CN108485845B - Jiabao fruit leaf handmade soap and making method thereof - Google Patents
Jiabao fruit leaf handmade soap and making method thereof Download PDFInfo
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- 241000123865 Gynura bicolor Species 0.000 claims abstract description 42
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 61
- 238000001256 steam distillation Methods 0.000 claims description 36
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- 239000011718 vitamin C Substances 0.000 description 1
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/04—Antibacterial agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P39/00—General protective or antinoxious agents
- A61P39/06—Free radical scavengers or antioxidants
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/442—Perfumes
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Veterinary Medicine (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Pharmacology & Pharmacy (AREA)
- Animal Behavior & Ethology (AREA)
- Public Health (AREA)
- Biochemistry (AREA)
- Toxicology (AREA)
- Communicable Diseases (AREA)
- Oncology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses jaboticaba leaf handmade soap and a preparation method thereof, wherein transparent soap base and rose hydrosol are mixed in a water bath and heated to be dissolved, 4 base oils which are respectively sweet almond oil, wheat germ oil, jojoba oil and olive oil are added to serve as humectants, jaboticaba leaf extract concentrated solution and gynura bicolor extract concentrated solution are added, citronella essential oil and mint essential oil are dropped into the concentrated solution, the mixture is uniformly stirred, molded, kept stand and dried in a ventilated mode, and then the jaboticaba leaf handmade soap is obtained. The handmade soap prepared by the invention is light brown semitransparent, natural and safe, is mild and smooth, has rich fragrance, contains the fragrance of myrciaria dubia leaves, the fragrance of roses, the fragrance of citronella and the fragrance of mint, and is a multifunctional handmade soap with the effects of oxidation resistance, antibiosis, itching relieving, mosquito repelling and the like.
Description
Technical Field
The invention belongs to the technical field of daily washing product processing, and particularly relates to jaboticaba leaf handmade soap and a preparation method thereof.
Background
Jiabao fruit (Jiabao fruit)Myrciaria cauliflora ) Also called as Vitis vinifera and precious fruit, is a tropical and subtropical evergreen shrub of the genus Pseuonymus of Myrtaceae, which can bloom and bear fruits all the year round. Jiabao fruitThe branches and leaves are luxuriant, the four seasons are evergreen, the leaves are opposite, the leaves are dark green and glossy, and the new leaves are light red. Research shows that in 4 jaba, early season, Fugang and Argentina varieties, the tender leaf of the jaba has the highest content of polyphenols, and the alcohol extract has higher antioxidant capacity and in vitro sugar reducing capacity than the fruit. The tender leaves of jaba jaboticaba have rich sources and obvious effects, and are possibly superior to fruits in medical application. At present, the development and utilization of jaboticaba are mainly focused on fruit storage, preservation and processing utilization, but the development and utilization of jaboticaba leaves are very little.
Citronella (Mosla chinensis Maxim) Is a general name of about 55 aromatic plants in the genus of citronella of the family Gramineae, also known as Cymbopogon citratus, and is one of the common vanilla. It is also called lemon grass because of its lemon fragrance. The citronella has good effect of treating rheumatism, and also has the effects of treating migraine, resisting infection, improving digestive function, deodorizing and expelling parasites. The handmade soap prepared from the citronella has the effects of resisting infection, astringing skin, softening skin, conditioning greasy and dirty skin, refreshing, and restoring physical and mental balance. The citronella essential oil has antibacterial effect on Escherichia coli and Staphylococcus aureus.
Radix Althaeae Macrophyllae (Begonia fimbristipula) Is a plant of the genus Begonia of the family Begoniaceae, which is a specific plant of China. The fresh and tender stem and leaf and shoot have high vitamin C content, and also contain flavonoid glycoside. The tender stem leaves are rich in calcium, iron and the like, have high nutritive value and medical values of hemostasis, antivirus and the like, so the tender stem leaves have a long history of being used for vegetable cultivation.
Mint (A), (B)Mentha haplocalyxBriq.) Tu named as "Yindancao" is a plant of Labiatae, has a green fragrance of the whole plant, has dual functions of medical use and eating, and can be taken by squeezing juice from stems and leaves as main edible parts. In eating, the mint can be used as a flavoring agent, a spice, wine, tea and the like. The bath can relax angry emotion, enhance spirit, make people happy, help sleep, and has antiseptic, antibacterial, antiviral, analgesic, and antipruritic effects.
