CN108157394B - Rosemary type insect repellant - Google Patents
Rosemary type insect repellant Download PDFInfo
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- CN108157394B CN108157394B CN201810001114.6A CN201810001114A CN108157394B CN 108157394 B CN108157394 B CN 108157394B CN 201810001114 A CN201810001114 A CN 201810001114A CN 108157394 B CN108157394 B CN 108157394B
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- 239000000077 insect repellent Substances 0.000 title claims abstract description 34
- 244000178231 Rosmarinus officinalis Species 0.000 title abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 39
- VSGNNIFQASZAOI-UHFFFAOYSA-L calcium acetate Chemical class [Ca+2].CC([O-])=O.CC([O-])=O VSGNNIFQASZAOI-UHFFFAOYSA-L 0.000 claims abstract description 36
- 235000014347 soups Nutrition 0.000 claims abstract description 31
- 239000007787 solid Substances 0.000 claims abstract description 29
- 238000010438 heat treatment Methods 0.000 claims abstract description 23
- 235000009051 Ambrosia paniculata var. peruviana Nutrition 0.000 claims abstract description 22
- 235000003097 Artemisia absinthium Nutrition 0.000 claims abstract description 22
- 240000001851 Artemisia dracunculus Species 0.000 claims abstract description 22
- 235000017731 Artemisia dracunculus ssp. dracunculus Nutrition 0.000 claims abstract description 22
- 235000003261 Artemisia vulgaris Nutrition 0.000 claims abstract description 22
- 239000001138 artemisia absinthium Substances 0.000 claims abstract description 22
- 239000000243 solution Substances 0.000 claims abstract description 22
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000000203 mixture Substances 0.000 claims abstract description 19
- 239000011259 mixed solution Substances 0.000 claims abstract description 14
- 239000007788 liquid Substances 0.000 claims abstract description 12
- 238000003756 stirring Methods 0.000 claims abstract description 12
- 238000002791 soaking Methods 0.000 claims abstract description 8
- 239000012535 impurity Substances 0.000 claims abstract description 6
- 238000001816 cooling Methods 0.000 claims abstract 2
- 239000001639 calcium acetate Substances 0.000 claims description 27
- 229960005147 calcium acetate Drugs 0.000 claims description 27
- 235000011092 calcium acetate Nutrition 0.000 claims description 27
- 241001529742 Rosmarinus Species 0.000 claims description 19
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 18
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 14
- 238000009835 boiling Methods 0.000 claims description 11
- 239000012047 saturated solution Substances 0.000 claims description 9
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 4
- 239000003814 drug Substances 0.000 claims 5
- 238000001704 evaporation Methods 0.000 claims 1
- 239000002244 precipitate Substances 0.000 claims 1
- 230000000749 insecticidal effect Effects 0.000 abstract description 11
- 230000000694 effects Effects 0.000 abstract description 8
- 239000000126 substance Substances 0.000 abstract description 5
- 239000003205 fragrance Substances 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 3
- 230000000172 allergic effect Effects 0.000 abstract description 2
- 208000010668 atopic eczema Diseases 0.000 abstract description 2
- 230000008569 process Effects 0.000 abstract description 2
- 239000003292 glue Substances 0.000 abstract 1
- 235000019441 ethanol Nutrition 0.000 description 18
- 239000002714 Extracts of rosemary Substances 0.000 description 7
- 239000000284 extract Substances 0.000 description 7
- 235000019306 extracts of rosemary Nutrition 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 241000238631 Hexapoda Species 0.000 description 6
- 230000006872 improvement Effects 0.000 description 5
- 230000001846 repelling effect Effects 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
- 238000005352 clarification Methods 0.000 description 4
- 238000001556 precipitation Methods 0.000 description 4
- 239000000428 dust Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 239000000779 smoke Substances 0.000 description 3
- 239000001569 carbon dioxide Substances 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000002917 insecticide Substances 0.000 description 2
