CN108464947A - Include the cosmetic composition and preparation method thereof of film forming agent and microsphere particle - Google Patents
Include the cosmetic composition and preparation method thereof of film forming agent and microsphere particle Download PDFInfo
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- CN108464947A CN108464947A CN201810327093.7A CN201810327093A CN108464947A CN 108464947 A CN108464947 A CN 108464947A CN 201810327093 A CN201810327093 A CN 201810327093A CN 108464947 A CN108464947 A CN 108464947A
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- film forming
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- cosmetic composition
- forming agent
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- 239000000203 mixture Substances 0.000 title claims abstract description 41
- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 30
- 239000002537 cosmetic Substances 0.000 title claims abstract description 29
- 239000002245 particle Substances 0.000 title claims abstract description 25
- 239000004005 microsphere Substances 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims description 18
- 239000000516 sunscreening agent Substances 0.000 claims abstract description 54
- 230000000475 sunscreen effect Effects 0.000 claims abstract description 18
- 239000000654 additive Substances 0.000 claims abstract description 16
- 230000000996 additive effect Effects 0.000 claims abstract description 16
- 229920001577 copolymer Polymers 0.000 claims description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
- 239000003921 oil Substances 0.000 claims description 21
- 150000002148 esters Chemical class 0.000 claims description 19
- 235000019198 oils Nutrition 0.000 claims description 19
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- 239000004519 grease Substances 0.000 claims description 14
- 239000004909 Moisturizer Substances 0.000 claims description 12
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 12
- 239000003995 emulsifying agent Substances 0.000 claims description 12
- 230000001333 moisturizer Effects 0.000 claims description 12
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 10
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 10
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 10
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 10
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- VAMFXQBUQXONLZ-UHFFFAOYSA-N n-alpha-eicosene Natural products CCCCCCCCCCCCCCCCCCC=C VAMFXQBUQXONLZ-UHFFFAOYSA-N 0.000 claims description 9
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- 229920000642 polymer Polymers 0.000 claims description 8
- 229910052708 sodium Inorganic materials 0.000 claims description 8
- 239000011734 sodium Substances 0.000 claims description 8
- 230000003020 moisturizing effect Effects 0.000 claims description 7
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- 238000003756 stirring Methods 0.000 claims description 6
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 5
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 5
- 229920001285 xanthan gum Polymers 0.000 claims description 5
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 4
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims description 4
- FMRHJJZUHUTGKE-UHFFFAOYSA-N Ethylhexyl salicylate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1O FMRHJJZUHUTGKE-UHFFFAOYSA-N 0.000 claims description 4
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- CBTVGIZVANVGBH-UHFFFAOYSA-N aminomethyl propanol Chemical compound CC(C)(N)CO CBTVGIZVANVGBH-UHFFFAOYSA-N 0.000 claims description 4
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- SMITZRKODWNNBA-UHFFFAOYSA-N hexadecyl dihydrogen phosphate;potassium Chemical compound [K].CCCCCCCCCCCCCCCCOP(O)(O)=O SMITZRKODWNNBA-UHFFFAOYSA-N 0.000 claims description 4
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims description 4
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- 239000004408 titanium dioxide Substances 0.000 claims description 4
- MXOAEAUPQDYUQM-QMMMGPOBSA-N (S)-chlorphenesin Chemical compound OC[C@H](O)COC1=CC=C(Cl)C=C1 MXOAEAUPQDYUQM-QMMMGPOBSA-N 0.000 claims description 3
- FBYFHODQAUBIOO-UHFFFAOYSA-N 2-(1-carboxyethoxy)propanoic acid Chemical compound OC(=O)C(C)OC(C)C(O)=O FBYFHODQAUBIOO-UHFFFAOYSA-N 0.000 claims description 3
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 3
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- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims description 3
- 229960003993 chlorphenesin Drugs 0.000 claims description 3
- JDRSMPFHFNXQRB-IBEHDNSVSA-N decyl glucoside Chemical compound CCCCCCCCCCO[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O JDRSMPFHFNXQRB-IBEHDNSVSA-N 0.000 claims description 3
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 claims description 3
- NOPFSRXAKWQILS-UHFFFAOYSA-N docosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCO NOPFSRXAKWQILS-UHFFFAOYSA-N 0.000 claims description 3
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- 238000004945 emulsification Methods 0.000 claims description 3
