nanomaterials show more excellent or unique properties in some aspects, such as higher strength and hardness, better fatigue performance and superplasticity, better Corrosion resistance, wear resistance and biological characteristics, etc. These excellent properties make ultra-fine-grained materials have broad application prospects in engineering fields such as aviation, aerospace, automobiles, marine, and biology, and also make people pay more attention to the development of ultra-fine-grained/nano-prepared technologies. Compared with traditional coarse-grained metal materials, ultrafine-grained/nanomaterials show more excellent or unique properties in some aspects. From the perspective of mechanical properties, for pure titanium, the grain size is refined from 45um to 0.4um, the yield strength can be increased from 354Mpa to 582Mpa, and the tensile strength can be increased from 487Mpa to 645Mpa. For some titanium alloys, when the grain size reaches about 1.2um, its room temperature tensile strength can reach more than 1300Mpa, which is 60% higher than that of the original billet. The improvement of fatigue performance of ultra-fine-grained materials is very significant. Compared with 20um coarse-grained titanium, the fatigue limit of ultra-fine-grained titanium with an average grain size of 0.25um is increased from 252Mpa to 403Mpa, and the cyclic stress is increased from 4.211N to 34.504N. It can be seen from the above that large-sized titanium alloy ultra-fine-grained rods have great potential in industrial applications.

采用塑性变形方式制备纳米级材料时其等效应变通常应大于6,传统塑性加工方法很难做到,应用超大塑性变形方法(Severe Plastic Deformation,SPD )能够实现。现代SPD始于Bridgemen 提出的大压力与剪切变形组合成形方式,迅猛发展始于20世纪70年代中期前苏联和西方国家,Segal发展了等通道转角挤压技术(Equal-Channel AngularPressing,ECAP),标志着SPD研究的显微结构时代的到来。近10余年来,成千上万研究成果公开发表。When using plastic deformation to prepare nano-scale materials, the equivalent strain should usually be greater than 6, which is difficult to achieve with traditional plastic processing methods, but can be achieved by applying Severe Plastic Deformation (SPD). Modern SPD started from the combined forming method of high pressure and shear deformation proposed by Bridgemen, and its rapid development began in the mid-1970s in the former Soviet Union and Western countries. Segal developed the Equal-Channel Angular Pressing technology (Equal-Channel Angular Pressing, ECAP), It marks the arrival of the microstructural era of SPD research. Over the past 10 years, thousands of research results have been published.

2006年后普遍认可的关于SPD定义:使块体产生超大应变但不明显改变块体几何尺寸,呈现大角度晶界的晶粒细化效果的金属成型方法,可以获得晶粒尺寸在微米级(100-1000nm)和纳米级(小于100nm),都可称为纳米SPD(简称nanoSPD)。由于nanoSPD材料具有大量含高密度位错和高内应力的大角度非平衡晶界组织,使得材料表现出不同于传统粗晶材料的力学行为及变形机理。The definition of SPD generally recognized after 2006: a metal forming method that produces super large strains in the block but does not significantly change the geometric size of the block, and presents a grain refinement effect of large-angle grain boundaries, which can obtain grain sizes in the micron level ( 100-1000nm) and nanoscale (less than 100nm), both can be called nano-SPD (nanoSPD for short). Because the nanoSPD material has a large number of large-angle non-equilibrium grain boundary structures containing high-density dislocations and high internal stress, the material exhibits mechanical behavior and deformation mechanism different from traditional coarse-grained materials.

目前现有的加工技术方案:典型的SPD方法有高压扭转(High Pressure Torsion,HPT)、等径转角挤压变形(equal channel angular press-ing,ECAP)、累积叠轧法(Accumulative Roll Bonding,ARB)、扭转挤压(Twist Extrusion,TE)和多向锻造(Multi-Directional Forging,MDF)。Currently available processing technology solutions: Typical SPD methods include High Pressure Torsion (HPT), equal channel angular press-ing (ECAP), and Accumulative Roll Bonding (ARB) ), twist extrusion (Twist Extrusion, TE) and multi-directional forging (Multi-Directional Forging, MDF).

其中,(1)高压扭转变形:将置于支撑槽中的原始样品(块或粉)施加数个GPa的压力,并相对转动上下两砧,使样品发生强烈剪切变形而细化晶粒,高压扭转的特点在于工件为盘状,尺寸较小,直径一般为10-20 mm,厚度为0.2-0.5 mm。Among them, (1) High-pressure torsional deformation: apply a pressure of several GPa to the original sample (block or powder) placed in the support tank, and relatively rotate the upper and lower anvils to cause strong shear deformation of the sample and refine the grains. The characteristic of high-pressure torsion is that the workpiece is disc-shaped and small in size, generally 10-20 mm in diameter and 0.2-0.5 mm in thickness.

(2)等径角挤压变形:通过模具中两个相交一定角度的等截面通道,将材料由一端向另一端挤出,通过弯曲角对材料运动方向的改变使之产生纯剪切变形,可重复进行该成型过程,剪切应变量随变形道次增加。(2) Equal-diameter angular extrusion deformation: Through two equal-section channels intersecting at a certain angle in the mold, the material is extruded from one end to the other end, and the bending angle changes the direction of material movement to produce pure shear deformation. The forming process can be repeated, and the amount of shear strain increases with the deformation pass.

(3)累积叠轧法:将原始板材经表面处理后双层堆垛,加热后轧焊在一起,然后从中间剪开送回表面处理后再进行下次轧焊循环,为保证轧制后板材能够焊在一起,每道次的压下量不得低于50%,但ARB加工过程中需要强烈的剪应力条件,不能使用润滑剂,这对轧辊的服役寿命是不利的。(3) Cumulative stacking rolling method: stack the original plates in double layers after surface treatment, roll and weld them together after heating, then cut them from the middle and send them back to the surface treatment before the next rolling and welding cycle. The plates can be welded together, and the reduction in each pass must not be less than 50%, but the ARB process requires strong shear stress conditions, and lubricants cannot be used, which is detrimental to the service life of the rolls.

