CN108238715A - A kind of inorganic fibre insulation board and preparation method thereof - Google Patents
A kind of inorganic fibre insulation board and preparation method thereof Download PDFInfo
- Publication number
- CN108238715A CN108238715A CN201810031081.XA CN201810031081A CN108238715A CN 108238715 A CN108238715 A CN 108238715A CN 201810031081 A CN201810031081 A CN 201810031081A CN 108238715 A CN108238715 A CN 108238715A
- Authority
- CN
- China
- Prior art keywords
- parts
- insulation board
- coalescents
- fibre
- cellulose ether
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000000835 fiber Substances 0.000 title claims abstract description 115
- 238000009413 insulation Methods 0.000 title claims abstract description 97
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- 229920003086 cellulose ether Polymers 0.000 claims abstract description 68
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 58
- 238000003723 Smelting Methods 0.000 claims abstract description 30
- 238000001035 drying Methods 0.000 claims abstract description 30
- 239000004113 Sepiolite Substances 0.000 claims abstract description 29
- 239000010881 fly ash Substances 0.000 claims abstract description 29
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 claims abstract description 29
- 235000019355 sepiolite Nutrition 0.000 claims abstract description 29
- 229910052624 sepiolite Inorganic materials 0.000 claims abstract description 29
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 29
- 239000004743 Polypropylene Substances 0.000 claims abstract description 25
- -1 polypropylene Polymers 0.000 claims abstract description 25
- 229920001155 polypropylene Polymers 0.000 claims abstract description 25
- 239000000919 ceramic Substances 0.000 claims abstract description 17
- 238000000034 method Methods 0.000 claims abstract description 17
- 239000000463 material Substances 0.000 claims abstract description 16
- 238000004806 packaging method and process Methods 0.000 claims abstract description 16
- 239000000203 mixture Substances 0.000 claims description 55
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 claims description 42
- 239000011265 semifinished product Substances 0.000 claims description 41
- 238000007873 sieving Methods 0.000 claims description 27
- IDQBJILTOGBZCR-UHFFFAOYSA-N 1-butoxypropan-1-ol Chemical compound CCCCOC(O)CC IDQBJILTOGBZCR-UHFFFAOYSA-N 0.000 claims description 26
- LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 claims description 16
- 235000019445 benzyl alcohol Nutrition 0.000 claims description 14
- 239000012535 impurity Substances 0.000 claims description 14
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 claims description 14
- 238000003860 storage Methods 0.000 claims description 14
- 239000012752 auxiliary agent Substances 0.000 claims description 2
- 239000000047 product Substances 0.000 claims description 2
- RWNUSVWFHDHRCJ-UHFFFAOYSA-N 1-butoxypropan-2-ol Chemical compound CCCCOCC(C)O RWNUSVWFHDHRCJ-UHFFFAOYSA-N 0.000 claims 1
- 230000000845 anti-microbial effect Effects 0.000 abstract description 9
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 238000012545 processing Methods 0.000 abstract description 4
- 239000003153 chemical reaction reagent Substances 0.000 abstract description 2
- 238000005520 cutting process Methods 0.000 abstract description 2
- XNWFRZJHXBZDAG-UHFFFAOYSA-N 2-METHOXYETHANOL Chemical compound COCCO XNWFRZJHXBZDAG-UHFFFAOYSA-N 0.000 description 12
- 229910052573 porcelain Inorganic materials 0.000 description 12
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 6
- 238000012546 transfer Methods 0.000 description 6
- HTMIBDQKFHUPSX-UHFFFAOYSA-N methdilazine Chemical group C1N(C)CCC1CN1C2=CC=CC=C2SC2=CC=CC=C21 HTMIBDQKFHUPSX-UHFFFAOYSA-N 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- DURPTKYDGMDSBL-UHFFFAOYSA-N 1-butoxybutane Chemical compound CCCCOCCCC DURPTKYDGMDSBL-UHFFFAOYSA-N 0.000 description 1
- 229920001817 Agar Polymers 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000008272 agar Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 239000008223 sterile water Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/005—Manufacture of flakes
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/04—Manufacture of glass fibres or filaments by using centrifugal force, e.g. spinning through radial orifices; Construction of the spinner cups therefor
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C13/00—Fibre or filament compositions
- C03C13/06—Mineral fibres, e.g. slag wool, mineral wool, rock wool
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Geochemistry & Mineralogy (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Thermal Insulation (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Laminated Bodies (AREA)
Abstract
The present invention discloses a kind of thermal insulation board and preparation method thereof, belongs to thermal insulation board production technical field, relates generally to a kind of inorganic fibre insulation board and preparation method thereof.A kind of inorganic fibre insulation board, by weight including following material：30 45 parts of gangue, 75 82 parts of basalt, 30 42 parts of silica, 12 15 parts of ceramics, 38 parts of nano-titanium dioxide, 10 15 parts of sepiolite fibre, 13 parts of coalescents, 0.3 0.5 parts of cellulose ether, 25 30 parts of flyash, 0.5 2 parts of polypropylene fibre；Present invention simultaneously discloses preparation methods, by drying dispatching, electric smelting into fine, pendulum and cutting packaging step, inorfil are carried out deep processing processing, forms the inorganic fibre insulation board with good thermal insulation property and anti-microbial property.The present invention is not required to addition chemical reagent, reduces the pollution of air, simple for process, it is easy to accomplish.
