CN108498396A - A series of disposable hypersorption type nanofiber functional masks and preparation method thereof - Google Patents
A series of disposable hypersorption type nanofiber functional masks and preparation method thereof Download PDFInfo
- Publication number
- CN108498396A CN108498396A CN201810371233.0A CN201810371233A CN108498396A CN 108498396 A CN108498396 A CN 108498396A CN 201810371233 A CN201810371233 A CN 201810371233A CN 108498396 A CN108498396 A CN 108498396A
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- series
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Classifications
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- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8158—Homopolymers or copolymers of amides or imides, e.g. (meth) acrylamide; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9717—Rhodophycota or Rhodophyta [red algae], e.g. Porphyra
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Abstract
The invention discloses a series of disposable hypersorption type nanofiber functional masks and preparation method thereof, it is related to facial mask technical field.By following weight proportion at being grouped as：Polysaccharide, modification of polysaccharides, the water soluble polymer of 5% 50% mass fractions, 1% 10% polymer substances with white-skinned face function, 0.001% 5% functional materials, 0.02% 2% Essences, surplus is water.The nanofiber functional mask produced using this method, using various functions substance as additive, mass production is carried out using electrostatic spinning technique using water-soluble modified polysaccharide or macromolecule as major solute.In use, a small amount of spraying Essence of cooperation, functional facial mask can be fully absorbed within a short period of time by face, without any residual, no longer need to carry out facial cleansing nursing.
Description
Technical field
The present invention relates to facial mask technical fields, and in particular to a series of disposable hypersorption type nanofiber functional masks
And preparation method thereof.
Background technology
Facial mask appears in ancient Egypt's period earliest, and using soil, facial mask is made, and also needs to clean for a long time after applying, reach
To the purpose of decontamination.Then dura mater occurs.It is basic material with medical gypsum, there is certain film forming, but still exist
Some lime stones harmful effect, being replaced by mantle quickly.First facial mask truly was born in last century
The nineties, it is made of seaweed in conjunction with other packing materials, is enhanced by the obturation effect to skin and is absorbed.But allotment is not square
Just, so that it is confined in specialized beauty parlors, hinder and be widely popularized.Nowadays, most commonly non-woven fabrics facial mask in the market, it is big
The big troublesome operation for simplifying mantle, make things convenient for customers nursing of being in.But the shortcomings that product, is：Non-woven fabrics and skin affinity are not
It is good, do not have the effect of imitative biological intelligence, only the carrier of Essence, so functioning only as applying the effect of face, in Essence
Nutrition transdermal absorption factor it is uncertain, effect is also not satisfactory.
In conclusion the present invention devises a series of disposable hypersorption type nanofiber functional masks and preparation method thereof.
Invention content
In view of the shortcomings of the prior art, purpose of the present invention is to be to provide a series of disposable hypersorption type Nanowires
Functional mask and preparation method thereof is tieed up, the nanofiber functional mask produced using this method, with water-soluble modified polysaccharide or height
Molecule is major solute, and using various functions substance as additive, mass production is carried out using electrostatic spinning technique.It is using
In the process, a small amount of spraying Essence of cooperation, functional facial mask can be fully absorbed within a short period of time by face, without any residual,
It no longer needs to carry out facial cleansing nursing.
To achieve the goals above, the present invention is to realize by the following technical solutions：A series of disposable hypersorption types
Nanofiber functional mask, by following weight proportion at being grouped as：It is the polysaccharide of 5%-50% mass fractions, modification of polysaccharides, water-soluble
Property macromolecule, 1%-10% has the polymer substance of white-skinned face function, and 0.001%-5% functional materials, 0.02%-2% Essences are remaining
Amount is water.
The polysaccharide, modification of polysaccharides, water soluble polymer are gelatin, gelatine, carragheen, carboxymethyl cellulose, methyl
One in cellulose, ethyl cellulose, hydroxyethyl cellulose, Sodium Hyaluronate, sodium alginate, polyethylene glycol, polyacrylamide
Kind is a variety of.
The polymer substance with white-skinned face function be vitamin C, tartaric acid, amides substance one kind or more
Kind.
The functional materials be Sodium Hyaluronate, carbohydrate isomer, parahydroxyacet-ophenone, 1,2- ethylene glycol,
Glycosylglycerol, green alga, red algae, brown alga, Cer NS, dipotassium glycyrrhizinate, De Minshu, Chinese herbal medicine extract, nonapeptide, hexapeptide,
Natural complex C, Thymus serpyllum extract, zinc gluconate, puridoxine hydrochloride, caryophyllin, carnosine, palmityl tripeptides, acetyl
Base octapeptide, Hydrolyzed Collagen, Herba Dendrobii extract it is one or more.