- 230000001804 emulsifying effect Effects 0.000 claims description 3
- UVCJGUGAGLDPAA-UHFFFAOYSA-N ensulizole Chemical compound N1C2=CC(S(=O)(=O)O)=CC=C2N=C1C1=CC=CC=C1 UVCJGUGAGLDPAA-UHFFFAOYSA-N 0.000 claims description 3
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- 238000011049 filling Methods 0.000 claims description 3
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- 239000006210 lotion Substances 0.000 claims description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 3
- FMJSMJQBSVNSBF-UHFFFAOYSA-N octocrylene Chemical compound C=1C=CC=CC=1C(=C(C#N)C(=O)OCC(CC)CCCC)C1=CC=CC=C1 FMJSMJQBSVNSBF-UHFFFAOYSA-N 0.000 claims description 3
- 229960000601 octocrylene Drugs 0.000 claims description 3
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 3
- 229940010747 sodium hyaluronate Drugs 0.000 claims description 3
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims description 3
- 125000003696 stearoyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 3
- 238000003786 synthesis reaction Methods 0.000 claims description 3
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- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 claims description 3
- 239000011787 zinc oxide Substances 0.000 claims description 3
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 claims description 2
- DMBUODUULYCPAK-UHFFFAOYSA-N 1,3-bis(docosanoyloxy)propan-2-yl docosanoate Chemical compound CCCCCCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCCCCCC DMBUODUULYCPAK-UHFFFAOYSA-N 0.000 claims description 2
- JGUMTYWKIBJSTN-UHFFFAOYSA-N 2-ethylhexyl 4-[[4,6-bis[4-(2-ethylhexoxycarbonyl)anilino]-1,3,5-triazin-2-yl]amino]benzoate Chemical compound C1=CC(C(=O)OCC(CC)CCCC)=CC=C1NC1=NC(NC=2C=CC(=CC=2)C(=O)OCC(CC)CCCC)=NC(NC=2C=CC(=CC=2)C(=O)OCC(CC)CCCC)=N1 JGUMTYWKIBJSTN-UHFFFAOYSA-N 0.000 claims description 2
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- ZDHRAACDPXUCHC-UHFFFAOYSA-N 3,4-diethyl-2-hexoxyphenol;5-methoxy-4-phenyltriazine Chemical compound COC1=CN=NN=C1C1=CC=CC=C1.CCCCCCOC1=C(O)C=CC(CC)=C1CC ZDHRAACDPXUCHC-UHFFFAOYSA-N 0.000 claims description 2
- 125000006181 4-methyl benzyl group Chemical group [H]C1=C([H])C(=C([H])C([H])=C1C([H])([H])[H])C([H])([H])* 0.000 claims description 2
- KBIWNQVZKHSHTI-UHFFFAOYSA-N 4-n,4-n-dimethylbenzene-1,4-diamine;oxalic acid Chemical compound OC(=O)C(O)=O.CN(C)C1=CC=C(N)C=C1 KBIWNQVZKHSHTI-UHFFFAOYSA-N 0.000 claims description 2
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- QYSXJUFSXHHAJI-XFEUOLMDSA-N Vitamin D3 Natural products C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C/C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-XFEUOLMDSA-N 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000005856 abnormality Effects 0.000 description 1
- 229920006243 acrylic copolymer Polymers 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 239000013590 bulk material Substances 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 229940082500 cetostearyl alcohol Drugs 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- KYKAJFCTULSVSH-UHFFFAOYSA-N chloro(fluoro)methane Chemical compound F[C]Cl KYKAJFCTULSVSH-UHFFFAOYSA-N 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 238000000205 computational method Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000007334 copolymerization reaction Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- DTPCFIHYWYONMD-UHFFFAOYSA-N decaethylene glycol Chemical compound OCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO DTPCFIHYWYONMD-UHFFFAOYSA-N 0.000 description 1
- FDATWRLUYRHCJE-UHFFFAOYSA-N diethylamino hydroxybenzoyl hexyl benzoate Chemical compound CCCCCCOC(=O)C1=CC=CC=C1C(=O)C1=CC=C(N(CC)CC)C=C1O FDATWRLUYRHCJE-UHFFFAOYSA-N 0.000 description 1
- 239000004205 dimethyl polysiloxane Substances 0.000 description 1
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000004088 foaming agent Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 229920001519 homopolymer Polymers 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- XUGNVMKQXJXZCD-UHFFFAOYSA-N isopropyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(C)C XUGNVMKQXJXZCD-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000000593 microemulsion method Methods 0.000 description 1
- 229940105132 myristate Drugs 0.000 description 1
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 230000019612 pigmentation Effects 0.000 description 1
- 239000011505 plaster Substances 0.000 description 1
- 229920000136 polysorbate Polymers 0.000 description 1
- 229950008882 polysorbate Drugs 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 230000004224 protection Effects 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000012925 reference material Substances 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 231100000444 skin lesion Toxicity 0.000 description 1
- 206010040882 skin lesion Diseases 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000005437 stratosphere Substances 0.000 description 1