Description
Technical field
The present invention relates to a kind of thermal insulation boards and preparation method thereof, belong to thermal insulation board production technical field, and in particular to a kind of
Inorganic fibre insulation board and preparation method thereof.
Background technology
As the development of science and technology and social progress, people are more and more stronger to the consciousness of environmental protection, some severes are dirty
The industrial processes product of dye starts to environmentally protective revolution in mode of production.Inorfil becomes in recent years as environment-friendly materials
The much-talked-about topic of people's research.At present, as long as to the processing of inorfil on some primary handicrafts, utilization rate is low.
Invention content
To solve the above-mentioned problems, the present invention discloses a kind of inorganic fibre insulation board and preparation method thereof, by inorganic
Inorfil advanced treating is processed in the processing of fiber, is formed the inorfil with good thermal insulation property and anti-microbial property and is protected
Warm plate.
The object of the present invention is achieved like this：
A kind of inorganic fibre insulation board, by weight including following material：30-45 parts of gangue, 75-82 parts of basalt, silica
30-42 parts, 12-15 parts of ceramics, 3-8 parts of nano-titanium dioxide, 10-15 parts of sepiolite fibre, 1-3 parts of coalescents, cellulose
0.3-0.5 parts of ether, 25-30 parts of flyash, 0.5-2 parts of polypropylene fibre.
Further, the coalescents include propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, and described the third two
The mass ratio of alcohol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol is 2:5:1.
A kind of preparation method of inorganic fibre insulation board, includes the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving.
Further, sieving described in step 1 screens out impurity using sieve, and the mesh size is 0.0025-0.0035
Denier.
Step 2：The mixture of step 1 is put into electric smelting in smelting furnace and, into melt, is separately added into coalescents and cellulose
Mixture after standing 45 minutes, is put into centrifuge into superfine fibre by ether.
Further, the adition process of coalescents described in step 2 and cellulose ether specifically includes：Add in 1/3 into
Film auxiliary agent and 2/3 cellulose ether；(2) mixture is stood 25 minutes；(3) 2/3 coalescents and 1/3 fiber are added
Plain ether.
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum.
Further, semi-finished product thermal insulation board described in step 3 is 4 laminates, and each laminate thickness is 1:3:5:2.
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
Compared with prior art, the present invention it has the advantages that：According to a kind of inorfil disclosed in this invention
Thermal insulation board and preparation method thereof by drying dispatching, electric smelting into fine, pendulum and cutting packaging step, inorfil is carried out deep
Working process is spent, forms the inorganic fibre insulation board with good thermal insulation property and anti-microbial property.The present invention is not required to addition chemistry
Reagent reduces the pollution of air, simple for process, it is easy to accomplish.
Specific embodiment
Heat-insulating property is tested：
Embodiment 1
A kind of inorganic fibre insulation board, by weight including following material：30 parts of gangue, 75 parts of basalt, 30 parts of silica, pottery
12 parts of porcelain, 10 parts of sepiolite fibre, 1 part of coalescents, 0.3 part of cellulose ether, 25 parts of flyash, gathers 3 parts of nano-titanium dioxide
0.5 part of tacryl.
The coalescents include propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, the propandiol butyl ether, third
The mass ratio of glycol methyl ether acetate and benzyl alcohol is 2:5:1.
A kind of preparation method of inorganic fibre insulation board, includes the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving；
Step 2：The mixture of step 1 is put into smelting furnace electric smelting into melt, is separately added into coalescents and cellulose ether, it is quiet
After putting 45 minutes, mixture is put into centrifuge into superfine fibre；
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum；
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
Sieving described in step 1 screens out impurity using sieve, and the mesh size is 0.0025 denier.