(4)扭转挤压:Beygelzime等提出该工艺。此方法也是通过剪切变形细化晶粒的成型技术,将柱状坯料挤压通过扭转模,与HPT类似,存在变形不均匀问题,细化晶粒效果低于ECAP和HPT。(4) Twisting extrusion: Beygelzime et al. proposed this process. This method is also a molding technique for refining grains through shear deformation. The columnar billet is extruded through a torsion die. Similar to HPT, there is a problem of uneven deformation, and the effect of grain refinement is lower than that of ECAP and HPT.

(5)多向锻造:该工艺通过多次正交改变自由锻方向,获得大变形。此类变形的晶粒细化效果要明显低于ECAP和HPT。(5) Multi-directional forging: This process obtains large deformation by changing the free forging direction orthogonally several times. The grain refinement effect of this type of deformation is significantly lower than that of ECAP and HPT.

另一类现有的加工技术方案:衍生方法,基本成型原理同以上方法,衍生了很多SPD成型新技术,这些方法力图简化工具设计,降低能耗,提高成材率,提升工件尺寸,升级自动化程度等,其中,包括:Another type of existing processing technology solution: derivative method, the basic forming principle is the same as the above method, and many new SPD forming technologies have been derived. These methods try to simplify tool design, reduce energy consumption, improve yield, increase workpiece size, and upgrade automation etc., including:

(1)ECAP衍生方法:反复折弯校直(RCS),坯料被放置折弯装置之间,随上模下移,坯料被折弯,变为波浪状;随后用2块平板进行校直,再进行折弯,通过不断重复,在不明显改变坯料尺寸的情况下累积足够的变形,细化材料组织。(1) ECAP derivative method: repeated bending and straightening (RCS), the blank is placed between the bending devices, and as the upper die moves down, the blank is bent and becomes wavy; then two flat plates are used for straightening, Bending is carried out again, and through continuous repetition, sufficient deformation is accumulated without significantly changing the size of the blank to refine the material structure.

(2)循环闭式模锻(CCDF),模具由某个截面腔体的下模和一个在腔体内垂直移动的相同截面的冲头组成。将带有石墨润滑剂的充分润滑的样品放入下模中,加热至一定温度。通过冲头将工件压入下模,取出后,沿同一方向围绕Z轴旋转90°,重新插入下模变形。这样,工件在连续的通道之间围绕Z轴旋转90°。以这种方式,分别经受1,3和5次压缩。(2) Cyclic Closed Die Forging (CCDF), the mold consists of a lower die with a cavity of a certain section and a punch of the same section that moves vertically in the cavity. Put the fully lubricated sample with graphite lubricant into the lower mold and heat it to a certain temperature. The workpiece is pressed into the lower mold by the punch, and after being taken out, it is rotated 90° around the Z axis in the same direction, and reinserted into the lower mold for deformation. In this way, the workpiece is rotated 90° around the Z axis between successive passes. In this way, 1, 3 and 5 compressions were subjected respectively.

(3)往复挤压(CEC),模具由两个模腔、一个压缩带和放置于两模腔内的冲头构成。两模腔截面积相等,在同一条轴线上,通过中间的压缩带连接。在挤压过程中,试样在冲头的作用下,到达压缩带,此时,试样将受到正挤压变形,挤压后的工件在另一个模腔的冲头作用下,发生镦粗变形。然后,另一边冲头将工件按上述过程反向压回,完成一个挤压循环。重复以上过程,直至获得所要的应变为止。(3) Reciprocating extrusion (CEC), the mold consists of two cavities, a compression belt and punches placed in the two cavities. The cross-sectional areas of the two cavities are equal, on the same axis, and connected by the middle compression belt. During the extrusion process, the sample reaches the compression zone under the action of the punch. At this time, the sample will be subjected to positive extrusion deformation, and the extruded workpiece will be upset under the action of the punch of another cavity. out of shape. Then, the punch on the other side presses the workpiece back in reverse according to the above process, completing an extrusion cycle. Repeat the above process until the desired strain is obtained.

(4)板材连续剪切变形,装置利用上模、下模和下辊构成了两个横截面积有少量差异的相互交叉的通道。将板材送入到模腔内,板材在模腔转角处发生强烈的塑形变形,再从模腔另一侧挤出。在送料辊表面加工出凹槽以用于增加摩擦力。由于变形前后材料的横截面积保持不变的特点,可以在同一模具内反复对板材进行多道次的塑形变形。(4) Continuous shear deformation of the plate. The device uses the upper mold, the lower mold and the lower roller to form two intersecting channels with a small difference in cross-sectional area. The sheet is fed into the cavity, and the sheet undergoes strong plastic deformation at the corner of the cavity, and then extrudes from the other side of the cavity. Grooves are machined on the surface of the feed roller for increased friction. Due to the fact that the cross-sectional area of the material remains unchanged before and after deformation, it is possible to repeatedly perform multiple passes of plastic deformation on the plate in the same mold.

