CN108362394B - Crystal optical waveguide speckle thermometry and system based on femtosecond laser write-in - Google Patents
Crystal optical waveguide speckle thermometry and system based on femtosecond laser write-in Download PDFInfo
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- GQYHUHYESMUTHG-UHFFFAOYSA-N lithium niobate Chemical compound [Li+].[O-][Nb](=O)=O GQYHUHYESMUTHG-UHFFFAOYSA-N 0.000 claims description 8
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- JNDMLEXHDPKVFC-UHFFFAOYSA-N aluminum;oxygen(2-);yttrium(3+) Chemical compound [O-2].[O-2].[O-2].[Al+3].[Y+3] JNDMLEXHDPKVFC-UHFFFAOYSA-N 0.000 description 6
- 229910019901 yttrium aluminum garnet Inorganic materials 0.000 description 6
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Abstract
Description
技术领域technical field
本发明属于温度测量技术领域,涉及晶体光波导散斑温度测量,尤其是一种基于飞秒激光写入的晶体光波导散斑温度测量方法及系统。The invention belongs to the technical field of temperature measurement, and relates to temperature measurement of crystal optical waveguide speckles, in particular to a method and system for measuring the temperature of crystal optical waveguide speckles based on femtosecond laser writing.
背景技术Background technique
散斑普遍存在于激光照明和相干成像系统,它由大量细微的高反差亮斑构成,是激光与物体相互作用后光强随机分布的现象,由于物体的位移或变形等状态变化必然引起散斑场的变化,因此通过测量散斑场的变化就可以获取物体的状态变化信息。Speckle is ubiquitous in laser lighting and coherent imaging systems. It is composed of a large number of fine high-contrast bright spots. It is a phenomenon of random distribution of light intensity after the interaction between laser and object. Speckle will inevitably be caused by state changes such as displacement or deformation of the object. Therefore, the state change information of the object can be obtained by measuring the change of the speckle field.
目前,温度测量技术是人类生产生活中不可或缺的技术之一,多模光纤散斑传感技术作为一种新兴传感技术也可用于环境温度的测量,它基于光纤中光传导模式的分布随外界温度变化而改变的原理,具有高灵敏度、低成本等优点。但是由于光纤的几何长度较长,绕圈之后固定较为麻烦,且占用体积较大,测量过程中测量精度和稳定性极易受震动影响;另一方面,散斑统计法只适用于较小的温度变化,所以此技术对于温度测量的动态范围较小,虽然通过建立新的参考散斑可以提升其动态范围,但这又会带来新的测量误差。At present, temperature measurement technology is one of the indispensable technologies in human production and life. As an emerging sensing technology, multimode optical fiber speckle sensing technology can also be used to measure ambient temperature. It is based on the distribution of light transmission modes in optical fibers. The principle of changing with the change of external temperature has the advantages of high sensitivity and low cost. However, due to the long geometric length of the optical fiber, it is troublesome to fix it after winding, and it occupies a large volume. The measurement accuracy and stability are easily affected by vibration during the measurement process; on the other hand, the speckle statistical method is only suitable for smaller Temperature changes, so the dynamic range of this technology for temperature measurement is small. Although the dynamic range can be improved by establishing a new reference speckle, this will bring new measurement errors.
因此,如何研发一种温度测量精度高、稳定性强且测量的动态范围大的晶体光波导散斑温度测量方法及系统是本领域技术人员需要解决的技术难题。Therefore, how to develop a crystal optical waveguide speckle temperature measurement method and system with high temperature measurement accuracy, strong stability and large measurement dynamic range is a technical problem to be solved by those skilled in the art.
发明内容Contents of the invention
本发明的目的在于提供一种设计合理、温度测量的动态范围大且测量精度高的基于飞秒激光写入的晶体光波导散斑温度测量方法及系统。The object of the present invention is to provide a crystal optical waveguide speckle temperature measurement method and system based on femtosecond laser writing with reasonable design, large dynamic range of temperature measurement and high measurement accuracy.
本发明解决其现实问题是采取以下技术方案实现的:The present invention solves its practical problems and is realized by taking the following technical solutions:
一种基于飞秒激光写入的晶体光波导散斑温度测量方法,包括以下步骤:A method for measuring the speckle temperature of a crystal optical waveguide based on femtosecond laser writing, comprising the following steps:
步骤1、采用飞秒激光写入技术在立方系晶体中写入不同几何形状的通道型包层光波导,且该通道型包层光波导的芯径取值范围为50μm-100μm;Step 1. Using femtosecond laser writing technology to write channel-type cladding optical waveguides with different geometric shapes in the cubic crystal, and the core diameter of the channel-type cladding optical waveguide ranges from 50 μm to 100 μm;
步骤2、采用端面耦合技术将不同波长的激光耦合进入所述步骤1的通道型包层光波导,并在改立方系晶体温度的同时记录温度变化过程中通道型包层光波导出射端的散斑图;Step 2. Coupling lasers of different wavelengths into the channel-type cladding optical waveguide in step 1 by using end-face coupling technology, and recording the speckle at the output end of the channel-type cladding optical waveguide during the temperature change process while changing the temperature of the cubic crystal picture;
步骤3、对步骤2中不同温度下所收集的散斑图样进行计算处理来解析温度变化。Step 3. Calculating and processing the speckle patterns collected at different temperatures in step 2 to analyze temperature changes.