- OULAJFUGPPVRBK-UHFFFAOYSA-N tetratriacontyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO OULAJFUGPPVRBK-UHFFFAOYSA-N 0.000 description 1
- 238000010257 thawing Methods 0.000 description 1
- 235000019166 vitamin D Nutrition 0.000 description 1
- 239000011710 vitamin D Substances 0.000 description 1
- 150000003710 vitamin D derivatives Chemical class 0.000 description 1
- 229940046008 vitamin d Drugs 0.000 description 1
- 238000004078 waterproofing Methods 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
- 229910052724 xenon Inorganic materials 0.000 description 1
- FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 description 1
Classifications
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
- A61K8/0279—Porous; Hollow
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- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0204—Specific forms not provided for by any of groups A61K8/0208 - A61K8/14
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4966—Triazines or their condensed derivatives
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- A61K8/55—Phosphorus compounds
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
- A61K8/8182—Copolymers of vinyl-pyrrolidones. Compositions of derivatives of such polymers
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
Landscapes
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- Cosmetics (AREA)
Abstract
The invention discloses a kind of cosmetic compositions, which is characterized in that includes at least one film forming agent and at least one microsphere particle.The sunscreen composition improves the service efficiency of sun-screening agent, to reduce the additive amount of sun-screening agent, and then reduce the safety issue brought due to high sun-screening agent dosage and it is greasy, spreadability is poor the problems such as.
Description
Technical field
The invention belongs to cosmetic field more particularly to a kind of sun care preparations combinations comprising film forming agent and microsphere particle
Object and preparation method thereof.
Background technology
Tellurian overwhelming majority biology, the especially existence of the mankind be unable to do without sunlight, wherein including ultraviolet light
(UV).Ultraviolet light (UV), which is conducive to synthesis in human body, can help the calcareous vitamin D deposited in bone, however due to people
Class largely uses refrigerant, foaming agent, the chloro-fluoro-carbon kind compound in cleaning agent and the polytetrafluoroethyl-ne alkenes as extinguishing chemical
Object is closed, the ozone (O in stratosphere is caused3) depletion, so that the ultraviolet radiation in earth surface environment sunlight is increased, excessive
Ultraviolet radioactive can cause a variety of skin lesions, such as sunburn, pigmentation, wrinkle, light aging, DNA damage, benign and malignant tumour
Deng therefore, being become more and more important for ultraviolet protection.
The sun care preparations type for being directed to ultraviolet protection on the market at present is various, and consumer prevents spf value, high PA values
The demand for shining cosmetics is also higher and higher.Sun-screening agent is the key substance that anti-sunlight function is played in sun care preparations, by protective action
Mechanism can be divided into physical sunscreen agent (i.e. ultraviolet light screener shields to skin by reflection and scatters ultraviolet), change
Sun-screening agent is learned (by absorbing the energy of ultraviolet light, then to release with thermal energy or harmless visible luminous effect, to protect people
Injury of the body skin from ultraviolet light) and natural biological sun-screening agent (i.e. pass through adjust skin immune function controlling, enhancing cell live
Property, resist and repair radiation injury, to cooperate with enhancing chemical sun that can resist the bioactive substance of ultraviolet radioactive).
So far the sun-screening agent developed in the world has more than 60 and plants, but since sun-screening agent is chemical substance, safety is
Various countries are paid attention to, some sun-screening agents have been removed from approval or the inventory that uses of interim approval or its safety due to safety problem
Property be reassessed in a timely manner, facing reduces usage amount or cancels the pressure that uses or predicament.By conventional art level, traditionally high SPF
A large amount of sun-screening agent is added in the sun care preparations requirement of value, PA values.Since generally there are certain safety issues for sun-screening agent, and
Mostly greasy, spreadability is poor or powdered ester type compound, sun-screening agent is largely added, in addition to there are potential security risks
Outside, it is also easy to cause sun care preparations is greasy, spreadability is poor etc. to use sense of discomfort.
Therefore, it is possible to provide high spf value, PA values, and effectively reduce sun-screening agent dosage technology or invention it is more and more important.