Disclosure of Invention
The invention aims to provide a multifunctional jaboticaba leaf handmade soap with the functions of resisting oxidation, resisting bacteria, relieving itching, repelling mosquitoes and the like and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
the jaboticaba leaf handmade soap is prepared from the following raw materials in parts by weight: 0.6-0.8 part of sweet almond oil, 0.6-0.8 part of wheat germ oil, 0.6-0.8 part of jojoba oil, 0.6-0.8 part of olive oil, 250-320 parts of transparent soap base, 45-55 parts of rose hydrosol, 50-70 parts of jaboticaba leaf extract concentrated solution, 20-30 parts of gynura bicolor extract concentrated solution, 0.8-1.2 parts of citronella essential oil and 0.6-0.8 part of mint essential oil.
The invention provides a manufacturing method of the jaboticaba leaf handmade soap, which comprises the following steps:
1) putting rose petals and water in a steam distillation device, extracting by adopting a steam distillation method, and collecting rose hydrosol;
2) drying fresh jaboticaba leaves, crushing by using a crusher, and sieving to obtain jaboticaba leaf fine powder; then mixing the fine powder of the jaboticaba leaves with 35-40% ethanol, placing the mixture in a constant-temperature shaking instrument, shaking and extracting at 25-30 ℃, centrifuging and filtering to obtain an alcohol extract of the jaboticaba leaves; then placing the jaboticaba leaf alcohol extract in a rotary evaporator, and taking out after rotary evaporation till no alcohol taste exists to obtain jaboticaba leaf extract concentrated solution;
3) crushing fresh gynura bicolor leaves, mixing the crushed gynura bicolor leaves with 65-70% ethanol, placing the mixture in a constant-temperature shaking instrument, shaking and extracting at 25-30 ℃, centrifuging and filtering to obtain a gynura bicolor ethanol extract; then placing the gynura bicolor alcohol extract in a rotary evaporator, and taking out after rotary evaporation until no alcohol smell exists to obtain a gynura bicolor extract concentrated solution;
4) placing fresh citronella cut into 4-6 cm small sections and water in a steam distillation device, and extracting by adopting a steam distillation method to obtain citronella essential oil;
5) putting fresh mint leaves and water into a steam distillation device, and extracting by adopting a steam distillation method to obtain mint essential oil;
6) mixing the transparent soap base and the rose hydrosol, sealing the mixture with a preservative film, heating the mixture in a water bath at the temperature of 75-85 ℃ until the transparent soap base is dissolved, and cooling the mixture at room temperature until the temperature of the mixed solution of the transparent soap base and the rose hydrosol is reduced to 50-55 ℃;
7) adding sweet almond oil, wheat germ oil, jojoba oil and olive oil into the mixed solution of the transparent soap base and the rose hydrosol, stirring uniformly, adding concentrated solution of jaboticaba leaf extract, concentrated solution of gynura bicolor extract, citronella essential oil and mint essential oil, and stirring uniformly;
8) pouring the mixed liquid obtained in the step 7) into a mold, removing foams, standing, performing freeze forming, demolding, and drying in a cool and ventilated place to obtain the jaboticaba leaf handmade soap.
In the step 1), the dosage ratio of the rose petals to the water is 2.5-3.0 kg: 6L; in the step 4), the dosage ratio of the citronella to the water is 2.5-3.5 kg: 5L; in the step 5), the dosage ratio of the mint leaves to the water is 3.0-4.0 kg: 5L.
In the step 2), the jaboticaba leaves are light red tender leaves of jaboticaba varieties.
In the step 2), drying is carried out in an oven at the temperature of 40-50 ℃ for 20-24 h, and the particle size of the jaboticaba leaf fine powder is 35-40 meshes.
In the step 2), the weight ratio of the jaboticaba leaf fine powder to the ethanol is 1: 55-65, the extraction time is 16-20 h, the centrifugation condition is 5500-6500 rpm, and the centrifugation time is 15-20 min.
In the step 2), the rotary evaporation is carried out in a water bath at 38-42 ℃, and the jaboticaba leaf alcohol extract is rotary evaporated until 50-60% of the volume of the jaboticaba leaf alcohol extract is left, so that jaboticaba leaf extract concentrated solution is obtained.