而且,所述步骤1的立方系晶体为铌酸锂晶体,在铌酸锂晶体中写入半圆形的通道型包层光波导,且该通道型包层光波导的芯径取值范围为60μm。Moreover, the cubic crystal in step 1 is a lithium niobate crystal, and a semicircular channel-type cladding optical waveguide is written in the lithium niobate crystal, and the core diameter of the channel-type cladding optical waveguide ranges from 60 μm.
而且,所述步骤3的具体方法为:设置初始温度下的散斑图为参考,采用如下公式计算出温度变化之后的散斑图与参考散斑图之间的平均强度变化,并将温度变化与对应的散斑强度变化进行线性拟合,并根据此线性关系来解析温度变化;Moreover, the specific method of step 3 is: set the speckle pattern at the initial temperature as a reference, use the following formula to calculate the average intensity change between the speckle pattern after the temperature change and the reference speckle pattern, and calculate the temperature change Perform linear fitting with the corresponding speckle intensity change, and analyze the temperature change according to this linear relationship;
上式中,AIV表示温度变化之后的散斑图与参考散斑图之间的平均强度变化,X·Y表示散斑图的像素大小,(x,y)表示散斑图中某个像素的坐标, 代表初始散斑图在(x,y)坐标处的像素灰度值,则为第i个温度状态下所拍摄散斑图在对应位置处的像素灰度值。In the above formula, AIV represents the average intensity change between the speckle image after the temperature change and the reference speckle image, X Y represents the pixel size of the speckle image, (x, y) represents the intensity of a certain pixel in the speckle image coordinate, Represents the pixel gray value of the initial speckle image at the (x, y) coordinates, is the pixel gray value at the corresponding position of the speckle image taken in the i-th temperature state.
一种用于实现步骤1的采用飞秒激光写入技术在立方系晶体中写入不同几何形状的通道型包层光波导的实验系统,包括飞秒激光器、半波片、格兰泰勒棱镜、中性滤波片、分色镜、三维电动平台、控制器、计算机、电动快门、照明光源、CCD、透镜和分束镜;所述飞秒激光器射出的飞秒激光依次经过半波片、格兰泰勒棱镜、中性滤波片和分色镜后由显微物镜聚焦在立方系晶体样品表面或内部,用于形成通道型包层光波导;所述电动快门设置在中性滤波片和分色镜之间,其一端与计算机相连接,用于控制飞秒激光器的开关;该计算机还通过控制器与三维电动平台连接,该三维电动平台上放置有立方系晶体样品,用于调控晶体样品的写入速率和写入深度的参数;所述照明光源依次经过分束镜、分色镜和显微物镜照射到立方系晶体样品上,反射光再依次经过显微物镜、分色镜、分束镜和透镜后投射到CCD,并将CCD与计算机连接,用于对通道型包层光波导刻制过程进行实时观察。An experimental system for writing channel-type cladding optical waveguides of different geometries in cubic crystals using femtosecond laser writing technology for implementing step 1, including femtosecond lasers, half-wave plates, Glan-Taylor prisms, Neutral filter, dichroic mirror, three-dimensional electric platform, controller, computer, electric shutter, illumination light source, CCD, lens and beam splitter; the femtosecond laser emitted by the femtosecond laser passes through the half-wave plate, the gran After the Taylor prism, neutral filter and dichroic mirror, the microscope objective lens is used to focus on the surface or inside of the cubic crystal sample to form a channel-type cladding optical waveguide; the electric shutter is set on the neutral filter and dichroic mirror Between, one end of it is connected with the computer to control the switch of the femtosecond laser; the computer is also connected with the three-dimensional electric platform through the controller, and the cubic crystal sample is placed on the three-dimensional electric platform, which is used to control the writing of the crystal sample. The parameters of input rate and writing depth; the illumination light source is irradiated onto the cubic crystal sample through a beam splitter, a dichroic mirror, and a microscopic objective lens in sequence, and the reflected light then passes through a microscopic objective lens, a dichroic mirror, and a beam splitter And the lens is projected to the CCD, and the CCD is connected to the computer for real-time observation of the channel-type cladding optical waveguide engraving process.
一种用于实现步骤2的采用端面耦合技术将不同波长的激光耦合进入通道型包层光波导,并在改立方系晶体温度的同时记录温度变化过程中通道型包层光波导出射端的散斑图的实验系统,包括三台波长不同的激光器、反射镜、分束镜、半波片、显微物镜、通道型包层光波导、半导体制冷片和CCD;所述三台波长不同的激光器平行放置,其出射激光分别经反射镜和分束镜置于同一水平轴,再经过半波片和显微物镜耦合进通道型包层光波导,该通道型包层光波导出射端的光经过显微物镜投射到CCD,用于散斑图的拍摄;所述半导体制冷片置于立方系晶体下方,用于对该立方系晶体施加温度变化。A method for realizing step 2 by coupling lasers of different wavelengths into the channel-type cladding optical waveguide using end-face coupling technology, and recording the speckle at the emission end of the channel-type cladding optical waveguide during the temperature change process while changing the cubic crystal temperature The experimental system of the figure includes three lasers with different wavelengths, reflectors, beam splitters, half-wave plates, microscope objectives, channel-type cladding optical waveguides, semiconductor refrigeration sheets and CCDs; the three lasers with different wavelengths are parallel Placed, the outgoing laser light is placed on the same horizontal axis through the reflector and the beam splitter, and then coupled into the channel-type cladding optical waveguide through the half-wave plate and the microscope objective lens. The objective lens is projected to the CCD for shooting the speckle pattern; the semiconductor cooling chip is placed under the cubic crystal to apply temperature changes to the cubic crystal.
