CN108184822A - A kind of working fluid that can retain camellia Fresh Cutting flower natural primary color and its application - Google Patents
A kind of working fluid that can retain camellia Fresh Cutting flower natural primary color and its application Download PDFInfo
- Publication number
- CN108184822A CN108184822A CN201711430555.XA CN201711430555A CN108184822A CN 108184822 A CN108184822 A CN 108184822A CN 201711430555 A CN201711430555 A CN 201711430555A CN 108184822 A CN108184822 A CN 108184822A
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- camellia
- working fluid
- primary color
- fresh cutting
- cutting flower
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N3/00—Preservation of plants or parts thereof, e.g. inhibiting evaporation, improvement of the appearance of leaves or protection against physical influences such as UV radiation using chemical compositions; Grafting wax
- A01N3/02—Keeping cut flowers fresh chemically
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Toxicology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of working fluid that can retain camellia Fresh Cutting flower natural primary color and its applications.The working fluid that camellia Fresh Cutting flower natural primary color can be retained is natural material oil, natural material resin, siloxanes, synthetic resin, adds one or more of water reaction type polyurethane, fatty acid ester and surfactant, and the pH value of the working fluid that can retain camellia Fresh Cutting flower natural primary color is 2~8.Preparation method is by each raw material mixing of formulation ratio, and it is 2~5 then to add in pH adjusting agent and adjust pH value；Using application of the working fluid for the reservation camellia Fresh Cutting flower natural primary color in camellia Fresh Cutting flower cellular content fill process is prepared.The present invention, which can produce, can keep natural colour and the camellia immortality close to camellia fresh flower nature is spent, and can save dyeing process, can retain camellia natural colour suitable for batch micro operations, particularly retain complicated and delicate tone camellia immortality flower.
Description
Technical field
The invention belongs to chemical technology fields, and in particular to a kind of working fluid that can retain camellia Fresh Cutting flower natural primary color and
It is applied.
Background technology
Immortality flower (PreservedFreshFlower) is also preserved flower, ecology flower, and foreign countries are called " forever amaranthine fresh
Flower ".Camellia immortality flower is by a series of complex such as dehydration, decoloration, drying, dyeing using high-tech means by camellia Fresh Cutting flower
The preserved flower that process is process, camellia immortality flower either color and luster, character, feel are almost no different with fresh flower, it not only keeps
The speciality of fresh flower, and can place 3~4 years under color more horn of plenty, purposes higher, certain preservation condition, it is expensive, it is deep
Liked and pursued by petty bourgeoisie personage, be the ideal Flower processing product of Floriculture Design, decorate home, celebration activity.Mesh
Preceding camellia immortality flower few in number in the market is largely only limitted to the making of monochromatic system immortality flower, because in tissue fluid
Dehydration in the primary colors of camellia Fresh Cutting flower taken off simultaneously, be replaced into preserve liquid during must not be without complicated
Color, thus the natural primary color of camellia can not be retained, the original sample of delicate tone retains and can hardly realize in particularly one flower polychrome,
The beautiful of camellia cannot be showed fully.Therefore, developing a kind of product that can be solved the above problems and method is very important.
Invention content
The first object of the present invention is to provide a kind of working fluid that can retain camellia Fresh Cutting flower natural primary color；Second purpose
It is to provide the preparation method of the working fluid that can retain camellia Fresh Cutting flower natural primary color；Third is designed to provide described
The working fluid that can retain camellia Fresh Cutting flower natural primary color application.
The first object of the present invention is achieved in that the working fluid that can retain camellia Fresh Cutting flower natural primary color is
Natural material oil, natural material resin, siloxanes, synthetic resin plus water reaction type polyurethane, fatty acid ester and surface-active
One or more of agent, the pH value of the working fluid that can retain camellia Fresh Cutting flower natural primary color is 2~8.
