[go: up one dir, main page]

CN108254100B - Optical fiber sensing liquid refractive index and temperature simultaneous measurement system and measurement method - Google Patents

Optical fiber sensing liquid refractive index and temperature simultaneous measurement system and measurement method Download PDF

Info

Publication number
CN108254100B
CN108254100B CN201810100428.1A CN201810100428A CN108254100B CN 108254100 B CN108254100 B CN 108254100B CN 201810100428 A CN201810100428 A CN 201810100428A CN 108254100 B CN108254100 B CN 108254100B
Authority
CN
China
Prior art keywords
optical fiber
liquid
sensing
refractive index
temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201810100428.1A
Other languages
Chinese (zh)
Other versions
CN108254100A (en
Inventor
王东
佟敬阔
靳宝全
王云才
王宇
张明江
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Taiyuan University of Technology
Original Assignee
Taiyuan University of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Taiyuan University of Technology filed Critical Taiyuan University of Technology
Priority to CN201810100428.1A priority Critical patent/CN108254100B/en
Publication of CN108254100A publication Critical patent/CN108254100A/en
Application granted granted Critical
Publication of CN108254100B publication Critical patent/CN108254100B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01KMEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
    • G01K11/00Measuring temperature based upon physical or chemical changes not covered by groups G01K3/00, G01K5/00, G01K7/00 or G01K9/00
    • G01K11/32Measuring temperature based upon physical or chemical changes not covered by groups G01K3/00, G01K5/00, G01K7/00 or G01K9/00 using changes in transmittance, scattering or luminescence in optical fibres
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01DMEASURING NOT SPECIALLY ADAPTED FOR A SPECIFIC VARIABLE; ARRANGEMENTS FOR MEASURING TWO OR MORE VARIABLES NOT COVERED IN A SINGLE OTHER SUBCLASS; TARIFF METERING APPARATUS; MEASURING OR TESTING NOT OTHERWISE PROVIDED FOR
    • G01D5/00Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable
    • G01D5/26Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light
    • G01D5/32Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light with attenuation or whole or partial obturation of beams of light
    • G01D5/34Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light with attenuation or whole or partial obturation of beams of light the beams of light being detected by photocells
    • G01D5/353Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light with attenuation or whole or partial obturation of beams of light the beams of light being detected by photocells influencing the transmission properties of an optical fibre
    • G01D5/35383Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light with attenuation or whole or partial obturation of beams of light the beams of light being detected by photocells influencing the transmission properties of an optical fibre using multiple sensor devices using multiplexing techniques
    • G01D5/35387Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light with attenuation or whole or partial obturation of beams of light the beams of light being detected by photocells influencing the transmission properties of an optical fibre using multiple sensor devices using multiplexing techniques using wavelength division multiplexing
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/41Refractivity; Phase-affecting properties, e.g. optical path length
    • G01N21/4133Refractometers, e.g. differential

Landscapes

  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Measuring Temperature Or Quantity Of Heat (AREA)
  • Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)

Abstract

一种光纤传感液体折射率和温度同时测量系统及测量方法,属于光纤传感检测领域。它是为了解决液体折射率和温度同时远距离在线测量的问题。本发明所述的一种光纤传感液体折射率和温度同时测量系统及测量方法,系统包括:光源(1),波分复用器(2)、光电探测器(3)、采集卡(4)、计算机(5)、光纤恒温槽(6)、传感光纤(7)和传感头(8)。其中传感头仅用一根传感光纤制作而成,包括液体折射率传感部分和和液体温度传感部分,具备体积小,制作简单,抗电磁干扰的特点,克服了现有技术中,传感器制作复杂,测量距离短,液体折射率和温度不能同时测量的局限。本发明适用于对液体的折射率和温度远距离同时在线测量需求领域。

An optical fiber sensing liquid refractive index and temperature simultaneous measurement system and measurement method belong to the field of optical fiber sensing detection. It is to solve the problem of simultaneous long-distance online measurement of liquid refractive index and temperature. A system and method for simultaneously measuring the refractive index and temperature of an optical fiber sensing liquid according to the present invention, the system includes: a light source (1), a wavelength division multiplexer (2), a photoelectric detector (3), and an acquisition card (4 ), computer (5), optical fiber constant temperature bath (6), sensing optical fiber (7) and sensing head (8). The sensing head is made of only one sensing optical fiber, including the liquid refractive index sensing part and the liquid temperature sensing part. It has the characteristics of small size, simple manufacture, and anti-electromagnetic interference, which overcomes the problems in the prior art. The sensor is complicated to make, the measurement distance is short, and the liquid refractive index and temperature cannot be measured at the same time. The invention is suitable for the field of long-distance and simultaneous online measurement of the liquid's refractive index and temperature.

Description

一种光纤传感液体折射率和温度同时测量系统及测量方法An optical fiber sensing liquid refractive index and temperature simultaneous measurement system and measurement method

技术领域technical field

本发明涉及光纤传感检测领域,特别是涉及一种光纤传感液体折射率和温度同时测量系统及测量方法。The invention relates to the field of optical fiber sensing and detection, in particular to an optical fiber sensing liquid refractive index and temperature simultaneous measurement system and measurement method.