本发明的优点和有益效果:Advantages and beneficial effects of the present invention:
1、本发明利用飞秒激光写入技术制备的不同几何形状的通道型包层光波导,在保障测量精度的同时,可以提升温度测量的动态范围,例如,在实验中,利用飞秒激光写入技术制备的钇铝石榴石通道型包层光波导用于温度传感的精度可达0.05℃,并且半圆形通道型包层光波导对于温度传感的动态范围可达10℃,明显优于矩形通道型包层光波导的动态范围通常为3℃。1. The present invention uses femtosecond laser writing technology to prepare channel-type cladding optical waveguides with different geometric shapes, which can improve the dynamic range of temperature measurement while ensuring measurement accuracy. For example, in the experiment, using femtosecond laser writing The yttrium aluminum garnet channel-type cladding optical waveguide prepared by the technology can be used for temperature sensing with an accuracy of 0.05°C, and the dynamic range of the semicircular channel-type clad optical waveguide for temperature sensing can reach 10°C, which is obviously superior. The dynamic range of a rectangular channel-type cladding optical waveguide is usually 3°C.
2、本发明采用相较于多模光纤几何尺寸更小的通道型包层光波导制备成各种几何结构,并且可以应用于多种材料(例如钇铝石榴石晶体、铌酸锂晶体等),这对于我们进行不同环境下的多种测试,并得到最优性能(诸如动态范围、传感精度等)提供了良好的选择,实验证明,在铌酸锂晶体中刻制的芯径为60μm的通道型包层光波导对于温度传感的动态范围可达20℃。2. The present invention adopts channel-type cladding optical waveguides with smaller geometric dimensions than multimode optical fibers to prepare various geometric structures, and can be applied to various materials (such as yttrium aluminum garnet crystals, lithium niobate crystals, etc.) , which provides a good choice for us to conduct a variety of tests in different environments and obtain optimal performance (such as dynamic range, sensing accuracy, etc.). Experiments have proved that the core diameter carved in lithium niobate crystals is 60 μm The dynamic range of the channel-type cladding optical waveguide for temperature sensing can reach 20 °C.
附图说明Description of drawings
图1是本发明的步骤1的利用飞秒激光技术加工通道型包层光波导的实验系统结构示意图;Fig. 1 is the experimental system structural representation of utilizing femtosecond laser technology to process channel-type cladding optical waveguide in step 1 of the present invention;
图2(a)-(c)是本发明的通道型包层光波导显微图与散斑图;Fig. 2 (a)-(c) is the channel-type cladding optical waveguide micrograph and speckle pattern of the present invention;
图3是本发明的步骤2的采用端面耦合技术将不同波长的激光耦合进入通道型包层光波导的试验系统结构示意图;Fig. 3 is a schematic structural diagram of a test system for coupling lasers of different wavelengths into a channel-type cladding optical waveguide using end-face coupling technology in step 2 of the present invention;
图4(a)-(f)是本发明的散斑强度变化随温度变化的关系的实验结果图;Fig. 4 (a)-(f) is the experimental result diagram of the relationship between the variation of speckle intensity and the variation of temperature in the present invention;
图5(a)是本发明的散斑强度变化在不同波长激光作用下随温度增加的变化趋势的半圆形通道型包层光波导实验结果图;Fig. 5 (a) is the semi-circular channel type cladding optical waveguide experimental result diagram of the variation trend of the speckle intensity variation with the increase of temperature under the action of different wavelength lasers of the present invention;
图5(b)是本发明的散斑强度变化在不同波长激光作用下随温度增加的变化趋势的矩形通道型包层光波导实验结果图;Fig. 5 (b) is a rectangular channel-type cladding optical waveguide experimental result diagram of the variation trend of the speckle intensity variation with the increase of temperature under the action of different wavelength lasers of the present invention;
图6(a)是本发明的在不同强度的激光作用下散斑强度变化随温度增加的变化趋势的半圆形通道型包层光波导实验结果图;Fig. 6 (a) is the semicircular channel type cladding optical waveguide experimental result diagram of the variation trend of speckle intensity variation with temperature increase under the action of different intensities of laser light according to the present invention;
图6(b)是本发明的在不同强度的激光作用下散斑强度变化随温度增加的变化趋势的矩形通道型包层光波导实验结果图。Fig. 6(b) is a graph showing the experimental results of the rectangular channel cladding optical waveguide of the variation trend of the speckle intensity variation with the increase of temperature under the action of different intensities of laser light according to the present invention.