Invention content
In view of the problems of the above-mentioned prior art, include film forming agent and microsphere particle the purpose of the present invention is to propose to one kind
Cosmetic composition and preparation method thereof.
The purpose of the present invention will be achieved by the following technical programs：A kind of cosmetic composition, including at least
A kind of film forming agent and at least one microsphere particle.
Wherein, the microsphere particle that the present invention uses is grain size in nanometer to micron range, hollow micro- with hollow cavity
Ball particle.Usually it is made by template, spray drying process, original flavor Hydrolyze method, gel method, microemulsion method, gravity Method etc., with
Traditional solid, bulk material are compared, and tiny balloon particle has larger specific surface area, smaller density, good mobility
With the physical properties such as special mechanics, light, electricity.For example, styrene/acrylic (ester) analog copolymer be it is a kind of utilize hollow ball
The microsphere particle polymer of technology causes ultraviolet light anti-by the difference of the refraction coefficient between shell itself and boring
It shines and generates bending of light and scattering in film, to extend the propagation path of light.A large amount of hollow ball forms ten hundreds of
" scattering center " largely increases the possibility that UV ray is contacted with sun-screening agent, is penetrated to UV to increase sun-screening agent
The absorptivity of line, and then the spf value of sun care preparations, PA values are improved, reduce the safety brought by the high dosage of sun-screening agent
Problem and it is greasy, spreadability is poor the problems such as.
Film forming agent according to the present invention is homopolymer, copolymer or the cross-linked polymeric that hydrophobic grouping is carried on strand
Object is generally dissolved in water, alcohol or oil phase, contributes to the dispersion of powder in cosmetic composition, when addition water resistant film forming agent
After sunscreen product smearing is dried on the skin, one layer of film continuous, not soluble in water can be formed.Since most sun-screening agents are hydrophobicitys
, and film forming agent has hydrophobic and hydrophilic radical simultaneously, the water resistant film forming agent with hydrophilic radical can migrate in the presence of water
To the surface contacted with water, self-control covering, package sun-screening agent make sun-screening agent be not easy to be washed with water, to play waterproof
Anti- sweat effect, effectively improves the effect that sunscreen product resists ultraviolet light, and then improves the component in cosmetic composition in skin
The durable activity on surface achievees the effect that durable water resistant, anti-sweat.
Film forming agent according to the present invention is applied in sun care preparations, can effectively help powder in sun care preparations
The dispersion of (such as physical sunscreen agent titanium dioxide, zinc oxide, microsphere particle) improves the sun-screening agent in sun care preparations in skin table
The stop in face, and then the loss of the skin surface sun-screening agent caused by rainwater, sweat etc. rinse skin is reduced, indirectly improve
Spf value, PA values extend sun-screening agent and resist the time that ultraviolet light radiates skin, and then realize and protect skin from ultraviolet light spoke
Shoot harmful purpose wounded.
Preferably, by weight percentage, the film forming agent is 0.01%~10.00%, and the microsphere particle is
0.01%~20.00%；Preferably, the film forming agent be 0.1%~5.00%, the microsphere particle be 0.1%~
10.00%.
Preferably, the film forming agent be selected from acrylic copolymer, polyvinyl compound, polyethylene crosslinking polymer,
Ethanedioic acid polymer, aqueous polyurethane, vinylpyrrolidone copolymer, it is preferable that the film forming agent is selected from VP/ eicosylenes
Copolymer, acrylic acid (ester) class/C12-22 alkanols methacrylate copolymer, octylpyrrolidone, the copolymerization of VP/ hexadecenes
One kind or combinations thereof in object, trimethylsiloxysilicates；
The microsphere particle is selected from one kind or combinations thereof in silica or styrene/acrylic (ester) analog copolymer.
Preferably, cosmetic composition further includes sun-screening agent, moisturizing grease, emulsifier, moisturizer, water, additive.
Preferably, in terms of by weight percent for 100%, including following component：
Sun-screening agent 0.10%~50.00%, film forming agent 0.10-5.00%, microsphere particle 0.10-10.00%, moisturizing grease
0.10-30.00%, emulsifier 0.10-10.00%, moisturizer 0.10-20.00%, water 0.10-80.00%, additive 0.01-
5.00%.
