CN108130222A - A kind of glasses cleaning agent and preparation method thereof - Google Patents
A kind of glasses cleaning agent and preparation method thereof Download PDFInfo
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- CN108130222A CN108130222A CN201810084007.4A CN201810084007A CN108130222A CN 108130222 A CN108130222 A CN 108130222A CN 201810084007 A CN201810084007 A CN 201810084007A CN 108130222 A CN108130222 A CN 108130222A
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- cleaning agent
- glasses cleaning
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/0078—Compositions for cleaning contact lenses, spectacles or lenses
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/042—Acids
-
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2079—Monocarboxylic acids-salts thereof
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38618—Protease or amylase in liquid compositions only
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38627—Preparations containing enzymes, e.g. protease or amylase containing lipase
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38636—Preparations containing enzymes, e.g. protease or amylase containing enzymes other than protease, amylase, lipase, cellulase, oxidase or reductase
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38645—Preparations containing enzymes, e.g. protease or amylase containing cellulase
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/008—Polymeric surface-active agents
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- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/42—Amino alcohols or amino ethers
- C11D1/44—Ethers of polyoxyalkylenes with amino alcohols; Condensation products of epoxyalkanes with amines
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- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/48—N-containing polycondensation products
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- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/62—Quaternary ammonium compounds
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- C11D1/66—Non-ionic compounds
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Abstract
The present invention is suitable for daily cleaning product technical field, provides a kind of glasses cleaning agent and preparation method thereof, glasses cleaning agent by weight, including following component：Amphoteric surfactant：1%~2%；Cationic surfactant：0.12%~0.2%；Enzyme preparation：0.5%~1.5%；PH adjusting agent：0.01%~0.02%；Surplus is deionized water.Glasses cleaning agent provided by the invention is compounded using a variety of mild non-stimulated green materials, builds neutral formula containing enzyme, the Oral toxicity LD of product50>5000mg/kg weight, it is safe, and the protein contaminants and pernicious bacteria of lens surface attachment can be effectively removed, no cleaning agent residual is non-stimulated to eye part skin.
Description
Technical field
The invention belongs to daily cleaning product technical fields more particularly to a kind of glasses cleaning agent and preparation method thereof.
Background technology
Glasses can be divided into four kinds of spectacles, spectacles for long sight, reading glasses and astigmatic glasses comprising contact lenses
With frame glasses.Glasses can be used for correction to improve eyesight, protect eyes or decoration etc..However, people are in wearing spectacles, due to
Glasses are closer to the distance with wearer's eye part skin, so its sweat, tear are just easy to that lens surface can be infected with.In addition,
Dust, bacterium in air etc. also easily adhere to, accumulate in lens surface.Time is grown, and the pollutant on the surface of glasses will
Dirt is deposited into, so as to influence the clarity of eyeglass, meanwhile, the bacterium amount reproduction of attachment extremely easily causes wearer's
Eye disease (such as keratitis, conjunctivitis), especially contact lens wearers -- directly and Corneal Contact, it is more prone to cause
Eye disease.Therefore, periodically or non-periodically cleaning glasses can not only keep the sanitation and hygiene of glasses, and also help wearing
The eye health of person.
However, clean dirt, the bacteria flora etc. that glasses can not remove its surface and deposit with clear water；It is and existing most of
The dirt (such as protein dirt) and the removal rate of bacteria flora that glasses cleaning agent adheres to lens surface be not high, cleaning
It is ineffective.
Invention content
The embodiment of the present invention provides a kind of glasses cleaning agent, it is intended to solve existing most of glasses cleaning agents for glasses
The problem of dirt of surface attachment and the removal rate of bacteria flora be not high, and cleaning effect is bad.
The embodiment of the present invention is achieved in that a kind of glasses cleaning agent, by weight, including following component：Both sexes table
Face activating agent：1%~2%；Cationic surfactant：0.12%~0.2%；Enzyme preparation：0.5%~1.5%；PH is adjusted
Agent：0.01%~0.02%；Surplus is deionized water.
Preferably, glasses cleaning agent, by weight, including following component：Amphoteric surfactant：2%；Cationic surface
Activating agent：0.2%；Enzyme preparation：1.5%；PH adjusting agent：0.01%；Surplus is deionized water.
Preferably, glasses cleaning agent, by weight, including following component：Amphoteric surfactant：1%~2%；Sun from
Sub- surfactant：0.12%~0.2%；Enzyme preparation：0.5%~1.5%；PH adjusting agent：0.01%~0.02%；Air
Work builder：1.5%~2.5%；Surplus is deionized water.
Preferably, glasses cleaning agent, by weight, including following component：Amphoteric surfactant：2%；Cationic surface
Activating agent：0.2%；Enzyme preparation：1.5%；PH adjusting agent：0.01%；Air chemical industry builder：1.5%；Surplus is deionization
Water.