(5)椭圆螺旋等通道挤压法(ECEA),坯料在挤压力的作用下,由圆棒料历经镦拔(圆—椭圆变换)、 扭转(椭圆截面扭转)和反向镦拔(椭圆—圆变换)过程变回圆棒料。金属主要在横截面上产生塑性流动,并累积应变。模具形状利用了圆和椭圆形状的特殊性,其型腔不存在尖角区,使金属易于流动。实现了一次工艺过程多种变形模式的组合。(5) Elliptical spiral equal channel extrusion method (ECEA), under the action of extrusion force, the billet undergoes upsetting (circle-ellipse transformation), torsion (elliptical cross-section twisting) and reverse upsetting (elliptical —circle transformation) the process changes back to a round bar. Metals flow plastically primarily in cross-section, and accumulate strain. The shape of the mold utilizes the particularity of the round and elliptical shapes, and there are no sharp corners in the cavity, which makes the metal flow easily. The combination of multiple deformation modes in one process is realized.

(6)连续摩擦角挤压(CFAE),驱动辊旋转并向工件施加压力P抵靠其支撑件。在驱动辊和工件支撑件之间形成第一个挤压通道,第二个通道是固定模具组件中的短槽。片状工件经过一至八次加工,最大等效真实应变可达5.3,片材取向始终保持恒定。(6) Continuous Friction Angular Extrusion (CFAE), the drive roller rotates and applies pressure P to the workpiece against its support. The first extrusion channel is formed between the drive roller and the workpiece support, and the second channel is a short slot in the stationary die assembly. After one to eight processings of the sheet-shaped workpiece, the maximum equivalent true strain can reach 5.3, and the orientation of the sheet remains constant.

一种HPT衍生方法,适用于管的高压扭转(HPTT),管位于刚性盘内,心轴放入管中,用压缩机在其弹性状态下压缩。由于心轴的轴向压缩,其沿径向膨胀,扩张受到管和圆盘的限制,在管中形成很大的静水应力,在管的两侧产生较大的摩擦力。在保持心轴固定的情况下,通过外部扭矩旋转盘实现管的变形。在扭转过程中,变形模式为局部剪切,剪切面法向为管的径向,剪切方向平行于圆周方向。An HPT derivative method for high-pressure torsion (HPTT) of tubes, with the tube inside a rigid disk and a mandrel placed in the tube, compressed in its elastic state with a compressor. Due to the axial compression of the mandrel, it expands in the radial direction, and the expansion is limited by the tube and the disk, forming a large hydrostatic stress in the tube and generating a large friction force on both sides of the tube. While keeping the mandrel fixed, deformation of the tube is achieved by rotating the disk with external torque. During the torsion process, the deformation mode is local shear, the normal direction of the shear plane is the radial direction of the tube, and the shear direction is parallel to the circumferential direction.

一种TE衍生方法,超高扭转(STS),通过局部加热和冷却使该区域比另外两个部分变形抗力低,使扭转应变(TS)区域局部化。在产生TS区的同时,杆沿着纵向轴线移动,因此在整个杆上连续产生超大塑性应变。这种新工艺STS包括相对于杆的其他部分产生局部软区以及区域沿纵向的运动的杆。STS的一个重要特征是杆的横截面尺寸在应变时保持不变。A TE-derived approach, Super High Torsion (STS), localizes the torsional strain (TS) region by localized heating and cooling to make this region less resistant to deformation than the other two parts. Simultaneously with the generation of the TS zone, the rod is moved along the longitudinal axis, thus continuously producing super large plastic strains throughout the rod. This new process, STS, involves a bar that creates a localized soft zone relative to the rest of the bar and the movement of the zone in the longitudinal direction. An important feature of STS is that the cross-sectional dimension of the rod remains constant under strain.

国内外对于钛合金超细晶工艺的专利报道相对较少。中南大学周科朝等人在专利【CN 103014574 A】提及了一种TC18超细晶钛合金的制备方法,其中提及详细的热处理及多道次镦拔的超细晶工艺参数。此工艺采用多向镦拔的方式进行变形,属于传统锻造方法。因单道次变形区范围和穿深较小,为了获得超细晶组织,一般需要8-10道次以上的反复变形。周期长,效率低,并且一般存在明显的变形不均匀现象。There are relatively few patent reports on titanium alloy ultrafine grain technology at home and abroad. In the patent [CN 103014574 A], Zhou Kechao et al. of Central South University mentioned a preparation method of TC18 ultra-fine-grained titanium alloy, which mentioned detailed heat treatment and ultra-fine-grain process parameters for multi-pass upsetting. This process adopts the method of multi-directional upsetting and drawing, which belongs to the traditional forging method. Due to the small range and penetration depth of single-pass deformation, in order to obtain ultra-fine grain structure, more than 8-10 times of repeated deformation are generally required. The cycle is long, the efficiency is low, and there is generally obvious uneven deformation.

上海交通大学王立强等人在专利【CN 103572186 A】中提及了采用等径弯曲通道变形制备超细晶钛基复合材料的方法,此方法本专利背景介绍已提出,虽然可反复进行剧烈塑性变形,但变形后尺寸为10X10 X100mm,难以满足工业级需求。西北工业大学杜随更在专利【CN 1446935 A】中提及了一种超细晶材料的制备方法。此方法主要集中于表面产生超细晶。虽然变形程度高,可反复变形,但只限于制备表面纳米晶,无法做到由心部到表面的整体超细晶。In the patent [CN 103572186 A], Wang Liqiang of Shanghai Jiaotong University and others mentioned a method for preparing ultra-fine-grained titanium-based composite materials by deformation of equal-diameter curved channels. This method has been proposed in the background introduction of this patent, although severe plastic deformation can be repeated. , but the size after deformation is 10X10 X100mm, which is difficult to meet the needs of industrial grade. Du Suigeng of Northwestern Polytechnical University mentioned a method for preparing ultrafine-grained materials in the patent [CN 1446935 A]. This method mainly focuses on producing ultra-fine grains on the surface. Although the degree of deformation is high and can be deformed repeatedly, it is only limited to the preparation of surface nanocrystals, and the overall ultrafine crystals from the center to the surface cannot be achieved.