- 239000000419 plant extract Substances 0.000 description 2
- 239000005871 repellent Substances 0.000 description 2
- 230000002940 repellent Effects 0.000 description 2
- 229940092258 rosemary extract Drugs 0.000 description 2
- 235000020748 rosemary extract Nutrition 0.000 description 2
- 239000001233 rosmarinus officinalis l. extract Substances 0.000 description 2
- 206010003399 Arthropod bite Diseases 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Mycology (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Botany (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
本发明涉及一种迷迭香型驱虫剂，将迷迭香和艾草剪碎混合成混合料，将混合料和乙醇倒入瓦罐中浸泡，浸泡结束后给瓦罐加热进行煎煮，将瓦罐内部的固体杂质过滤得到初步药汤，将初步药汤加热浓缩得到浓缩药汤；在醋酸钙饱和溶液中分批加入浓缩药汤得到混合液，对混合液进行加热、搅拌直至出现胶状沉淀时停止搅拌和加热，冷却后即得固体状迷迭香型驱虫剂。该迷迭香型驱虫剂为固体状，体积小，物理、化学稳定性好，存储、运输、使用、携带方便，保质期长达3年；即可制成液态驱虫液，也可加热或点燃使用，使用方法多种多样；香味自然，成本较低，流香时间长，杀虫、驱虫效果好；使用过程中，污染少，人体不易过敏，副作用小。The invention relates to a rosemary-type insect repellent. Rosemary and wormwood are cut into pieces and mixed into a mixture, the mixture and ethanol are poured into a crock pot for soaking, and the crock pot is heated for decoction after soaking. The solid impurities inside the crock pot are filtered to obtain the preliminary medicinal soup, and the preliminary medicinal soup is heated and concentrated to obtain the concentrated medicinal soup; the concentrated medicinal soup is added in batches to the saturated calcium acetate solution to obtain a mixed solution, and the mixed solution is heated and stirred until glue appears. The stirring and heating were stopped when the solid state was precipitated, and the solid rosemary-type insect repellent was obtained after cooling. The rosemary-type insect repellent is solid, small in size, good in physical and chemical stability, convenient for storage, transportation, use, and carrying, and has a shelf life of up to 3 years; it can be made into liquid insect repellent, or heated or It can be used in a variety of ways; the fragrance is natural, the cost is low, the fragrance lasts for a long time, and the insecticidal and deworming effects are good; during the use process, the pollution is less, the human body is not easy to be allergic, and the side effects are small.
Description
技术领域technical field
本发明涉及驱虫剂技术领域，尤其涉及一种迷迭香型驱虫剂。The invention relates to the technical field of repellents, in particular to a rosemary-type insect repellent.
背景技术Background technique
随着生活水平的逐步提高，人们对生活用品的需求也越来越高，夏季蚊虫叮咬一直危害着人们的身体健康。目前常用的驱虫剂主要是有机合成杀虫剂或者一些天然植物提取物，有机合成杀虫剂一般气味较大，并且其中含有一些对人体不利的成分（如对人体不利的有机溶剂），易造成体质敏感的人（如小孩）过敏或不适。一些天然植物提取物如迷迭香提取物，其也具有杀虫成分，但是目前迷迭香提取物一般都用水煮或者有机溶剂萃取的方式提取，采用水煮得到的提取物，虽然成本低，但是保存时间只有3~6个月；即使添加防腐剂，其保质期一般也不超过1年。而用有机溶剂萃取得到的提取物，萃取成本高，得到的提取物浓度高，如果直接喷洒使用易造成不适，需要稀释，这使得其体积进一步增大，再加上其为液体，存储、运输、使用、携带不方便，并且液体状提取物，限制了其使用方法。With the gradual improvement of living standards, people's demand for daily necessities is also getting higher and higher, and mosquito bites in summer have always endangered people's health. At present, the commonly used insect repellants are mainly organic synthetic insecticides or some natural plant extracts. Organic synthetic insecticides generally have a strong odor and contain some components that are unfavorable to the human body (such as organic solvents that are unfavorable to the human body). Causes allergies or discomfort to people with sensitive constitutions (such as children). Some natural plant extracts, such as rosemary extract, also have insecticidal components, but at present, rosemary extract is generally extracted by boiling or organic solvent extraction. The extract obtained by boiling is low in cost. However, the shelf life is only 3 to 6 months; even if preservatives are added, the shelf life is generally not more than 1 year. The extract obtained by extraction with organic solvents has high extraction cost and high concentration of the obtained extract. If it is directly sprayed and used, it is easy to cause discomfort and needs to be diluted, which further increases its volume. In addition, it is a liquid, storage and transportation. , It is inconvenient to use and carry, and the liquid extract limits its use.