The second object of the present invention is achieved in that each raw material mixing of formulation ratio, is then added in pH and is adjusted
Agent adjusts pH value and obtains the working fluid of object reservation camellia Fresh Cutting flower natural primary color for 2~8, and the pH adjusting agent is second
Acid, oxalic acid, citric acid, formic acid, amino acid, hydrochloric acid, sodium hydroxide, sodium carbonate, sodium bicarbonate, sodium hypochlorite, disodium hydrogen phosphate, phosphorus
Arbitrary 2~5 kinds of mixture in acid dihydride potassium, sulfate.
The third object of the present invention is achieved in that the working fluid of the reservation camellia Fresh Cutting flower natural primary color is being made
Application in standby camellia Fresh Cutting flower cellular content fill process.
The Fresh Cutting flower is camellia Fresh Cutting flower.
Camellia Fresh Cutting flower time for impregnating in the working fluid for retaining natural primary color is 12~96h, preferably 24~
48h。
Light processing on envelope is carried out after the completion of dipping, the quasi- finished product of preserved flower obtained from working fluid needs to stand (during standing
Between be 1~30h, preferably 3~10h) after be soaked in again in fruit glaze agent glazing solution, it is therefore an objective to plant surface be coated with it is one layer thin
Film is that the appearance of camellia Fresh Cutting flower is natural, bright；The glazing agent is in epoxy resin, lacquer, varnish or polyurethane resin
One or more.The glazing agent that debita spissitudo is diluted to through pretreatment liquid solvent for use can also be used, in these glazing liquid
For 1~2min of middle dipping to a few days progress glazing, soaking time is preferably 1~3h.
One or more of described pretreatment liquid alcohol, petroleum product and hydrocarbon system solvent, pH value are 2~5.
The pretreatment liquid solvent for use is the hydrophilic solvent that carbon atom number is 2~8, such as butanol, isopropanol, junket
Acid, acetone,-dioxane of Isosorbide-5-Nitrae, 2- methyl -2,4 pentanediol, isoamyl alcohol, cyclohexanol, cellosolve, butyl cellosolve, the molten fibre of methyl
Agent, 2- ethyl -1,3- hexylene glycols, 3- methyl-1s, 5 pentanediols, 2- (2- ethyl hexyl oxies) ethyl alcohol or polypropylene glycol.
Application process of the pretreatment liquid in camellia Fresh Cutting flower dehydration nondiscoloration treatment process is prepared is the camellia tea
It is 10~72h, preferably 12~48h to spend the time that Fresh Cutting flower is impregnated in pretreatment liquid.
Taking out to cure to dry curing at 35~37 DEG C and can obtain after fruit glaze agent glazing immersion treatment plump full, soft has
Elasticity has color and luster as fresh flower and the camellia preserved flower of feel.
Meanwhile the suitable sodium chloride of addition, chlorine before the working fluid dipping of the reservation camellia Fresh Cutting flower natural primary color
Change potassium, sodium sulphate, potassium sulfate, sodium phosphate, potassium phosphate, alum, the inorganic salts such as soda ash or sodium acetate, sodium oxalate, potassium oxalate,
The organic salts such as sodium tartrate, sodium succinate can then add closer to the color of natural reservation camellia Fresh Cutting flower, above-mentioned salt
Dosage is the working fluid mass percent 2~6% for retaining camellia Fresh Cutting flower natural primary color.
The present invention has accomplished dehydration nondiscoloration in the pretreatment liquid for retaining camellia Fresh Cutting flower natural primary color to camellia Fresh Cutting flower,
Can retain flower natural primary color, particularly one flower polychrome in delicate tone original sample retain on the basis of.The present invention can manufacture
Go out to keep natural colour and the camellia immortality close to camellia fresh flower nature is spent, and can save dyeing process, suitable for batch
Manufacture can retain camellia natural colour, particularly retain complicated and delicate tone camellia immortality flower.
Specific embodiment
With reference to embodiment, the present invention is further illustrated, but the present invention is not limited in any way,
Based on present invention teach that any transformation or replacement made, all belong to the scope of protection of the present invention.