The adition process of coalescents described in step 2 and cellulose ether specifically includes：Add in 1/3 coalescents and
2/3 cellulose ether；(2) mixture is stood 25 minutes；(3) 2/3 coalescents and 1/3 cellulose ether are added.
Semi-finished product thermal insulation board described in step 3 is 4 laminates, and each laminate thickness is 1:3:5:2.
Embodiment 2
A kind of inorganic fibre insulation board, by weight including following material：33 parts of gangue, 78 parts of basalt, 33 parts of silica, pottery
13 parts of porcelain, 4 parts of nano-titanium dioxide, 12 parts of sepiolite fibre, 1.5 parts of coalescents, 0.35 part of cellulose ether, flyash 26
Part, 0.8 part of polypropylene fibre.
The coalescents include propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, the propandiol butyl ether, third
The mass ratio of glycol methyl ether acetate and benzyl alcohol is 2:5:1.
A kind of preparation method of inorganic fibre insulation board, includes the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving；
Step 2：The mixture of step 1 is put into smelting furnace electric smelting into melt, is separately added into coalescents and cellulose ether, it is quiet
After putting 45 minutes, mixture is put into centrifuge into superfine fibre；
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum；
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
Sieving described in step 1 screens out impurity using sieve, and the mesh size is 0.0028 denier.
The adition process of coalescents described in step 2 and cellulose ether specifically includes：Add in 1/3 coalescents and
2/3 cellulose ether；(2) mixture is stood 25 minutes；(3) 2/3 coalescents and 1/3 cellulose ether are added.
Semi-finished product thermal insulation board described in step 3 is 4 laminates, and each laminate thickness is 1:3:5:2.
Embodiment 3
A kind of inorganic fibre insulation board, by weight including following material：36 parts of gangue, 80 parts of basalt, 35 parts of silica, pottery
13.5 parts of porcelain, 6 parts of nano-titanium dioxide, 13 parts of sepiolite fibre, 2 parts of coalescents, 0.4 part of cellulose ether, 27 parts of flyash,
1 part of polypropylene fibre.
The coalescents include propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, the propandiol butyl ether, third
The mass ratio of glycol methyl ether acetate and benzyl alcohol is 2:5:1.
A kind of preparation method of inorganic fibre insulation board, includes the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving；
Step 2：The mixture of step 1 is put into smelting furnace electric smelting into melt, is separately added into coalescents and cellulose ether, it is quiet
After putting 45 minutes, mixture is put into centrifuge into superfine fibre；
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum；
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
Sieving described in step 1 screens out impurity using sieve, and the mesh size is 0.0030 denier.
The adition process of coalescents described in step 2 and cellulose ether specifically includes：Add in 1/3 coalescents and
2/3 cellulose ether；(2) mixture is stood 25 minutes；(3) 2/3 coalescents and 1/3 cellulose ether are added.
Semi-finished product thermal insulation board described in step 3 is 4 laminates, and each laminate thickness is 1:3:5:2.
Embodiment 4
A kind of inorganic fibre insulation board, by weight including following material：40 parts of gangue, 81 parts of basalt, 40 parts of silica, pottery
14 parts of porcelain, 7 parts of nano-titanium dioxide, 14 parts of sepiolite fibre, 2.5 parts of coalescents, 0.45 part of cellulose ether, flyash 28
Part, 1.5 parts of polypropylene fibre.
The coalescents include propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, the propandiol butyl ether, third
The mass ratio of glycol methyl ether acetate and benzyl alcohol is 2:5:1.
A kind of preparation method of inorganic fibre insulation board, includes the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving；
Step 2：The mixture of step 1 is put into smelting furnace electric smelting into melt, is separately added into coalescents and cellulose ether, it is quiet
After putting 45 minutes, mixture is put into centrifuge into superfine fibre；
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum；
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
Sieving described in step 1 screens out impurity using sieve, and the mesh size is 0.0032 denier.
The adition process of coalescents described in step 2 and cellulose ether specifically includes：Add in 1/3 coalescents and
2/3 cellulose ether；(2) mixture is stood 25 minutes；(3) 2/3 coalescents and 1/3 cellulose ether are added.
Semi-finished product thermal insulation board described in step 3 is 4 laminates, and each laminate thickness is 1:3:5:2.