背景技术Background technique

折射率是液体介质重要的物理参数之一,在日常生产生活中的各个方面都具有着重要的地位,此外,液体介质的许多性质都可以从其折射率上得到反映,例如液体浓度、温度、混合物成分以及PH值等。所以对于液体折射率的测量在生化分析,环境污染监测,医疗食品等领域有着广泛的应用。折射率的测量方法有多种,其中常用的折射率测量仪器为阿贝测量仪,这种方法需要将被测物放入仪器进行测量,无法满足远距离在线自动化测量的要求。随着光纤传感技术的快速发展,光纤传感器本身因具备体积小,耐腐蚀,抗电磁干扰等特点,采用光纤传感的方法测量液体折射率的方法和技术渐渐受到关注。此外,由于液体折射率受液体的浓度、温度等因素的影响,因而,只有在一定温度下测得的折射率才有意义。因此,需要对折射率和温度同时进行测量。The refractive index is one of the important physical parameters of the liquid medium, which plays an important role in all aspects of daily production and life. In addition, many properties of the liquid medium can be reflected from its refractive index, such as liquid concentration, temperature, Mixture composition and pH value etc. Therefore, the measurement of liquid refractive index has a wide range of applications in biochemical analysis, environmental pollution monitoring, medical food and other fields. There are many ways to measure the refractive index. The commonly used refractive index measuring instrument is the Abbe meter. This method needs to put the measured object into the instrument for measurement, which cannot meet the requirements of long-distance online automatic measurement. With the rapid development of optical fiber sensing technology, the optical fiber sensor itself has the characteristics of small size, corrosion resistance, and anti-electromagnetic interference. The method and technology of measuring the refractive index of liquid by optical fiber sensing has gradually attracted attention. In addition, since the refractive index of liquid is affected by factors such as the concentration and temperature of the liquid, only the refractive index measured at a certain temperature is meaningful. Therefore, simultaneous measurement of the refractive index and temperature is required.

发明内容Contents of the invention

本发明是为了解决远距离液体折射率和温度同时在线测量的问题,现提供一种光纤传感液体折射率和温度同时测量系统及测量方法。The invention aims to solve the problem of simultaneous on-line measurement of long-distance liquid refractive index and temperature, and now provides a simultaneous measurement system and measurement method of optical fiber sensing liquid refractive index and temperature.

一种光纤传感液体折射率和温度同时测量系统,包括:光源,波分复用器、光电探测器、采集卡、计算机、光纤恒温槽、传感光纤和传感头;A system for simultaneously measuring the refractive index and temperature of an optical fiber sensing liquid, comprising: a light source, a wavelength division multiplexer, a photodetector, an acquisition card, a computer, an optical fiber constant temperature bath, a sensing optical fiber, and a sensing head;

所述波分复用器有四个端口,分别为a,b,c,d端口;光源输出的脉冲由波分复用器的a端口输入,波分复用器的b端口通过光纤恒温槽与传感光纤相连接,传感光纤另一端与浸没在待测液体中的传感头相连接;波分复用器的c、d端口共同与光电探测器相连接,光电探测器的信号输出端与采集卡的信号输入端相连接;采集卡的信号输出端与计算机的信号输入端相连接;光纤恒温槽的温度信息通过串口传输至计算机;波分复用器具备滤波功能,可以将b端口输入的由传感头所探测到的光滤波后得到拉曼反斯托克斯光和拉曼斯托克斯光,并分别由c,d端口输出至光电探测器。The wavelength division multiplexer has four ports, namely a, b, c, and d ports; the pulse output by the light source is input by the a port of the wavelength division multiplexer, and the b port of the wavelength division multiplexer passes through the optical fiber thermostat It is connected with the sensing fiber, and the other end of the sensing fiber is connected with the sensing head immersed in the liquid to be tested; the c and d ports of the wavelength division multiplexer are connected with the photodetector together, and the signal output of the photodetector is terminal is connected with the signal input end of the acquisition card; the signal output end of the acquisition card is connected with the signal input end of the computer; the temperature information of the optical fiber constant temperature bath is transmitted to the computer through the serial port; The light detected by the sensor head input through the port is filtered to obtain Raman anti-Stokes light and Raman Stokes light, which are respectively output to the photodetector through ports c and d.

光源发出的脉冲光经a端口进入波分复用器,经b端口输出传输至光纤恒温槽,然后经传感光纤传输至传感头,传感头浸没在待测液体中,传感头探测到的信号沿传感光纤返回,经b端口进入波分复用器,返回的信号经波分复用器滤波后得到拉曼斯托克斯光从c端口输出,拉曼反斯托克斯光从d端口输出,二者经光电探测器转换为电信号后传输至采集卡,采集卡将采集到的信号传输至计算机进行液体折射率和温度信息的解调显示。光纤恒温槽的温度信息通过串口传输至计算机。The pulsed light emitted by the light source enters the wavelength division multiplexer through the a port, and is transmitted to the optical fiber constant temperature bath through the b port, and then transmitted to the sensing head through the sensing optical fiber. The sensing head is immersed in the liquid to be tested, and the sensing head detects The received signal returns along the sensing fiber, enters the wavelength division multiplexer through the b port, and the returned signal is filtered by the wavelength division multiplexer to obtain Raman Stokes light output from the c port, Raman anti-Stokes The light is output from the d port, and the two are converted into electrical signals by the photodetector and then transmitted to the acquisition card. The acquisition card transmits the collected signal to the computer for demodulation and display of the liquid refractive index and temperature information. The temperature information of the fiber optic constant temperature bath is transmitted to the computer through the serial port.