具体实施方式Detailed ways
以下结合附图对本发明实施例作进一步详述:Embodiments of the present invention are described in further detail below in conjunction with the accompanying drawings:
一种基于飞秒激光写入的晶体光波导散斑温度测量方法,包括以下步骤:A method for measuring the speckle temperature of a crystal optical waveguide based on femtosecond laser writing, comprising the following steps:
步骤1、采用飞秒激光写入技术在立方系晶体中写入不同几何形状的通道型包层光波导,且该通道型包层光波导的芯径取值范围为50μm-100μm;Step 1. Using femtosecond laser writing technology to write channel-type cladding optical waveguides with different geometric shapes in the cubic crystal, and the core diameter of the channel-type cladding optical waveguide ranges from 50 μm to 100 μm;
所述立方系晶体可为钇铝石榴石晶体或铌酸锂晶体等,在本实施例中,所述采用飞秒激光写入技术在钇铝石榴石晶体(Nd:YAG晶体)中写入通道型包层光波导,这将为步骤2的温度测量提供最重要的感应元件。并根据需要将该通道型包层光波导制备成不同几何形状(我们这里制备成矩形和半圆形)以便比较其对动态范围的影响,且该通道型包层光波导的芯径应该在50-100μm左右以保证光在其中传输时呈现多种模式,从而为步骤2散斑图的采集提供良好的前提条件。The cubic crystals can be yttrium aluminum garnet crystals or lithium niobate crystals, etc. In this embodiment, the femtosecond laser writing technology is used to write channels in yttrium aluminum garnet crystals (Nd:YAG crystals) Type cladding optical waveguide, which will provide the most important sensing element for the temperature measurement in step 2. And prepare the channel-type cladding optical waveguide into different geometric shapes (rectangular and semicircular) according to the needs so as to compare its influence on the dynamic range, and the core diameter of the channel-type cladding optical waveguide should be 50 -100 μm or so to ensure that the light presents multiple modes when it is transmitted, thus providing a good precondition for the acquisition of the speckle pattern in step 2.
在本实施例中,所述步骤1的采用飞秒激光写入技术在立方系晶体中写入通道型包层光波导的实验系统如图1所示,包括飞秒激光器、半波片、格兰泰勒棱镜(用作偏振器)、中性滤波片、分色镜、三维电动平台、控制器、计算机、电动快门、照明光源、CCD(图像传感器)、透镜和分束镜;所述飞秒激光器射出的飞秒激光依次经过半波片、格兰泰勒棱镜(用作偏振器)、中性滤波片和分色镜后由显微物镜聚焦在晶体样品表面或内部,用于形成通道型包层光波导;所述电动快门设置在中性滤波片和分色镜之间,其一端与计算机相连接,用于控制飞秒激光器的开关;该计算机还通过控制器与三维电动平台连接,该三维电动平台上放置有立方系晶体样品,用于调控晶体样品的写入速率和写入深度的参数;所述照明光源依次经过分束镜、分色镜和显微物镜照射到立方系晶体样品上,反射光再依次经过显微物镜、分色镜、分束镜和透镜后,投射到CCD,并将CCD与计算机连接,用于对通道型包层光波导刻制过程进行实时观察。In this embodiment, the experimental system for writing channel-type cladding optical waveguides in cubic crystals using femtosecond laser writing technology in step 1 is shown in Figure 1, including femtosecond lasers, half-wave plates, lattice Lan Taylor prism (used as polarizer), neutral filter, dichroic mirror, three-dimensional motorized stage, controller, computer, motorized shutter, illumination source, CCD (image sensor), lens and beam splitter; the femtosecond The femtosecond laser emitted by the laser passes through the half-wave plate, Glan-Taylor prism (used as a polarizer), neutral filter and dichroic mirror, and then is focused on the surface or inside of the crystal sample by the microscope objective lens to form a channel-type package. layer optical waveguide; the electric shutter is arranged between the neutral filter and the dichroic mirror, and one end thereof is connected with a computer for controlling the switch of the femtosecond laser; the computer is also connected with a three-dimensional electric platform through a controller, the Cubic crystal samples are placed on the three-dimensional motorized platform, which is used to control the parameters of the writing rate and writing depth of the crystal samples; the illumination light source sequentially passes through the beam splitter, dichroic mirror and microscopic objective lens to illuminate the cubic crystal samples After the reflected light passes through the microscope objective, dichroic mirror, beam splitter and lens in turn, it is projected to the CCD, and the CCD is connected to the computer for real-time observation of the engraving process of the channel-type cladding optical waveguide.
利用该实验系统在钇铝石榴石晶体(Nd:YAG晶体)中写入通道型包层光波导的加工过程为:将样品放置在水平方向(XY方向)分辨率为100nm,垂直方向(Z方向)分辨率为1μm的XYZ三维电动平台上,由飞秒激光器射出的飞秒激光依次经过半波片、格兰泰勒棱镜(用作偏振器)、中性滤波片和分色镜的光学元件后由显微物镜聚焦在样品表面或内部;并通过调节光学元件可以实现对飞秒激光的偏振、脉冲能量等参数进行调整,焦点处材料折射率升高或降低,最终经过一次或数次扫描,形成通道光波导。Using this experimental system to write channel-type cladding optical waveguides in yttrium aluminum garnet crystals (Nd:YAG crystals) is as follows: the sample is placed in the horizontal direction (XY direction) with a resolution of 100nm, and the vertical direction (Z direction) ) on an XYZ three-dimensional motorized platform with a resolution of 1 μm, the femtosecond laser emitted by the femtosecond laser passes through the optical components of the half-wave plate, the Glan Taylor prism (used as a polarizer), the neutral filter and the dichroic mirror in sequence The microscopic objective lens is focused on the surface or inside of the sample; and by adjusting the optical components, the parameters such as polarization and pulse energy of the femtosecond laser can be adjusted. The refractive index of the material at the focal point increases or decreases, and finally after one or several scans, A channel optical waveguide is formed.