Embodiment 5
A kind of inorganic fibre insulation board, by weight including following material：45 parts of gangue, 82 parts of basalt, 42 parts of silica, pottery
15 parts of porcelain, 15 parts of sepiolite fibre, 3 parts of coalescents, 0.5 part of cellulose ether, 30 parts of flyash, gathers 8 parts of nano-titanium dioxide
2 parts of tacryl.
The coalescents include propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, the propandiol butyl ether, third
The mass ratio of glycol methyl ether acetate and benzyl alcohol is 2:5:1.
A kind of preparation method of inorganic fibre insulation board, includes the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving；
Step 2：The mixture of step 1 is put into smelting furnace electric smelting into melt, is separately added into coalescents and cellulose ether, it is quiet
After putting 45 minutes, mixture is put into centrifuge into superfine fibre；
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum；
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
Sieving described in step 1 screens out impurity using sieve, and the mesh size is 0.0035 denier.
The adition process of coalescents described in step 2 and cellulose ether specifically includes：Add in 1/3 coalescents and
2/3 cellulose ether；(2) mixture is stood 25 minutes；(3) 2/3 coalescents and 1/3 cellulose ether are added.
Semi-finished product thermal insulation board described in step 3 is 4 laminates, and each laminate thickness is 1:3:5:2.
Comparative example 1
A kind of inorganic fibre insulation board, by weight including following material：28 parts of gangue, 70 parts of basalt, 25 parts of silica, pottery
10 parts of porcelain, 2 parts of nano-titanium dioxide, 8 parts of sepiolite fibre, 0.5 part of coalescents, 0.2 part of cellulose ether, 20 parts of flyash,
0.3 part of polypropylene fibre.
The coalescents include propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, the propandiol butyl ether, third
The mass ratio of glycol methyl ether acetate and benzyl alcohol is 2:5:1.
A kind of preparation method of inorganic fibre insulation board, includes the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving；
Step 2：The mixture of step 1 is put into smelting furnace electric smelting into melt, is separately added into coalescents and cellulose ether, it is quiet
After putting 45 minutes, mixture is put into centrifuge into superfine fibre；
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum；
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
Sieving described in step 1 screens out impurity using sieve, and the mesh size is 0.0020 denier.
The adition process of coalescents described in step 2 and cellulose ether specifically includes：Add in 1/3 coalescents and
2/3 cellulose ether；(2) mixture is stood 25 minutes；(3) 2/3 coalescents and 1/3 cellulose ether are added.
Semi-finished product thermal insulation board described in step 3 is 4 laminates, and each laminate thickness is 1:3:5:2.
Heat-insulating property test method：According to heat balance principle, thermal insulation board to be measured in embodiment 1-5 and comparative example 1 is put
Winter indoor and outdoor meteorological condition is established respectively between the babinet of two different temperatures, in the two babinets to be tested.Hot tank
Simulate winter indoor air temperature, wind speed；Ice chest simulation winter outdoor temperature, wind speed and radiation condition.By several hours
Operation, whole device reach stable state.After forming stable temperature field and velocity field, the air of thermal insulation board both sides to be measured is tested
Temperature and surface velocity, and calculate Coefficient K.
The formula of Coefficient K is represented by：
In formula,To carry out the total heat flow of heat exchange；For the metering area perpendicular to hot-fluid；Environment for hot tank side
Temperature；Environment temperature for ice chest side.Test result is as follows shown in table 1.
1 heat-insulating property of table is tested
Upper table 1 represents the heat-insulating property of the inorganic fibre insulation board under different ratio in embodiment 1-5 and comparative example 1, from table 1
As can be seen that compared with prior art, the heat transfer coefficient of embodiment 1 reduces 31.12%, and thermal center province rate improves 11.42%, in fact
Applying the heat transfer coefficient of example 2 reduces 33.86%, and thermal center province rate improves 13.05%, and the heat transfer coefficient of embodiment 3 reduces
37.96%, thermal center province rate improves 15.15%, and the heat transfer coefficient of embodiment 4 reduces 44.81%, and thermal center province rate improves
17.72%, the heat transfer coefficient of embodiment 5 reduces 48.34%, and thermal center province rate improves 19.05%.
The above result shows that according to inorganic fibre insulation board manufactured in the present embodiment, heat transfer coefficient continuously decreases, and thermal center saves
Rate gradually rises, and heat-insulating property gradually enhances compared with prior art.