一种光纤传感液体折射率和温度同时测量系统,包括光源,波分复用器、光电探测器、采集卡、计算机、光纤恒温槽、传感光纤、传感头和多通道光开关;所述传感光纤和传感头均为多个;A simultaneous measurement system for optical fiber sensing liquid refractive index and temperature, including light source, wavelength division multiplexer, photoelectric detector, acquisition card, computer, optical fiber constant temperature tank, sensing optical fiber, sensing head and multi-channel optical switch; There are multiple sensing optical fibers and sensing heads;

所述波分复用器有四个端口,分别为a,b,c,d端口;光源输出的脉冲由波分复用器的a端口输入,波分复用器的b端口通过光纤恒温槽与多通道光开关相连接,多通道光开关与多个传感光纤相连接,每个传感光纤的另一端均连接有一个浸没在待测液体中的传感头;波分复用器的c、d端口共同与光电探测器相连接,光电探测器的信号输出端与采集卡的信号输入端相连接;采集卡的信号输出端与计算机的信号输入端相连接;光纤恒温槽的温度信息通过串口传输至计算机;波分复用器具备滤波功能,可以将b端口输入的由传感头所探测到的光滤波后得到拉曼反斯托克斯光和拉曼斯托克斯光,并分别由c,d端口输出至光电探测器。The wavelength division multiplexer has four ports, namely a, b, c, and d ports; the pulse output by the light source is input by the a port of the wavelength division multiplexer, and the b port of the wavelength division multiplexer passes through the optical fiber thermostat It is connected with a multi-channel optical switch, and the multi-channel optical switch is connected with a plurality of sensing optical fibers, and the other end of each sensing optical fiber is connected with a sensing head immersed in the liquid to be measured; the wavelength division multiplexer The c and d ports are connected with the photodetector together, and the signal output end of the photodetector is connected with the signal input end of the acquisition card; the signal output end of the acquisition card is connected with the signal input end of the computer; the temperature information of the optical fiber constant temperature bath It is transmitted to the computer through the serial port; the wavelength division multiplexer has a filtering function, which can filter the light detected by the sensor head input by the b port to obtain Raman anti-Stokes light and Raman Stokes light, And output to the photodetector through the c and d ports respectively.

光源发出的脉冲光经a端口进入波分复用器,经b端口输出传输至光纤恒温槽,然后脉冲光进入多通道光开关,经多通道光开关选择传感通道,然后经传感光纤传输至传感头,传感头浸没在待测液体中,传感头探测到的信号沿传感光纤返回,经b端口进入波分复用器,返回的信号经波分复用器滤波后得到拉曼斯托克斯光从c端口输出,拉曼反斯托克斯光从d端口输出,二者经光电探测器转换为电信号后传输至采集卡,采集卡将采集到的信号传输至计算机进行液体折射率和温度信息的解调显示。光纤恒温槽的温度信息通过串口传输至计算机。The pulsed light emitted by the light source enters the wavelength division multiplexer through the a port, and is transmitted to the optical fiber constant temperature tank through the b port output, and then the pulsed light enters the multi-channel optical switch, selects the sensing channel through the multi-channel optical switch, and then transmits it through the sensing fiber To the sensor head, the sensor head is immersed in the liquid to be tested, the signal detected by the sensor head returns along the sensing fiber, enters the wavelength division multiplexer through the b port, and the returned signal is filtered by the wavelength division multiplexer to obtain Raman Stokes light is output from port c, and Raman anti-Stokes light is output from port d. The two are converted into electrical signals by photodetectors and then transmitted to the acquisition card. The acquisition card transmits the collected signals to The computer performs demodulation and display of liquid refractive index and temperature information. The temperature information of the fiber optic constant temperature bath is transmitted to the computer through the serial port.

所述传感头包括两部分:光纤环和光纤末端;其中光纤环作为液体温度传感器,光纤末端作为液体折射率传感器,光纤末端需剥去包层,切割成垂直光滑的表面,为了避免光纤弯曲损耗,光纤环的直径应大于5厘米。The sensor head consists of two parts: an optical fiber ring and an optical fiber end; the optical fiber ring is used as a liquid temperature sensor, and the optical fiber end is used as a liquid refractive index sensor. The optical fiber end needs to be stripped of the cladding and cut into a vertical smooth surface. loss, the diameter of the fiber optic ring should be greater than 5 cm.

一种光纤传感液体折射率和温度同时测量方法,该方法是基于上述系统实现的,包括以下步骤:A method for simultaneously measuring the refractive index and temperature of an optical fiber sensing liquid, the method is realized based on the above system, and includes the following steps:

步骤一:将传感头浸入蒸馏水中,利用上述系统获得拉曼反斯托克斯光强度(I0as)作为液体折射率传感基准值,利用上述系统获得拉曼反斯托克斯光强度(I0as)和拉曼斯托克斯光强度(I0s)的比值R(T0)作为液体温度传感基准值,然后执行步骤二;Step 1: Immerse the sensing head in distilled water, use the above system to obtain the Raman anti-Stokes light intensity (I 0as ) as the reference value for liquid refractive index sensing, and use the above system to obtain the Raman anti-Stokes light intensity (I 0as ) and the ratio R(T 0 ) of the Raman Stokes light intensity (I 0s ) as the liquid temperature sensing reference value, and then perform step 2;

步骤二:将传感头浸入待测液体中,利用上述系统获得拉曼反斯托克斯光强度(Ias)作为液体折射率传感测量值,利用上述系统获得拉曼反斯托克斯光强度(Ias)和拉曼斯托克斯光强度(Is)比值R(T)作为液体温度传感测量值,然后执行步骤三;Step 2: Immerse the sensor head in the liquid to be measured, use the above system to obtain the Raman anti-Stokes light intensity (I as ) as the liquid refractive index sensing value, and use the above system to obtain the Raman anti-Stokes Light intensity (I as ) and Raman Stokes light intensity (I s ) ratio R(T) is used as liquid temperature sensing measurement value, and then perform step three;