在本实施例中,与计算机连接的电动快门配合写入加工程序,用来控制飞秒激光器的开关。CCD可以提供直观、实时的加工图像,为实现精细加工提供保障。三维电动平台由计算机软件控制,可以根据实验需求编写程序代码,调控写入速率、写入深度等参数。In this embodiment, the electric shutter connected to the computer is used to write the processing program to control the switch of the femtosecond laser. CCD can provide intuitive and real-time processing images, providing guarantee for the realization of fine processing. The three-dimensional electric platform is controlled by computer software, and the program code can be written according to the experimental requirements, and parameters such as writing rate and writing depth can be adjusted.
在本实施例中,飞秒激光的工作中心波长为800nm,脉宽为120fs,重复频率为1kHz,最高脉冲能量为1mJ。飞秒激光经过40×的显微物镜(Leica,N.A.=0.65)聚焦在Nd:YAG晶体表面(10×10mm2)或内部开始写入。In this embodiment, the working center wavelength of the femtosecond laser is 800 nm, the pulse width is 120 fs, the repetition frequency is 1 kHz, and the highest pulse energy is 1 mJ. The femtosecond laser is focused on the surface (10×10mm2) or inside of the Nd:YAG crystal through a 40×microscopic objective lens (Leica, N.A.=0.65) to start writing.
并为避免写入过程中激光能量过高形成晶体裂痕或能量过低无法形成明显的折射率改变,飞秒激光经中性滤波片、半波片以及线偏振片等光学元件后,其单脉冲能量被设定为0.2~0.4μJ,并以700μm/s的扫描速率对样品进行扫描。通过多次扫描过程中调整激光聚焦深度,在晶体内部形成大量间隔为3~4μm、不同深度的写入痕迹。这些写入痕迹处折射率降低,其包裹区域折射率相对升高,该区域即为通道型包层光波导。And in order to avoid crystal cracks caused by too high laser energy or too low energy to form obvious refractive index changes during the writing process, after the femtosecond laser passes through optical components such as neutral filters, half-wave plates, and linear polarizers, its single pulse The energy was set at 0.2-0.4 μJ, and the sample was scanned at a scan rate of 700 μm/s. By adjusting the laser focus depth during multiple scans, a large number of written traces with intervals of 3-4 μm and different depths are formed inside the crystal. The refractive index of these written traces decreases, and the refractive index of the surrounding area relatively increases, and this area is the channel-type cladding optical waveguide.
图2为晶体光波导显微图与散斑图,其中图2(a)和图2(b)分别为半圆形和矩形波导的显微镜截面图及其460nm波长下的散斑图,图2(c)为矩形波导的显微镜俯视图像,可以很清楚地观察到飞秒激光在晶体中写入的痕迹。Figure 2 is the microscopic image and speckle image of the crystal optical waveguide, in which Figure 2(a) and Figure 2(b) are the microscopic cross-sectional views of the semicircular and rectangular waveguides and their speckle images at a wavelength of 460nm, respectively, Figure 2 (c) is a microscope top view image of the rectangular waveguide, where the traces written by the femtosecond laser in the crystal can be clearly observed.
步骤2、采用端面耦合技术将不同波长的激光耦合进入所述步骤1的通道型包层光波导,在通道型包层光波导的出射端面会出现由于多模式干涉而形成的散斑图,并在改变立方系晶体样本温度的同时用图像传感器记录温度变化过程中通道型包层光波导出射端的散斑图;Step 2: Coupling laser light of different wavelengths into the channel-type cladding optical waveguide in step 1 by using end-face coupling technology, a speckle pattern formed due to multi-mode interference will appear on the exit end face of the channel-type cladding optical waveguide, and While changing the temperature of the cubic crystal sample, an image sensor is used to record the speckle pattern at the exit end of the channel-type cladding optical waveguide during the temperature change process;
在本实施例中,所述步骤2的实验系统如图3所示,包括波长不同的三台激光器(波长分别为633nm、532nm和460nm)、反射镜、分束镜、半波片、显微物镜、通道型包层光波导、半导体制冷片和CCD;所述波长不同的三台激光器平行放置,其出射激光分别经反射镜和分束镜置于同一水平轴,再经过半波片和显微物镜耦合进通道型包层光波导,该通道型包层光波导出射端的光经过显微物镜投射到CCD,用于散斑图的拍摄;所述半导体制冷片置于立方系晶体下方,用于对该立方系晶体施加温度变化。In this embodiment, the experimental system of step 2 is shown in Figure 3, including three lasers with different wavelengths (wavelengths are 633nm, 532nm and 460nm), mirrors, beam splitters, half-wave plates, microscope Objective lens, channel-type cladding optical waveguide, semiconductor cooling plate and CCD; the three lasers with different wavelengths are placed in parallel, and the outgoing laser light is placed on the same horizontal axis through a reflector and a beam splitter, and then passes through a half-wave plate and a display. The micro-objective lens is coupled into the channel-type cladding optical waveguide, and the light at the output end of the channel-type cladding optical waveguide is projected to the CCD through the micro-objective lens for shooting the speckle pattern; A temperature change is applied to the cubic crystal.