Anti-microbial property test：
Embodiment 6
A kind of inorganic fibre insulation board, by weight including following material：30 parts of gangue, 75 parts of basalt, 30 parts of silica, pottery
12 parts of porcelain, 10 parts of sepiolite fibre, 1 part of coalescents, 0.3 part of cellulose ether, 25 parts of flyash, gathers 3 parts of nano-titanium dioxide
0.5 part of tacryl.
The coalescents include propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, the propandiol butyl ether, third
The mass ratio of glycol methyl ether acetate and benzyl alcohol is 2:5:1.
A kind of preparation method of inorganic fibre insulation board, includes the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving；
Step 2：The mixture of step 1 is put into smelting furnace electric smelting into melt, is separately added into coalescents and cellulose ether, it is quiet
After putting 45 minutes, mixture is put into centrifuge into superfine fibre；
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum；
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
Sieving described in step 1 screens out impurity using sieve, and the mesh size is 0.0025 denier.
The adition process of coalescents described in step 2 and cellulose ether specifically includes：Add in 1/3 coalescents and
2/3 cellulose ether；(2) mixture is stood 25 minutes；(3) 2/3 coalescents and 1/3 cellulose ether are added.
Semi-finished product thermal insulation board described in step 3 is 4 laminates, and each laminate thickness is 1:3:5:2.
Embodiment 7
A kind of inorganic fibre insulation board, by weight including following material：33 parts of gangue, 78 parts of basalt, 33 parts of silica, pottery
13 parts of porcelain, 4 parts of nano-titanium dioxide, 12 parts of sepiolite fibre, 1.5 parts of coalescents, 0.35 part of cellulose ether, flyash 26
Part, 0.8 part of polypropylene fibre.
The coalescents include propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, the propandiol butyl ether, third
The mass ratio of glycol methyl ether acetate and benzyl alcohol is 2:5:1.
A kind of preparation method of inorganic fibre insulation board, includes the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving；
Step 2：The mixture of step 1 is put into smelting furnace electric smelting into melt, is separately added into coalescents and cellulose ether, it is quiet
After putting 45 minutes, mixture is put into centrifuge into superfine fibre；
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum；
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
Sieving described in step 1 screens out impurity using sieve, and the mesh size is 0.0028 denier.
The adition process of coalescents described in step 2 and cellulose ether specifically includes：Add in 1/3 coalescents and
2/3 cellulose ether；(2) mixture is stood 25 minutes；(3) 2/3 coalescents and 1/3 cellulose ether are added.
Semi-finished product thermal insulation board described in step 3 is 4 laminates, and each laminate thickness is 1:3:5:2.
Embodiment 8
A kind of inorganic fibre insulation board, by weight including following material：36 parts of gangue, 80 parts of basalt, 35 parts of silica, pottery
13.5 parts of porcelain, 6 parts of nano-titanium dioxide, 13 parts of sepiolite fibre, 2 parts of coalescents, 0.4 part of cellulose ether, 27 parts of flyash,
1 part of polypropylene fibre.
The coalescents include propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, the propandiol butyl ether, third
The mass ratio of glycol methyl ether acetate and benzyl alcohol is 2:5:1.
A kind of preparation method of inorganic fibre insulation board, includes the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving；
Step 2：The mixture of step 1 is put into smelting furnace electric smelting into melt, is separately added into coalescents and cellulose ether, it is quiet
After putting 45 minutes, mixture is put into centrifuge into superfine fibre；
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum；
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
Sieving described in step 1 screens out impurity using sieve, and the mesh size is 0.0030 denier.
The adition process of coalescents described in step 2 and cellulose ether specifically includes：Add in 1/3 coalescents and
2/3 cellulose ether；(2) mixture is stood 25 minutes；(3) 2/3 coalescents and 1/3 cellulose ether are added.
Semi-finished product thermal insulation board described in step 3 is 4 laminates, and each laminate thickness is 1:3:5:2.
Embodiment 9
A kind of inorganic fibre insulation board, by weight including following material：40 parts of gangue, 81 parts of basalt, 40 parts of silica, pottery
14 parts of porcelain, 7 parts of nano-titanium dioxide, 14 parts of sepiolite fibre, 2.5 parts of coalescents, 0.45 part of cellulose ether, flyash 28
Part, 1.5 parts of polypropylene fibre.
The coalescents include propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, the propandiol butyl ether, third
The mass ratio of glycol methyl ether acetate and benzyl alcohol is 2:5:1.