步骤三:利用液体折射率传感基准值I0as和液体折射率传感测量值Ias,获得光纤末端与待测液体接触面的反射率R,利用液体温度传感基准值R(T0)和液体温度传感测量值R(T)的比值,获得待测液体温度的指示量M,然后执行步骤四;Step 3: Use the liquid refractive index sensing reference value I 0as and the liquid refractive index sensing measurement value I as to obtain the reflectivity R of the contact surface between the end of the optical fiber and the liquid to be measured, and use the liquid temperature sensing reference value R(T 0 ) and the ratio of the liquid temperature sensor measurement value R (T), to obtain the indicated amount M of the temperature of the liquid to be measured, and then perform step 4;

步骤四:利用步骤三获得的光纤末端与待测液体接触面的反射率R,获得待测液体的折射率ns;利用步骤三获得的待测液体温度的指示量M,获得待测液体的温度T。Step 4: Use the reflectivity R of the contact surface between the end of the optical fiber and the liquid to be measured obtained in step 3 to obtain the refractive index n s of the liquid to be measured; use the indicated amount M of the temperature of the liquid to be measured obtained in step 3 to obtain the liquid to be measured temperature T.

本发明所述的一种光纤传感液体折射率和温度同时测量系统及测量方法,克服了现有技术中,传感器制作复杂,测量距离短,液体折射率和温度不能同时测量的局限,适用于对液体的折射率和温度实现远距离同时在线测量。The optical fiber sensing liquid refractive index and temperature simultaneous measurement system and measurement method described in the present invention overcome the limitations in the prior art that the sensor is complicated to make, the measurement distance is short, and the liquid refractive index and temperature cannot be measured simultaneously, and is suitable for Realize long-distance simultaneous online measurement of the refractive index and temperature of the liquid.

附图说明Description of drawings

图1为一种光纤传感液体折射率和温度同时测量的系统的一种结构示意图;Fig. 1 is a kind of structure schematic diagram of the system of a kind of optical fiber sensing liquid refractive index and temperature measurement simultaneously;

图2为一种光纤传感液体折射率和温度同时测量的系统另一种结构示意图;Fig. 2 is another structural schematic diagram of a system for simultaneously measuring the refractive index and temperature of a fiber-optic sensing liquid;

图3为光纤传感头结构示意图;Fig. 3 is a structural schematic diagram of an optical fiber sensing head;

图4为一种光纤传感液体折射率和温度同时测量方法的流程图。Fig. 4 is a flow chart of a method for simultaneously measuring the refractive index and temperature of an optical fiber sensing liquid.

1-光源,2-波分复用器,3-光电探测器,4-采集卡,5-计算机,6-光纤恒温槽,7-传感光纤,8-传感头,9-多通道光开关。1-light source, 2-wavelength division multiplexer, 3-photodetector, 4-acquisition card, 5-computer, 6-optical fiber constant temperature tank, 7-sensing optical fiber, 8-sensing head, 9-multi-channel light switch.

具体实施方式Detailed ways

具体实施方式一:参照图1具体说明本实施方式,本实施方式所述一种光纤传感液体折射率和温度同时测量的系统,它包括:光源1,波分复用器2、光电探测器3、采集卡4、计算机5,光纤恒温槽6、传感光纤7和传感头8;Specific embodiment 1: This embodiment is described in detail with reference to Fig. 1, a system for simultaneously measuring the refractive index and temperature of an optical fiber sensing liquid described in this embodiment, which includes: a light source 1, a wavelength division multiplexer 2, a photodetector 3. Acquisition card 4, computer 5, optical fiber constant temperature bath 6, sensing optical fiber 7 and sensing head 8;

光源发出的脉冲光经a端口进入波分复用器,经b端口输出传输至光纤恒温槽,然后经传感光纤传输至传感头,传感头浸没在待测液体中,传感头探测到的信号沿传感光纤返回,经b端口进入波分复用器,返回的信号经波分复用器滤波后得到拉曼斯托克斯光从c端口输出,拉曼反斯托克斯光从d端口输出,二者经光电探测器转换为电信号后传输至采集卡,采集卡将采集到的信号传输至计算机进行液体折射率和温度信息的解调显示。光纤恒温槽的温度信息通过串口传输至计算机。The pulsed light emitted by the light source enters the wavelength division multiplexer through the a port, and is transmitted to the optical fiber constant temperature bath through the b port, and then transmitted to the sensing head through the sensing optical fiber. The sensing head is immersed in the liquid to be tested, and the sensing head detects The received signal returns along the sensing fiber, enters the wavelength division multiplexer through the b port, and the returned signal is filtered by the wavelength division multiplexer to obtain Raman Stokes light output from the c port, Raman anti-Stokes The light is output from the d port, and the two are converted into electrical signals by the photodetector and then transmitted to the acquisition card. The acquisition card transmits the collected signal to the computer for demodulation and display of the liquid refractive index and temperature information. The temperature information of the fiber optic constant temperature bath is transmitted to the computer through the serial port.