东北大学刘国怀等人在专利【CN 107030111 A】提及了一种等厚度超细晶TC4钛合金板材的制备方法。此方法与专利背景介绍中的累积叠轧类似,该过程需要强烈的剪应力条件,载荷较大,对其尺寸条件限制较大,只能制备板材,无法制备棒材。从钛合金超细晶工艺的论文报道而言,其大多使用ECAP、HPT的方式对钛合金进行变形,所涉及的制品尺寸较小,难以产生工业级整体超细晶的大尺寸块体材料。The patent [CN 107030111 A] by Liu Guohuai and others from Northeastern University mentioned a preparation method of an ultra-fine-grained TC4 titanium alloy sheet with equal thickness. This method is similar to the cumulative stack rolling in the patent background introduction. This process requires strong shear stress conditions, large loads, and large restrictions on its size conditions. Only plates can be prepared, but bars cannot be prepared. From the paper reports on titanium alloy ultra-fine grain technology, most of them use ECAP and HPT to deform titanium alloy, and the size of the products involved is small, so it is difficult to produce large-size bulk materials with industrial-grade overall ultra-fine grain.

综合分析可知:现有专利或论文中提及的钛合金超细晶工艺,均采用传统HPT、ECAP和ARB等方法在极高的载荷下制备小尺寸的均匀超细晶材料,目前都只限于实验室研制,难以制备工业级整体超细晶的大尺寸材料。A comprehensive analysis shows that the titanium alloy ultra-fine grain technology mentioned in existing patents or papers all use traditional HPT, ECAP and ARB methods to prepare small-sized uniform ultra-fine grain materials under extremely high loads, which are currently limited to Developed in the laboratory, it is difficult to prepare large-scale materials with industrial-grade overall ultra-fine crystals.

发明内容Contents of the invention

本发明目的在于提供一种大尺寸钛合金超细晶棒材的等距螺旋轧制方法,以解决上述背景技术中提出的尺寸受限、载荷大和效率低等问题。The purpose of the present invention is to provide a method for equidistant spiral rolling of large-sized titanium alloy ultra-fine-grained rods, so as to solve the problems of limited size, large load and low efficiency in the above-mentioned background technology.

本发明一种大尺寸钛合金超细晶棒材的等距螺旋轧制方法,其特征在于,包括以下步骤:The present invention is an equidistant spiral rolling method for large-scale titanium alloy ultra-fine-grained rods, which is characterized in that it comprises the following steps:

S1:选取直径尺寸D为40-150mm,长度为300-5000mm的钛合金坯料;S1: Select a titanium alloy blank with a diameter D of 40-150mm and a length of 300-5000mm;

S2:将上述钛合金坯料放置加热炉内加热至840-1025℃,加热时间为:钛合金坯料直径D×(0.6-0.8)min;S2: Place the above titanium alloy billet in a heating furnace and heat it to 840-1025°C. The heating time is: diameter of titanium alloy billet D×(0.6-0.8) min;

S3:将加热后的钛合金坯料从加热炉转运至斜轧机导料槽内,转运时间为5-20s;S3: transfer the heated titanium alloy billet from the heating furnace to the guide groove of the skew rolling mill, and the transfer time is 5-20s;

S4:在斜轧机的导料槽内进行送料,将钛合金坯料送入斜轧机入口和出口之间的变形区,钛合金坯料在变形区内螺旋运动直至变形结束,得到直径为Dm的TC18钛合金棒材,其中m为轧制次数,轧制一次得到的TC18钛合金棒材的直径为D1,轧制两次得到的TC18钛合金棒材的直径为D2,以此类推;S4: Feed in the guide groove of the skew rolling mill, and send the titanium alloy billet into the deformation zone between the entrance and the exit of the skew rolling mill. The titanium alloy billet moves spirally in the deformation zone until the deformation is completed, and the TC18 titanium with a diameter of Dm is obtained Alloy bar, where m is the number of times of rolling, the diameter of the TC18 titanium alloy bar obtained by rolling once is D1, the diameter of the TC18 titanium alloy bar obtained by rolling twice is D2, and so on;

S5:重复上述S2-S4步骤,对钛合金坯料进行2-6次螺旋轧制得到TC18钛合金整体超细晶棒材;S5: Repeating the above steps S2-S4, performing 2-6 times of spiral rolling on the titanium alloy billet to obtain TC18 titanium alloy overall ultra-fine grain bar;

所述斜轧机为二辊斜轧机,所述轧辊均为单锥形轧辊,锥角γ1为17-19度,且轧辊咬入钛合金坯料的圆弧半径r为50-380mm,轧辊送进角α为15-17度,轧辊的辗轧角β为17-19度,两个轧辊之间的轧辊间距Dg为钛合金坯料直径D的86%-94%,轧辊转速n为28-50r/min;The skew rolling mill is a two-roller skew rolling mill, the rolls are all single-tapered rolls, the cone angle γ1 is 17-19 degrees, and the arc radius r of the rolls biting into the titanium alloy billet is 50-380 mm, and the feed angle of the rolls is 50-380 mm. α is 15-17 degrees, the rolling angle β of the rolls is 17-19 degrees, the roll spacing Dg between the two rolls is 86%-94% of the diameter D of the titanium alloy billet, and the roll speed n is 28-50r/min ;

所述钛合金坯料为大尺寸棒材;The titanium alloy blank is a large-size bar;

所述S5步骤中重复轧制过程的加热时间均为TC18钛合金棒材直径Dm×(0.3-0.4)min。The heating time of the repeated rolling process in the step S5 is the diameter of the TC18 titanium alloy rod Dm×(0.3-0.4) min.

优选地,轧辊小端面设置为圆弧面,且圆弧面半径为50-380mm。Preferably, the small end surface of the roll is set as an arc surface, and the radius of the arc surface is 50-380mm.