Preferably, the one kind or combinations thereof of the sun-screening agent in inorganic sunscreen and Orangic sunscreen；
One kind in plant source grease, animal sources grease, petroleum source grease, Synthetic Oil of the moisturizing grease or its
Combination；
The one kind or combinations thereof of the emulsifier in oil-water emulsifiers and water-in-oil emulsifier；
The one kind or combinations thereof of the moisturizer in natural origin moisturizer and synthesis moisturizer；
The additive includes one kind or combinations thereof in essence, thickener, pH adjusting agent, preservative, chelating agent.
Preferably, the one kind or combinations thereof of the inorganic sunscreen in titanium dioxide and zinc oxide；
The Orangic sunscreen be selected from Avobenzone, butylmethoxy hexichol be acylated methane, Homosalate, Octocrilene,
Ethylhexyl methoxy cinnamate, ethylhexyl salicylate, benzophenone-3, Phenylbenzimidazolesulfonic acid, Uvinul T 150,
Uvinul A Plus, bis-ethylhexoxyphenol methoxyphenyl triazine, di-2-ethylhexylphosphine oxide-benzotriazole base
One kind or combinations thereof in tetramethyl butyl phenol, Dimethicodiethylbenzalmalonate, 4- methyl benzyl subunits camphor, UVNUL MS-40, benzophenone -5；
The moisturizing grease be selected from jojoba seed oil, Butyrospermum parkii fruit fat, saualane, horse fat, dormant oil, vaseline, paraffin,
C12-15 alcohol benzoic ethers, docosyl alcohol, dimethyl silicone polymer, ring five dimethyl silicone polymer, octyl polymethyl siloxane, whale
One kind or combinations thereof in wax stearyl alcohol, isopropyl palmitate etc.；
The emulsifier be selected from five stearate of Natrulon H-10, PEG-100 stearates, stearoyl dilactic acid sodium,
C12-20 alkyl glucosides, Phosphoric acid monohexadecyl ester potassium, tribehenin essence PEG-20 esters, polysorbate -20, Natrulon H-10 meat
The smooth olive oleate of myristate, Plantacare 818, sorb, lauryl PEG-9 polydimethylsiloxanes ethyl polydimethylsiloxanes
One kind or combinations thereof in alkane, PEG-10 Polydimethylsiloxane etc.；
The moisturizer be selected from glycerine, glycine betaine, Sodium Hyaluronate, butanediol, propylene glycol, 1,3-PD, pungent glycol,
One kind or combinations thereof in dipropylene glycol, Sensiva SC50, ethoxy urea, polyglutamic acid sodium；
The additive be selected from essence, xanthans, ammonium acryloyl taurate/VP copolymer, acrylic acid (ester) class/
C10-30 alkylol acrylamide acid esters cross-linked polymer, aminomethyl propanol, tetra- sodium of EDTA, EDTA disodiums, Phenoxyethanol, Chlorphenesin
Middle one kind or combinations thereof.
A kind of preparation method of cosmetic composition, includes the following steps：
1) each component for belonging to oil phase is added in oil phase pot, while being heated with stirring to 82-87 DEG C, rotating speed 10-50rpm fills
Divide and be stirred until homogeneous, obtains oil mixture；
2) each component for belonging to water phase is added in water phase pot, while being heated with stirring to 82-87 DEG C, rotating speed 10-50rpm fills
Divide and be stirred until homogeneous, obtains aqueous mixture；
3) by oil mixture, aqueous mixture pass sequentially through strainer valve be pumped into vacuum emulsification pot in, with rotating speed be 30~
35rpm is stirred, and is then that 2500~3200rpm progress homogeneous is uniform to emulsifying, then speed of agitator is down to 10 with rotating speed
~30rpm is cooled to 45 DEG C, and additive is added, continues to discharge after being stirred until homogeneous；
4) after detection is qualified it is filling to get.
A kind of sunscreen product including above-mentioned cosmetic composition, the sunscreen product includes suncream, sun-proof
Lotion or sunscreen spray.
Compared with prior art, a kind of cosmetic composition including film forming agent and microsphere particle provided by the invention
And preparation method thereof, what is reached has the technical effect that：The present invention scientifically and rationally combines film forming agent and microsphere particle, is applied to anti-
It shines in composition, improves the service efficiency of sun-screening agent, to reduce the additive amount of sun-screening agent, and then reduce since high sun-screening agent is used
Measure the safety issue brought and it is greasy, spreadability is poor the problems such as.
Below just in conjunction with the embodiments and attached drawing, the embodiment of the present invention is described in further detail, so that technology
Scheme is more readily understood, grasps.
Description of the drawings
Fig. 1 is the waterproof effect test chart of the film forming agent (VP/ eicosene copolymers) of test example 2.