Preferably, the enzyme preparation is protease, lipase, amylase, cellulase, staphylococcal nuclease or molten
Arbitrary two kinds or at least three kinds of mixture in bacterium enzyme.
Preferably, the amphoteric surfactant is stearamide propyl glycine betaine, lauroyl oat amino acid sodium, cocounut oil
Acyl Sodium Glycinate, Sodium Lauroamphoacetate, lauryl betaine, Cocoamidopropyl betaine or cocounut oil acyl both sexes base
In diethyl acid disodium any one or at least two mixture.
Preferably, the cationic surfactant for laureth sodium sulfovinate, didecyl Dimethy ammonium chloride,
Laureth sulfuric ester ammonium, polyquaternium -7 either any one in ethoxylated alkylamine or two kinds of mixture.
Preferably, the pH adjusting agent is any one in citric acid, boric acid, malic acid or sorbic acid or two kinds
Mixture.
Preferably, the amphoteric surfactant includes the substance of following weight ratio：Cocoamidopropyl betaine
2%；
The cationic surfactant includes the substance of following weight ratio：Didecyl Dimethy ammonium chloride 0.2%；
The enzyme preparation includes the substance of following weight ratio：Proteinase-10 .5%, staphylococcal nuclease 1%；
The pH adjusting agent includes the substance of following weight ratio：Citric acid 0.01%.
In embodiments of the present invention, air chemical industry builder can be NOnidet sF-5 surfactants.
The embodiment of the present invention also provides the preparation method of glasses cleaning agent, includes the following steps：
Step 1：Formula according to above-mentioned glasses cleaning agent weighs each component, spare.
Step 2：The part deionized water is added in into ingredients pot；Preferably, 80%~90% is added in into ingredients pot
The deionized water of (weight ratio).
Step 3：The amphoteric surfactant and cationic surfactant are added in into the ingredients pot, and is stirred
To being completely dissolved.
Step 4：The remaining deionized water is added in, puts into the enzyme preparation, and is stirred to being completely dissolved.
Step 5：The pH adjusting agent is put into the ingredients pot, adjusts pH value as neutrality, obtains the glasses cleaning
Agent.
Below to each raw material in above-mentioned glasses cleaning agent the effect of and ingredient do specific description：
Protease：Protein can be hydrolyzed into soluble amino acid, so as to be easy to be washed away, such as blood, sweat stain, coffee
Wait albumen dirt.
Lipase：It is capable of the oily matter of effective human secretory.
Amylase：Starch dirt such as chocolate, mashed potatoes, noodles, congee etc. can be resolved into dextrin or maltose.
Cellulase:Cellulase can remove the microtriche and bobbles remained in glasses gap.
Staphylococcal nuclease：Bacterial biofilm is that a large amount of cells are attached to the surface of solids and organism surface living
Micropopulation.The formation of biofilm can increase the ability that bacterium resists antibiotic and escapes host immunity attack, so as to
The prolonged and repeated infection of many bacteriosis is caused to occur.Staphylococcal nuclease is one of staphylococcus aureus important
There is direct contact between the formation of virulence factor, staphylococcal nuclease and biofilm, play and inhibit what biofilm was formed
Important function.
Lysozyme：It is a kind of to hydrolyze the alkaline enzyme that polysaccharide is sticked in pathogenic bacteria.Mainly by destroying the N- acetyl in cell wall
β-Isosorbide-5-Nitrae glycosidic bond between muramic acid and n-acetylglucosamine makes the insoluble glutinous polysaccharide of cell wall resolve into soluble glycopeptide,
Cell wall rupture content is caused to escape and make bacterolysis.Lysozyme can also with negatively charged virus protein directly in conjunction with,
Double salt is formed with DNA, RNA, apoprotein, is made virally inactivated.Therefore, which has the effects that antibacterial, anti-inflammatory, antiviral,
It is and safe.
Cocoamidopropyl betaine：Source is healthy and safe, and property is extremely mild, nonirritant and sensitization.With breast
The effects that changing, permeate, blistering, foam is especially abundant stable and flexible, can mildly remove skin sweat stain and spot.
Stearamide propyl glycine betaine：With excellent decontamination, dispersion, emulsification, foaming, foam stabilizing, antistatic, thickening energy
Power.Property is mild, can reduce the irritation of other surfaces activating agent, resistance to hard water, and compatibility is good.