发明内容SUMMARY OF THE INVENTION
本发明针对现有技术存在的不足，提供了一种迷迭香型驱虫剂，具体技术方案如下：In view of the deficiencies existing in the prior art, the present invention provides a rosemary-type insect repellent, and the specific technical scheme is as follows:
一种迷迭香型驱虫剂，将迷迭香和艾草剪碎混合成混合料，将混合料和乙醇倒入瓦罐中浸泡3~5h，浸泡结束后给瓦罐加热，瓦罐内部的液体加热至沸腾进行煎煮，煎煮8~10h，将瓦罐内部的固体杂质过滤得到初步药汤，将初步药汤加热浓缩得到浓缩药汤，浓缩药汤的体积是初步药汤体积的三分之一；将醋酸分多次加到碳酸钙中不断搅拌，搅拌至澄清得到醋酸钙溶液，将所得到的醋酸钙溶液蒸发浓缩制成醋酸钙饱和溶液；在醋酸钙饱和溶液中分批加入浓缩药汤得到混合液，对混合液进行加热至沸腾，加热过程中不断搅拌直至出现胶状沉淀时停止搅拌和加热，待混合液冷却后即得到固体状迷迭香型驱虫剂。A rosemary-type insect repellent, the rosemary and wormwood are chopped and mixed into a mixture, the mixture and ethanol are poured into a crock pot and soaked for 3 to 5 hours. The liquid is heated to boiling for decocting, decocted for 8~10 hours, the solid impurities inside the crock are filtered to obtain the preliminary medicinal soup, the preliminary medicinal soup is heated and concentrated to obtain the concentrated medicinal soup, and the volume of the concentrated medicinal soup is the volume of the preliminary medicinal soup. 1/3; add acetic acid to calcium carbonate for several times and continuously stir, stir until clarification to obtain calcium acetate solution, evaporate and concentrate the obtained calcium acetate solution to make calcium acetate saturated solution; in calcium acetate saturated solution in batches The concentrated medicinal soup is added to obtain a mixed solution, the mixed solution is heated to boiling, and the stirring is continued during the heating process until the gelatinous precipitation occurs, and the stirring and heating are stopped. After the mixed solution is cooled, a solid rosemary-type insect repellent is obtained.
作为上述技术方案的改进，所述迷迭香和艾草按照质量比10:（1.2~1.3）的比例混合制成混合料。As an improvement of the above-mentioned technical scheme, the rosemary and wormwood are mixed according to the mass ratio of 10: (1.2~1.3) to make a mixture.
作为上述技术方案的改进，所述混合料和乙醇按照质量比1:（12~15）的比例在瓦罐中浸泡3~5h。As an improvement of the above technical solution, the mixture and ethanol are soaked in a crock pot for 3 to 5 hours according to a mass ratio of 1: (12 to 15).
作为上述技术方案的改进，所述醋酸钙饱和溶液和浓缩药汤按照质量比1:（11~12）的比例混合得到混合液。As the improvement of the above-mentioned technical scheme, described calcium acetate saturated solution and concentrated medicinal soup are mixed according to the ratio of mass ratio 1:(11～12) to obtain mixed solution.