A kind of preparation method of inorganic fibre insulation board, includes the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving；
Step 2：The mixture of step 1 is put into smelting furnace electric smelting into melt, is separately added into coalescents and cellulose ether, it is quiet
After putting 45 minutes, mixture is put into centrifuge into superfine fibre；
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum；
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
Sieving described in step 1 screens out impurity using sieve, and the mesh size is 0.0032 denier.
The adition process of coalescents described in step 2 and cellulose ether specifically includes：Add in 1/3 coalescents and
2/3 cellulose ether；(2) mixture is stood 25 minutes；(3) 2/3 coalescents and 1/3 cellulose ether are added.
Semi-finished product thermal insulation board described in step 3 is 4 laminates, and each laminate thickness is 1:3:5:2.
Embodiment 10
A kind of inorganic fibre insulation board, by weight including following material：45 parts of gangue, 82 parts of basalt, 42 parts of silica, pottery
15 parts of porcelain, 15 parts of sepiolite fibre, 3 parts of coalescents, 0.5 part of cellulose ether, 30 parts of flyash, gathers 8 parts of nano-titanium dioxide
2 parts of tacryl.
The coalescents include propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, the propandiol butyl ether, third
The mass ratio of glycol methyl ether acetate and benzyl alcohol is 2:5:1.
A kind of preparation method of inorganic fibre insulation board, includes the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving；
Step 2：The mixture of step 1 is put into smelting furnace electric smelting into melt, is separately added into coalescents and cellulose ether, it is quiet
After putting 45 minutes, mixture is put into centrifuge into superfine fibre；
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum；
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
Sieving described in step 1 screens out impurity using sieve, and the mesh size is 0.0035 denier.
The adition process of coalescents described in step 2 and cellulose ether specifically includes：Add in 1/3 coalescents and
2/3 cellulose ether；(2) mixture is stood 25 minutes；(3) 2/3 coalescents and 1/3 cellulose ether are added.
Semi-finished product thermal insulation board described in step 3 is 4 laminates, and each laminate thickness is 1:3:5:2.
Comparative example 2
A kind of inorganic fibre insulation board, by weight including following material：28 parts of gangue, 70 parts of basalt, 25 parts of silica, pottery
10 parts of porcelain, 2 parts of nano-titanium dioxide, 8 parts of sepiolite fibre, 0.5 part of coalescents, 0.2 part of cellulose ether, 20 parts of flyash,
0.3 part of polypropylene fibre.
The coalescents include propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, the propandiol butyl ether, third
The mass ratio of glycol methyl ether acetate and benzyl alcohol is 2:5:1.
A kind of preparation method of inorganic fibre insulation board, includes the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving；
Step 2：The mixture of step 1 is put into smelting furnace electric smelting into melt, is separately added into coalescents and cellulose ether, it is quiet
After putting 45 minutes, mixture is put into centrifuge into superfine fibre；
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum；
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
Sieving described in step 1 screens out impurity using sieve, and the mesh size is 0.0020 denier.
The adition process of coalescents described in step 2 and cellulose ether specifically includes：Add in 1/3 coalescents and
2/3 cellulose ether；(2) mixture is stood 25 minutes；(3) 2/3 coalescents and 1/3 cellulose ether are added.
Semi-finished product thermal insulation board described in step 3 is 4 laminates, and each laminate thickness is 1:3:5:2.
Anti-microbial property test method：Embodiment 6-10 and comparative example 2 inorganic fibre insulation board being configured are crushed into powder
Each powder, is then dissolved in sterile water by end, quantitative sample and bacterium solution is gone to add in PBS solution and shake after mixing, Ran Houqu
Go out mixed liquor and add in agar medium culture, check that each clump count obtains anti-microbial property after 24 hours.Test result such as 2 institute of table
Show.
2 anti-microbial property test of table
Upper table 2 represents the anti-microbial property of the inorganic fibre insulation board under different ratio in embodiment 6-10 and comparative example 2, from table 2
In as can be seen that compared with prior art, the clump count of embodiment 6 reduces 28.13%, and the clump count of embodiment 7 reduces
43.75%, the clump count of embodiment 8 reduces 53.13%, and the clump count of embodiment 9 reduces 61.56%, the bacterium colony of embodiment 10
Number reduces 67.5%.
The above result shows that according to inorganic fibre insulation board manufactured in the present embodiment, as clump count continuously decreases, heat preservation
The anti-microbial property of plate gradually enhances compared with prior art.