Lauroyl oat amino acid sodium：It is good with the compatibility of skin, there is excellent emulsification, dispersion, decontamination, antistatic energy
Power.To hair and skin as mild as a dove, there is stronger skin water lock ability, lasting moisture retention is provided, there is remarkable hair
Steep performance and foam stability energy.Under the bad conditions such as hard water and sebum greasy dirt, performance is outstanding.It easily thickens, not viscosity reduction.Low coloration,
Low smell, available for no perfumed products.
Sodium cocoyl glycinate：It is widely used in the personal-care supplies such as shampoo, bath foam, facial cleanser field.With skin, hair
Hair has outstanding compatibility, is applicable to sensitive skin type.
Sodium Lauroamphoacetate：Mild amphoteric surfactant, whole body can be reduced by living in compounding with anion table
The irritation of system has excellent foaminess in the range of extensive pH, has a wide range of application, and has fabulous compatibility.With
Human skin structure height is consistent, and safety is good, easily biological-degradable.
Lauryl betaine：There are excellent dissolubility and compatibility, there is excellent foaminess and significant thickening property, tool
There are low irritant and bactericidal properties, compatible use can significantly improve softness, conditioning and the low-temperature stability of washing class product, to soap base
There are thickening properties.
Cocounut oil acyl both sexes base diethyl acid disodium：With good surface-active, soil release performance, solubilising, foaming characteristic, spumescence
Matter is stablized.Acid and alkali-resistance, resistance to hard water, compatibility is good, nontoxic non-stimulated, easily biological-degradable.It is antistatic with good rust inhibition
Property.
Didecyl Dimethy ammonium chloride：Polar solvent is soluble in, is slightly soluble in water, there is excellent antistatic and anticorrosion
Property, there are preferable dispersion, emulsification, barbotage.There is good compatibility with cation, nonionic, zwitterionic surfactant
Property.
Polyquaternium -7：It is soluble easily in water, safe and nontoxic, hydrolytic stability is good for cationic high-molecular polymer, it is right
PH value variation is adaptable, and wettability reversal will not occur.With splendid wetability, flexibility, film forming.With water and it is cloudy from
Son, nonionic surfactant have good compatibility, viscous so as to increase for that can form salty complex compound in detergent
Degree.
Ethoxylated alkylamine：It can be matched with the various surfactants including cation, solubility takes in water
Certainly in the pH of degree of ethoxylation, fat-based chain length, stabilization and medium.Ethoxylated alkylamine frequently as conditioner also through adding in
In hair care and skincare product.
Laureth sodium sulfovinate：There is washing, emulsification, wetting, there is excellent biological degradability and low temperature
Activity, active matter content is higher, is not influenced by the water hardness.
Laureth sulfuric ester ammonium：It is usually used in personal cleanliness's articles for use, particularly the product of low ph value.Irritation is low,
Foaming abundancy is fine and smooth, strong detergency, biodegradable good.With good hard water resistance performance, degreasing power is moderate.
Citric acid：Belong to one kind of tartaric acid, available for preparing buffer solution, adjust pH.
Boric acid：Its aqueous solution is in faintly acid, can be used as pH adjusting agent.
Malic acid：It is present in the fruits such as jejune apple, grape, hawthorn, it also can be by fumaric acid through biofermentation
It is made, has special happy, soft tart flavour, pH value can be reduced, there is antibacterial and oxidation resistant effect.
Sorbic acid：White crystalline powder, tasteless, odorless, optimal use pH ranges are less than 4.5.It becomes reconciled to mould, yeast
Gas bacterium has inhibiting effect, but nearly unavailable to anaerobies endospore forming bacteria and lactobacillus acidophilus.It is commonly used for the anti-of cosmetics
Rotten agent is mainly used as the fungal preservation agent of cream, lotion, is most widely used acid type food preservative in the world.
NOnidet sF-5 surfactants：It is a kind of low bubble nonionic surfactant, there are multiple functions, be suitable for
Various low bubble cleanings.NOnidet sF-5 surfactants are based on straight chain base alcohol, have 100% activity, suitable for foam volume
As low as possible, quick humidification, convenient for rinsing, emulsifiability it is good, dirt-removing power is strong, can with most of surfactants, without machine aided
Agent and chelating agent compatibility.
Glasses cleaning agent provided in an embodiment of the present invention is compounded using a variety of mild non-stimulated green materials, is built
Neutral formula containing enzyme, the Oral toxicity LD of product50>5000mg/kg weight, it is safe, and can effectively remove glasses table
The protein contaminants and pernicious bacteria of face attachment, no cleaning agent residual are non-stimulated to eye part skin.
Specific embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, below in conjunction with specific embodiment, to this
Invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, not
For limiting the present invention.
Glasses cleaning agent provided in an embodiment of the present invention is compounded using a variety of mild non-stimulated green materials, is built
Neutral formula containing enzyme, the Oral toxicity LD of product50>5000mg/kg weight, it is safe, and can effectively remove glasses table
The protein contaminants and pernicious bacteria of face attachment, no cleaning agent residual are non-stimulated to eye part skin.