具体实施方式二:参照图2具体说明本实施方式,本实施方式所述一种光纤传感液体折射率和温度同时测量的系统,它包括:光源1,波分复用器2、光电探测器3、采集卡4、计算机5,光纤恒温槽6、多通道光开关9、传感光纤7和传感头8;Specific embodiment two: this embodiment is described in detail with reference to Fig. 2, a kind of optical fiber sensing liquid refractive index and temperature measurement system simultaneously described in this embodiment, it comprises: light source 1, wavelength division multiplexer 2, photodetector 3. Acquisition card 4, computer 5, optical fiber constant temperature tank 6, multi-channel optical switch 9, sensing optical fiber 7 and sensing head 8;

光源发出的脉冲光经a端口进入波分复用器,经b端口输出传输至光纤恒温槽,然后脉冲光进入多通道光开关,经多通道光开关选择传感通道,然后经传感光纤传输至传感头,传感头浸没在待测液体中,传感头探测到的信号沿传感光纤返回,经b端口进入波分复用器,返回的信号经波分复用器滤波后得到拉曼斯托克斯光从c端口输出,拉曼反斯托克斯光从d端口输出,二者经光电探测器转换为电信号后传输至采集卡,采集卡将采集到的信号传输至计算机进行液体折射率和温度信息的解调显示。光纤恒温槽的温度信息通过串口传输至计算机。The pulsed light emitted by the light source enters the wavelength division multiplexer through the a port, and is transmitted to the optical fiber constant temperature tank through the b port output, and then the pulsed light enters the multi-channel optical switch, selects the sensing channel through the multi-channel optical switch, and then transmits it through the sensing fiber To the sensor head, the sensor head is immersed in the liquid to be tested, the signal detected by the sensor head returns along the sensing fiber, enters the wavelength division multiplexer through the b port, and the returned signal is filtered by the wavelength division multiplexer to obtain Raman Stokes light is output from port c, and Raman anti-Stokes light is output from port d. The two are converted into electrical signals by photodetectors and then transmitted to the acquisition card. The acquisition card transmits the collected signals to The computer performs demodulation and display of liquid refractive index and temperature information. The temperature information of the fiber optic constant temperature bath is transmitted to the computer through the serial port.

具体实施方式三:本实施方式是对具体实施方式一所述的波分复用器作进一步说明,本实施例中,所述波分复用器有四个端口,分别为a,b,c,d端口,波分复用器具备滤波功能,可以将d端口输入的光滤波得到拉曼反斯托克斯光和拉曼斯托克斯光。Specific embodiment three: this embodiment is a further description of the wavelength division multiplexer described in specific embodiment one, in this embodiment, the wavelength division multiplexer has four ports, respectively a, b, c , the d port, the wavelength division multiplexer has a filtering function, and can filter the light input at the d port to obtain Raman anti-Stokes light and Raman Stokes light.

具体实施方式四:参照图3具体说明本实施方式,本实施方式是对具体实施方式一或二所述的传感头作进一步说明,本实施例中,所述传感头包括两部分:一个光纤末端和一个光纤环;其中光纤环作为液体温度传感器,光纤末端作为液体折射率传感器,光纤末端需剥去包层,切割成垂直光滑的表面,为了避免光纤弯曲损耗,光纤环的直径应大于5厘米。Specific Embodiment 4: This embodiment will be described in detail with reference to Fig. 3. This embodiment is a further description of the sensor head described in Embodiment 1 or 2. In this embodiment, the sensor head includes two parts: a The fiber end and a fiber ring; the fiber ring is used as a liquid temperature sensor, and the fiber end is used as a liquid refractive index sensor. The fiber end needs to be stripped of the cladding and cut into a vertical smooth surface. In order to avoid fiber bending loss, the diameter of the fiber ring should be larger than 5 cm.

具体实施方式五:参照图4具体说明本实施方式,本实施方式所述的一种光纤传感液体折射率和温度同时测量的方法,该方法是基于上述系统实现的,具体实施包括以下步骤:Specific embodiment five: this embodiment is specifically described with reference to Fig. 4, a kind of optical fiber sensing liquid refractive index and the method for temperature simultaneous measurement described in this embodiment, this method is realized based on above-mentioned system, concrete implementation comprises the following steps:

步骤一:将传感头浸入蒸馏水中,利用上述系统获得拉曼反斯托克斯光强度(I0as)作为液体折射率传感基准值,利用上述系统获得拉曼反斯托克斯光强度(I0as)和拉曼斯托克斯光强度(I0s)的比值R(T0)作为液体温度传感基准值,然后执行步骤二;Step 1: Immerse the sensing head in distilled water, use the above system to obtain the Raman anti-Stokes light intensity (I 0as ) as the reference value for liquid refractive index sensing, and use the above system to obtain the Raman anti-Stokes light intensity (I 0as ) and the ratio R(T 0 ) of the Raman Stokes light intensity (I 0s ) as the liquid temperature sensing reference value, and then perform step 2;

步骤二:将传感头浸入待测液体中,利用上述系统获得拉曼反斯托克斯光强度(Ias)作为液体折射率传感测量值,利用上述系统获得拉曼反斯托克斯光强度(Ias)和拉曼斯托克斯光强度(Is)比值R(T)作为液体温度传感测量值,然后执行步骤三;Step 2: Immerse the sensor head in the liquid to be measured, use the above system to obtain the Raman anti-Stokes light intensity (I as ) as the liquid refractive index sensing value, and use the above system to obtain the Raman anti-Stokes Light intensity (I as ) and Raman Stokes light intensity (I s ) ratio R(T) is used as liquid temperature sensing measurement value, and then perform step three;

步骤三:利用液体折射率传感基准值I0as和液体折射率传感测量值Ias,获得光纤末端与待测液体接触面的反射率R,利用液体温度传感基准值R(T0)和液体温度传感测量值R(T)的比值,获得待测液体温度的指示量M,然后执行步骤四;Step 3: Use the liquid refractive index sensing reference value I 0as and the liquid refractive index sensing measurement value I as to obtain the reflectivity R of the contact surface between the end of the optical fiber and the liquid to be measured, and use the liquid temperature sensing reference value R(T 0 ) and the ratio of the liquid temperature sensor measurement value R (T), to obtain the indicated amount M of the temperature of the liquid to be measured, and then perform step 4;

步骤四:利用步骤三获得的光纤末端与待测液体接触面的反射率R,获得待测液体的折射率ns;利用步骤三获得的待测液体温度的指示量M,获得待测液体的温度T。Step 4: Use the reflectivity R of the contact surface between the end of the optical fiber and the liquid to be measured obtained in step 3 to obtain the refractive index n s of the liquid to be measured; use the indicated amount M of the temperature of the liquid to be measured obtained in step 3 to obtain the liquid to be measured temperature T.