利用反射镜和分束镜将三台不同波长的激光束同轴放置(用来验证不同波长激光对于系统灵敏度的影响),激光束经物镜聚焦并耦合到通道型包层光波导中,并在通道型包层光波导中激发多种模式,这些模式在通道型包层光波导出射端相互干涉形成的散斑图经物镜成像到图像传感器(CCD),并由CCD记录下来,半导体制冷片主要用于对晶体施加温度变化。Three laser beams with different wavelengths are coaxially placed by using mirrors and beam splitters (to verify the influence of different wavelength lasers on the sensitivity of the system). The laser beams are focused by the objective lens and coupled into the channel-type cladding optical waveguide. A variety of modes are excited in the channel-type cladding optical waveguide, and the speckle pattern formed by the mutual interference of these modes at the exit end of the channel-type cladding optical waveguide is imaged to the image sensor (CCD) by the objective lens and recorded by the CCD. The semiconductor refrigeration chip mainly Used to apply a temperature change to the crystal.
所述步骤2的工作原理为:The working principle of the step 2 is:
采用端面耦合技术,利用显微物镜将入射激光汇聚后,经波导入射端面垂直耦合进入波导内,经传输后由对应波导端面出射,出射光经过物镜收集后可以进行测量。不同波长的激光耦合进波导后,会在波导中激发多种传播模式,这些模式的随机干涉会在波导出射端形成含有亮暗斑点的散斑图,半导体制冷器对晶体施加的温度变化会引起热膨胀效应从而导致晶体的微小形变以及折射率的微小变化,使得光波导中的模式重新分布,最终导致光波导出射端散斑图产生变化,图像传感器(CCD)则用来记录温度变化过程中通道型包层光波导出射端的散斑图样。Using the end-face coupling technology, the incident laser light is converged by the microscope objective lens, then vertically coupled into the waveguide through the incident end face of the waveguide, and then exits from the corresponding waveguide end face after transmission, and the outgoing light can be measured after being collected by the objective lens. After lasers of different wavelengths are coupled into the waveguide, multiple propagation modes will be excited in the waveguide. The random interference of these modes will form a speckle pattern containing bright and dark spots at the waveguide emission end. The temperature change imposed by the semiconductor refrigerator on the crystal will cause The thermal expansion effect leads to small deformation of the crystal and small changes in the refractive index, which redistributes the modes in the optical waveguide, and finally leads to changes in the speckle pattern at the exit end of the optical waveguide. The image sensor (CCD) is used to record the channel during the temperature change process. The speckle pattern at the exit end of a cladding waveguide.
步骤3、对步骤2中不同温度下所收集的一系列散斑图样进行计算处理来解析温度变化,我们设置初始温度下的散斑图为参考,计算出温度变化之后的散斑图与参考散斑图之间的平均强度变化(即两张散斑图对应像素间的灰度差值的绝对值取平均),并将温度变化与对应的散斑强度变化进行线性拟合,根据此线性关系来解析温度变化。Step 3. Calculate and process a series of speckle patterns collected at different temperatures in step 2 to analyze the temperature change. We set the speckle pattern at the initial temperature as a reference, and calculate the speckle pattern after the temperature change and the reference scatter pattern. The average intensity change between the speckle patterns (that is, the absolute value of the gray level difference between the corresponding pixels of the two speckle patterns is averaged), and the temperature change is linearly fitted with the corresponding speckle intensity change. According to this linear relationship to analyze temperature changes.
在本实施例中,所述步骤3的具体方法是:对不同温度下所收集的一系列散斑图样进行计算处理,我们设置初始温度下的散斑图为参考,采用MATLAB软件和如下公式计算出温度变化之后的散斑图与参考散斑图之间的平均强度变化(Average intensityvariation,AIV),即两张散斑图对应像素间的灰度差值的绝对值取平均,算法如公式1所示,并将温度变化与对应的散斑强度变化进行线性拟合,并根据此线性关系来解析温度变化。In this embodiment, the specific method of step 3 is: calculate and process a series of speckle patterns collected at different temperatures, we set the speckle pattern at the initial temperature as a reference, and use MATLAB software and the following formula to calculate Average intensity variation (AIV) between the speckle image after the temperature change and the reference speckle image, that is, the absolute value of the gray level difference between the corresponding pixels of the two speckle images is averaged, the algorithm is shown in formula 1 As shown, and the temperature change is linearly fitted with the corresponding speckle intensity change, and the temperature change is analyzed according to this linear relationship.