In the step 3), the weight ratio of the gynura bicolor leaves to the ethanol is 1: 8-12, the extraction time is 16-20 h, the centrifugation condition is 5500-6500 rpm, and the centrifugation time is 15-20 min.
In the step 3), the rotary evaporation is carried out in a water bath at 38-42 ℃, and the alcohol extract of gynura bicolor is rotary evaporated until 20-30% of the volume of the alcohol extract is left, so that a gynura bicolor extract concentrated solution is obtained.
In the step 8), the standing time is 0.5-1 h, the freezing temperature is-20 ℃ or below, the freezing time is 0.5-1 h, and the ventilation drying time is 1-2 weeks.
The invention adopts the technical scheme that the jaboticaba leaf alcohol extract rich in polyphenols is selected as the antioxidant; the alcohol extract of the tender stem and leaf of gynura bicolor with the effects of stopping bleeding, resisting virus and resisting oxidation is added, meanwhile, the tender stem and leaf of gynura bicolor is rich in trace elements, can provide enough nutrient components for skin, and has double oxidation resisting effects when being combined with the myrciaria dubia leaf; the citronella essential oil is used as an aromatic on one hand, and has multiple effects of repelling mosquitoes, inhibiting bacteria, softening skin and the like on the other hand; the mint essential oil has the effects of resisting virus, easing pain, preventing corrosion, relieving itching and the like, and also endows the handmade soap with cool skin feeling, and the handmade soap is matched with the citronella essential oil for use, so that the fragrance is enriched, and the sterilization effect is enhanced.
The invention has the following remarkable advantages:
(1) according to the invention, the leaf of the rare fruit tree jaboticaba and the tender stem leaf of the wild vegetable gynura bicolor are jointly applied to the preparation of the handmade soap, and the prepared handmade soap has good antioxidant effect by utilizing the characteristic that the leaf and the tender stem leaf of the wild vegetable gynura bicolor are rich in polyphenol.
(2) The extraction of the effective components of the plants adopts a method combining leaching and ethanol extraction, and is a mild extraction method, so that the effective components can be effectively extracted, and the damage of an extraction mode to the effective components is reduced.
(3) The extracts used in the invention are all concentrated solutions obtained after ethanol is removed, the irritation of the handmade soap to skin can be reduced, meanwhile, the concentrated solution increases the percentage of antioxidant ingredients in the handmade soap, the liquid-solid ratio in the handmade soap is reduced, and the handmade soap is easier to form.
(4) The invention provides an effective utilization form of the rare fruit tree jaboticaba leaves, and promotes the comprehensive utilization of jaboticaba.
Detailed Description
The jaboticaba leaf handmade soap is prepared from the following raw materials in parts by weight: 0.6-0.8 part of sweet almond oil, 0.6-0.8 part of wheat germ oil, 0.6-0.8 part of jojoba oil, 0.6-0.8 part of olive oil, 250-320 parts of transparent soap base, 45-55 parts of rose hydrosol, 50-70 parts of jaboticaba leaf extract concentrated solution, 20-30 parts of gynura bicolor extract concentrated solution, 0.8-1.2 parts of citronella essential oil and 0.6-0.8 part of mint essential oil.