Technical scheme of the present invention and technique effect are described further below by way of specific embodiment.
Embodiment 1：
A kind of glasses cleaning agent, by weight, including following component：Amphoteric surfactant (cocamidopropyl propyl amide beet
Alkali 1%)；Cationic surfactant (didecyl Dimethy ammonium chloride 0.12%)；Enzyme preparation (proteinase-10 .25%, grape
Gonorrhoeae nucleic acid enzyme 0.25%), totally 0.5%；PH adjusting agent (citric acid 0.01%)；Air chemical industry builder (NOnidet sF-5
2.5%)；Surplus is deionized water.
In embodiments of the present invention, the preparation method of above-mentioned glasses cleaning agent, includes the following steps：
Step 1：Formula according to above-mentioned glasses cleaning agent weighs each component, spare.
Step 2：Portions of de-ionized water is added in into ingredients pot；Preferably, 80%~90% (weight is added in into ingredients pot
Amount ratio) deionized water.
Step 3：Amphoteric surfactant, cationic surfactant and air chemical industry builder are added in into ingredients pot,
And it stirs to being completely dissolved.
Step 4：It adds in remaining deionized water, puts into enzyme preparation, and stir to being completely dissolved.
Step 5：PH adjusting agent is put into ingredients pot, pH value is adjusted as neutrality, obtains glasses cleaning agent.
Embodiment 2：
A kind of glasses cleaning agent, by weight, including following component：Amphoteric surfactant (cocamidopropyl propyl amide beet
Alkali 1.5%)；Cationic surfactant (didecyl Dimethy ammonium chloride 0.15%)；Enzyme preparation (proteinase-10 .5%, grape
Gonorrhoeae nucleic acid enzyme 0.5%), totally 1.5%；PH adjusting agent (citric acid 0.02%)；Air chemical industry builder (NONIDET SF-5
2%)；Surplus is deionized water.
In embodiments of the present invention, the preparation method of glasses cleaning agent is same as Example 1.
Embodiment 3：
A kind of glasses cleaning agent, by weight, including following component：Amphoteric surfactant (cocamidopropyl propyl amide beet
Alkali 2%)；Cationic surfactant (didecyl Dimethy ammonium chloride 0.2%)；Enzyme preparation (proteinase-10 .5%, grape ball
Bacterium nuclease 1%), totally 1.5%；PH adjusting agent (citric acid 0.01%)；Air chemical industry builder (NONIDET SF-5
1.5%)；Surplus is deionized water.
In embodiments of the present invention, the preparation method of glasses cleaning agent is same as Example 1.
Embodiment 4：
A kind of glasses cleaning agent, by weight, including following component：Amphoteric surfactant (cocamidopropyl propyl amide beet
Alkali 1.5%)；Cationic surfactant (didecyl Dimethy ammonium chloride 0.12%)；Enzyme preparation (proteinase-10 .4%, grape
Gonorrhoeae nucleic acid enzyme 0.6%), totally 1%；PH adjusting agent (citric acid 0.01%)；Air chemical industry builder (NONIDET SF-5
1.5%)；Surplus is deionized water.
In embodiments of the present invention, the preparation method of glasses cleaning agent is same as Example 1.
Embodiment 5：
A kind of glasses cleaning agent, by weight, including following component：Amphoteric surfactant (cocamidopropyl propyl amide beet
Alkali 1.5%)；Cationic surfactant (didecyl Dimethy ammonium chloride 0.12%)；Enzyme preparation (protease 1.2%, grape
Gonorrhoeae nucleic acid enzyme 0.3%), totally 1.5%；PH adjusting agent (citric acid 0.02%)；Air chemical industry builder (NONIDET SF-5
2%)；Surplus is deionized water.
In embodiments of the present invention, the preparation method of glasses cleaning agent is same as Example 1.
Embodiment 6：
A kind of glasses cleaning agent, by weight, including following component：Amphoteric surfactant (lauroyl both sexes guanidine-acetic acid
Sodium 1%, Cocoamidopropyl betaine 1%), totally 2%；Cationic surfactant (didecyl Dimethy ammonium chloride
0.1%th, polyquaternium -7 0.05%), totally 0.15%；Enzyme preparation (proteinase-10 .4%, staphylococcal nuclease 0.4%, bacteriolyze
Enzyme 0.4%), totally 1.2%；PH adjusting agent (citric acid 0.01%, malic acid 0.005%), totally 0.015%；Air chemical industry, which helps, to be washed
Agent (NONIDET SF-5 1.8%)；Surplus is deionized water.
