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CN108445017A - A kind of supper-fast silicon substrate surface quality detecting system - Google Patents

A kind of supper-fast silicon substrate surface quality detecting system Download PDF

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CN108445017A
CN108445017A CN201810215816.4A CN201810215816A CN108445017A CN 108445017 A CN108445017 A CN 108445017A CN 201810215816 A CN201810215816 A CN 201810215816A CN 108445017 A CN108445017 A CN 108445017A
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silicon
surface quality
fiber
lens
quality detection
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李朝晖
王绍祥
冯元华
甄智燊
吴振华
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Sun Yat Sen University
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    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
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    • G01N21/84Systems specially adapted for particular applications
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Abstract

本发明涉及硅基表面质量检测的技术领域,更具体地,涉及一种超快速的硅基表面质量检测系统。包括以下装置:锁模飞秒脉冲光源,中红外光波滤波器,色散光纤,掺铒光纤放大器(EDFA),衍射光栅,基于透镜组成的4f成像系统,物镜,数字相干接收机,高速采样示波器以及数据处理恢复所需的电脑。另外还包括所需要用到的环形器,耦合器,光纤,光纤偏振控制器,准直器等。

The invention relates to the technical field of silicon-based surface quality detection, and more particularly relates to an ultra-fast silicon-based surface quality detection system. Including the following devices: mode-locked femtosecond pulse light source, mid-infrared light wave filter, dispersive fiber, erbium-doped fiber amplifier (EDFA), diffraction grating, 4f imaging system based on lens, objective lens, digital coherent receiver, high-speed sampling oscilloscope and Computers required for data processing and restoration. In addition, it also includes the required circulators, couplers, optical fibers, optical fiber polarization controllers, collimators, etc.

Description

一种超快速的硅基表面质量检测系统An ultra-fast silicon-based surface quality detection system

技术领域technical field

本发明涉及硅基表面质量检测的技术领域,更具体地,涉及一种超快速的硅基表面质量检测系统。The invention relates to the technical field of silicon-based surface quality detection, and more particularly relates to an ultra-fast silicon-based surface quality detection system.

背景技术Background technique

硅半导体材料目前是当今许多工业上的一种非常关键的基础材料。硅半导体对清洁能源和军事工业等产业的发展具有相当重要的作用。世界上目前90%以上的半导体器件都是用硅材料制成的。硅产业在过去的一些年中,以每年大于百分之十的速度在增长。单晶硅抛光片已经广泛应用于制造各种分立元件; 硅的制造过程十分复杂,由于工业上工艺流程的不完善以及各种加工中的缺陷很容易在硅表面形成缺陷,从而硅产品的性能产生严重的影响。目前,硅生产厂商通过批次抽检对硅产品加工进行质量控制,在表面质量检测这方面主要检测产品表面的粗糙度、弯曲度、裂纹、刮痕以及油污等缺陷。目前对于硅基表面质量检测的技术有许多种方法,但绝大部分受限于它的成本以及速度,使之应用于工业上大规模硅晶表面质量检测成为障碍。2009年,美国的B.Jalali实验室提出了一种基于时间拉伸的成像手段,这种手段能够极大的提升成像速度,最快能达到数十兆HZ。利用这种成像技术,能够观察到曾经传统CCD所不能探测到的现象。经过近几年的发展,基于时间拉伸的这种成像手段已经达到了非常成熟的地步,B.Jalali等实验室利用这种成像技术成功的进行了大规模癌细胞筛选等实验,实现了高速以及准确率很高的细胞筛选。若将这种技术应用于工业上的硅晶表面质量检测,势必能大幅度提升硅晶产业的检测速率并且大大降低产品的不良率。Silicon semiconductor material is currently a very critical building block material in many industries today. Silicon semiconductors play an important role in the development of industries such as clean energy and military industry. At present, more than 90% of semiconductor devices in the world are made of silicon materials. In the past few years, the silicon industry has been growing at a rate of more than ten percent per year. Single crystal silicon polished wafers have been widely used in the manufacture of various discrete components; the manufacturing process of silicon is very complicated, due to the imperfection of the industrial process and defects in various processing, it is easy to form defects on the surface of silicon, so that the performance of silicon products have serious consequences. At present, silicon manufacturers control the quality of silicon product processing through batch sampling inspection. In terms of surface quality inspection, they mainly detect defects such as roughness, curvature, cracks, scratches, and oil stains on the product surface. At present, there are many methods for silicon-based surface quality detection technology, but most of them are limited by their cost and speed, which makes it an obstacle to apply large-scale silicon surface quality detection in industry. In 2009, the B.Jalali laboratory in the United States proposed an imaging method based on time stretching, which can greatly increase the imaging speed, reaching tens of MHZ at the fastest. Using this imaging technology, it is possible to observe phenomena that were once undetectable by traditional CCDs. After several years of development, this imaging method based on time stretching has reached a very mature stage. B. Jalali and other laboratories have successfully carried out large-scale cancer cell screening experiments using this imaging technology, achieving high-speed And cell screening with high accuracy. If this technology is applied to the inspection of silicon crystal surface quality in industry, it is bound to greatly increase the detection rate of the silicon crystal industry and greatly reduce the defective rate of products.