The preparation method of the jaboticaba leaf handmade soap comprises the following steps:
1) putting rose petals and water into a steam distillation device according to the dosage ratio of 2.5-3.0 kg: 6L, extracting by adopting a steam distillation method, and collecting rose hydrosol;
2) drying fresh jaboticaba leaves in an oven at the temperature of 40-50 ℃ for 20-24 hours, then crushing by using a crusher, and sieving by using a 35-40-mesh sieve to obtain jaboticaba leaf fine powder; then mixing the fine powder of the jaboticaba leaves with 35-40% ethanol according to the weight ratio of 1: 55-65, placing the mixture in a constant-temperature oscillator, carrying out oscillation extraction at 25-30 ℃ for 16-20 h, then centrifuging at 5500-6500 rpm for 15-20 min, and filtering to obtain an alcohol extract of the jaboticaba leaves; then placing the jaboticaba leaf alcohol extract in a rotary evaporator, carrying out rotary evaporation in water bath at 38-42 ℃ until no alcohol taste exists, and taking out to obtain jaboticaba leaf extract concentrated solution (the volume of the jaboticaba leaf alcohol extract is 50-60%);
3) according to the weight ratio of 1: 8-12, crushing fresh gynura bicolor leaves, mixing the crushed gynura bicolor leaves with 65-70% ethanol, placing the mixture in a constant-temperature shaking instrument, shaking and extracting for 16-20 h at 25-30 ℃, centrifuging for 15-20 min at 5500-6500 rpm, and filtering to obtain gynura bicolor ethanol extract; then placing the alcohol extract of gynura bicolor in a rotary evaporator, carrying out rotary evaporation in a water bath at 38-42 ℃ until no alcohol smell exists, and taking out to obtain a concentrated extract of gynura bicolor (the volume of the concentrated extract is 20-30% of the alcohol extract of gynura bicolor);
4) cutting fresh citronella into 4-6 cm small sections, then placing the citronella and water in a steam distillation device according to the dosage ratio of 2.5-3.5 kg: 5L, and extracting by adopting a steam distillation method to obtain citronella essential oil;
5) putting fresh mint leaves and water into a steam distillation device according to the dosage ratio of 3.0-4.0 kg: 5L, and extracting by adopting a steam distillation method to obtain mint essential oil;
6) mixing the transparent soap base and the rose hydrosol, sealing the mixture by using a preservative film, heating the mixture in a water bath at the temperature of 75-85 ℃ until the transparent soap base is dissolved, and cooling the mixture to the room temperature until the temperature of the mixed solution of the transparent soap base and the rose hydrosol is reduced to 50-55 ℃;
7) adding sweet almond oil, wheat germ oil, jojoba oil and olive oil into the mixed solution of the transparent soap base and the rose hydrosol, stirring uniformly, adding concentrated solution of jaboticaba leaf extract, concentrated solution of gynura bicolor extract, citronella essential oil and mint essential oil, and stirring uniformly;
8) pouring the mixed liquid obtained in the step 7) into a mold, scraping off foams, standing for 0.5-1 h, freezing for 0.5-1 h at-20 ℃, demolding after molding, and placing in a shady and ventilated place for ventilation for 1-2 weeks to obtain the jaboticaba leaf handmade soap.
Furthermore, the jaboticaba leaves used in the invention are light red tender leaves of jaboticaba variety.
Example 1
The jaboticaba leaf handmade soap is prepared from the following raw materials in parts by weight: sweet almond oil 0.7 parts, wheat germ oil 0.7 parts, jojoba oil 0.7 parts, olive oil 0.7 parts, transparent soap base 285 parts, rose hydrosol 50 parts, jaboticaba leaf extract concentrate 60 parts, gynura bicolor extract concentrate 25 parts, citronella essential oil 1 part, and mint essential oil 0.7 part;
the preparation method of the jaboticaba leaf handmade soap comprises the following steps:
1) putting rose petals and water into a steam distillation device according to the dosage ratio of 2.75 kg: 6L, extracting by adopting a steam distillation method, and collecting rose hydrosol;
2) drying fresh jaboticaba leaves in an oven at the temperature of 45 ℃ for 22 h, then crushing by using a crusher, and sieving by using a 40-mesh sieve to obtain jaboticaba leaf fine powder; then mixing the fine powder of the jaboticaba leaves and 40% ethanol according to the weight ratio of 1: 60, placing the mixture in a constant-temperature shaking instrument, shaking and extracting for 18 h at 28 ℃, then centrifuging at 6000 rpm for 15 min, and filtering to obtain an alcohol extract of the jaboticaba leaves; then placing the jaboticaba leaf alcohol extract in a rotary evaporator, carrying out rotary evaporation in water bath at 40 ℃ until no alcohol taste exists, and taking out to obtain jaboticaba leaf extract concentrated solution;