In embodiments of the present invention, the preparation method of glasses cleaning agent is same as Example 1.
Embodiment 7：
A kind of glasses cleaning agent, by weight, including following component：Amphoteric surfactant (stearamide propyl beet
Alkali 0.5%, lauroyl oat amino acid sodium 0.5%, Cocoamidopropyl betaine 1%), totally 2%；Cationic surfactant
(laureth sodium sulfovinate 0.01%, didecyl Dimethy ammonium chloride 0.09%, laureth sulfuric ester ammonium
0.02%th, polyquaternium -7 0.02%, ethoxylated alkylamine 0.04%), totally 0.18%；Enzyme preparation (proteinase-10 .1%, fat
Fat enzyme 0.15%, staphylococcal nuclease 0.2%, lysozyme 0.05%), totally 0.5%；PH adjusting agent (citric acid 0.008%,
Boric acid 0.002%), totally 0.01%；Surplus is deionized water.
In embodiments of the present invention, the preparation method of glasses cleaning agent is substantially the same manner as Example 1, the difference lies in：
Step 3：Amphoteric surfactant, cationic surfactant are added in into ingredients pot, and is stirred to being completely dissolved.
Embodiment 8：
A kind of glasses cleaning agent, by weight, including following component：Amphoteric surfactant (sodium cocoyl glycinate
0.3%th, Sodium Lauroamphoacetate 0.2%, Cocoamidopropyl betaine 0.8%), totally 1.3%；Cation surface activating
Agent (laureth sodium sulfovinate 0.02%, didecyl Dimethy ammonium chloride 0.08%, ethoxylated alkylamine 0.02%),
Totally 0.12%；Enzyme preparation (proteinase-10 .3%, cellulase 0.2%, staphylococcal nuclease 0.4%, lysozyme 0.6%), altogether
1.5%；PH adjusting agent (citric acid 0.006%, boric acid 0.005%, malic acid 0.005%, sorbic acid 0.004%), altogether
0.02%；Surplus is deionized water.
In embodiments of the present invention, the preparation method of glasses cleaning agent is same as Example 7.
Embodiment 9：
A kind of glasses cleaning agent, by weight, including following component：Amphoteric surfactant (lauryl betaine
0.3%th, Cocoamidopropyl betaine 0.5%, cocounut oil acyl both sexes base diethyl acid disodium 0.2%), totally 1%；Cationic surface is lived
Property agent (laureth sodium sulfovinate 0.05%, didecyl Dimethy ammonium chloride 0.1%, laureth sulfuric ester ammonium
0.05%), totally 0.2%；Enzyme preparation (proteinase-10 .2%, lipase 0.3%, amylase 0.2%, staphylococcal nuclease
0.2%), totally 0.9%；PH adjusting agent (citric acid %, boric acid %), totally 0.014%；Surplus is deionized water.
In embodiments of the present invention, the preparation method of glasses cleaning agent is same as Example 7.
Embodiment 10：
A kind of glasses cleaning agent, by weight, including following component：Amphoteric surfactant (stearamide propyl beet
Alkali 0.4%, Sodium Lauroamphoacetate 0.2%, lauryl betaine 0.4%, Cocoamidopropyl betaine 1%), altogether
2%；Cationic surfactant (laureth sodium sulfovinate 0.05%, didecyl Dimethy ammonium chloride 0.15%), altogether
0.2%；Enzyme preparation (proteinase-10 .3%, lipase 0.3%, amylase 0.3%, cellulase 0.2%, staphylococcal nuclease
0.2%th, lysozyme 0.2%), totally 1.5%；PH adjusting agent (citric acid 0.01%)；Surplus is deionized water.
In embodiments of the present invention, the preparation method of glasses cleaning agent is same as Example 7.
It should be noted that in embodiments of the present invention, enzyme preparation is protease, lipase, amylase, cellulase,
Arbitrary two kinds or at least three kinds of mixture in staphylococcal nuclease or lysozyme.For convenience of description, above-mentioned implementation
Example illustrates only several preferred combinations therein, in practical applications, can arbitrarily choose at least two enzyme therein and carry out
Compounding, it is only necessary to which keeping the enzyme preparation, shared weight ratio is 0.5%~1.5% in formula, herein just not one by one
Enumerate one of the various combinations.
Based on it is above-mentioned identical the reasons why, the present embodiments relate to amphoteric surfactant be stearamide propyl beet
Alkali, lauroyl oat amino acid sodium, sodium cocoyl glycinate, Sodium Lauroamphoacetate, lauryl betaine, coconut oleoyl amine
Propyl betaine either any one in cocounut oil acyl both sexes base diethyl acid disodium or at least two mixture；Cation form
Face activating agent is laureth sodium sulfovinate, didecyl Dimethy ammonium chloride, laureth sulfuric ester ammonium, polyquaternary amine
Salt -7 either any one in ethoxylated alkylamine or two kinds of mixture；PH adjusting agent is citric acid, boric acid, apple
The mixture of any one or two kinds in acid or sorbic acid.The various combinations of these above-mentioned components are also not herein one by one
It enumerates.