上式中,AIV表示温度变化之后的散斑图与参考散斑图之间的平均强度变化,X·Y表示散斑图的像素大小,(x,y)表示散斑图中某个像素的坐标, 代表初始散斑图在(x,y)坐标处的像素灰度值,则为第i个温度状态下所拍摄散斑图在对应位置处的像素灰度值。In the above formula, AIV represents the average intensity change between the speckle image after the temperature change and the reference speckle image, X Y represents the pixel size of the speckle image, (x, y) represents the intensity of a certain pixel in the speckle image coordinate, Represents the pixel gray value of the initial speckle image at the (x, y) coordinates, is the pixel gray value at the corresponding position of the speckle image taken in the i-th temperature state.
图4为散斑强度变化随温度变化的关系的实验结果图,其中,图4(a)-(c)为半圆形波导的计算结果,(a)、(b)、(c)分别为不同温度变化幅度下的实验结果,(d-f)为矩形波导的计算结果。由图可以看出平均强度变化随温度增加呈稳定良好的线性变化关系,其中半圆形波导的动态范围可达10℃(见图4(a)),而矩形波导的动态范围只有3℃左右(见图4(d)),此外,两种形状的波导的传感精度都能达到0.05℃(见图4(c),(f))。如图4所示的实验结果表明,散斑强度变化在一定范围内随温度增加呈稳定良好的线性关系,而这个范围(即动态范围)会因为晶体波导的形状不同而略有差异,其中矩形波导的动态范围为3℃,而半圆形波导的动态范围可达10℃,这意味着我们可以通过制备不同形状的波导来提升散斑传感器的动态范围,这种方法相较于建立新的参考散斑来说具有更小的误差。Figure 4 is the experimental results diagram of the relationship between the change of speckle intensity and the temperature change, in which Figure 4 (a)-(c) is the calculation result of the semicircular waveguide, (a), (b), and (c) are respectively Experimental results under different temperature ranges, (d-f) are calculation results for rectangular waveguides. It can be seen from the figure that the average intensity change shows a stable and good linear relationship with the increase of temperature, and the dynamic range of the semicircular waveguide can reach 10°C (see Figure 4(a)), while the dynamic range of the rectangular waveguide is only about 3°C (see Fig. 4(d)), in addition, the sensing accuracy of both shapes of waveguides can reach 0.05°C (see Fig. 4(c), (f)). The experimental results shown in Figure 4 show that the variation of speckle intensity has a stable and good linear relationship with the increase of temperature within a certain range, and this range (ie dynamic range) will be slightly different due to the different shapes of the crystal waveguide, among which the rectangular The dynamic range of the waveguide is 3°C, while the dynamic range of the semicircular waveguide can reach 10°C, which means that we can improve the dynamic range of the speckle sensor by preparing waveguides of different shapes. The reference speckle has a smaller error.
图5是采用不同波长的激光得到的实验结果图;其中,图5(a)是本发明的散斑强度变化在不同波长激光作用下随温度增加的变化趋势的半圆形通道型包层光波导实验结果图;图5(b)是本发明的散斑强度变化在不同波长激光作用下随温度增加的变化趋势的矩形通道型包层光波导实验结果图;Fig. 5 is the experimental result graph that adopts the laser of different wavelengths to obtain; Wherein, Fig. 5 (a) is the semicircular channel type cladding light of the variation trend of the speckle intensity variation of the present invention with the increase of temperature under the action of different wavelength lasers Waveguide experiment result diagram; Fig. 5 (b) is the rectangular channel type cladding optical waveguide experiment result diagram of the change trend of the speckle intensity variation of the present invention with the increase of temperature under the action of different wavelength lasers;
理论上入射激光波长越短,光波导中的模式越多,温度变化引起的模间的相位差越大,从而使得由于模间干涉而形成的散斑图的强度变化更大,有利于提高晶体光波导温度传感器的灵敏度。如图5所示,在不同激光作用下,平均强度变化仍然随温度增加呈线性变化,并且系统所选的入射激光波长越短,散斑的平均强度变化越大,意味着波导的传感灵敏度越高。这一现象与理论分析相符。Theoretically, the shorter the incident laser wavelength, the more modes there are in the optical waveguide, and the greater the phase difference between the modes caused by temperature changes, so that the intensity of the speckle pattern formed due to the interference between the modes changes more greatly, which is conducive to improving the quality of the crystal. Sensitivity of optical waveguide temperature sensors. As shown in Figure 5, under different laser effects, the average intensity change still changes linearly with the increase of temperature, and the shorter the incident laser wavelength selected by the system, the greater the average intensity change of the speckle, which means that the sensing sensitivity of the waveguide higher. This phenomenon is consistent with theoretical analysis.