具体实施方式六:本实施方式是对具体实施方式五所述的一种光纤传感液体折射率和温度同时测量的方法作进一步说明,本实施方式中,根据如下公式获得光纤末端与待测液体接触面的反射率R,Specific embodiment six: This embodiment is a further description of the method for simultaneously measuring the refractive index and temperature of a fiber-optic sensing liquid described in specific embodiment five. In this embodiment, the optical fiber end and the liquid to be measured are obtained according to the following formula The reflectivity R of the contact surface,

其中,nf为光纤纤芯折射率,n0位蒸馏水的折射率。Among them, n f is the refractive index of the fiber core, and n is the refractive index of distilled water at the 0 position.

具体实施方式七:本实施方式是对具体实施方式五所述的一种光纤传感液体折射率和温度同时测量的方法作进一步说明,本实施方式中,根据如下公式获得待测液体的折射率nsSpecific embodiment seven: This embodiment is a further description of the method for simultaneously measuring the refractive index and temperature of a fiber-optic sensing liquid described in specific embodiment five. In this embodiment, the refractive index of the liquid to be measured is obtained according to the following formula n s ,

具体实施方式八:本实施方式是对具体实施方式五所述的一种光纤传感液体折射率和温度同时测量的方法作进一步说明,本实施方式中,根据如下公式获得液体温度传感基准值R(T0)和液体温度传感测量值R(T),Embodiment 8: This embodiment is a further description of the method for simultaneously measuring the refractive index and temperature of a fiber-optic sensing liquid described in Embodiment 5. In this embodiment, the liquid temperature sensing reference value is obtained according to the following formula R(T 0 ) and liquid temperature sensing measurement R(T),

其中,vas和vs分别为反斯托克斯和斯托克斯光的频率,h为普朗克常量,c为光速,k为玻尔兹曼常量,Δv为拉曼声子频率。where v as and v s are the frequencies of anti-Stokes and Stokes light, respectively, h is Planck's constant, c is the speed of light, k is Boltzmann's constant, and Δv is the Raman phonon frequency.

具体实施方式九:本实施方式是对具体实施方式五所述的一种光纤传感液体折射率和温度同时测量的方法作进一步说明,本实施方式中,根据如下公式获得待测液体温度的指示量M,Specific embodiment nine: This embodiment is a further description of the method for simultaneously measuring the refractive index and temperature of a fiber-optic sensing liquid described in specific embodiment five. In this embodiment, the indication of the temperature of the liquid to be measured is obtained according to the following formula amount M,

具体实施方式十:本实施方式是对具体实施方式五所述的一种光纤传感液体折射率和温度同时测量的方法作进一步说明,本实施方式中,根据如下公式获得待测液体温度T,Embodiment 10: This embodiment is a further description of the method for simultaneously measuring the refractive index and temperature of a fiber-optic sensing liquid described in Embodiment 5. In this embodiment, the temperature T of the liquid to be measured is obtained according to the following formula,

以上所述实施例仅表达了本发明的几种实施方式,其描述较为具体和详细,但并不能因此而理解为对发明专利范围的限制。应当指出的是,对于本领域的普通技术人员来说,在不脱离本发明构思的前提下,还可以做出若干变形和改进,这些都属于本发明的保护范围。The above-mentioned embodiments only express several implementation modes of the present invention, and the descriptions thereof are relatively specific and detailed, but should not be construed as limiting the patent scope of the invention. It should be pointed out that those skilled in the art can make several modifications and improvements without departing from the concept of the present invention, and these all belong to the protection scope of the present invention.

Claims (4)