The advantageous effect for the glasses cleaning agent that embodiment provides in order to further illustrate the present invention, below in conjunction with specific experiment
Example elaborates.
Experiment one：Ocular irritation/erosion test
1st, test specimen：Glasses cleaning agent sample provided in an embodiment of the present invention.
2nd, test method：With reference to SN/T 2329-2009 cosmetics eye irritation/corrosive chick chorioallantoic membrane examination
It tests.
3rd, result of the test refers to the following table 1.
Table 1
Eye part skin is the skin of fragility the most delicate and to be easy to infected and allergy in human body.Use glasses
Cleaning agent clean glasses when, particularly cleaning contact lenses when, if do not rinse well or glasses on remaining cleaning fluid residue,
Certain stimulation can be caused to eye.And the glasses provided in an embodiment of the present invention cleaning it can be seen from the result of the test of upper table 1
Agent is nonirritant to eye, i.e., product is mildly non-stimulated to skin, and safety is good.
Experiment two：Human skin patch test
(1) skin closure type patch test
1st, test specimen：Glasses cleaning agent provided in an embodiment of the present invention.
2nd, test method：From a certain 33 volunteers of regional choice, the age of volunteer, body was good between 20~45 years old
Health, in the recent period non-drug administration, nonbreast-fed women or gravid woman, non-constitution sensitive subjects.Volunteer is divided into 11 groups at random,
Every group of three people.Wherein, group 1 is blank control group, and the small interior of spot examination device does not place any substance, spot is tried the low sensitization glue of device
Band is pasted on the back of volunteer or forearm bends side, is gently pressed with palm and is allowed to equably stick on the skin；Group 2~groups 11 with
The processing method of group 1 is identical, unlike：The glasses cleaning agent that will be provided respectively added with the 0.025mL embodiment of the present invention 1~10
It is put into the small interior of spot examination device；I.e. group 2 it is corresponding be the embodiment of the present invention 1 provide glasses cleaning agent, group 3 it is corresponding be the present invention
The glasses cleaning agent that embodiment 2 provides, it is glasses cleaning agent ... that the embodiment of the present invention 3 provides that group 4 is corresponding,
Group 11 it is corresponding be the embodiment of the present invention 10 provide glasses cleaning agent.After each group test duration 24 hours, 48 hours, spot is removed
30min after examination device, after impression disappearance, observation sticks the response situation and record of place's skin.
Wherein, skin closure type patch test dermoreaction grade scale see the table below 2.
Table 2
During entire experiment, the subject's of group 1- groups 11 is reacted negative by gesture area skin.Thus
As can be seen that glasses cleaning agent provided in an embodiment of the present invention will not cause the allergy and stimulate the reaction of skin, safety is good.
(2) repeatability is opening smears experiment
1st, test specimen：Glasses cleaning agent provided in an embodiment of the present invention.
2nd, from a certain region select 33 volunteers, the age of volunteer between 20-45 Sui, health, in the recent period
Non- drug administration, nonbreast-fed women or gravid woman, non-constitution sensitive subjects.Volunteer is divided into 11 groups, every group three at random
It is personal.Wherein, group 1 is blank control group, is bent using forearm as recipient site, 3 × 3cm of area2, recipient site holding drying,
It avoids contact with before tested and during by gesture other external preparations, with ultra-pure water 0.05 ± 0.005g/ times, equably smears tested portion
Position；Group 2~groups 11 are respectively test group, unlike group 1：The glasses cleaning agent provided using the embodiment of the present invention 1~10
0.05 equably smears recipient site ± 0.005g/ times；Wherein, group 2 corresponds to the glasses cleaning agent that the embodiment of the present invention 1 provides,
Group 3 corresponds to the glasses cleaning agent that the embodiment of the present invention 2 provides, and group 4 corresponds to the glasses cleaning agent ... that the embodiment of the present invention 3 provides
And so on, group 11 corresponds to the glasses cleaning agent that the embodiment of the present invention 10 provides.Each group carries out equably smearing for 2 times daily tested
Position, long run test complete experiment after 7 days, observe the dermoreaction situation of the recipient site of subject daily and record.It is trying
During testing, during if there is 3 points or more in such as the following table 3 of dermoreaction situation, it can stop continuing to test and recording knot
Fruit.
Wherein, table 3 tests dermoreaction judgment criteria table for opening smear of skin repeatability.