Specific implementation mode
Below by specific embodiment, the present invention will be described, but the present invention is not limited thereto.In following embodiments
The experimental method is unless otherwise specified conventional method；The reagent and material unless otherwise specified can be from business
Approach obtains, and following example is not to limit the scope of the claims of the present invention, all equivalence enforcements without departing from carried out by the present invention
Or change, it is intended to be limited solely by the scope of this patent.
The preparation method of cosmetic composition：1) each component for belonging to oil phase is added in oil phase pot, side stirring adds
Heat is stirred well to uniformly to 82-87 DEG C, rotating speed 10-50rpm, obtains oil mixture；
2) each component for belonging to water phase is added in water phase pot, while being heated with stirring to 82-87 DEG C, rotating speed 10-50rpm fills
Divide and be stirred until homogeneous, obtains aqueous mixture；
3) by oil mixture, aqueous mixture pass sequentially through strainer valve be pumped into vacuum emulsification pot in, with rotating speed be 30~
35rpm is stirred, and is then that 2500~3200rpm progress homogeneous is uniform to emulsifying, then speed of agitator is down to 10 with rotating speed
~30rpm is cooled to 45 DEG C, and additive is added, continues to discharge after being stirred until homogeneous；
4) after detection is qualified it is filling to get.
1 cosmetic composition of embodiment
The cosmetic composition of the present embodiment is composed of the following components：1) oil phase：Octocrilene 5.00%, C12-
15 alcohol benzoic ethers 2.00%, ethylhexyl salicylate 6.00%, butyl methoxy dibenzoyl methane 5.00%, docosyl alcohol
(and) five stearate of Natrulon H-10 (and) stearoyl dilactic acid sodium 2.00%, titanium dioxide (and) dimethyl silicone polymer
4.50%, ring five dimethyl silicone polymer 5.00%, dimethyl silicone polymer 3.00%, polyvinylpyrrolidone/eicosylene
Copolymer 2.00%；
2) water phase：Water 50.20%, butanediol 8.00%, Phenylbenzimidazolesulfonic acid 3.00%, styrene/acrylic
(ester) analog copolymer 0.50%, Phosphoric acid monohexadecyl ester potassium 1.50%, xanthans 0.20%, tetra- sodium 0.05% of EDTA；
3) additive：Aminomethyl propanol 1.05%, Phenoxyethanol (and) Sensiva SC50 0.60%, 1,3- propylene glycol
(and) pungent glycol 0.30%, essence 0.10%.
2 cosmetic composition of embodiment
The cosmetic composition of the present embodiment is composed of the following components：1) oil phase：Ethylhexyl methoxy cinnamate
5.00%, ring five dimethyl silicone polymer 6.00%, cetostearyl alcohol 1.50%, ethylhexyl salicylate 5.00%, ethyl hexyl
Base triazinone 3.50%, ring five dimethyl silicone polymer (and) trimethylsiloxysilicates 1.50%, diethylamino oxybenzene formyl
The own ester 2.00% of yl benzoic acid, octyl polymethyl siloxane 1.00%；
2) water phase：Water 56.30%, polysorbate -200.50%, Phosphoric acid monohexadecyl ester potassium 0.80%, styrene/propylene
Sour (ester) analog copolymer 2.50%, Natrulon H-10 myristinate 0.50%, Sodium Hyaluronate 0.10%, glycine betaine 1.50%,
Ammonium acryloyl taurate/VP copolymer 0.60%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymerics
Object 0.40%, EDETATE SODIUM 0.10%, propylene glycol 8.00%, xanthans 0.15%, water (and) di-2-ethylhexylphosphine oxide-benzotriazole base four
Methyl butyl phenol (and) Plantacare 818 (and) propylene glycol (and) xanthans 2.00%；
3) additive：Aminomethyl propanol 0.10%, Phenoxyethanol (and) pungent glycol (and) Chlorphenesin 0.80%, essence
0.15%.
Embodiment 3 is with embodiment 2 the difference is that " trimethyl silicane alkoxy esters of silicon acis " is changed to " VP/ 20
Carbene copolymer ".
Embodiment 4-7
Embodiment 4-7 is identical with the type of the sun-screening agent of embodiment 3 and additive amount, the difference is that film forming agent and
The type or content of microsphere particle are different, are specifically shown in Table 1.