本发明的有益效果：本发明所述迷迭香型驱虫剂为固体状，体积小，物理、化学稳定性好，存储、运输、使用、携带方便，保质期长达3年；即可制成液态驱虫液，也可加热或点燃使用，使用方法多种多样；香味自然，成本较低，流香时间长，杀虫、驱虫效果好；使用过程中，污染少，人体不易过敏，副作用小。Beneficial effects of the present invention: the rosemary-type insect repellent of the present invention is solid, small in size, good in physical and chemical stability, convenient for storage, transportation, use and carrying, and has a shelf life of up to 3 years; it can be made into The liquid insect repellent can also be heated or ignited, and can be used in a variety of ways; the fragrance is natural, the cost is low, the fragrance lasts for a long time, and the insecticidal and deworming effects are good; during use, the pollution is less, the human body is not easy to be allergic, and the side effects Small.
具体实施方式Detailed ways
为了使本发明的目的、技术方案及优点更加清楚明白，以下结合实施例，对本发明进行进一步详细说明。应当理解，此处所描述的具体实施例仅仅用以解释本发明，并不用于限定本发明。In order to make the objectives, technical solutions and advantages of the present invention clearer, the present invention will be further described in detail below with reference to the embodiments. It should be understood that the specific embodiments described herein are only used to explain the present invention, but not to limit the present invention.
实施例1Example 1
将剪碎的迷迭香和剪碎的艾草按照质量比10:1.2的比例混合成混合料，将混合料和乙醇按照质量比1:12的比例倒入瓦罐中浸泡3h，浸泡结束后给瓦罐加热，瓦罐内部的液体加热至沸腾进行煎煮，煎煮8h，将瓦罐内部的固体杂质过滤得到初步药汤，将初步药汤加热浓缩得到浓缩药汤，浓缩药汤的体积是初步药汤体积的三分之一；将醋酸分多次加到碳酸钙中不断搅拌，搅拌至澄清得到醋酸钙溶液，将所得到的醋酸钙溶液蒸发浓缩制成醋酸钙饱和溶液；所述醋酸钙饱和溶液和浓缩药汤按照质量比1:11的比例混合得到混合液，所述浓缩药汤是分批加入到醋酸钙饱和溶液中进行混合，对混合液进行加热至沸腾，加热过程中不断搅拌直至出现胶状沉淀时停止搅拌和加热，待混合液冷却后即得到固体状迷迭香型驱虫剂。该固体状迷迭香型驱虫剂的物理、化学稳定性好，存储、运输、使用、携带方便，保质期长达3年。The chopped rosemary and chopped wormwood are mixed into a mixture according to the mass ratio of 10:1.2, and the mixture and ethanol are poured into a crock pot according to the mass ratio of 1:12 and soaked for 3 hours. After soaking Heating the crock pot, heating the liquid inside the crock pot to boiling for decocting, decocting for 8 hours, filtering the solid impurities inside the crock pot to obtain a preliminary medicinal soup, heating and concentrating the preliminary medicinal soup to obtain a concentrated medicinal soup, and concentrating the volume of the medicinal soup It is one-third of the volume of the preliminary medicinal soup; the acetic acid is added to the calcium carbonate for several times and continuously stirred, stirred until clarification to obtain a calcium acetate solution, and the obtained calcium acetate solution is evaporated and concentrated to make a calcium acetate saturated solution; The saturated calcium acetate solution and the concentrated medicinal decoction are mixed according to the mass ratio of 1:11 to obtain a mixed solution. The concentrated medicinal decoction is added to the saturated calcium acetate solution in batches for mixing, and the mixed solution is heated to boiling. During the heating process The stirring and heating are stopped until the gelatinous precipitation occurs, and the solid rosemary-type insect repellent is obtained after the mixture is cooled. The solid rosemary-type insect repellent has good physical and chemical stability, is convenient to store, transport, use and carry, and has a shelf life of up to 3 years.