优选地,孔型椭圆度系数为导板距Dd与辊距Dg之比,S4步骤中钛合金坯料在变形区内采用孔型椭圆度系数为1.2-1.4进行轧制。Preferably, the pass ellipticity coefficient is the ratio of the guide plate distance Dd to the roll distance Dg, and in step S4, the titanium alloy billet is rolled in the deformation zone with a pass ellipticity coefficient of 1.2-1.4.

优选地,在钛合金坯料轧制过程中,两个轧辊之间的辊距Dg固定不变,有利于实现多道次重复轧制。Preferably, during the rolling process of the titanium alloy billet, the roll distance Dg between the two rolls is constant, which is beneficial to realize multi-pass repeated rolling.

优选地,在S5步骤重复轧制过程中,变形区形状保持不变。Preferably, during the repeated rolling process of step S5, the shape of the deformation zone remains unchanged.

本发明与现有技术相比,本发明的有益效果是:The present invention compares with prior art, the beneficial effect of the present invention is:

(1)变形区穿深大,能够获得大尺寸整体超细晶组织。斜轧过程中材料内部的塑性变形由两部分组成,一是轧辊间的压缩变形,此变形为周期性间断变形,另一部分是持续发生的扭转变形。压缩和扭转变形的叠加使斜轧过程中变形区内产生明显区别于常规锻造的三维剧烈塑性变形;(2)斜轧前后棒材直径保持不变可往复进行多道次轧制。斜轧过程存在宽展,钛合金坯料横截面内的等效直径保持不变;(3)连续稳定局部变形,轧制载荷小,变形过程平稳。斜轧过程中工件与钛合金坯料的实际接触面积仅为钛合金坯料表面积的很小一部分,为局部接触变形,因而载荷小;(4)压-扭复合三维剧烈变形,能够获得理想的晶粒细化效果。(1) The penetration depth of the deformation zone is large, and a large-scale overall ultra-fine grain structure can be obtained. The plastic deformation inside the material during the cross rolling process consists of two parts, one is the compression deformation between the rolls, which is a periodic intermittent deformation, and the other is the continuous torsional deformation. The superimposition of compression and torsional deformation produces three-dimensional severe plastic deformation in the deformation zone during the cross rolling process, which is obviously different from conventional forging; (2) The diameter of the bar before and after cross rolling remains unchanged and can be reciprocated for multi-pass rolling. There is widening in the cross-rolling process, and the equivalent diameter in the cross-section of the titanium alloy billet remains unchanged; (3) Continuous and stable local deformation, rolling load is small, and the deformation process is stable. In the cross rolling process, the actual contact area between the workpiece and the titanium alloy billet is only a small part of the surface area of the titanium alloy billet, which is a local contact deformation, so the load is small; (4) The compression-torsion combined three-dimensional severe deformation can obtain ideal grains Refinement effect.

附图说明Description of drawings

图1为本发明轧辊示意图。Fig. 1 is a schematic diagram of a roll of the present invention.

图2为原始组织β晶粒示意图。Figure 2 is a schematic diagram of the original structure β grains.

图3为本发明实施例一轧制次数为2次示意图。Fig. 3 is a schematic diagram of embodiment 1 of the present invention that the number of rolling is 2 times.

图4为本发明实施例一轧制次数为6次示意图。Fig. 4 is a schematic diagram of embodiment 1 of the present invention that the number of rolling times is 6.

图5为本发明斜轧过程各模具相对位置Fig. 5 is the relative position of each mold in the skew rolling process of the present invention

图6为本发明斜轧过程各模具相对位置俯视图。Fig. 6 is a top view of the relative positions of the molds in the skew rolling process of the present invention.

图7为本发明斜轧穿过程各模具相对位置左视图。Fig. 7 is a left side view of the relative positions of the molds in the skew rolling process of the present invention.

图8为本发明斜轧过程变形区示意图。Fig. 8 is a schematic diagram of the deformation zone in the cross rolling process of the present invention.

附图标记:1-轧辊、2-钛合金坯料、3-导板。Reference signs: 1-roller, 2-titanium alloy blank, 3-guide plate.

具体实施方式Detailed ways

本发明一种大尺寸钛合金超细晶棒材的等距螺旋轧制方法,其特征在于,包括以下步骤:The present invention is an equidistant spiral rolling method for large-scale titanium alloy ultra-fine-grained rods, which is characterized in that it comprises the following steps:

S1:选取直径尺寸D为40-150mm,长度为300-5000mm的钛合金坯料2;S1: Select a titanium alloy blank 2 with a diameter D of 40-150 mm and a length of 300-5000 mm;

S2:将上述钛合金坯料2放置加热炉内加热至840-1025℃,加热时间为:钛合金坯料2直径D×(0.6-0.8)min;S2: Place the above-mentioned titanium alloy billet 2 in a heating furnace and heat it to 840-1025°C. The heating time is: diameter D of the titanium alloy billet 2×(0.6-0.8) min;

S3:将加热后的钛合金坯料2从加热炉转运至斜轧机导料槽内,转运时间为5-20s;S3: transfer the heated titanium alloy billet 2 from the heating furnace to the guide groove of the skew rolling mill, and the transfer time is 5-20s;