The content difference of 1 film forming agent of table and microsphere particle is to sun-proof influence
Compared with embodiment 1-7, the dosage of film forming agent or microsphere particle, sun protection factor are increased significantly in comparative example 4,5
Be not obviously improved, but will appear skin sense is greasy, spreadability is poor, smear after the appearance poor usage experience such as unnatural or go out
Now stablize sexual abnormality.
Test example 1
The indices of the embodiment 1-7 cosmetic compositions prepared are subjected to performance detection, are as a result met as follows
Standard：
Lotion appearance：White smooth emulsion；
Stability：Heat-resisting 50 DEG C, 1 month stable testing；It is -15 DEG C to -5 DEG C cold-resistant, 4 freeze thawing, a month low-temperature stabilization；
Illumination, 1 month stable testing；
Use feeling：When smearing on the skin, skin sense silk is sliding, easily sprawls, without greasy and sense of closure；
UV protecting factors：Embodiment 1 is SPF43PA+++, embodiment 2 is SPF47PA++++, embodiment 3 is SPF45PA
+++, the protecting factor of embodiment 4-7 is shown in Table 1；
Foundation：《Cosmetics health specification》(version in 2015)；
Standard reference material：Spf value 3.751.01 is prepared by Japan's JCIA standard recipes；
Subject：Totally 10 people, male 8 people, 2 people of female, age 23-48 Sui, average age 34.009.35 Sui；Light source：Daylight
Simulator xenon arc lamp；
The method of inspection：According to《Sun care preparations long wave ultraviolet protection index assay method》Specific requirement carries out；
The computational methods of spf value：SPF=does not add the MED of the MED/ sample protecting skins of protecting skin.
The waterproof effect of 2 film forming agent of test example (VP/ eicosene copolymers) is tested
Experimental subjects：Embodiment 3, comparative example 1
Comparative example 1 is with embodiment 3 the difference is that deleting " VP/ eicosene copolymers ".
This test example is the waterproof effect for verifying " VP/ eicosene copolymers " in sunscreen product, is removed using adhesive plaster
Method by a kind of embodiment 3 containing " VP/ eicosene copolymers " and does not contain the same anti-of " VP/ eicosene copolymers "
The comparative example 1 of solarization composition is done water proofing property and is compared, and the results are shown in Figure 1, illustrates the waterproof effect of the embodiment 3 because of addition " VP/
Eicosene copolymer " and have improvement greatly.In addition, because not adding film forming agent " VP/ eicosene copolymers ", sun protection factor also by
SPF45 PA+++ drop to SPF40 PA++.
Several preferred embodiments of the present invention have shown and described in above description, but as previously described, it should be understood that the present invention
Be not limited to form disclosed herein, be not to be taken as excluding other embodiments, and can be used for various other combinations,
Modification and environment, and the above teachings or related fields of technology or knowledge can be passed through in the scope of the invention is set forth herein
It is modified.And changes and modifications made by those skilled in the art do not depart from the spirit and scope of the present invention, then it all should be in this hair
In the protection domain of bright appended claims.
Claims (9)
1. a kind of cosmetic composition, which is characterized in that include at least one film forming agent and at least one microsphere particle.
2. cosmetic composition according to claim 1, which is characterized in that by weight percentage, the film forming
Agent is 0.01%~10.00%, and the microsphere particle is 0.01%~20.00%；Preferably, the film forming agent be 0.1%~
5.00%, the microsphere particle is 0.1%~10.00%.
3. cosmetic composition according to claim 1, which is characterized in that the film forming agent is total selected from acrylic compounds
Polymers, polyvinyl compound, polyethylene crosslinking polymer, ethanedioic acid polymer, aqueous polyurethane, vinyl pyrrolidone are total
Polymers, it is preferable that the film forming agent is selected from VP/ eicosene copolymers, acrylic acid (ester) class/C12-22 alkanol methacrylic acids
One kind or combinations thereof in ester copolymer, octylpyrrolidone, VP/ hexadecene copolymers, trimethylsiloxysilicates；
The microsphere particle is selected from one kind or combinations thereof in silica or styrene/acrylic (ester) analog copolymer.
4. according to claim 1-3 any one of them cosmetic compositions, which is characterized in that further include sun-screening agent, profit
Skin grease, emulsifier, moisturizer, water, additive.
5. cosmetic composition according to claim 4, which is characterized in that by weight percent be 100% in terms of, packet
Include following component：
Sun-screening agent 0.10%~50.00%, film forming agent 0.10-5.00%, microsphere particle 0.10-10.00%, moisturizing grease
0.10-30.00%, emulsifier 0.10-10.00%, moisturizer 0.10-20.00%, water 0.10-80.00%, additive 0.01-
5.00%.