It should be understood that above description is to illustrate rather than to be limited.By reading foregoing description,
Many embodiments and many applications except the example provided all will be apparent for a person skilled in the art.
Therefore, the scope of the present invention should not be determined with reference to foregoing description, but should be with reference to preceding claims and these power
Profit requires the four corner of possessed equivalent to determine.For comprehensive purpose, all articles and reference include patent Shen
The disclosure that please and announce is all by reference to being incorporated herein.Any of theme disclosed herein is omitted in preceding claims
Aspect is not intended to abandon the body matter, also should not be considered as applicant and the theme is not thought of as to disclosed application
A part for theme.
Those listed above it is a series of be described in detail only for the application feasibility embodiment specifically
Bright, they are not limiting the protection domain of the application, all equivalent implementations made without departing from the application skill spirit
Or change should be included within the protection domain of the application.
Claims (6)
1. a kind of inorganic fibre insulation board, it is characterised in that：Include following material by weight：30-45 parts of gangue, basalt
75-82 parts, 30-42 parts of silica, 12-15 parts of ceramics, 3-8 parts of nano-titanium dioxide, 10-15 parts of sepiolite fibre, coalescents
1-3 parts, 0.3-0.5 parts of cellulose ether, 25-30 parts of flyash, 0.5-2 parts of polypropylene fibre.
2. a kind of inorganic fibre insulation board according to claim 1, it is characterised in that：The coalescents include propylene glycol
Butyl ether, propylene glycol methyl ether acetate and benzyl alcohol, the mass ratio of the propandiol butyl ether, propylene glycol methyl ether acetate and benzyl alcohol
It is 2:5:1.
3. a kind of preparation method of inorganic fibre insulation board, it is characterised in that：Include the following steps：
Step 1：Gangue, basalt, silica, ceramics, nano-titanium dioxide, sepiolite fibre, flyash and polypropylene is fine
The mixture of dimension is sufficiently stirred, spare through drying machine drying after sieving；
Step 2：The mixture of step 1 is put into smelting furnace electric smelting into melt, is separately added into coalescents and cellulose ether, it is quiet
After putting 45 minutes, mixture is put into centrifuge into superfine fibre；
Step 3：Superfine fibre in step 2 is beaten into semi-finished product thermal insulation board through pendulum；
Step 4：Semi-finished product thermal insulation board in step 3 is precuted, packaging and storage.
4. a kind of preparation method of inorganic fibre insulation board according to claim 3, it is characterised in that：Mistake described in step 1
Sieve screens out impurity using sieve, and the mesh size is 0.0025-0.0035 denier.
5. a kind of preparation method of inorganic fibre insulation board according to claim 3, it is characterised in that：Described in step 2 into
The adition process of film auxiliary agent and cellulose ether specifically includes：(1) 1/3 coalescents and 2/3 cellulose ether are added in；It (2) will be mixed
It closes object and stands 25 minutes；(3) 2/3 coalescents and 1/3 cellulose ether are added.
6. a kind of preparation method of inorganic fibre insulation board according to claim 3, it is characterised in that：Half described in step 3
Finished product thermal insulation plate is 4 laminates, and each laminate thickness is 1:3:5:2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810031081.XA CN108238715A (en) | 2018-01-12 | 2018-01-12 | A kind of inorganic fibre insulation board and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810031081.XA CN108238715A (en) | 2018-01-12 | 2018-01-12 | A kind of inorganic fibre insulation board and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108238715A true CN108238715A (en) | 2018-07-03 |
Family
ID=62699541
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810031081.XA Withdrawn CN108238715A (en) | 2018-01-12 | 2018-01-12 | A kind of inorganic fibre insulation board and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108238715A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108867035A (en) * | 2018-07-04 | 2018-11-23 | 合肥远科服装设计有限公司 | A kind of amendatory knitting fabric of flame retardant property and preparation method thereof |
| CN111763062A (en) * | 2020-05-18 | 2020-10-13 | 唐山华纤科技有限公司 | Inorganic fiber insulation board and preparation method and application thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000073233A1 (en) * | 1999-05-28 | 2000-12-07 | Rockwool International A/S | Production of mineral fibres |