S4:在斜轧机的导料槽内进行送料,将钛合金坯料2送入斜轧机入口和出口之间的变形区,钛合金坯料2在变形区内螺旋运动直至变形结束,得到直径为Dm的TC18钛合金棒材棒材,其中m为轧制次数,轧制一次得到的TC18钛合金棒材的直径为D1,轧制两次得到的TC18钛合金棒材的直径为D2,以此类推;S4: Feed in the guide groove of the skew rolling mill, and send the titanium alloy billet 2 into the deformation zone between the entrance and the exit of the skew rolling mill, and the titanium alloy billet 2 spirally moves in the deformation zone until the deformation is completed, and the diameter Dm is obtained. TC18 titanium alloy bar bar, where m is the number of rolling times, the diameter of the TC18 titanium alloy bar obtained by rolling once is D1, the diameter of the TC18 titanium alloy bar obtained by rolling twice is D2, and so on;

S5:重复上述S2-S4步骤,对钛合金坯料2进行2-6次螺旋轧制得到TC18钛合金整体超细晶棒材;S5: repeating the above steps S2-S4, performing 2-6 times of spiral rolling on the titanium alloy blank 2 to obtain the TC18 titanium alloy overall ultra-fine-grained bar;

所述斜轧机为二辊斜轧机,所述轧辊1均为单锥形轧辊1,锥角γ1为17-19度,且轧辊1咬入钛合金坯料2的圆弧半径r为50-380mm,轧辊1送进角α为15-17度,轧辊1的辗轧角β为17-19度,两个轧辊1之间的轧辊1间距Dg为钛合金坯料2直径D的86%-94%,轧辊1转速n为28-50r/min;The skew rolling mill is a two-roll skew rolling mill, and the rolls 1 are all single-tapered rolls 1, the cone angle γ1 is 17-19 degrees, and the arc radius r of the roll 1 biting into the titanium alloy blank 2 is 50-380 mm, The feeding angle α of the roll 1 is 15-17 degrees, the rolling angle β of the roll 1 is 17-19 degrees, and the distance Dg between the two rolls 1 is 86%-94% of the diameter D of the titanium alloy billet 2, Roller 1 speed n is 28-50r/min;

所述钛合金坯料2为大尺寸TC18钛合金棒材;The titanium alloy blank 2 is a large-size TC18 titanium alloy rod;

所述S5步骤中重复轧制过程的加热时间均为TC18钛合金棒材直径Dm×(0.3-0.4)min。The heating time of the repeated rolling process in the step S5 is the diameter of the TC18 titanium alloy rod Dm×(0.3-0.4) min.

轧辊1小端面设置为圆弧面,且圆弧面半径为50-380mm。The small end surface of the roll 1 is set as an arc surface, and the radius of the arc surface is 50-380mm.

孔型椭圆度系数为导板3距Dd与辊距Dg之比,S4步骤中钛合金坯料2在变形区内采用孔型椭圆度系数为1.2-1.4进行轧制。The pass ellipticity coefficient is the ratio of the guide plate 3 distance D d to the roll distance Dg. In step S4, the titanium alloy billet 2 is rolled in the deformation zone with a pass ellipticity coefficient of 1.2-1.4.

在钛合金坯料2轧制过程中,两个轧辊1之间的辊距Dg固定不变,有利于实现多道次重复轧制。During the rolling process of the titanium alloy billet 2, the roll distance Dg between the two rolls 1 is constant, which is beneficial to realize multi-pass repeated rolling.

在S5步骤重复轧制过程中,变形区形状保持不变。During the repeated rolling process in step S5, the shape of the deformation zone remains unchanged.

本发明中轧辊1小端面为圆弧面,这可以快速将圆柱形钛合金坯料2变为椭圆柱形,为恒定辊缝螺旋轧制时提供足够的变形量;轧辊1主体形状为单锥形,锥角与辗轧角相等,与普通轧辊1相比,外径压缩变形区长度增加到2倍长度,轧件经过比普通轧制更长的变形区后,累积可发生大的塑性变形;采用较大椭圆度系数轧制,钛合金坯料2被拽入轧辊1后,横断面变为椭圆形,在螺旋前进过程中,由于椭圆长轴半径大于轧辊1间距,钛合金坯料2一直承受轧辊1的小变形量压缩,变形区任意点旋转一圈,被轧辊1压缩两次;可反复多次实现螺旋轧制,由于大的椭圆度,螺旋轧制后的棒材直径大于辊距,变形后的轧件可以反复多次在同一变形参数条件下,被反复轧制,这样可以获得更大的变形量;采用大送进角和大辗轧角,可以获得更加稳定的螺旋前进动力,以适应大塑性变形的需求。In the present invention, the small end face of the roll 1 is a circular arc surface, which can quickly change the cylindrical titanium alloy blank 2 into an elliptical column, and provide sufficient deformation for constant roll gap spiral rolling; the main body shape of the roll 1 is a single taper , the cone angle is equal to the rolling angle, compared with the ordinary roll 1, the length of the compression deformation zone of the outer diameter is increased to twice the length, and after the rolled piece passes through a longer deformation zone than ordinary rolling, the accumulated large plastic deformation can occur; Rolling with a large ellipticity coefficient, after the titanium alloy billet 2 is pulled into the roll 1, the cross section becomes elliptical. The small deformation of 1 is compressed, and any point in the deformation zone rotates one circle, and is compressed twice by roll 1; the spiral rolling can be realized many times. Due to the large ellipticity, the diameter of the bar after spiral rolling is larger than the roll distance, and the deformation The final rolled piece can be repeatedly rolled under the same deformation parameter conditions, so that a larger deformation can be obtained; the use of a large feeding angle and a large rolling angle can obtain a more stable spiral forward power, and To meet the needs of large plastic deformation.