实施例2Example 2
将剪碎的迷迭香和剪碎的艾草按照质量比10:1.26的比例混合成混合料，将混合料和乙醇按照质量比1:13的比例倒入瓦罐中浸泡4h，浸泡结束后给瓦罐加热，瓦罐内部的液体加热至沸腾进行煎煮，煎煮9h，将瓦罐内部的固体杂质过滤得到初步药汤，将初步药汤加热浓缩得到浓缩药汤，浓缩药汤的体积是初步药汤体积的三分之一；将醋酸分多次加到碳酸钙中不断搅拌，搅拌至澄清得到醋酸钙溶液，将所得到的醋酸钙溶液蒸发浓缩制成醋酸钙饱和溶液；所述醋酸钙饱和溶液和浓缩药汤按照质量比1:11.7的比例混合得到混合液，所述浓缩药汤是分批加入到醋酸钙饱和溶液中进行混合，对混合液进行加热至沸腾，加热过程中不断搅拌直至出现胶状沉淀时停止搅拌和加热，待混合液冷却后即得到固体状迷迭香型驱虫剂。该固体状迷迭香型驱虫剂的物理、化学稳定性好，存储、运输、使用、携带方便，保质期长达3年。The chopped rosemary and chopped wormwood are mixed into a mixture according to the mass ratio of 10:1.26, and the mixture and ethanol are poured into a crock pot according to the mass ratio of 1:13 and soaked for 4 hours. Heating the crock pot, heating the liquid inside the crock pot to boiling for decocting, decocting for 9 hours, filtering the solid impurities inside the crock pot to obtain a preliminary medicinal soup, heating and concentrating the preliminary medicinal soup to obtain a concentrated medicinal soup, and concentrating the volume of the medicinal soup It is one-third of the volume of the preliminary medicinal soup; the acetic acid is added to the calcium carbonate for several times and continuously stirred, stirred until clarification to obtain a calcium acetate solution, and the obtained calcium acetate solution is evaporated and concentrated to make a calcium acetate saturated solution; The saturated calcium acetate solution and the concentrated medicinal decoction are mixed according to a mass ratio of 1:11.7 to obtain a mixed solution. The concentrated medicinal decoction is added to the saturated calcium acetate solution in batches for mixing, and the mixed solution is heated to boiling. During the heating process The stirring and heating are stopped until the gelatinous precipitation occurs, and the solid rosemary-type insect repellent is obtained after the mixture is cooled. The solid rosemary-type insect repellent has good physical and chemical stability, is convenient to store, transport, use and carry, and has a shelf life of up to 3 years.
实施例3Example 3
将剪碎的迷迭香和剪碎的艾草按照质量比10:1.3的比例混合成混合料，将混合料和乙醇按照质量比1:15的比例倒入瓦罐中浸泡5h，浸泡结束后给瓦罐加热，瓦罐内部的液体加热至沸腾进行煎煮，煎煮10h，将瓦罐内部的固体杂质过滤得到初步药汤，将初步药汤加热浓缩得到浓缩药汤，浓缩药汤的体积是初步药汤体积的三分之一；将醋酸分多次加到碳酸钙中不断搅拌，搅拌至澄清得到醋酸钙溶液，将所得到的醋酸钙溶液蒸发浓缩制成醋酸钙饱和溶液；所述醋酸钙饱和溶液和浓缩药汤按照质量比1:12的比例混合得到混合液，所述浓缩药汤是分批加入到醋酸钙饱和溶液中进行混合，对混合液进行加热至沸腾，加热过程中不断搅拌直至出现胶状沉淀时停止搅拌和加热，待混合液冷却后即得到固体状迷迭香型驱虫剂。该固体状迷迭香型驱虫剂的物理、化学稳定性好，存储、运输、使用、携带方便，保质期长达3年。The chopped rosemary and chopped wormwood are mixed into a mixture according to the mass ratio of 10:1.3, and the mixture and ethanol are poured into the crock pot according to the mass ratio of 1:15 and soaked for 5 hours. Heating the crock pot, heating the liquid inside the crock pot to boiling for decocting, decocting for 10 hours, filtering the solid impurities inside the crock pot to obtain a preliminary medicinal soup, heating and concentrating the preliminary medicinal soup to obtain a concentrated medicinal soup, and concentrating the volume of the medicinal soup It is one-third of the volume of the preliminary medicinal soup; the acetic acid is added to the calcium carbonate for several times and continuously stirred, stirred