1. An optical fiber sensing system for simultaneously measuring the refractive index and temperature of a liquid, comprising: the device comprises a light source (1), a wavelength division multiplexer (2), a photoelectric detector (3), a collection card (4), a computer (5), an optical fiber thermostatic bath (6), a sensing optical fiber (7) and a sensing head (8);
The wavelength division multiplexer (2) is provided with four ports, namely a port, b port, c port and d port; pulses output by the light source (1) are input from an a port of the wavelength division multiplexer (2), a b port of the wavelength division multiplexer (2) is connected with a sensing optical fiber (7) through an optical fiber thermostatic bath (6), and the other end of the sensing optical fiber (7) is connected with a sensing head (8) immersed in liquid to be measured; the ports c and d of the wavelength division multiplexer (2) are connected with the photoelectric detector (3) together, and the signal output end of the photoelectric detector (3) is connected with the signal input end of the acquisition card (4); the signal output end of the acquisition card (4) is connected with the signal input end of the computer (5); the temperature information of the optical fiber thermostatic bath (6) is transmitted to the computer (5) through a serial port; the wavelength division multiplexer (2) has a filtering function, can filter light which is input from a port b and detected by the sensing head (8) to obtain Raman anti-Stokes light and Raman Stokes light, and outputs the Raman anti-Stokes light and the Raman Stokes light to the photoelectric detector (3) from ports c and d respectively; the sensor head (8) comprises two parts: an optical fiber ring (8-1) and an optical fiber end (8-2); wherein the optical fiber ring (8-1) is used as a liquid temperature sensor, the optical fiber tail end (8-2) is used as a liquid refractive index sensor, and the cladding of the optical fiber tail end (8-2) needs to be stripped and cut into a vertical and smooth surface; the diameter of the optical fiber ring (8-1) is more than 5 cm.
2. The utility model provides an optical fiber sensing liquid refracting index and temperature simultaneous measurement system which characterized in that: the device comprises a light source (1), a wavelength division multiplexer (2), a photoelectric detector (3), an acquisition card (4), a computer (5), an optical fiber thermostatic bath (6), a sensing optical fiber (7), a sensing head (8) and a multi-channel optical switch (9); the sensing optical fibers (7) and the sensing heads (8) are multiple;
The wavelength division multiplexer (2) is provided with four ports, namely a port, b port, c port and d port; pulses output by the light source (1) are input from an a port of the wavelength division multiplexer (2), a b port of the wavelength division multiplexer (2) is connected with a multi-channel optical switch (9) through an optical fiber thermostatic bath (6), the multi-channel optical switch (9) is connected with a plurality of sensing optical fibers (7), and the other end of each sensing optical fiber (7) is connected with a sensing head (8) immersed in liquid to be measured; the ports c and d of the wavelength division multiplexer (2) are connected with the photoelectric detector (3) together, and the signal output end of the photoelectric detector (3) is connected with the signal input end of the acquisition card (4); the signal output end of the acquisition card (4) is connected with the signal input end of the computer (5); the temperature information of the optical fiber thermostatic bath (6) is transmitted to the computer (5) through a serial port; the wavelength division multiplexer (2) has a filtering function, can filter light which is input from a port b and detected by the sensing head (8) to obtain Raman anti-Stokes light and Raman Stokes light, and outputs the Raman anti-Stokes light and the Raman Stokes light to the photoelectric detector (3) from ports c and d respectively; the sensor head (8) comprises two parts: an optical fiber ring (8-1) and an optical fiber end (8-2); wherein the optical fiber ring (8-1) is used as a liquid temperature sensor, the optical fiber tail end (8-2) is used as a liquid refractive index sensor, and the cladding of the optical fiber tail end (8-2) needs to be stripped and cut into a vertical and smooth surface; the diameter of the optical fiber ring (8-1) is more than 5 cm.
3. The system for simultaneously measuring the refractive index and the temperature of the liquid by the optical fiber sensing according to claim 1 or 2, wherein the light source (1) is connected with the acquisition card (4), and the signal output end of the computer (5) is connected with the signal input end of the light source (1).
4. A method for simultaneously measuring the refractive index and the temperature of a liquid by optical fiber sensing, which is realized by the system of any one of claims 1 to 3, and comprises the following steps:
The method comprises the following steps: the sensor head (8) is immersed in distilled water, and the Raman anti-Stokes light intensity I is obtained by using the system0asThe Raman anti-Stokes light intensity I is obtained by using the system as a liquid refractive index sensing reference value0asAnd Raman Stokes light intensity I0sratio R (T)0) Taking the liquid temperature as a liquid temperature sensing reference value, and then executing a step two;
Step two: the sensing head (8) is immersed in the liquid to be measured, and the Raman anti-Stokes light intensity I is obtained by using the systemasas a liquid refractive index sensing measurement value, the system is used for obtaining the Raman anti-Stokes light intensity Iasand Raman Stokes light intensity IsTaking the ratio R (T) as a liquid temperature sensing measurement value, and then executing a third step;
Step three: sensing reference value I by using liquid refractive index0asAnd liquid refractive index sensing measurement IasObtaining the reflectivity R of the contact surface of the optical fiber end (8-2) and the liquid to be detected, and utilizing the liquid temperature sensing reference value R (T)0) And the liquid temperature sensing measured value R (T) to obtain the indicated quantity M of the liquid temperature to be measured, and then executing the step four;
Step four: obtaining the refractive index n of the liquid to be detected by utilizing the reflectivity R of the contact surface of the optical fiber tail end (8-2) and the liquid to be detected obtained in the step threes(ii) a Obtaining the temperature T of the liquid to be measured by using the indication quantity M of the temperature of the liquid to be measured obtained in the step three;
The reflectivity R of the contact surface of the optical fiber tail end (8-2) and the liquid to be detected is obtained according to the following formula,
Wherein n isfIs the refractive index of the core of the optical fiber, n0Is the refractive index of distilled water; obtaining the refractive index n of the liquid to be measured according to the following formulas
the liquid temperature sensing reference value R (T) is obtained according to the following formula0) And a liquid temperature sensing measurement R (T),
wherein v isasAnd vsThe frequencies of the anti-stokes light and the stokes light respectively, h is the Planck constant, c is the speed of light, k is the Boltzmann constant, Deltav is the Raman phonon frequency,
the indicated quantity M of the temperature of the liquid to be measured is obtained according to the following formula,
The temperature T of the liquid to be measured is obtained according to the following formula,
CN201810100428.1A 2018-02-01 2018-02-01 Optical fiber sensing liquid refractive index and temperature simultaneous measurement system and measurement method Active CN108254100B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810100428.1A CN108254100B (en) 2018-02-01 2018-02-01 Optical fiber sensing liquid refractive index and temperature simultaneous measurement system and measurement method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810100428.1A CN108254100B (en) 2018-02-01 2018-02-01 Optical fiber sensing liquid refractive index and temperature simultaneous measurement system and measurement method

Publications (2)

Publication Number Publication Date
CN108254100A CN108254100A (en) 2018-07-06
CN108254100B true CN108254100B (en) 2019-12-13

Family

ID=62743588

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810100428.1A Active CN108254100B (en) 2018-02-01 2018-02-01 Optical fiber sensing liquid refractive index and temperature simultaneous measurement system and measurement method