Table 3
During entire experiment, the dermoreaction by gesture position of the subject of group 1~groups 11 is negative.By
This, which can be seen that glasses cleaning agent provided in an embodiment of the present invention, will not cause the allergy and stimulate the reaction of skin, and safety is good.
Experiment three：Acute oral toxicity test
1st, test specimen：Glasses cleaning agent provided in an embodiment of the present invention.
2nd, test method：25 grams of glasses rinse product to the number for weighing Examples 1 to 10 offer respectively is 1~10
In volumetric flask, add in ultra-pure water and be settled to 100mL, mixing is as experimental liquid.
Trial test：Oral gavage experiment is carried out to experimental animal using the experimental liquid of 5000mg/kg body weight doses, is not found
There is death in experimental animal, therefore formal test design dosage is 5000mg/kg weight.
Formal test：110 healthy, 18~20 grams of weight SPF grade kunming mices are chosen, stochastic averagina is divided into 11
Group, every group each 10, half male and half female, and it is 1~11 to number, wherein, group 1 is blank control group, by the amount of 0.2mL/10g weight
Ultra-pure water is given with oral 1 gavage of gastric perfusion needle；Group 2~groups 11 are respectively by oral 1 time of the amount gastric perfusion needle of 0.2mL/10g weight
Gavage gives 1~No. 10 experimental liquid, that is, organizes 2 and give No. 1 experimental liquid, group 3 gives No. 2 experimental liquids, and group 4 gives No. 3 experimental liquids, group
5 give No. 4 experimental liquids ..., and group 11 gives No. 10 experimental liquids.Each group animal fasting 16 hours, freely drink before gavage
Water gives normal diet after gavage, the Routine Management under conditions of 22 ± 1 DEG C of room temperature, humidity 60 ± 5%；Raise identical day
Number observes the poisoning symptom and death condition of mouse daily, and after the completion of experiment in 14 days, data statistics is carried out to result of the test.
Wherein, it during this experiment, is poisoned during finger to finger test, mouse occurs trembling, twitches, salivates, diarrhea, drowsiness
With stupor etc. symptoms.Oral toxicity classification such as following table, shown in 4：
Table 4
| LD50(mg/Kg) | ≤50 | 51~500 | 501~5000 | ＞ 5000 |
| Toxicity grading | High poison | Medium poison | Low toxicity | It is practical nontoxic |
During entire experiment, the diet activity of each group animal subject normally has no apparent poisoning symptom and death.By
This is as it can be seen that the mouse oral toxicity LD50 of glasses cleaning agent provided in an embodiment of the present invention>5000mg/kg weight, safety are good.
Experiment four：Cleaning sterilization effect test
1st, test specimen：(extra large pari's grace is stealthy near for the glasses cleaning agent and contrast product that the embodiment of the present invention 1~10 provides
Glasses detergent, Hydron U.S. pupil stealth spectacles).
2nd, test method：The volunteer of 120 contact lens is randomly choosed, and is randomly divided into 12 groups, every group of 10 people.
The glasses cleaning agent test group that wherein group 1~10 is provided for the embodiment of the present invention 1~10 is organized 1 and is provided for the embodiment of the present invention 1
Glasses cleaning agent test group, the glasses cleaning agent test groups that group 2 is provided for the embodiment of the present invention 2, group 3 is the embodiment of the present invention
The 3 glasses cleaning agent test groups ... provided and so on, the glasses cleaning agent experiment that group 10 is provided for the embodiment of the present invention 10
Group；Group 11 is extra large pari's grace stealth spectacles detergent test group, and group 12 is Hydron U.S. pupil stealth spectacles test group.
During experiment, volunteers unload glasses at 9 points at night, unload glasses in 9 contact lens in morning
Afterwards, it detects the staphylococcus aureus of each group contact lenses on piece, Escherichia coli, Aspergillus, hemolytic streptococcus, be deposited on mirror
The average content of the tear protein matter of on piece, and record.Then, per test group using a concentration of 1% test specimen liquid to this
The glasses of group carry out cleaning 5min, detect the average content and record of each strain and tear protein matter on each group eyeglass again.
3rd, result of the test：The following table 5 is referred to, wherein, sterilizing rate=100% × (wash preceding colony counts-wash rear colony counts)/
Wash preceding colony counts；
Tear protein resolution ratio=100% × (wash preceding tear protein quantity-washes rear tear protein quantity)/wash preceding clump count
Amount.