3) pulverizing fresh folium Nerviliae Fordii at a weight ratio of 1: 10, mixing with 70% ethanol, placing in a constant temperature shaking apparatus, shaking and extracting at 28 deg.C for 18 hr, centrifuging at 6000 rpm for 15 min, and filtering to obtain folium Nerviliae Fordii alcohol extract; then placing the gynura bicolor alcohol extract in a rotary evaporator, carrying out rotary evaporation in water bath at 40 ℃ until no alcohol smell exists, and taking out to obtain a gynura bicolor extract concentrated solution;
4) cutting fresh citronella into 4-6 cm small sections, then placing the citronella and water in a steam distillation device according to the dosage ratio of 3 kg to 5L, and extracting by adopting a steam distillation method to obtain citronella essential oil;
5) according to the dosage ratio of 3.0 kg to 5L, putting fresh mint leaves and water in a steam distillation device, and extracting by adopting a steam distillation method to obtain mint essential oil;
6) mixing transparent soap base and rose hydrosol, sealing with preservative film, heating in 80 deg.C water bath until transparent soap base is dissolved, and cooling at room temperature until the temperature of the mixture of transparent soap base and rose hydrosol is reduced to 52.5 deg.C;
7) adding sweet almond oil, wheat germ oil, jojoba oil and olive oil into the mixed solution of the transparent soap base and the rose hydrosol, stirring uniformly, adding concentrated solution of jaboticaba leaf extract, concentrated solution of gynura bicolor extract, citronella essential oil and mint essential oil, and stirring uniformly;
8) pouring the mixed liquid obtained in the step 7) into a mold, scraping off foams, standing for 1 h, freezing for 1 h at-20 ℃, forming, demolding, and placing in a shady and ventilated place for ventilation for 1.5 weeks (10 d) to obtain the jaboticaba leaf handmade soap.
Example 2
The jaboticaba leaf handmade soap is prepared from the following raw materials in parts by weight: sweet almond oil 0.6 parts, wheat germ oil 0.8 parts, jojoba oil 0.6 parts, olive oil 0.8 parts, transparent soap base 250 parts, rose hydrosol 55 parts, jaboticaba leaf extract concentrate 50 parts, gynura bicolor extract concentrate 30 parts, citronella essential oil 0.8 parts, and mint essential oil 0.8 parts;
the preparation method of the jaboticaba leaf handmade soap comprises the following steps:
1) putting rose petals and water into a steam distillation device according to the dosage ratio of 2.5 kg to 6L, extracting by adopting a steam distillation method, and collecting rose hydrosol;
2) drying fresh jaboticaba leaves in an oven at the temperature of 40 ℃ for 24 hours, then crushing by using a crusher, and sieving by using a 40-mesh sieve to obtain jaboticaba leaf fine powder; then mixing the fine powder of the jaboticaba leaves and 40% ethanol according to the weight ratio of 1: 55, placing the mixture in a constant-temperature shaking instrument, shaking and extracting for 20 hours at 25 ℃, then centrifuging for 20 min at 5500 rpm, and filtering to obtain an alcohol extract of the jaboticaba leaves; then placing the jaboticaba leaf alcohol extract in a rotary evaporator, carrying out rotary evaporation in water bath at 38 ℃ until no alcohol smell exists, and taking out to obtain jaboticaba leaf extract concentrated solution;
3) pulverizing fresh folium Nerviliae Fordii at a weight ratio of 1: 8, mixing with 65% ethanol, placing in a constant temperature shaking apparatus, shaking and extracting at 25 deg.C for 20 hr, centrifuging at 5500 rpm for 20 min, and filtering to obtain folium Nerviliae Fordii ethanol extract; then placing the gynura bicolor alcohol extract in a rotary evaporator, carrying out rotary evaporation in a water bath at 38 ℃ until no alcohol smell exists, and taking out to obtain a gynura bicolor extract concentrated solution;
4) cutting fresh citronella into 4-6 cm small sections, then placing the citronella and water in a steam distillation device according to the dosage ratio of 2.5 kg to 5L, and extracting by adopting a steam distillation method to obtain citronella essential oil;
5) according to the dosage ratio of 3.5 kg to 5L, putting fresh mint leaves and water in a steam distillation device, and extracting by adopting a steam distillation method to obtain mint essential oil;
6) mixing transparent soap base and rose hydrosol, sealing with preservative film, heating in 75 deg.C water bath until transparent soap base is dissolved, and cooling at room temperature until the temperature of the mixture of transparent soap base and rose hydrosol is reduced to 50 deg.C;
7) adding sweet almond oil, wheat germ oil, jojoba oil and olive oil into the mixed solution of the transparent soap base and the rose hydrosol, stirring uniformly, adding concentrated solution of jaboticaba leaf extract, concentrated solution of gynura bicolor extract, citronella essential oil and mint essential oil, and stirring uniformly;
8) pouring the mixed liquid obtained in the step 7) into a mold, scraping off foams, standing for 0.5 h, freezing for 0.5 h at-20 ℃, forming, demolding, and placing in a shady and ventilated place for 2 weeks to obtain the jaboticaba leaf handmade soap.