6. cosmetic composition according to claim 4, which is characterized in that the sun-screening agent is selected from inorganic sunscreen
With one kind or combinations thereof in Orangic sunscreen；
The one kind or its group of the moisturizing grease in plant source grease, animal sources grease, petroleum source grease, Synthetic Oil
It closes；
The one kind or combinations thereof of the emulsifier in oil-water emulsifiers and water-in-oil emulsifier；
The one kind or combinations thereof of the moisturizer in natural origin moisturizer and synthesis moisturizer；
The one kind or combinations thereof of the additive in essence, thickener, pH adjusting agent, preservative, chelating agent.
7. cosmetic composition according to claim 6, which is characterized in that the inorganic sunscreen is selected from titanium dioxide
One kind in titanium and zinc oxide or combinations thereof；
The Orangic sunscreen is selected from Avobenzone, butylmethoxy hexichol is acylated methane, Homosalate, Octocrilene, methoxy
Base 2-Ethylhexyl cinnamate, ethylhexyl salicylate, benzophenone-3, Phenylbenzimidazolesulfonic acid, Uvinul T 150, diethyl
The own ester of amino oxybenzene formylbenzoate, bis-ethylhexoxyphenol methoxyphenyl triazine, di-2-ethylhexylphosphine oxide-benzotriazole base tetramethyl
One kind or combinations thereof in base butylphenol, Dimethicodiethylbenzalmalonate, 4- methyl benzyl subunits camphor, UVNUL MS-40, benzophenone -5；
The moisturizing grease is selected from jojoba seed oil, Butyrospermum parkii fruit fat, saualane, horse fat, dormant oil, vaseline, paraffin, C12-15
Alcohol benzoic ether, docosyl alcohol, dimethyl silicone polymer, ring five dimethyl silicone polymer, octyl polymethyl siloxane, cetearyl alcohol
One kind or combinations thereof in alcohol, isopropyl palmitate；
The emulsifier is selected from five stearate of Natrulon H-10, PEG-100 stearates, stearoyl dilactic acid sodium, C12-20
Alkyl glucoside, Phosphoric acid monohexadecyl ester potassium, tribehenin essence PEG-20 esters, polysorbate -20, Natrulon H-10 myristic acid
The smooth olive oleate of ester, Plantacare 818, sorb, lauryl PEG-9 Polydimethylsiloxyethyl Dimethicone, PEG-
One kind or combinations thereof in 10 dimethyl silicone polymers；
The moisturizer is selected from glycerine, glycine betaine, Sodium Hyaluronate, butanediol, propylene glycol, 1,3-PD, pungent glycol, double third
One kind or combinations thereof in glycol, Sensiva SC50, ethoxy urea, polyglutamic acid sodium；
The additive is selected from essence, xanthans, ammonium acryloyl taurate/VP copolymer, acrylic acid (ester) class/C10-
One in 30 alkylol acrylamide acid esters cross-linked polymers, aminomethyl propanol, tetra- sodium of EDTA, EDETATE SODIUM, Phenoxyethanol, Chlorphenesin
Kind or combinations thereof.
8. a kind of preparation method of cosmetic composition according to claim 4, which is characterized in that including walking as follows
Suddenly：1) each component for belonging to oil phase is added in oil phase pot, while being heated with stirring to 82-87 DEG C, rotating speed 10-50rpm is sufficiently stirred
To uniform, oil mixture is obtained；
2) each component for belonging to water phase is added in water phase pot, while being heated with stirring to 82-87 DEG C, rotating speed 10-50rpm is fully stirred
It mixes to uniform, obtains aqueous mixture；
3) oil mixture, aqueous mixture are passed sequentially through strainer valve to be pumped into vacuum emulsification pot, with rotating speed for 30~35rpm
It is stirred, it is uniform to emulsifying then to be that 2500~3200rpm carries out homogeneous with rotating speed, then speed of agitator is down to 10~
30rpm is cooled to 45 DEG C, and additive is added, continues to discharge after being stirred until homogeneous；
4) after detection is qualified it is filling to get.
9. a kind of sunscreen product including claim 1-7 any one of them cosmetic compositions, which is characterized in that institute
It includes suncream, ultra light sun block lotion or sunscreen spray to state sunscreen product.
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| CN115089505A (en) * | 2022-07-08 | 2022-09-23 | 上海百雀羚生物科技有限公司 | Synergistic film-forming agent composition and application thereof |
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Application publication date: 20180831 |