The Essence is that jojoba seed oil, grape seed oil, shea butter, caprylic/capric with certain function are sweet
One or more of oily three esters, parahydroxyacet-ophenone, phytosterol/canola oil glyceride, avocado butyl oleate add
Enter the solution into ultra-pure water.
A series of preparation method of disposable hypersorption type nanofiber functional masks, includes the following steps：
1, the preparation of spinning solution：The solution concentration of spinning solution is controlled between 5%-50%, using ultra-pure water or pure water as the molten of solution
Agent, respectively by polysaccharide, modification of polysaccharides, the water soluble polymer such as polyvinyl alcohol of 5%-50% mass fractions（PVA）, polyvinyl pyrrole
Alkanone（PVP）Etc. being added to the water, the agitation and filtration in 20 DEG C -50 DEG C of water bath with thermostatic control prepares homogeneous and transparent solution A；
Then by the polymer substance with white-skinned face function, such as vitamin C, the substance of tartaric acid, amides, 1%- by mass percentage
10%, it is added in solution A, 6h or so is stirred equally in 20 DEG C -50 DEG C of water bath with thermostatic control, form homogeneous and transparent solution B；
Finally according to the difference of its realization of functions, the mass fraction of 0.001%-5% is pressed respectively, and being added has replenishing water and preserving moisture（It is such as transparent
Matter acid sodium class）, reparation of releiving（Ceramide, dipotassium glycyrrhizinate class）, highlight shining coloured silk（Polypeptide）, long-acting oil control（Gluconic acid
Zinc, natural plant extracts etc.）, crease-resistant compact（Collagen, natural plant extracts etc.）Equal substances, are stirred at ambient temperature
6h is mixed, a series of homogeneous and transparent spinning solution C are formed.
2, the configuration of Essence：By the mass fraction of 0.02%-2%, by the jojoba seed oil with certain function, grape pip
Oil, shea butter, caprylic/capric triglyceride, parahydroxyacet-ophenone, phytosterol/canola oil glyceride, avocado oil
One or more of acid butyl ester is added in ultra-pure water, and uniform Essence is made in mechanical agitation or supersound process 4h or so.
3, the preparation of facial mask：A series of spinning solution C of above-mentioned preparation are subjected to function using needle-free electrostatic spinning apparatus
The preparation of property nanofiber facial mask.Needle-free electrostatic spinning apparatus yield is big, and prepared nanofiber film uniformity is good, is suitble to
Large batch of industrialization production.It is to receive substrate with various non-woven fabrics, depositing nanofibers, and then formation nanofiber on it
Functional mask.The humidity for controlling spinning environment is 30%-50%, and spinning distance is 140mm-220mm, spinning voltage 40KV-
80KV.The nano fibrous membrane prepared under this technological parameter, relatively uniform, strength is good.
Beneficial effects of the present invention：
1, with polysaccharide, modification of polysaccharides, polyvinyl alcohol（PVA）, polyvinylpyrrolidone（PVP）Equal water soluble polymers are as nanometer
The bulk composition of fiber functional mask has many advantages, such as to have excellent performance, is easy to use and environmentally friendly.Not only to human body without appoint
What side effect, also has preferable compatibility with skin, is conducive to the absorption of nutriment and functional materials.
2, the preparation of spinning solution is divided into three phases, can effectively ensure that water-soluble high-molecular substance and various functions object
Matter is thoroughly mixed together, and ensures to be uniformly dispersed during electrostatic spinning and uniform and stable in nanofiber facial mask, have
Absorption conducive to skin to functional materials is conducive to the effect of functioning property substance.
3, the corresponding different Essence of different function.Essence cooperates with nanofiber functional mask, collaboration hair
The effect of waving, plays a multiplier effect.
4, during using a, it need to only coordinate a small amount of Essence, nanofiber facial mask that can all be inhaled by skin of face
It receives, there is no waste and the undesirable problems of effect.
Specific implementation mode
To make the technical means, the creative features, the aims and the efficiencies achieved by the present invention be easy to understand, with reference to
Specific implementation mode, the present invention is further explained.
Present embodiment uses following technical scheme：A series of disposable hypersorption type nanofiber functional masks, by
Following weight proportion at being grouped as：Polysaccharide, modification of polysaccharides, the water soluble polymer of 5%-50% mass fractions, 1%-10% have
The polymer substance of white-skinned face function, 0.001%-5% functional materials, 0.02%-2% Essences, surplus are water.