Example 3
The jaboticaba leaf handmade soap is prepared from the following raw materials in parts by weight: sweet almond oil 0.8 parts, wheat germ oil 0.6 parts, jojoba oil 0.8 parts, olive oil 0.6 parts, transparent soap base 320 parts, rose hydrosol 45 parts, jaboticaba leaf extract concentrate 70 parts, gynura bicolor extract concentrate 20 parts, citronella essential oil 1.2 parts, and mint essential oil 0.6-0.8 parts;
the preparation method of the jaboticaba leaf handmade soap comprises the following steps:
1) putting rose petals and water into a steam distillation device according to the dosage ratio of 3 kg to 6L, extracting by adopting a steam distillation method, and collecting rose hydrosol;
2) drying fresh jaboticaba leaves in an oven at the temperature of 50 ℃ for 20 hours, then crushing by using a crusher, and sieving by using a 35-mesh sieve to obtain jaboticaba leaf fine powder; then mixing the fine powder of the jaboticaba leaves and 35% ethanol according to the weight ratio of 1: 65, placing the mixture in a constant-temperature shaking instrument, shaking and extracting for 16 h at 30 ℃, then centrifuging for 15 min at 6500 rpm, and filtering to obtain an alcohol extract of the jaboticaba leaves; then placing the jaboticaba leaf alcohol extract in a rotary evaporator, carrying out rotary evaporation in water bath at 42 ℃ until no alcohol taste exists, and taking out to obtain jaboticaba leaf extract concentrated solution;
3) pulverizing fresh folium Nerviliae Fordii at a weight ratio of 1: 12, mixing with 65% ethanol, placing in a constant temperature shaking apparatus, shaking and extracting at 30 deg.C for 16 h, centrifuging at 6500 rpm for 15 min, and filtering to obtain folium Nerviliae Fordii ethanol extract; then placing the gynura bicolor alcohol extract in a rotary evaporator, carrying out rotary evaporation in water bath at 42 ℃ until no alcohol smell exists, and taking out to obtain a gynura bicolor extract concentrated solution;
4) cutting fresh citronella into 4-6 cm small sections, then placing the citronella and water in a steam distillation device according to the dosage ratio of 3.5 kg to 5L, and extracting by adopting a steam distillation method to obtain citronella essential oil;
5) according to the dosage ratio of 4.0 kg to 5L, putting fresh mint leaves and water in a steam distillation device, and extracting by adopting a steam distillation method to obtain mint essential oil;
6) mixing transparent soap base and rose hydrosol, sealing with preservative film, heating in 85 deg.C water bath until transparent soap base is dissolved, and cooling at room temperature until the temperature of the mixture of transparent soap base and rose hydrosol is reduced to 55 deg.C;
7) adding sweet almond oil, wheat germ oil, jojoba oil and olive oil into the mixed solution of the transparent soap base and the rose hydrosol, stirring uniformly, adding concentrated solution of jaboticaba leaf extract, concentrated solution of gynura bicolor extract, citronella essential oil and mint essential oil, and stirring uniformly;
8) pouring the mixed liquid obtained in the step 7) into a mold, scraping off foams, standing for 0.75 h, freezing for 0.8 h at-20 ℃, forming, demolding, and placing in a shady and ventilated place for ventilation for 1 week to obtain the jaboticaba leaf handmade soap.
The handmade soap is natural and safe, is in a light brown semitransparent state, is mild and non-irritating, has the flavor of jaboticaba leaves, the flavor of roses, the flavor of citronella and the flavor of mint, and is multifunctional handmade soap with the effects of resisting oxidation, sterilizing, relieving itching, repelling mosquitoes and the like.
The above description is only a preferred embodiment of the present invention, and all equivalent changes and modifications made in accordance with the claims of the present invention should be covered by the present invention.