入射激光的光强也是影响波导传感灵敏度的一个因素,图6是采用460nm激光以不同强度入射波导得到的实验结果;其中,图6(a)是本发明的在不同强度的激光作用下散斑强度变化随温度增加的变化趋势的半圆形通道型包层光波导实验结果图;图6(b)是本发明的在不同强度的激光作用下散斑强度变化随温度增加的变化趋势的矩形通道型包层光波导实验结果图。如图所示,入射激光光强越大,散斑图之间的平均强度变化越大,这意味着适度增大入射光强可以提升波导的传感灵敏度,适当增加入射激光的强度也会提升其灵敏度,这对于传感系统的优化提供了良好的选择条件。但是需要注意的是光强一般被限制在不使CCD的像素灰度值出现饱和的范围内,如果测试光强较高,可以通过添加衰减片的方式降低光强,防止CCD设备遭受损坏。The light intensity of the incident laser is also a factor that affects the waveguide sensing sensitivity. Figure 6 is the experimental result obtained by using a 460nm laser to incident the waveguide with different intensities; The semicircular channel type cladding optical waveguide experimental result diagram of the change trend of the spot intensity change with the temperature increase; Fig. 6 (b) is the change trend of the speckle intensity change with the temperature increase under the action of different intensities of laser light of the present invention Experimental results of a rectangular channel-type cladding optical waveguide. As shown in the figure, the greater the incident laser light intensity, the greater the average intensity change between speckle patterns, which means that moderately increasing the incident light intensity can improve the sensing sensitivity of the waveguide, and appropriately increasing the incident laser intensity will also improve Its sensitivity provides a good selection condition for the optimization of the sensing system. However, it should be noted that the light intensity is generally limited within the range that does not saturate the pixel gray value of the CCD. If the test light intensity is high, the light intensity can be reduced by adding an attenuation film to prevent the CCD device from being damaged.
本发明的工作原理是:The working principle of the present invention is:
飞秒激光写入技术是目前制备光波导最有效的技术之一,它不需要结合光刻掩膜技术,加工过程快速高效,对实验环境等条件要求低;该技术适用性广泛,可以应用于玻璃、晶体、陶瓷等多种材料中制备光波导;其空间分辨率较高,可以达到几十纳米加工精度,实现精准维纳加工,且加工过程中热效应不明显,不易对材料产生损坏;另外,飞秒激光加工技术是一项真正的三维加工技术,它可以在衬底材料内任意深度完成具有任意长度和角度的波导结构制备,便于制备不同几何形状的光波导器件。Femtosecond laser writing technology is currently one of the most effective technologies for preparing optical waveguides. It does not need to be combined with photolithography mask technology, the processing process is fast and efficient, and it has low requirements on the experimental environment and other conditions; Optical waveguides can be prepared in various materials such as glass, crystals, and ceramics; their spatial resolution is high, and the processing accuracy can reach tens of nanometers, realizing precise Wiener processing, and the thermal effect is not obvious during processing, and it is not easy to damage the material; in addition , femtosecond laser processing technology is a true three-dimensional processing technology, which can complete the preparation of waveguide structures with arbitrary lengths and angles at any depth in the substrate material, which is convenient for the preparation of optical waveguide devices with different geometric shapes.
飞秒激光写入制备光波导主要是通过具有较强穿透能力近红外超短脉冲激光在透明光学材料中进行激光诱导从而改变材料的折射率,完成制备工作。激光诱导过程中,飞秒激光脉冲能量主要通过非线性光学过程被材料吸收,如双光子或多光子吸收,并在短时间内引起隧穿电离和雪崩电离,从而引起应力场改变,致使焦点处材料折射率升高或降低,最终经过一次或数次扫描,形成通道光波导。The fabrication of optical waveguides by femtosecond laser writing is mainly through laser induction in transparent optical materials by near-infrared ultrashort pulse lasers with strong penetrating ability, so as to change the refractive index of the materials and complete the preparation work. In the laser induction process, the femtosecond laser pulse energy is mainly absorbed by the material through nonlinear optical processes, such as two-photon or multi-photon absorption, and causes tunneling ionization and avalanche ionization in a short time, thereby causing changes in the stress field, resulting in The refractive index of the material increases or decreases, and finally passes through one or several scans to form a channel optical waveguide.
采用飞秒激光写入技术在晶体(如:钕掺杂钇铝石榴石晶体,铌酸锂晶体等)中制备的较大尺寸的包层光波导,激光在波导结构中传输时通常呈现多种模式,这种现象显然不利于激光晶体在波导激光方面的应用,但是由于多种模式干涉引起的散斑现象恰好属于散斑计量技术范畴,因此我们可以借助散斑计量技术,基于大尺寸包层光波导结构中的散斑模式,实现对晶体所处环境温度变化的高精度传感测量。Using femtosecond laser writing technology to prepare larger-sized cladding optical waveguides in crystals (such as: Nd-doped yttrium aluminum garnet crystals, lithium niobate crystals, etc.), the laser usually presents various mode, this phenomenon is obviously not conducive to the application of laser crystals in waveguide lasers, but the speckle phenomenon caused by multi-mode interference just belongs to the category of speckle metrology technology, so we can use speckle metrology technology to The speckle pattern in the optical waveguide structure realizes high-precision sensing and measurement of the temperature change of the crystal's environment.
需要强调的是,本发明所述实施例是说明性的,而不是限定性的,因此本发明包括并不限于具体实施方式中所述实施例,凡是由本领域技术人员根据本发明的技术方案得出的其他实施方式,同样属于本发明保护的范围。It should be emphasized that the embodiments of the present invention are illustrative rather than restrictive, so the present invention includes and is not limited to the embodiments described in the specific implementation, and those who are obtained by those skilled in the art according to the technical solutions of the present invention Other implementation modes mentioned above also belong to the protection scope of the present invention.
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