A series of preparation method of disposable hypersorption type nanofiber functional masks：1, the preparation of spinning solution：Control spinning
The solution concentration of liquid is between 5%-50%, using ultra-pure water or pure water as the solvent of solution, respectively by the more of 5%-50% mass fractions
Sugar, modification of polysaccharides, water soluble polymer such as polyvinyl alcohol（PVA）, polyvinylpyrrolidone（PVP）Etc. being added to the water, 20
Agitation and filtration in DEG C -50 DEG C of water bath with thermostatic control, prepares homogeneous and transparent solution A；Then by the macromolecule with white-skinned face function
Substance, such as vitamin C, the substance of tartaric acid, amides, 1%-10%, is added in solution A by mass percentage, equally 20 DEG C-
6h or so is stirred in 50 DEG C of water bath with thermostatic control, forms homogeneous and transparent solution B；Finally according to the difference of its realization of functions, divide
Not An 0.001%-5% mass fraction, be added have replenishing water and preserving moisture（Such as Sodium Hyaluronate class）, reparation of releiving（It is ceramide, sweet
Oxalic acid dipotassium class）, highlight shining coloured silk（Polypeptide）, long-acting oil control（Zinc gluconate, natural plant extracts etc.）, crease-resistant compact
（Collagen, natural plant extracts etc.）Equal substances, stir 6h, form a series of homogeneous and transparent spinning at ambient temperature
Liquid C.
2, the configuration of Essence：By the mass fraction of 0.02%-2%, by the jojoba seed oil with certain function, grape pip
Oil, shea butter, caprylic/capric triglyceride, parahydroxyacet-ophenone, phytosterol/canola oil glyceride, avocado oil
One or more of acid butyl ester is added in ultra-pure water, and uniform Essence is made in mechanical agitation or supersound process 4h or so.
3, the preparation of facial mask：A series of spinning solution C of above-mentioned preparation are subjected to function using needle-free electrostatic spinning apparatus
The preparation of property nanofiber facial mask.Needle-free electrostatic spinning apparatus yield is big, and prepared nanofiber film uniformity is good, is suitble to
Large batch of industrialization production.It is to receive substrate with various non-woven fabrics, depositing nanofibers, and then formation nanofiber on it
Functional mask.The humidity for controlling spinning environment is 30%-50%, and spinning distance is 140mm-220mm, spinning voltage 40KV-
80KV.The nano fibrous membrane prepared under this technological parameter, relatively uniform, strength is good.
The application method of present embodiment：Nanofiber facial mask is stripped down from base material, according to the position of regulation
It sets and is attached at face, spray a small amount of Essence on nanofiber facial mask, nanofiber facial mask can gradually dissolve, by pressing
It rubs, various functions substance will be fully absorbed by skin of face, and residue problem is not present, and no longer need to carry out face cleaning.Simultaneously
The problem of avoiding the waste of traditional facial mask Essence.
The nanofiber of present embodiment has larger specific surface area and higher draw ratio, in every field
All have a wide range of applications.The method of production nanofiber has much at present, wherein electrostatic spinning technique can connect as one kind
The method of continuous controllable preparation nanofiber, has obtained large-scale application.And the electrostatic spinning apparatus used in this method is
Needle-free electrostatic spinning apparatus, yield is high, and operability is strong, has larger technology excellent in industrialization prepares nanofiber field
Gesture.Various functions substance is combined together by way of co-blended spinning with nanofiber in the method, forms a system
One organism.And various functions substance is easy to discharge from nanofiber, faster can more efficiently act on face, reach
To corresponding functional effect.In use, coordinate a small amount of Essence, nanofiber functional mask can be by facial complete
It absorbs, various functions ingredient can give full play to effectiveness, not generate any residuals, no longer need to carry out facial cleansing.Greatly
It is big to save usage time and use step, greatly improve user experience.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (6)
1. a series of disposable hypersorption type nanofiber functional masks, which is characterized in that by following weight proportion at being grouped as：
Polysaccharide, modification of polysaccharides, the water soluble polymer of 5%-50% mass fractions, 1%-10% have the polymer substance of white-skinned face function,
0.001%-5% functional materials, 0.02%-2% Essences, surplus are water.
2. a series of disposable hypersorption type nanofiber functional masks according to claim 1, which is characterized in that described
Polysaccharide, modification of polysaccharides, water soluble polymer are gelatin, gelatine, carragheen, carboxymethyl cellulose, methylcellulose, ethyl cellulose
It is one or more in element, hydroxyethyl cellulose, Sodium Hyaluronate, sodium alginate, polyethylene glycol, polyacrylamide.
3. a series of disposable hypersorption type nanofiber functional masks according to claim 1, which is characterized in that described
Polymer substance with white-skinned face function be vitamin C, tartaric acid, amides substance it is one or more.
4. a series of disposable hypersorption type nanofiber functional masks according to claim 1, which is characterized in that described
Functional materials are Sodium Hyaluronate, carbohydrate isomer, parahydroxyacet-ophenone, 1,2- ethylene glycol, glycosylglycerol, green
Algae, red algae, brown alga, Cer NS, dipotassium glycyrrhizinate, De Minshu, Chinese herbal medicine extract, nonapeptide, hexapeptide, natural complex C,
Thymus serpyllum extract, zinc gluconate, puridoxine hydrochloride, caryophyllin, carnosine, palmityl tripeptides, acetyl group octapeptide, hydrolysis glue
Former albumen, Herba Dendrobii extract it is one or more.
5. a series of disposable hypersorption type nanofiber functional masks according to claim 1, which is characterized in that described
Essence is the jojoba seed oil with certain function, grape seed oil, shea butter, caprylic/capric triglyceride, para hydroxybenzene
One or more of ethyl ketone, phytosterol/canola oil glyceride, avocado butyl oleate are added to molten in ultra-pure water
Liquid.
6. a series of preparation method of disposable hypersorption type nanofiber functional masks, which is characterized in that include the following steps：
(1), the preparation of spinning solution：The solution concentration of spinning solution is controlled between 5%-50%, using ultra-pure water or pure water as solution
The polysaccharide, modification of polysaccharides, water soluble polymer of 5%-50% mass fractions are added to the water, at 20 DEG C -50 DEG C by solvent respectively
Agitation and filtration in water bath with thermostatic control prepares homogeneous and transparent solution A；Then the polymer substance with white-skinned face function is pressed into quality
Percentage 1%-10%, is added in solution A, and 6h or so is stirred equally in 20 DEG C -50 DEG C of water bath with thermostatic control, forms transparent and homogeneous
Solution B；Finally according to the difference of its realization of functions, the mass fraction of 0.001%-5% is pressed respectively, and being added, there is moisturizing to protect
Wet, reparation of releiving highlights one or more in shining coloured silk, long-acting oil control, the crease-resistant substance that compacts, stirs 6h at ambient temperature,
Form a series of homogeneous and transparent spinning solution C;(2), the configuration of Essence：By the mass fraction of 0.02%-2%, will have certain
The jojoba seed oil of function, grape seed oil, shea butter, caprylic/capric triglyceride, parahydroxyacet-ophenone, phytosterol/low
One or more of erucic acid vegetable seeds oil glyceride, avocado butyl oleate are added in ultra-pure water, mechanical agitation or supersound process
Uniform Essence is made in 4h or so；(3), the preparation of facial mask：A series of spinning solution C of above-mentioned preparation are used into needle-free electrostatic
Device for spinning carries out the preparation of functional nano fiber facial mask；Needle-free electrostatic spinning apparatus yield is big, prepared Nanowire
It is good to tie up film uniformity, is suitble to large batch of industrialization production；It is to receive substrate with various non-woven fabrics, deposits Nanowire on it
Dimension, and then form nanofiber functional mask；The humidity for controlling spinning environment is 30%-50%, and spinning distance is 140mm-
220mm, spinning voltage 40KV-80KV;The nano fibrous membrane prepared under this technological parameter, relatively uniform, strength is good.
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| CN109234827A (en) * | 2018-09-26 | 2019-01-18 | 冷秀红 | A kind of preparation method of the face paper using the siliceous binding material of rose-red |
| CN109674685A (en) * | 2019-01-21 | 2019-04-26 | 诺斯贝尔化妆品股份有限公司 | Collagen nano instant mask with pullulanase polysaccharide as skeleton and preparation method thereof |
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| CN111743785B (en) * | 2019-03-28 | 2021-10-22 | 珀莱雅化妆品股份有限公司 | Nanofiber membrane with whitening and tightening effects and preparation method thereof |
| CN112626712A (en) * | 2019-10-08 | 2021-04-09 | 轴心纤维有限公司 | Polysaccharide and protein nanofiber matrices with functional ingredients for skin care products |
| WO2021071365A1 (en) * | 2019-10-08 | 2021-04-15 | Revolution Fibres Limited | Nanofibre matrix made of natural polymers with natural functional ingredients for cosmetic products |
| US20220354752A1 (en) * | 2019-10-08 | 2022-11-10 | Nanolayr Limited | Nanofibre matrix made of natural polymers with natural functional ingredients for cosmetic products |
| CN111000751A (en) * | 2019-12-11 | 2020-04-14 | 无限极（中国）有限公司 | Solid mask and preparation method thereof |
| CN111000751B (en) * | 2019-12-11 | 2023-05-05 | 无限极（中国）有限公司 | Solid mask and preparation method thereof |
| WO2023285812A3 (en) * | 2021-07-12 | 2023-03-09 | Mccormack Innovation Ltd | Dissolvable face sheet mask |
| CN113558998A (en) * | 2021-09-01 | 2021-10-29 | 浙江理工大学绍兴柯桥研究院有限公司 | Nanofiber mask and preparation method thereof |
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