The working fluid of the present invention that camellia Fresh Cutting flower natural primary color can be retained is natural material oil, natural material tree
Fat, synthetic resin, adds one or more of water reaction type polyurethane, fatty acid ester and surfactant at siloxanes, described
The working fluid that can retain camellia Fresh Cutting flower natural primary color pH value be 2~8.
The working fluid that camellia Fresh Cutting flower natural primary color can be retained, it is characterised in that described can retain camellia fresh-cut
The working fluid of flower natural primary color includes the use of the alcohol such as methanol, ethyl alcohol, butanol, isopropanol, isoamyl alcohol, cyclohexanol；Kerosene, gasoline,
The petroleum products such as raw gasoline；And the hydrocarbon systems such as methyl acetate, ethyl acetate, toluene, acetone, benzene, methyl ethyl ketone, hexane are molten
Agent.As solvent preferred hydrophilic solvent, and specifically, it is preferable to the butanol, isopropanol, Isosorbide-5-Nitrae-Er Evil that the use of carbon atom number are 2~8
Alkane, 2- methyl -2,4-PD, isoamyl alcohol, cyclohexanol, 3- methyl-1s, 5- pentanediols, gather 2- (2- ethyl hexyl oxies) ethyl alcohol
The hydrophilic solvents such as propylene glycol (molecular weight 500~700 or so).Particularly, with butanol：2- methyl -2,4-PD：3- first
Base -1,5- pentanediols：2- (2- ethyl hexyl oxies) ethyl alcohol is 1：1：2：3 are uniformly mixed into most preferably.
The natural material oil is turpentine oil, godied oil, whale oil, stand oil, linseed oil, camellia oil, olive oil, vegetable seed
Oil, salad oil, sesame oil or camphorated oil.
The natural material resin is rosin, animal glue, wax, beeswax, rubber or paint.
The fatty acid ester is saturated fatty acid and unrighted acid, the esters of lower alcohol or polyalcohol.
The saturated fatty acid and unrighted acid are lauric acid, palmitic acid, stearic acid or myristic acid；Described
Lower alcohol is methanol, ethyl alcohol, isopropanol, butanol, octanol, pentaerythrite or 2-Ethylhexyl Alcohol；The polyalcohol is glycerine, gathers
Ethylene oxide alcohol, sorbierite or diethanol amine.
The siloxanes is ethyl dichlorosilane, ethyl trichlorosilane, dimethyldichlorosilane, tetramethylsilane, three
Chlorosilane, three (trimethyl silyl) silane, trim,ethylchlorosilane, vinyl trichlorosilane, polymethoxy silane, methyl two
Chlorosilane or methyl trichlorosilane.
The surfactant is fatty diglycollic amide, polyoxyethylene alkyl ether or polyoxyethylene alkylphenyl
Ether.
It is of the present invention retain camellia Fresh Cutting flower natural primary color working fluid, be by each raw material mixing of formulation ratio,
Then it adds in pH adjusting agent adjusting pH value and obtains the working fluid of object reservation camellia Fresh Cutting flower natural primary color for 2~8, it is described
PH adjusting agent is acetic acid, oxalic acid, citric acid, formic acid, amino acid, hydrochloric acid, sodium hydroxide, sodium carbonate, sodium bicarbonate, hypochlorous acid
Arbitrary 2~5 kinds of mixture in sodium, disodium hydrogen phosphate, potassium dihydrogen phosphate, sulfate.
The application of the working fluid of the present invention for retaining camellia Fresh Cutting flower natural primary color is the reservation camellia fresh-cut
Application of the working fluid of flower natural primary color in camellia Fresh Cutting flower cellular content fill process is prepared.