Country Status (1)

Country Link
CN (1) CN108254100B (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109164065A (en) * 2018-10-24 2019-01-08 深圳大学 The measuring system and measurement method of thermo-optical coeffecient
CN109709070B (en) * 2018-12-29 2021-07-20 天津大学 A dual-parameter measurement method of refractive index and temperature using composite fiber grating sensor
CN109884063B (en) * 2019-04-24 2021-08-20 杭州翔毅科技有限公司 Acquisition structure for liquid sensor
CN110906988A (en) * 2019-12-25 2020-03-24 天津工业大学 A dual-parameter optical fiber sensing and detection device with dual microfluidic channels

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1963400A (en) * 2006-11-16 2007-05-16 国家纳米技术与工程研究院 Fibre optic sensor for measuring temperature and refractive index of liquid contemporarily
CN201034625Y (en) * 2006-12-08 2008-03-12 东华大学 Multi-parameter optical sensor
CN102313568A (en) * 2011-08-30 2012-01-11 杭州布里特威光电技术有限公司 Distributed optical fiber sensing device for simultaneously detecting Brillouin scattering and Raman scattering
CN202648678U (en) * 2012-04-05 2013-01-02 陈云钦 Optical fiber probe and compound liquid optical fiber concentration meter using same
CN204188523U (en) * 2014-07-23 2015-03-04 中国计量学院 The real-time measuring optical fiber sensor of a kind of solution concentration based on Fresnel reflection
CN106404217A (en) * 2016-11-17 2017-02-15 太原理工大学 Novel temperature demodulation method based on distributed optical fiber Raman temperature measurement
CN107402027A (en) * 2017-06-28 2017-11-28 宋章启 Physical amount measuring method based on intensity modulation optical fiber sensor

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1963400A (en) * 2006-11-16 2007-05-16 国家纳米技术与工程研究院 Fibre optic sensor for measuring temperature and refractive index of liquid contemporarily
CN201034625Y (en) * 2006-12-08 2008-03-12 东华大学 Multi-parameter optical sensor
CN102313568A (en) * 2011-08-30 2012-01-11 杭州布里特威光电技术有限公司 Distributed optical fiber sensing device for simultaneously detecting Brillouin scattering and Raman scattering
CN202648678U (en) * 2012-04-05 2013-01-02 陈云钦 Optical fiber probe and compound liquid optical fiber concentration meter using same
CN204188523U (en) * 2014-07-23 2015-03-04 中国计量学院 The real-time measuring optical fiber sensor of a kind of solution concentration based on Fresnel reflection
CN106404217A (en) * 2016-11-17 2017-02-15 太原理工大学 Novel temperature demodulation method based on distributed optical fiber Raman temperature measurement
CN107402027A (en) * 2017-06-28 2017-11-28 宋章启 Physical amount measuring method based on intensity modulation optical fiber sensor

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
基于AWG的液体折射率多点测量光纤传感器研究;李记辉;《中国优秀硕士学位论文全文数据库(信息科技辑)》;20150215(第2期);第25-26页 *

Also Published As

Publication number Publication date
CN108254100A (en) 2018-07-06

Similar Documents

Publication Publication Date Title
CN108254100B (en) Optical fiber sensing liquid refractive index and temperature simultaneous measurement system and measurement method
CN111006786B (en) Dual-channel high-precision temperature demodulation method based on distributed optical fiber Raman sensing system
CN106596474B (en) A three-channel SPR sensor based on seven-core fiber
CN111006788B (en) High-precision optical fiber Raman temperature detection method based on anti-Stokes light self-demodulation
CN111006787B (en) Distributed fiber Raman double-ended temperature demodulation method based on differential temperature compensation
CN106442340B (en) Device and method for detecting seawater salinity by long-period fiber gratings
CN102914518B (en) Laser online sensing device and method for simultaneously measuring turbidity and particle size
CN202453113U (en) Sensor for measuring temperature and salinity of seawater based on fibre Bragg grating (FBG)
CN103196475B (en) Hybrid fiber bragg grating sensing system for simultaneously measuring temperature, humidity and gas concentration
CN205091262U (en) Glycerine concentration detection system that combines smart mobile phone and single mode - thin core - single mode fiber
CN202420549U (en) Transformer multi-parameter fiber on-line monitoring system
CN110567893A (en) An optofluidic detector for the determination of phosphorus content in seawater based on mobile phone APP
CN102519907B (en) Reflection type refractive index sensor based on optical fibre and micro-fluidic chip
JPS5489680A (en) Optical measuring method and optical measuring apparatus
Liyun et al. Optical fiber sensor determination of the water salinity based on surface plasmon resonance
CN110196070A (en) A kind of novel micro nanometer Fiber Bragg Grating index sensor
CN212482511U (en) A device for large-scale high-precision fiber grating sensing based on cavity ring-down
Jiang et al. Design of optical fiber SPR sensing system for water quality monitoring
CN102226763B (en) AWG-based star-shaped topological quasi-distributed multipoint refractive index sensing system
CN202255625U (en) Spectrometer based on fiber grating time domain reflection technology
CN106908401A (en) A kind of binary channels water quality environment fibre-optical sensing device and method based on cascade cavity-type BPM
CN207423802U (en) Optical fibre refractivity sensing device based on capture card
CN208366829U (en) It is a kind of to utilize the device of optical fiber cavity-type BPM measurement optically-active solution concentration containing polarization maintaining optical fibre
CN205898162U (en) Measurement system of multiplicable fiber grating rate of utilization
CN206331138U (en) A kind of new microflute polymer light fiber liquid level sensing device

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant