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CN108436090A - A kind of zincincation of powder metallurgy holder - Google Patents

A kind of zincincation of powder metallurgy holder Download PDF

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Publication number
CN108436090A
CN108436090A CN201810298639.0A CN201810298639A CN108436090A CN 108436090 A CN108436090 A CN 108436090A CN 201810298639 A CN201810298639 A CN 201810298639A CN 108436090 A CN108436090 A CN 108436090A
Authority
CN
China
Prior art keywords
powder metallurgy
seconds
minutes
holder
room temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810298639.0A
Other languages
Chinese (zh)
Inventor
童日光
秦宏进
顾恩天
薛小江
张秋琴
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
GUANGDONG HONGTU (NANTONG) DIE-CASTING Co Ltd
Guangdong Hongtu Technology Holdings Co Ltd
Original Assignee
GUANGDONG HONGTU (NANTONG) DIE-CASTING Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by GUANGDONG HONGTU (NANTONG) DIE-CASTING Co Ltd filed Critical GUANGDONG HONGTU (NANTONG) DIE-CASTING Co Ltd
Priority to CN201810298639.0A priority Critical patent/CN108436090A/en
Publication of CN108436090A publication Critical patent/CN108436090A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/24After-treatment of workpieces or articles
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D3/00Electroplating: Baths therefor
    • C25D3/02Electroplating: Baths therefor from solutions
    • C25D3/22Electroplating: Baths therefor from solutions of zinc
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/34Pretreatment of metallic surfaces to be electroplated
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/48After-treatment of electroplated surfaces
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/48After-treatment of electroplated surfaces
    • C25D5/52After-treatment of electroplated surfaces by brightening or burnishing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/24After-treatment of workpieces or articles
    • B22F2003/241Chemical after-treatment on the surface
    • B22F2003/242Coating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/24After-treatment of workpieces or articles
    • B22F2003/247Removing material: carving, cleaning, grinding, hobbing, honing, lapping, polishing, milling, shaving, skiving, turning the surface

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Chemically Coating (AREA)
  • Electroplating Methods And Accessories (AREA)

Abstract

The invention discloses a kind of zincincations of powder metallurgy holder, including powder metallurgy holder infiltration to handle, and hole is closed;Powder metallurgy rack surface blasting treatment removes surface iron rust;Powder metallurgy rack surface is zinc-plated, and powder metallurgy holder is dried.Powder metallurgy holder is zinc-plated and quality is guaranteed the present invention provides can allow, and can produce in batches.