until clarification to obtain a calcium acetate solution, and the obtained calcium acetate solution is evaporated and concentrated to make a calcium acetate saturated solution; The saturated calcium acetate solution and the concentrated medicinal decoction are mixed according to the mass ratio of 1:12 to obtain a mixed solution. The concentrated medicinal decoction is added to the saturated calcium acetate solution in batches for mixing, and the mixed solution is heated to boiling. The stirring and heating are stopped until the gelatinous precipitation occurs, and the solid rosemary-type insect repellent is obtained after the mixture is cooled. The solid rosemary-type insect repellent has good physical and chemical stability, is convenient to store, transport, use and carry, and has a shelf life of up to 3 years.
实施例4Example 4
取实施例1~3任一实施例中得到的固体状迷迭香型驱虫剂，切下小块，将小块固体状迷迭香型驱虫剂放入到水中浸泡，所述小块固体状迷迭香型驱虫剂与水之间的质量比为1:（20~30），浸泡20~30分钟后将浸泡液喷洒在需要驱虫的场所。由于醋酸钙与酒精会形成凝胶，该凝胶会将迷迭香和艾草的提取物包裹在其中。因此，固体状迷迭香型驱虫剂的主要成分为醋酸钙、乙醇、以及迷迭香和艾草的提取物。由于醋酸钙、乙醇、迷迭香和艾草的提取物均易溶于水，迷迭香和艾草的提取物中的杀虫成分会缓缓释放到水中，因此本实施例中的浸泡液能够进行驱虫、杀虫。Get the solid rosemary-type insect repellent obtained in any of Examples 1 to 3, cut off small pieces, put the small piece of solid rosemary-type insect repellent into water and soak, the small pieces The mass ratio between the solid rosemary-type insect repellent and water is 1: (20~30). After soaking for 20~30 minutes, spray the soaking liquid on the place that needs to be repelled. Because calcium acetate forms a gel with alcohol, the gel encapsulates the rosemary and wormwood extracts. Therefore, the main components of the solid rosemary-type insect repellent are calcium acetate, ethanol, and extracts of rosemary and wormwood. Since the extracts of calcium acetate, ethanol, rosemary and wormwood are easily soluble in water, the insecticidal components in the extracts of rosemary and wormwood will be slowly released into the water, so the soaking solution in this example Can deworm and kill insects.
实施例5Example 5
取实施例1~3任一实施例中得到的固体状迷迭香型驱虫剂，将其切成长条状或螺旋状，然后将其点燃进行驱虫、杀虫。在该方案中，由于固体状迷迭香型驱虫剂的主要成分为醋酸钙、乙醇、以及迷迭香和艾草的提取物，乙醇能够被点燃，醋酸钙在高温下分解成碳酸钙和丙酮，丙酮和乙醇燃烧生成二氧化碳和水，而迷迭香和艾草的提取物中的杀虫成分会缓缓释放到空气中，从而驱虫、杀虫；该燃烧过程不会产生大量烟尘，污染小，醋酸钙、乙醇、以及迷迭香和艾草的提取物等燃烧不会对人体带来副作用。Take the solid rosemary-type insect repellent obtained in any one of Examples 1 to 3, cut it into strips or spirals, and then ignite it to drive and kill insects. In this scheme, since the main components of the solid rosemary repellent are calcium acetate, ethanol, and extracts of rosemary and wormwood, the ethanol can be ignited, and the calcium acetate is decomposed into calcium carbonate and Acetone, acetone and ethanol are burned to generate carbon dioxide and water, and the insecticidal ingredients in the extracts of rosemary and wormwood will be slowly released into the air, thereby repelling and killing insects; the combustion process does not produce a lot of smoke and dust, The pollution is small, and the burning of calcium acetate, ethanol, and rosemary and wormwood extracts will not cause side effects to the human body.