发明内容Contents of the invention

本发明为克服上述现有技术所述的至少一种缺陷,提供一种超快速的硅基表面质量检测系统,结合相干接受探测手段,不仅能够获取硅基表面的图像信息,还能通过恢复相位信息从而识别不同表面质量缺陷。更为重要的是,由于此种方法基于锁模飞秒脉冲激光作为光源,实现了兆赫兹的成像帧数,极大的提升了现有的一些硅基表面质量检测的技术。In order to overcome at least one of the defects described in the above-mentioned prior art, the present invention provides an ultra-fast silicon-based surface quality detection system, combined with coherent detection means, not only can obtain the image information of the silicon-based surface, but also can recover the phase information to identify different surface quality defects. More importantly, since this method is based on the mode-locked femtosecond pulsed laser as the light source, it realizes the number of megahertz imaging frames, which greatly improves some existing silicon-based surface quality detection technologies.

本发明的技术方案是:一种超快速的硅基表面质量检测系统,其中,包括锁模飞秒脉冲光源,中红外光波滤波器,色散光纤,掺铒光纤放大器,衍射光栅,基于透镜组成的4f成像系统,物镜,数字相干接收机,高速采样示波器以及数据处理恢复所需的电脑,另外还包括实验中所需用到的一些光纤,环形器,耦合器,光纤偏振控制器,准直器;The technical solution of the present invention is: an ultra-fast silicon-based surface quality detection system, which includes a mode-locked femtosecond pulse light source, a mid-infrared light wave filter, a dispersion fiber, an erbium-doped fiber amplifier, a diffraction grating, and a lens-based 4f imaging system, objective lens, digital coherent receiver, high-speed sampling oscilloscope, and computer required for data processing and recovery, as well as some optical fibers, circulators, couplers, fiber polarization controllers, and collimators used in experiments ;

还包括相位延迟线,透镜,硅基样品;Also includes phase delay lines, lenses, silicon-based samples;

所述的锁模飞秒脉冲光源、中红外光波滤波器、色散光纤、掺铒光纤放大器依次连接,掺铒光纤放大器再通过相位延迟线或光纤偏振控制器连接数字相干接收机,数字相干接收机再连接示波器以及电脑;The mode-locked femtosecond pulse light source, mid-infrared light wave filter, dispersion fiber, and erbium-doped fiber amplifier are connected in sequence, and the erbium-doped fiber amplifier is connected to a digital coherent receiver through a phase delay line or a fiber polarization controller, and the digital coherent receiver Then connect the oscilloscope and computer;

所述的光纤偏振控制器还依次连接环形器、准直器、衍射光栅、透镜、物镜、硅基样品。The fiber polarization controller is also sequentially connected with a circulator, a collimator, a diffraction grating, a lens, an objective lens, and a silicon-based sample.

考虑到相干接收的原理,滤波器在滤波之后,要使得功率在不同频率上尽可能相同,这样在分为本征光和信号光之后,用相干接收机处理的数据会尽更准确。在这里,我们使用一个waveshaper作为我们的光谱滤波器。Considering the principle of coherent reception, after the filter is filtered, the power should be as equal as possible at different frequencies, so that after being divided into intrinsic light and signal light, the data processed by the coherent receiver will be as accurate as possible. Here we use a waveshaper as our spectral filter.

采用锁模飞秒脉冲激光作为光源之后,利用锁模飞秒脉冲具有重复相应频率高这一特点达到对于硅基表面超快速表面检测的目的。After using the mode-locked femtosecond pulse laser as the light source, the ultra-fast surface detection of the silicon-based surface is achieved by using the mode-locked femtosecond pulse with the characteristic of high repetition frequency.

进一步的,所述的色散光纤的色散值与滤波后的光谱宽度的乘积不应大于脉冲的周期时间。否则会造成相邻的信号在时域上重叠,从而恢复不出硅基表面的图像。所述的衍射光栅使光在空间上能够一维的展开,并且不同过的空间位置具有不同的频率。Further, the product of the dispersion value of the dispersion fiber and the filtered spectral width should not be greater than the cycle time of the pulse. Otherwise, adjacent signals will overlap in the time domain, so that the image of the silicon-based surface cannot be recovered. The diffraction grating enables light to expand in one dimension in space, and different spatial positions have different frequencies.

与现有技术相比,有益效果是:本发明相对于现有的一些硅基表面质量检测手段,能够大幅度的提升表面质量检测的速度,并且不损耗检测精度。并且由于在探测末端引入相干接收探测,使得我们能够更准确的相位信息,即硅基表面的高低起伏变化,使得我们可以准确的分辨出所探测的硅基的表面的缺陷类别。Compared with the prior art, the beneficial effect is: compared with some existing silicon-based surface quality detection methods, the present invention can greatly increase the speed of surface quality detection without loss of detection accuracy. And because of the introduction of coherent receiving detection at the end of the detection, we can obtain more accurate phase information, that is, the fluctuation of the surface of the silicon substrate, so that we can accurately distinguish the type of defect on the surface of the silicon substrate detected.

附图说明Description of drawings

图1是本发明整体结构示意图。Fig. 1 is a schematic diagram of the overall structure of the present invention.

具体实施方式Detailed ways

附图仅用于示例性说明,不能理解为对本专利的限制;为了更好说明本实施例,附图某些部件会有省略、放大或缩小,并不代表实际产品的尺寸;对于本领域技术人员来说,附图中某些公知结构及其说明可能省略是可以理解的。附图中描述位置关系仅用于示例性说明,不能理解为对本专利的限制。The accompanying drawings are for illustrative purposes only, and should not be construed as limitations on this patent; in order to better illustrate this embodiment, certain components in the accompanying drawings will be omitted, enlarged or reduced, and do not represent the size of the actual product; for those skilled in the art It is understandable that some well-known structures and descriptions thereof may be omitted in the drawings. The positional relationship described in the drawings is for illustrative purposes only, and should not be construed as a limitation on this patent.

如图1所示,一种超快速的硅基表面质量检测系统,其中,包括锁模飞秒脉冲光源1,中红外光波滤波器2,色散光纤3,掺铒光纤放大器4,衍射光栅9,基于透镜组成的4f成像系统,物镜11,数字相干接收机13,高速采样示波器14以及数据处理恢复所需的电脑15,另外还包括实验中所需用到的一些光纤,环形器7,耦合器,光纤偏振控制器6,准直器8;As shown in Figure 1, a kind of ultra-fast silicon-based surface quality detection system, wherein, comprises mode-locked femtosecond pulse light source 1, mid-infrared light wave filter 2, dispersive optical fiber 3, erbium-doped optical fiber amplifier 4, diffraction grating 9, 4f imaging system based on lens, objective lens 11, digital coherent receiver 13, high-speed sampling oscilloscope 14 and computer 15 required for data processing and recovery, also includes some optical fibers, circulator 7 and coupler needed in the experiment , fiber polarization controller 6, collimator 8;

还包括相位延迟线5,透镜10,硅基样品12;It also includes a phase delay line 5, a lens 10, and a silicon-based sample 12;

锁模飞秒脉冲光源1、中红外光波滤波器2、色散光纤3、掺铒光纤放大器4依次连接,掺铒光纤放大器4再通过相位延迟线5或光纤偏振控制器6连接数字相干接收机13,数字相干接收机13再连接示波器14以及电脑15;A mode-locked femtosecond pulse light source 1, a mid-infrared light wave filter 2, a dispersion fiber 3, and an erbium-doped fiber amplifier 4 are connected in sequence, and the erbium-doped fiber amplifier 4 is connected to a digital coherent receiver 13 through a phase delay line 5 or a fiber polarization controller 6 , the digital coherent receiver 13 is then connected to the oscilloscope 14 and the computer 15;

光纤偏振控制器6还依次连接环形器7、准直器8、衍射光栅9、透镜10、物镜11、硅基样品12。The fiber polarization controller 6 is also sequentially connected with a circulator 7 , a collimator 8 , a diffraction grating 9 , a lens 10 , an objective lens 11 , and a silicon-based sample 12 .

基于时间拉伸的超快速硅基表面成像具有如下步骤。Time-stretch-based ultrafast silicon-based surface imaging has the following steps.

首先,具有几十兆赫兹重复频率的锁模飞秒脉冲激光光源经过光波滤波器之后,在频谱上具有15纳米左右的宽度,并且此时不同频率光的功率在保持大致相同。此时经过滤波后的脉冲光经过色散光纤进行时间拉伸,在时域上是一个比原脉冲更宽脉宽的脉冲(一般展宽到纳秒级),并且此时由于色散的作用,在不同时域上,已经是不同频率的光。此时相当于是完成了时间到频率的一一映射。First, the mode-locked femtosecond pulsed laser light source with a repetition rate of tens of megahertz has a width of about 15 nanometers in the frequency spectrum after passing through the light wave filter, and the power of light of different frequencies remains approximately the same at this time. At this time, the filtered pulsed light is time-stretched through the dispersion fiber. In the time domain, it is a pulse with a wider pulse width than the original pulse (generally extended to the nanosecond level), and at this time due to the effect of dispersion, the In the simultaneous domain, there are already lights of different frequencies. At this point, it is equivalent to completing the one-to-one mapping from time to frequency.

然后,完成时间频率一一映射的光经过掺铒光纤放大器(EDFA)进行功率放大。因为此时的光由于色散光纤的作用在功率上已经有很大有一部分衰减,所以此时需要功率经过放大。经过参铒光纤放大器(EDFA)之后,经过耦合器分为两路,交本征路和信号路,两路的功率保持相等。Then, the time-frequency-mapped light is amplified through an erbium-doped fiber amplifier (EDFA). Because the light at this time has been greatly attenuated in power due to the effect of the dispersion fiber, so the power needs to be amplified at this time. After passing through the erbium fiber amplifier (EDFA), it is divided into two paths through the coupler, the intrinsic path and the signal path, and the power of the two paths is kept equal.

在信号路上,光经过准直器入射到空间光路部分。空间部分首先是一个经过一个衍射光栅,衍射光栅的作用是将不同频率的光对应到不同的空间位置上,实际上相当于完成频率到空间的一一映射过程。此后,展开的光经过4f系统,然后经过准直入射到物镜,此时硅基样品放在物镜的工作焦距上,光照射在样品表面之后就携带硅基表面的信息沿原路返回。依次通过物镜,4f系统,衍射光栅,准直器耦合进光纤,最后到达环形器,传输到相干接收机。On the signal path, the light is incident on the spatial light path through the collimator. The space part first passes through a diffraction grating. The function of the diffraction grating is to correspond light of different frequencies to different spatial positions, which is actually equivalent to completing the one-to-one mapping process from frequency to space. Afterwards, the expanded light passes through the 4f system, and then collimates and enters the objective lens. At this time, the silicon-based sample is placed on the working focal length of the objective lens. It passes through the objective lens, the 4f system, the diffraction grating, the collimator and is coupled into the optical fiber in turn, and finally reaches the circulator and is transmitted to the coherent receiver.

在本征路上,放置一个相位延迟线,并且通过调整光程使得本征路和信号路的光程一致。相位延迟线的作用是精确调节光程使得本征路和信号路的光到达相干接收机之后能够产生拍频效果。On the eigenpath, a phase delay line is placed, and the optical path of the eigenpath and the signal path are consistent by adjusting the optical path. The role of the phase delay line is to precisely adjust the optical path so that the light in the eigenpath and the signal path can produce a beat frequency effect after reaching the coherent receiver.

经相干接收机探测后由高速采样示波器去获取拍频后的数据。由于本方案采用相干探测技术,所以一共有4个通道的数据需要采集,并且将获取的数据实时传递给进行数据处理的电脑,经过一定的算法恢复处理之后获取硅基表面的图像。将恢复的表面图像放入硅基表面缺陷分类识别模块,从而实现硅基表面的超快速质量检测。After being detected by a coherent receiver, a high-speed sampling oscilloscope is used to obtain the beat-frequency data. Since this scheme adopts coherent detection technology, there are 4 channels of data to be collected, and the acquired data is transmitted to the computer for data processing in real time, and the image of the silicon-based surface is obtained after a certain algorithm recovery process. Put the restored surface image into the silicon-based surface defect classification and recognition module, so as to realize the ultra-fast quality inspection of the silicon-based surface.

显然,本发明的上述实施例仅仅是为清楚地说明本发明所作的举例,而并非是对本发明的实施方式的限定。对于所属领域的普通技术人员来说,在上述说明的基础上还可以做出其它不同形式的变化或变动。这里无需也无法对所有的实施方式予以穷举。凡在本发明的精神和原则之内所作的任何修改、等同替换和改进等,均应包含在本发明权利要求的保护范围之内。Apparently, the above-mentioned embodiments of the present invention are only examples for clearly illustrating the present invention, rather than limiting the implementation of the present invention. For those of ordinary skill in the art, other changes or changes in different forms can be made on the basis of the above description. It is not necessary and impossible to exhaustively list all the implementation manners here. All modifications, equivalent replacements and improvements made within the spirit and principles of the present invention shall be included within the protection scope of the claims of the present invention.

Claims (3)

1.一种超快速的硅基表面质量检测系统,其特征在于,包括锁模飞秒脉冲光源(1),中红外光波滤波器(2),色散光纤(3),掺铒光纤放大器(4),衍射光栅(9),基于透镜组成的4f成像系统,物镜(11),数字相干接收机(13),高速采样示波器(14)以及数据处理恢复所需的电脑(15),另外还包括实验中所需用到的一些光纤,环形器(7),耦合器,光纤偏振控制器(6),准直器(8);1. An ultra-fast silicon-based surface quality detection system is characterized in that it includes a mode-locked femtosecond pulse light source (1), a mid-infrared light wave filter (2), a dispersion fiber (3), and an erbium-doped fiber amplifier (4 ), a diffraction grating (9), a lens-based 4f imaging system, an objective lens (11), a digital coherent receiver (13), a high-speed sampling oscilloscope (14) and a computer (15) required for data processing and recovery, and also includes Some optical fibers used in the experiment, circulator (7), coupler, fiber polarization controller (6), collimator (8); 还包括相位延迟线(5),透镜(10),硅基样品(12);It also includes a phase delay line (5), a lens (10), and a silicon-based sample (12); 所述的锁模飞秒脉冲光源(1)、中红外光波滤波器(2)、色散光纤(3)、掺铒光纤放大器(4)依次连接,掺铒光纤放大器(4)再通过相位延迟线(5)或光纤偏振控制器(6)连接数字相干接收机(13),数字相干接收机(13)再连接示波器(14)以及电脑(15);The mode-locked femtosecond pulse light source (1), mid-infrared light wave filter (2), dispersion fiber (3), and erbium-doped fiber amplifier (4) are connected in sequence, and the erbium-doped fiber amplifier (4) passes through the phase delay line (5) or the fiber optic polarization controller (6) is connected to a digital coherent receiver (13), and the digital coherent receiver (13) is then connected to an oscilloscope (14) and a computer (15); 所述的光纤偏振控制器(6)还依次连接环形器(7)、准直器(8)、衍射光栅(9)、透镜(10)、物镜(11)、硅基样品(12)。The fiber polarization controller (6) is also sequentially connected to a circulator (7), a collimator (8), a diffraction grating (9), a lens (10), an objective lens (11), and a silicon-based sample (12). 2.根据权利要求1所述的一种超快速的硅基表面质量检测系统,其特征在于:所述的色散光纤的色散值与滤波后的光谱宽度的乘积不应大于脉冲的周期时间。2. An ultra-fast silicon-based surface quality detection system according to claim 1, characterized in that: the product of the dispersion value of the dispersion fiber and the filtered spectral width should not be greater than the cycle time of the pulse. 3.根据权利要求1所述的一种超快速的硅基表面质量检测系统,其特征在于:所述的衍射光栅使光在空间上能够一维的展开,并且不同过的空间位置具有不同的频率。3. A kind of ultra-fast silicon-based surface quality detection system according to claim 1, characterized in that: said diffraction grating enables light to be expanded one-dimensionally in space, and different spatial positions have different frequency.
CN201810215816.4A 2018-03-15 2018-03-15 A kind of supper-fast silicon substrate surface quality detecting system Pending CN108445017A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110411954A (en) * 2019-07-03 2019-11-05 武汉大学 An ultrafast time-domain stretch imaging device and method
CN111855508A (en) * 2020-07-22 2020-10-30 天津凌视科技有限公司 Liquid detection device and liquid detection method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110411954A (en) * 2019-07-03 2019-11-05 武汉大学 An ultrafast time-domain stretch imaging device and method
CN111855508A (en) * 2020-07-22 2020-10-30 天津凌视科技有限公司 Liquid detection device and liquid detection method

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