一般以再结晶温度区分材料加工的类型,再结晶温度以上为热加工,再结晶温度以下为冷加工,现有技术制备超细晶均采用冷加工,由于变形量不够,只能以位错累计获得较小的晶粒,但是这种晶粒热稳定性差,不能进行热处理。本专利的目的是获得能够热处理的晶粒,即通过累积大变形通过再结晶的方式获得超细晶,从而区别于传统的冷加工区别开。Generally, the type of material processing is distinguished by the recrystallization temperature. Above the recrystallization temperature is hot processing, and below the recrystallization temperature is cold processing. In the prior art, cold processing is used to prepare ultra-fine grains. Due to insufficient deformation, relatively small amounts can only be obtained by accumulating dislocations. Small grains, but such grains have poor thermal stability and cannot be heat treated. The purpose of this patent is to obtain grains that can be heat treated, that is, to obtain ultra-fine grains by accumulating large deformation and recrystallization, so as to distinguish them from traditional cold working.

因此本专利为大尺寸TC18整体超细晶棒材的工业化制备提供了一个现实性的选择。Therefore, this patent provides a realistic choice for the industrial production of large-scale TC18 integral ultra-fine-grained rods.

实施例一:Embodiment one:

采用上述技术参数,设计加工轧辊1如图1所示;Adopt above-mentioned technical parameter, design and process roll 1 as shown in Figure 1;

S1:主要变形参数选用钛合金TC18,直径D为100mm,长度为800mm;螺旋辊形的咬入圆弧半径r为100mm,送进角α为16°,锥角为17°,辗轧角为17°,轧辊1间距Dg为坯料直径D的87.5%,孔型椭圆度系数为1.23,轧辊1转速n为40r/min;S1: The main deformation parameters are titanium alloy TC18, the diameter D is 100mm, and the length is 800mm; the radius r of the biting arc of the spiral roll shape is 100mm, the feeding angle α is 16°, the cone angle is 17°, and the rolling angle is 17°, the distance Dg between rolls 1 is 87.5% of the billet diameter D, the pass ellipticity coefficient is 1.23, and the speed n of roll 1 is 40r/min;

S2:在加热炉中加热圆柱状钛合金坯料2至845℃,加热时间为70分钟;S2: Heating the cylindrical titanium alloy blank at 2 to 845°C in a heating furnace for 70 minutes;

S3:将加热到温的钛合金坯料2从加热炉转运至斜轧机导料槽内,转运时间10s;S3: transfer the heated titanium alloy billet 2 from the heating furnace to the guide groove of the skew rolling mill, and the transfer time is 10s;

S4:钛合金坯料2在变形区内螺旋运动直至变形结束。S4: The titanium alloy blank 2 moves helically in the deformation zone until the deformation ends.

S5:反复轧制2次和6次取样分析,其对于钛合金晶粒细化的作用显著,晶粒尺寸细小,且重复轧制过程的加热时间为:TC18钛合金棒材直径Dm×(0.3-0.4)min,其中m为轧制次数,轧制一次得到的TC18钛合金棒材的直径为D1,轧制两次,是采用直径为D1的TC18钛合金棒材作为坯料进行再次轧制,得到的TC18钛合金棒材的直径为D2,以此类推,变形区形状保持不变。S5: Repeated rolling 2 times and 6 times sampling analysis, its effect on titanium alloy grain refinement is significant, the grain size is small, and the heating time of repeated rolling process is: TC18 titanium alloy rod diameter Dm×(0.3 -0.4) min, where m is the number of rolling times, the diameter of the TC18 titanium alloy bar obtained by rolling once is D1, and rolling twice is to use the TC18 titanium alloy bar with a diameter of D1 as the blank for rolling again, The diameter of the obtained TC18 titanium alloy rod is D2, and so on, and the shape of the deformation zone remains unchanged.

基于上述实例,原始组织如图2所示,图中以β晶粒为主,β晶粒平均尺寸为80um;其采用本发明方法,图3为轧制次数为2的典型钛合金晶粒图,其中晶粒尺寸为7.5um左右,晶粒细化程度为90.63%;图4为轧制次数为6的钛合金晶粒图,其中晶粒尺寸为1.2um左右,晶粒细化程度为98.5%。Based on the above examples, the original structure is as shown in Figure 2. Among the figures, the β grains are the main, and the average size of the β grains is 80um; it adopts the method of the present invention, and Figure 3 is a typical titanium alloy grain diagram with 2 rolling times. , where the grain size is about 7.5um, and the degree of grain refinement is 90.63%; Figure 4 is the grain diagram of titanium alloy with rolling times of 6, where the grain size is about 1.2um, and the degree of grain refinement is 98.5% %.

本发明一种大尺寸钛合金超细晶棒材的等距螺旋轧制方法,通过单锥形轧辊1的外形,且保持变形区内辊距不变,采用变形区超大孔型椭圆度系数进行反复多道次轧制,逐步累积超大塑性变形;而且,由于本方法可多道次进行螺旋轧制,对于不同种类钛合金,轧制次数在2-6范围内,对于钛合金晶粒细化的作用最佳,所获的超细晶尺寸最小。该工艺适用于各种尺寸规格和种类的钛合金棒材低载荷连续剧烈塑性变形。用于制备1000-3000nm的整体细晶或超细晶棒材,并可克服现有剧烈塑性变形工艺载荷大,只能加工小尺寸工件的不足。The present invention is an equidistant spiral rolling method for large-sized titanium alloy ultra-fine-grained rods. The shape of the single-tapered roll 1 is adopted, and the roll distance in the deformation zone is kept constant, and the ellipticity coefficient of the super-large pass in the deformation zone is used. Repeated multi-pass rolling to gradually accumulate super large plastic deformation; moreover, since this method can perform multi-pass spiral rolling, for different types of titanium alloys, the number of rolling times is in the range of 2-6, and for titanium alloy grain refinement The effect is the best, and the obtained ultrafine crystal size is the smallest. The process is suitable for continuous severe plastic deformation of titanium alloy rods of various sizes and types under low load. It is used to prepare 1000-3000nm overall fine-grained or ultra-fine-grained rods, and can overcome the shortcomings of the existing severe plastic deformation process, which has a large load and can only process small-sized workpieces.