Description

A kind of zincincation of powder metallurgy holder
Technical field
The present invention relates to a kind of zincincations of powder metallurgy holder.
Background technology
Powder metallurgy holder itself can have many holes, pickling cannot be carried out also can not directly carry out it is zinc-plated, because of nothing The iron rust that method carries out pickled surface can not remove, if directly zinc-plated can subsequently cause surface from mildewing.
Invention content
The purpose of the present invention is to overcome above-mentioned limitation, to provide one kind keep powder metallurgy holder zinc-plated and Quality is guaranteed, and the zincincation for the powder metallurgy holder that can be produced in batches.
The purpose of the present invention is achieved through the following technical solutions:
A kind of zincincation of powder metallurgy holder, is as follows:
A, the infiltration of powder metallurgy holder is handled;
B, powder metallurgy rack surface blasting treatment removes surface iron rust, and the proportioning of blasting treatment sand is 0.3mm:0.1mm= 70%:30%, the purpose using 30% 0.1mm fine sands is by the iron rust removal in workpiece surface little groove, it is ensured that iron rust energy It is completely removed;10~20 minutes time of blasting treatment;
C, powder metallurgy rack surface is zinc-plated, the specific steps are:Electroplating pool carry out it is zinc-plated, washing three times, first time light extraction, ultrasound Wave cleaning, is dried at second of light extraction for the first time, and oven temperature setting is 75 °~100 °, dries 30 minutes, passivation, again water Wash three times, pure water, second dry, oven temperature setting is 75 °~100 °, is dried 30 minutes;
D, it is verified by salt mist experiment zinc-plated whether effective.
Preferably, the specific steps are be put into product in pressure vacuum tank, vacuum pressure is wanted for the infiltration processing of step A In 0.09mpa or more, then negative pressure sucking infiltration liquid, infiltration liquid will be higher by 50~80mm of product, continue to vacuumize 10~15 points Then clock is slowly unloaded down toward normal pressure, is being impregnated 5 minutes;Then product taking-up is placed on dryer infiltration liquid drying is net;Again Product is put into washing tank, the infiltration liquid of excess surface is cleaned up with clear water;Product is finally put into water cure pond In, constant water temperature infiltrates after solidification in 90 DEG C ± 5 DEG C, 15~20 minutes hardening times and closes hole;
Preferably, in the powder metallurgy rack surface zincincation of step C, electroplating pool carries out zinc-plated temperature and controls 5 ~35 DEG C, washing is the room temperature in rinsing bowl three times, and 20~30 seconds every time, first time light extraction was the room temperature in nitric acid and hydrochloric acid pond 15~25 seconds, ultrasonic cleaning was to be cleaned 20~40 seconds in supersonic wave cleaning machine room temperature, and second of light extraction is in nitric acid and hydrochloric acid Room temperature 15~25 seconds in pond are passivated as 10~35 DEG C of temperature in passivation pool, are passivated 10~20 seconds, and it is washing three times to wash again Room temperature in slot, 20~30 seconds every time, pure water was that room temperature cleans 20~30 seconds.
In conclusion the present invention has the following advantages:Allow that powder metallurgy holder is zinc-plated and quality is guaranteed, and It can produce in batches, it is cost-effective.
Specific implementation mode
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, the embodiment It is only used for explaining the present invention, be not intended to limit the scope of the present invention..
A kind of zincincation of powder metallurgy holder, is as follows:
Powder metallurgy holder infiltration handle, product is put into pressure vacuum tank, vacuum pressure will be in 0.09mpa or more, then Negative pressure sucking infiltration liquid, infiltration liquid will be higher by 50~80mm of product, continue to vacuumize 10~15 minutes, then slowly unload down toward normal Pressure is being impregnated 5 minutes;Then product taking-up is placed on dryer infiltration liquid drying is net;Product is put into washing tank again The infiltration liquid of excess surface is cleaned up with clear water;Finally product is put into water cure pond, constant water temperature is at 90 DEG C ± 5 DEG C, 15~20 minutes hardening times infiltrated after solidification and close hole;
Powder metallurgy rack surface blasting treatment removes surface iron rust, and the proportioning of blasting treatment sand is 0.3mm:0.1mm= 70%:30%, the purpose using 30% 0.1mm fine sands is by the iron rust removal in workpiece surface little groove, it is ensured that iron rust energy It is completely removed;10~20 minutes time of blasting treatment;
Powder metallurgy rack surface is zinc-plated, the specific steps are:Electroplating pool progress is zinc-plated, and electroplating pool carries out zinc-plated temperature control and exists 5~35 DEG C, washing is the room temperature in rinsing bowl three times, and 20~30 seconds every time, first time light extraction was normal in nitric acid and hydrochloric acid pond Temperature 15~25 seconds, ultrasonic cleaning are to be cleaned 20~40 seconds in supersonic wave cleaning machine room temperature, and second of light extraction is in nitric acid and salt Room temperature 15~25 seconds in sour pond are dried for the first time, and oven temperature setting is 75 °~100 °, are dried 30 minutes, are passivated as blunt Change pond in 10~35 DEG C of temperature, wash again three times be rinsing bowl in room temperature, 20~30 seconds every time, pure water be room temperature cleaning 20~ 30 seconds, second of drying, oven temperature setting was 75 °~100 °, is dried 30 minutes.
Embodiment 1:
Powder metallurgy rack surface blasting treatment, removes surface iron rust, and the proportioning of sand is:0.3mm:0.1mm=70%:30%; The 10 minutes time of blasting treatment;
Powder metallurgy rack surface is zinc-plated, and powder metallurgy holder is dried;Drying before passivation, is dried after passivation after the completion of cleaning It dries, oven temperatures are set as:It 75 °, dries 30 minutes.
Embodiment 2:
Powder metallurgy rack surface blasting treatment, removes surface iron rust, and the proportioning of sand is:0.3mm:0.1mm=70%:30%; The 15 minutes time of blasting treatment;
Powder metallurgy rack surface is zinc-plated, and powder metallurgy holder is dried;Drying before passivation, is dried after passivation after the completion of cleaning It dries, oven temperatures are set as:It 85 °, dries 30 minutes.
Embodiment 3:
Powder metallurgy rack surface blasting treatment, removes surface iron rust, and the proportioning of the sand is:0.3mm:0.1mm= 70%:30%;The 20 minutes time of blasting treatment;
Powder metallurgy rack surface is zinc-plated, and powder metallurgy holder is dried;Drying before passivation, is dried after passivation after the completion of cleaning It dries, oven temperatures are set as:It 100 °, dries 30 minutes.

Claims (3)