Case is embodied, the present invention will be further described below：
Embodiment 1
In the solution for adding in citric acid adjustment pH3.5 into isopropanol 100mL with weight ratio about 5%, will have pink
The camellia Elizabethan of color and white powder duotone color impregnates 24 hours.Then, with 1：2：1：1.5 mixing isopropanols, silica
Alkane, methyl laurate and methyl ethyl ketone in the solution 100mL for adding in citric acid adjustment pH4 thereto, move into aforementioned tea
Flower impregnates 48 hours.Then, it takes out and spontaneously dries 24 hours from solution.
As a result it is the camellia of the duotone color of obtained pink and white powder, remains duotone color as former state, and
It is kept for fresh 2 years or more.
Embodiment 2
In the solution for adding in citric acid adjustment pH into isopropanol 100mL with weight ratio 2%, dipping is with purple and light
After the camellia purple shellfish of red compound tone widens rose 72 hours, aforementioned camellia is moved into 5：3 mixing isopropanols and polyoxy
In the solution 100mL of ethylene-monolaurate, dipping takes out after 48 hours from solution, spontaneously dries 24 hours.
As a result it is that obtained secondary color camellia retains original natural color as former state, is kept for fresh 2 years or more.
Claims (10)
1. a kind of working fluid that can retain camellia Fresh Cutting flower natural primary color, it is characterised in that described can retain camellia Fresh Cutting flower certainly
The working fluid of right primary colors is natural material oil, natural material resin, siloxanes, synthetic resin, adds water reaction type polyurethane, fat
One or more of esters of gallic acid and surfactant, the pH value of the working fluid that camellia Fresh Cutting flower natural primary color can be retained
It is 2~8.
2. the working fluid according to claim 1 that camellia Fresh Cutting flower natural primary color can be retained, it is characterised in that the energy
The working fluid for retaining camellia Fresh Cutting flower natural primary color includes the use of the alcohol of methanol, ethyl alcohol, butanol, isopropanol, isoamyl alcohol, cyclohexanol
Class solvent；Kerosene, gasoline, raw gasoline petroleum product；And methyl acetate, ethyl acetate, toluene, acetone, benzene, Methylethyl
The hydrocarbon system solvent of ketone, hexane.
3. the working fluid according to claim 1 or 2 for retaining camellia Fresh Cutting flower natural primary color, it is characterised in that the day
Right material oil is turpentine oil, godied oil, whale oil, stand oil, linseed oil, camellia oil, olive oil, rapeseed oil, salad oil, sesame oil
Or camphorated oil.
4. the working fluid according to claim 1 or 2 for retaining camellia Fresh Cutting flower natural primary color, it is characterised in that the day
Right material resin is rosin, animal glue, wax, beeswax, rubber or paint.
5. the working fluid according to claim 1 or 2 for retaining camellia Fresh Cutting flower natural primary color, it is characterised in that the fat
Fat esters of gallic acid is saturated fatty acid and unrighted acid, the esters of lower alcohol or polyalcohol.
6. the working fluid according to claim 5 for retaining camellia Fresh Cutting flower natural primary color, it is characterised in that the saturation
Aliphatic acid and unrighted acid are lauric acid, palmitic acid, stearic acid or myristic acid；The lower alcohol for methanol, ethyl alcohol,
Isopropanol, butanol, octanol, pentaerythrite or 2-Ethylhexyl Alcohol；The polyalcohol for glycerine, polyoxyethylene alcohol, sorbierite or
Diethanol amine.
7. the working fluid according to claim 1 or 2 for retaining camellia Fresh Cutting flower natural primary color, it is characterised in that the silicon
Oxygen alkane is ethyl dichlorosilane, ethyl trichlorosilane, dimethyldichlorosilane, tetramethylsilane, trichlorosilane, three (trimethyls
Silicyl) silane, trim,ethylchlorosilane, vinyl trichlorosilane, polymethoxy silane, dimethyl dichlorosilane (DMCS) or methyl trichlorine
Silane.