Claims (3)
1. A manufacturing method of jaboticaba leaf handmade soap is characterized by comprising the following steps: the handmade soap is prepared from the following raw materials in parts by weight: 0.6-0.8 part of sweet almond oil, 0.6-0.8 part of wheat germ oil, 0.6-0.8 part of jojoba oil, 0.6-0.8 part of olive oil, 250-320 parts of transparent soap base, 45-55 parts of rose hydrosol, 50-70 parts of jaboticaba leaf extract concentrated solution, 20-30 parts of gynura bicolor extract concentrated solution, 0.8-1.2 parts of citronella essential oil and 0.6-0.8 part of mint essential oil;
the method comprises the following steps:
1) putting rose petals and water in a steam distillation device, extracting by adopting a steam distillation method, and collecting rose hydrosol;
2) drying fresh jaboticaba leaves, crushing, and sieving to obtain jaboticaba leaf fine powder, wherein the jaboticaba leaves are light red tender leaves of jaboticaba; mixing the jaboticaba leaf fine powder and 35-40% ethanol according to the weight ratio of 1: 55-65, placing the mixture in a constant-temperature oscillator, performing oscillation extraction at 25-30 ℃ for 16-20 h, centrifuging at the rotating speed of 5500-6500 rpm for 15-20 min, and filtering to obtain jaboticaba leaf ethanol extract; then placing the jaboticaba leaf alcohol extract in a rotary evaporator, carrying out rotary evaporation in water bath at 38-42 ℃ until 50-60% of the volume of the jaboticaba leaf alcohol extract is free of alcohol smell, and taking out to obtain jaboticaba leaf extract concentrated solution;
3) crushing fresh gynura bicolor leaves, mixing the crushed fresh gynura bicolor leaves with 65-70% ethanol according to the weight ratio of 1: 8-12, placing the mixture in a constant-temperature oscillator, performing oscillation extraction at 25-30 ℃ for 16-20 hours, centrifuging at the rotating speed of 5500-6500 rpm, and filtering to obtain a gynura bicolor ethanol extract; then placing the alcohol extract of gynura bicolor in a rotary evaporator, carrying out rotary evaporation in a water bath at 38-42 ℃ until 20-30% of the volume of the alcohol extract is free of alcohol smell, and taking out the alcohol extract to obtain a concentrated extract of gynura bicolor;
4) placing fresh citronella cut into 4-6 cm small sections and water in a steam distillation device, and extracting by adopting a steam distillation method to obtain citronella essential oil;
5) putting fresh mint leaves and water into a steam distillation device, and extracting by adopting a steam distillation method to obtain mint essential oil;
6) mixing the transparent soap base and the rose hydrosol, sealing the mixture with a preservative film, heating the mixture in a water bath at the temperature of 75-85 ℃ until the transparent soap base is dissolved, and cooling the mixture at room temperature until the temperature of the mixed solution of the transparent soap base and the rose hydrosol is reduced to 50-55 ℃;
7) adding sweet almond oil, wheat germ oil, jojoba oil and olive oil into the mixed solution of the transparent soap base and the rose hydrosol, stirring uniformly, adding concentrated solution of jaboticaba leaf extract, concentrated solution of gynura bicolor extract, citronella essential oil and mint essential oil, and stirring uniformly;
8) pouring the mixed liquid obtained in the step 7) into a mold, scraping off foams, standing for 0.5-1 h, freezing for 0.5-1 h at the temperature of-20 ℃ and below, demolding after freezing molding, and drying in a cool and ventilated place for 1-2 weeks to obtain the jaboticaba leaf handmade soap.
2. The manufacturing method of the jaboticaba leaf handmade soap according to claim 1, characterized in that: in the step 1), the dosage ratio of the rose petals to the water is 2.5-3.0 kg: 6L; in the step 4), the dosage ratio of the citronella to the water is 2.5-3.5 kg: 5L; in the step 5), the dosage ratio of the mint leaves to the water is 3.0-4.0 kg: 5L.
3. The manufacturing method of the jaboticaba leaf handmade soap according to claim 1, characterized in that: in the step 2), drying is carried out in an oven at the temperature of 40-50 ℃ for 20-24 h, and the particle size of the jaboticaba leaf fine powder is 35-40 meshes.
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