以上所述,仅为本发明较佳的具体实施方式,但本发明的保护范围并不局限于此,任何熟悉本技术领域的技术人员在本发明揭露的技术范围内,根据本发明的技术方案及其发明构思加以等同替换或改变,都应涵盖在本发明的保护范围之内。The above is only a preferred embodiment of the present invention, but the scope of protection of the present invention is not limited thereto, any person familiar with the technical field within the technical scope disclosed in the present invention, according to the technical solution of the present invention Any equivalent replacement or change of the inventive concepts thereof shall fall within the protection scope of the present invention.

Claims (5)

1. a kind of isometric helix milling method of large-scale titanium alloy ultra fine grained steel bar, which is characterized in that include the following steps:
S1:It is 40-150mm to choose diameter dimension D, and length is the titanium alloy blank of 300-5000mm(2);
S2:By above-mentioned titanium alloy blank(2)It places in heating furnace and is heated to 840-1025 DEG C, heating time is:Titanium alloy blank (2)Diameter D ×(0.6-0.8)min;
S3:By the titanium alloy blank after heating(2)It is transported in skew rolling mill deflector chute from heating furnace, transhipment time 5-20s;
S4:Feeding is carried out in the deflector chute of skew rolling mill, by titanium alloy blank(2)The change being sent between skew rolling mill entrance and exit Shape area, titanium alloy blank(2)In deformed area, inside spin movement terminates until deforming, and obtains the TC18 titanium alloy bars of a diameter of Dm Material, wherein m are rolling number;
S5:Above-mentioned S2-S4 steps are repeated, to titanium alloy blank(2)2-6 screw rolling of progress obtains TC18 titanium alloys and integrally surpasses Fine grain bar;
The skew rolling mill is two-roller skew-rolling machine, the roll(1)It is single cone-shaped roll(1), cone angle gamma 1 is 17-19 degree, and is rolled Roller(1)Bite titanium alloy blank(2)Arc radius r be 50-380mm, roll(1)Feed angle α is 15-17 degree, roll(1)'s Roll off angle beta is 17-19 degree, two rolls(1)Between roll(1)Space D g is titanium alloy blank(2)The 86%-94% of diameter D, Roll(1)Rotating speed n is 28-50r/min;
The titanium alloy blank(2)For large scale bar;
In the S5 steps repeat the operation of rolling heating time be TC18 titanium alloy rod bar diameters Dm ×(0.3-0.4)min.
2. a kind of isometric helix milling method of large-scale titanium alloy ultra fine grained steel bar as described in claim 1, which is characterized in that The roll(1)Small end face is set as arc surface, and circular arc radius surface is 50-380mm.
3. a kind of isometric helix milling method of large-scale titanium alloy ultra fine grained steel bar as described in claim 1, which is characterized in that Groove Ovality Factor is guide plate(3)Away from DdThe ratio between with roll spacing Dg, titanium alloy blank in S4 steps(2)Hole is used in deformed area Type ellipse coefficient is that 1.2-1.4 is rolled.
4. a kind of isometric helix milling method of large-scale titanium alloy ultra fine grained steel bar as described in claim 1, which is characterized in that In titanium alloy blank(2)In the operation of rolling, two rolls(1)Between roll spacing Dg immobilize.
5. a kind of isometric helix milling method of large-scale titanium alloy ultra fine grained steel bar as described in claim 1, which is characterized in that In S5 steps repeat the operation of rolling, deformed area shape remains unchanged.
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CN109909296A (en) * 2019-02-28 2019-06-21 西安建筑科技大学 A method for ultra-fine grain rolling of large-size titanium alloy bars with reverse tapered helical rolls
CN110076198A (en) * 2019-04-30 2019-08-02 北京科技大学 A kind of two roller oblique milling forming device of pole material and method
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CN109772890A (en) * 2019-02-28 2019-05-21 西北工业大学 A kind of ultrafine grain rolling method of large size superalloy bar
CN109807176A (en) * 2019-02-28 2019-05-28 西安东耘新金属材料有限公司 A kind of Ultra-fine Grained milling method of 45 steel bar of large scale
CN109807175A (en) * 2019-02-28 2019-05-28 西安东耘新金属材料有限公司 A kind of Ultra-fine Grained milling method of large-scale titanium alloy bar
CN109807174A (en) * 2019-02-28 2019-05-28 西安东耘新金属材料有限公司 A kind of inverted cone helical roller Ultra-fine Grained milling method of 45 steel bar of large scale
CN109909295A (en) * 2019-02-28 2019-06-21 西安建筑科技大学 A kind of ultra-fine grain rolling method of large-size aluminum alloy bar
CN109909296A (en) * 2019-02-28 2019-06-21 西安建筑科技大学 A method for ultra-fine grain rolling of large-size titanium alloy bars with reverse tapered helical rolls
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CN109909296B (en) * 2019-02-28 2020-04-07 西安建筑科技大学 Reverse-cone spiral roller superfine crystal rolling method for large-size titanium alloy bar
CN109807176B (en) * 2019-02-28 2020-05-15 西安东耘新金属材料有限公司 Superfine crystal rolling method for large-size 45 steel bar
CN110076198A (en) * 2019-04-30 2019-08-02 北京科技大学 A kind of two roller oblique milling forming device of pole material and method
CN111441020A (en) * 2020-04-30 2020-07-24 西安建筑科技大学 A low-cost method for preparing TC4 titanium alloy sputtering target
CN111441020B (en) * 2020-04-30 2022-05-10 西安建筑科技大学 Method for preparing TC4 titanium alloy sputtering target material at low cost

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