8. the working fluid according to claim 7 for retaining camellia Fresh Cutting flower natural primary color, it is characterised in that the surface
Activating agent is fatty diglycollic amide, polyoxyethylene alkyl ether or polyoxyethylene alkyl phenyl ether.
9. a kind of working fluid of any reservation camellia Fresh Cutting flower natural primary color of claim 1~8, it is characterised in that be by
Then each raw material mixing of formulation ratio adds in pH adjusting agent adjusting pH value and obtains object reservation camellia Fresh Cutting flower certainly for 2~8
The working fluid of right primary colors, the pH adjusting agent is acetic acid, oxalic acid, citric acid, formic acid, amino acid, hydrochloric acid, sodium hydroxide, carbon
Arbitrary 2~5 kinds of mixture in sour sodium, sodium bicarbonate, sodium hypochlorite, disodium hydrogen phosphate, potassium dihydrogen phosphate, sulfate.
10. a kind of application of the working fluid of any reservation camellia Fresh Cutting flower natural primary color of claim 1~8, feature
It is working fluid the answering in camellia Fresh Cutting flower cellular content fill process of the reservation camellia Fresh Cutting flower natural primary color
With.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711430555.XA CN108184822A (en) | 2017-12-26 | 2017-12-26 | A kind of working fluid that can retain camellia Fresh Cutting flower natural primary color and its application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711430555.XA CN108184822A (en) | 2017-12-26 | 2017-12-26 | A kind of working fluid that can retain camellia Fresh Cutting flower natural primary color and its application |
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| Publication Number | Publication Date |
|---|---|
| CN108184822A true CN108184822A (en) | 2018-06-22 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711430555.XA Pending CN108184822A (en) | 2017-12-26 | 2017-12-26 | A kind of working fluid that can retain camellia Fresh Cutting flower natural primary color and its application |
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| Country | Link |
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| CN (1) | CN108184822A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113966738A (en) * | 2021-11-25 | 2022-01-25 | 云南欣绿茶花股份有限公司 | Pretreatment liquid for preserving primary color of fresh cut camellia and application thereof |
| CN114041459A (en) * | 2021-11-25 | 2022-02-15 | 云南欣绿茶花股份有限公司 | Processing liquid for preserving natural primary color of fresh cut camellia and application thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004099605A (en) * | 2002-08-19 | 2004-04-02 | Yoshihisa Sakamoto | Method for preserving cut flower |
| CN101861092A (en) * | 2007-11-07 | 2010-10-13 | 坂本好央 | Method for production of preserved flower, and processing solution for use in the method |
| CN104621098A (en) * | 2015-01-29 | 2015-05-20 | 宁波远鸿生物科技有限公司 | Preparation method of plump preserved flowers |
| CN105145976A (en) * | 2015-08-26 | 2015-12-16 | 昆明紫色青阳生物科技有限公司 | Processing method of preserved camellia |
-
2017
- 2017-12-26 CN CN201711430555.XA patent/CN108184822A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004099605A (en) * | 2002-08-19 | 2004-04-02 | Yoshihisa Sakamoto | Method for preserving cut flower |
| CN101861092A (en) * | 2007-11-07 | 2010-10-13 | 坂本好央 | Method for production of preserved flower, and processing solution for use in the method |
| CN104621098A (en) * | 2015-01-29 | 2015-05-20 | 宁波远鸿生物科技有限公司 | Preparation method of plump preserved flowers |
| CN105145976A (en) * | 2015-08-26 | 2015-12-16 | 昆明紫色青阳生物科技有限公司 | Processing method of preserved camellia |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113966738A (en) * | 2021-11-25 | 2022-01-25 | 云南欣绿茶花股份有限公司 | Pretreatment liquid for preserving primary color of fresh cut camellia and application thereof |
| CN114041459A (en) * | 2021-11-25 | 2022-02-15 | 云南欣绿茶花股份有限公司 | Processing liquid for preserving natural primary color of fresh cut camellia and application thereof |
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Application publication date: 20180622 |