实施例6Example 6
取实施例1~3任一实施例中得到的固体状迷迭香型驱虫剂，将其切成片状，然后将使用电热片对其加热，使得其中的杀虫成分会缓缓释放到空气中，从而驱虫、杀虫。在该方案中，由于固体状迷迭香型驱虫剂的主要成分为醋酸钙、乙醇、以及迷迭香和艾草的提取物，而迷迭香和艾草的提取物中的杀虫成分会随着乙醇缓缓释放到空气中，从而驱虫、杀虫；该过程不会产生烟尘，无污染，残留物处理方便，不会对人体带来副作用。Take the solid rosemary-type insect repellent obtained in any one of Examples 1 to 3, cut it into sheets, and then heat it with an electric heating sheet, so that the insecticidal ingredients are slowly released to the In the air, thereby repelling and killing insects. In this scheme, since the main components of the solid rosemary-type insect repellent are calcium acetate, ethanol, and the extracts of rosemary and wormwood, the insecticidal components in the extracts of rosemary and wormwood are It will be slowly released into the air with the ethanol, thereby repelling and killing insects; the process will not produce smoke and dust, no pollution, and the residues are easy to handle, and will not bring side effects to the human body.
在上述实施例中，迷迭香具有驱虫、杀虫作用。艾草还具有杀虫作用。迷迭香和艾草配合能够进一步提高所述固体状迷迭香型驱虫剂的杀虫、驱虫效果。迷迭香和艾草中的杀虫成分溶于乙醇，迷迭香和艾草中的杀虫成分溶于乙醇后被制成迷迭香和艾草的提取物。醋酸与碳酸钙反应生成醋酸钙、水、二氧化碳。醋酸钙易溶于水而难溶于酒精，当两种溶液相混合时，醋酸钙在酒精中成为凝胶析出，液体便逐渐从浑浊到稠厚，最后凝聚为一整块，就得到固体迷迭香型驱虫剂。该固体迷迭香型驱虫剂无论是被制成驱虫液还是加热、点燃使用，均不会产生大量烟尘，污染小，对人体的副作用小。In the above embodiment, rosemary has the effect of repelling and killing insects. Wormwood also has insecticidal properties. The combination of rosemary and wormwood can further improve the insecticidal and repelling effects of the solid rosemary-type insect repellent. The insecticidal components in rosemary and wormwood are dissolved in ethanol, and the insecticidal components in rosemary and wormwood are dissolved in ethanol to make extracts of rosemary and wormwood. Acetic acid reacts with calcium carbonate to form calcium acetate, water and carbon dioxide. Calcium acetate is easily soluble in water but insoluble in alcohol. When the two solutions are mixed, calcium acetate forms a gel in the alcohol, and the liquid gradually changes from turbid to thick, and finally condenses into a whole piece to obtain a solid Mary-type insect repellent. Whether the solid rosemary-type insect repellent is made into insect repellent liquid or used by heating and lighting, it does not generate a lot of smoke and dust, has little pollution and has little side effect on the human body.
以上所述仅为本发明的较佳实施例而已，并不用以限制本发明，凡在本发明的精神和原则之内所作的任何修改、等同替换和改进等，均应包含在本发明的保护范围之内。The above descriptions are only preferred embodiments of the present invention and are not intended to limit the present invention. Any modifications, equivalent replacements and improvements made within the spirit and principles of the present invention shall be included in the protection of the present invention. within the range.
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