| CN105199505A (en) * | 2014-06-27 | 2015-12-30 | 上海雷恩节能建材有限公司 | Inorganic fiber heat-insulating paste material and preparation method thereof |
| CN105672506A (en) * | 2016-01-29 | 2016-06-15 | 卓达新材料科技集团有限公司 | Rock wool silicon-aluminum aerogel composite sandwiched insulation fireproof plate |
| CN105732951A (en) * | 2016-03-31 | 2016-07-06 | 常州达奥新材料科技有限公司 | Method for preparing sepiolite composite basalt fiber reinforced shape memory polyurethane |
-
2018
- 2018-01-12 CN CN201810031081.XA patent/CN108238715A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000073233A1 (en) * | 1999-05-28 | 2000-12-07 | Rockwool International A/S | Production of mineral fibres |
| CN105199505A (en) * | 2014-06-27 | 2015-12-30 | 上海雷恩节能建材有限公司 | Inorganic fiber heat-insulating paste material and preparation method thereof |
| CN105672506A (en) * | 2016-01-29 | 2016-06-15 | 卓达新材料科技集团有限公司 | Rock wool silicon-aluminum aerogel composite sandwiched insulation fireproof plate |
| CN105732951A (en) * | 2016-03-31 | 2016-07-06 | 常州达奥新材料科技有限公司 | Method for preparing sepiolite composite basalt fiber reinforced shape memory polyurethane |
Non-Patent Citations (3)
| Title |
|---|
| 徐峰: "《建筑涂料与涂装技术》", 31 May 1998, 化学工业出版社 * |
| 王杏等: "《纳米二氧化钛的生产与应用》", 31 July 2014, 贵州科技出版社 * |
| 郭铁男等: "《中国消防手册》", 31 December 2007, 上海科学技术出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108867035A (en) * | 2018-07-04 | 2018-11-23 | 合肥远科服装设计有限公司 | A kind of amendatory knitting fabric of flame retardant property and preparation method thereof |
| CN111763062A (en) * | 2020-05-18 | 2020-10-13 | 唐山华纤科技有限公司 | Inorganic fiber insulation board and preparation method and application thereof |
| CN111763062B (en) * | 2020-05-18 | 2022-02-18 | 唐山华纤科技有限公司 | Inorganic fiber insulation board and preparation method and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102786295B (en) | A kind of water-soluble ceramic core and preparation method thereof | |
| CN103877870B (en) | Total heat exchange membrane and total heat exchanger with antibacterial and antifungal functions | |
| CN108238715A (en) | A kind of inorganic fibre insulation board and preparation method thereof | |
| CN102741469A (en) | Polymer composite materials for building air conditioning or dehumidification and preparation method thereof | |
| CN102115626A (en) | Herbaceous fiber paint and preparation method thereof | |
| CN116178870A (en) | Heat-insulating waterproof composite material and preparation process thereof | |
| CN104497759A (en) | Thermo-regulated water-based paint for interior wall and preparation method of thermo-regulated water-based paint | |
| CN108238716A (en) | A kind of poisonous and harmful solid waste comprehensive utilization product and preparation method | |
| CN105669089B (en) | A kind of construction material of adjusting humidity and preparation method thereof | |
| CN106587813B (en) | Multifunction wall material and preparation method thereof | |
| CN106280442A (en) | A kind of ortho position acid imide functionalization benzoxazine resins carbon fiber laminating composite material and preparation method thereof | |
| CN108275886B (en) | Aerogel heat preservation felt prepared from industrial solid waste and preparation method | |
| CN103274660B (en) | Light building composite material and preparation method thereof | |
| CN102964938A (en) | Efficient vegetable liquid nano coating | |
| Elzaidabi | Low energy, wind catcher assisted indirect-evaporative cooling system for building applications | |
| CN108247797A (en) | A kind of preparation method of the not mould non-ignitable recombination bamboo flooring of no aldehyde | |
| CN108251913A (en) | A kind of ultra-fine inorganic fibre spray coating heat preservation material and preparation method thereof | |
| CN105344345A (en) | Photocatalysis composite material having performances of regulating temperature and moisture as well as preparation method thereof | |
| CN108238714A (en) | A kind of method of sludge production thermal insulation board | |
| CN204612119U (en) | A kind of idle call water spilage tray | |
| CN102503352A (en) | Enclosed baffle special for super highways and preparation method for enclosed baffle | |
| CN112870991A (en) | A novel ternary mixed matrix total heat exchange membrane and preparation method thereof | |
| CN104327616B (en) | Glass-wool inorganic heat-insulating coating | |
| CN104118980A (en) | Method for preparing aperture-controllable low-temperature foam glass | |
| CN207230798U (en) | A kind of industrial humidification dedusting type air cooler |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20180703 |
|
| WW01 | Invention patent application withdrawn after publication |