1. a kind of zincincation of powder metallurgy holder, it is characterised in that:It is as follows:
A, the infiltration of powder metallurgy holder is handled;
B, powder metallurgy rack surface blasting treatment removes surface iron rust, and the proportioning of the blasting treatment sand is 0.3mm: 0.1mm=70%:30%, the purpose using 30% 0.1mm fine sands is by the iron rust removal in workpiece surface little groove, it is ensured that Iron rust can be completely removed;10~20 minutes time of blasting treatment;
C, powder metallurgy rack surface is zinc-plated, the specific steps are:Electroplating pool carry out it is zinc-plated, washing three times, first time light extraction, ultrasound Wave cleaning, is dried at second of light extraction for the first time, and oven temperature setting is 75 °~100 °, dries 30 minutes, passivation, again water Wash three times, pure water, second dry, oven temperature setting is 75 °~100 °, is dried 30 minutes;
D, it is verified by salt mist experiment zinc-plated whether effective.
2. a kind of zincincation of powder metallurgy holder according to claim 1, it is characterised in that:Leaching described in step A Ooze processing the specific steps are, product is put into pressure vacuum tank, vacuum pressure will in 0.09mpa or more, then negative pressure suck Infiltration liquid, infiltration liquid will be higher by 50~80mm of product, continue to vacuumize 10~15 minutes, then slowly unload down toward normal pressure, soaking Bubble 5 minutes;Then product taking-up is placed on dryer infiltration liquid drying is net;Product is put into washing tank again and uses clear water handle The infiltration liquid of excess surface cleans up;Finally product is put into water cure pond, constant water temperature is at 90 DEG C ± 5 DEG C, solidification 15~20 minutes time infiltrated after solidification and closes hole.
3. a kind of zincincation of powder metallurgy holder according to claim 1, it is characterised in that:Described in step C In powder metallurgy rack surface zincincation, the electroplating pool carries out zinc-plated temperature and controls at 5~35 DEG C, and the washing is three times For the room temperature in rinsing bowl, 20~30 seconds every time, the first time light extraction was room temperature 15~25 seconds, institute in nitric acid and hydrochloric acid pond It is to be cleaned 20~40 seconds in supersonic wave cleaning machine room temperature to state ultrasonic cleaning, and second of light extraction is in nitric acid and hydrochloric acid pond Room temperature 15~25 seconds, the passivation are 10~35 DEG C of temperature in passivation pool, are passivated 10~20 seconds, described wash again is three times Room temperature in rinsing bowl, 20~30 seconds every time, the pure water was that room temperature cleans 20~30 seconds.
CN201810298639.0A 2018-04-04 2018-04-04 A kind of zincincation of powder metallurgy holder Pending CN108436090A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810298639.0A CN108436090A (en) 2018-04-04 2018-04-04 A kind of zincincation of powder metallurgy holder

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810298639.0A CN108436090A (en) 2018-04-04 2018-04-04 A kind of zincincation of powder metallurgy holder

Publications (1)

Publication Number Publication Date
CN108436090A true CN108436090A (en) 2018-08-24

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Country Status (1)

Country Link
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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63143285A (en) * 1986-12-04 1988-06-15 Furukawa Alum Co Ltd Production of clad material for heat exchanger
CN1786288A (en) * 2005-11-09 2006-06-14 万向钱潮股份有限公司 Galvanization technology
CN104368818A (en) * 2014-10-24 2015-02-25 苏州莱特复合材料有限公司 Iron-based powder metallurgical material electroplating technology
CN104651908A (en) * 2013-11-25 2015-05-27 中国兵器科学研究院宁波分院 Preparation method and hole sealing method of magnesium alloy surface ceramic coating
CN105369311A (en) * 2015-11-17 2016-03-02 扬州市佳佳镀锌有限公司 Bright dipping method for galvanized workpiece
CN105665246A (en) * 2014-11-19 2016-06-15 重庆尚科机械制造有限公司 Impregnation process
CN106425316A (en) * 2016-11-18 2017-02-22 淮北智淮科技有限公司 Double-lug plate for hinging work-pieces and manufacturing technology thereof

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63143285A (en) * 1986-12-04 1988-06-15 Furukawa Alum Co Ltd Production of clad material for heat exchanger
CN1786288A (en) * 2005-11-09 2006-06-14 万向钱潮股份有限公司 Galvanization technology
CN104651908A (en) * 2013-11-25 2015-05-27 中国兵器科学研究院宁波分院 Preparation method and hole sealing method of magnesium alloy surface ceramic coating
CN104368818A (en) * 2014-10-24 2015-02-25 苏州莱特复合材料有限公司 Iron-based powder metallurgical material electroplating technology
CN105665246A (en) * 2014-11-19 2016-06-15 重庆尚科机械制造有限公司 Impregnation process
CN105369311A (en) * 2015-11-17 2016-03-02 扬州市佳佳镀锌有限公司 Bright dipping method for galvanized workpiece
CN106425316A (en) * 2016-11-18 2017-02-22 淮北智淮科技有限公司 Double-lug plate for hinging work-pieces and manufacturing technology thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
中华人民共和国机械工业部统: "《粉末冶金工艺学》", 30 September 1987, 科学普及出版社 *
李国英: "《表面工程手册 第6篇 电镀》", 9 December 1989, 机械工业出版社 *

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Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
TA01 Transfer of patent application right
TA01 Transfer of patent application right

Effective date of registration: 20181210

Address after: 226000 Xingyuan West Road, Nantong High-tech Industrial Development Zone, Jiangsu Province, 777

Applicant after: Guangdong Hongtu (Nantong) Die-Casting Co., Ltd.

Applicant after: Guangdong Hongtu Technology (Holdings) Co., Ltd.

Address before: 215300 Xingyuan West Road 777, Nantong High-tech Industrial Development Zone, Nantong City, Jiangsu Province

Applicant before: Guangdong Hongtu (Nantong) Die-Casting Co., Ltd.

RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20180824