Table 5
Staphylococcus aureus, Aspergillus in contact lenses can cause the eye diseases such as keratitis, conjunctivitis.By upper table
5 result of the test it is found that the glasses cleaning agent that provides of the embodiment of the present invention 1~10 for staphylococcus aureus, Escherichia coli,
Mould, hemolytic streptococcus sterilizing rate up to more than 99%, and for lens surface deposition tear protein matter resolution ratio
Up to more than 99%, obviously higher than contrast product, i.e. this product can effectively remove the pernicious bacteria adhered in lens surface
And protein contaminants.
Wherein, the cleaning sterilization effect of the glasses cleaning agent of the embodiment of the present invention 3 is best, i.e., when enzyme preparation for protease and
During the compound of staphylococcal nuclease, bactericidal effect is good.
Glasses cleaning agent provided in an embodiment of the present invention is compounded using a variety of mild non-stimulated green materials, is built
Neutral formula containing enzyme, the Oral toxicity LD of product50>5000mg/kg weight, it is safe, and can effectively remove glasses table
The protein contaminants and pernicious bacteria of face attachment, no cleaning agent residual are non-stimulated to eye part skin.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
All any modification, equivalent and improvement made within refreshing and principle etc., should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of glasses cleaning agent, which is characterized in that by weight, including following component：
Amphoteric surfactant：1%~2%；
Cationic surfactant：0.12%~0.2%；
Enzyme preparation：0.5%~1.5%；
PH adjusting agent：0.01%~0.02%；
Surplus is deionized water.
2. glasses cleaning agent as described in claim 1, which is characterized in that by weight, including following component：
Amphoteric surfactant：2%；
Cationic surfactant：0.2%；
Enzyme preparation：1.5%；
PH adjusting agent：0.01%；
Surplus is deionized water.
3. glasses cleaning agent as described in claim 1, which is characterized in that by weight, including following component：
Amphoteric surfactant：1%~2%；
Cationic surfactant：0.12%~0.2%；
Enzyme preparation：0.5%~1.5%；
PH adjusting agent：0.01%~0.02%；
Air chemical industry builder：1.5%~2.5%；
Surplus is deionized water.
4. glasses cleaning agent as claimed in claim 3, which is characterized in that by weight, including following component：
Amphoteric surfactant：2%；
Cationic surfactant：0.2%；
Enzyme preparation：1.5%；
PH adjusting agent：0.01%；
Air chemical industry builder：1.5%；
Surplus is deionized water.
5. glasses cleaning agent as described in claim 1, which is characterized in that the enzyme preparation is protease, lipase, starch
Arbitrary two kinds or at least three kinds of mixture in enzyme, cellulase, staphylococcal nuclease or lysozyme.
6. glasses cleaning agent as described in claim 1, which is characterized in that the amphoteric surfactant is stearamide propyl
Glycine betaine, lauroyl oat amino acid sodium, sodium cocoyl glycinate, Sodium Lauroamphoacetate, lauryl betaine, cocounut oil
Amido propyl betaine either any one in cocounut oil acyl both sexes base diethyl acid disodium or at least two mixture.
7. glasses cleaning agent as described in claim 1, which is characterized in that the cationic surfactant is laureth
Sodium sulfovinate, didecyl Dimethy ammonium chloride, laureth sulfuric ester ammonium, polyquaternium -7 or ethoxylated alkylamine
In any one or two kinds mixture.
8. glasses cleaning agent as described in claim 1, which is characterized in that the pH adjusting agent is citric acid, boric acid, malic acid
Or the mixture of any one or two kinds in sorbic acid.
9. the glasses cleaning agent as described in claim 3 or 4, which is characterized in that the amphoteric surfactant includes following weight
The substance of amount ratio：Cocoamidopropyl betaine 2%；
The cationic surfactant includes the substance of following weight ratio：Didecyl Dimethy ammonium chloride 0.2%；
The enzyme preparation includes the substance of following weight ratio：Proteinase-10 .5%, staphylococcal nuclease 1%；
The pH adjusting agent includes the substance of following weight ratio：Citric acid 0.01%.
10. the preparation method of glasses cleaning agent as claimed in any one of claims 1 to 9 wherein, which is characterized in that including walking as follows
Suddenly：
Formula according to glasses cleaning agent as claimed in any one of claims 1 to 9 wherein weighs each component, spare；
The part deionized water is added in into ingredients pot；
It adds in the amphoteric surfactant and cationic surfactant into the ingredients pot, and stirs to being completely dissolved；
The remaining deionized water is added in, puts into the enzyme preparation, and is stirred to being completely dissolved；
The pH adjusting agent is put into the ingredients pot, pH value is adjusted as neutrality, obtains the glasses cleaning agent.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110527602A (en) * | 2019-08-30 | 2019-12-03 | 合肥学院 | A kind of portable computer impregnated wipe |
| CN112080353A (en) * | 2020-09-02 | 2020-12-15 | 广东丽臣奥威实业有限公司 | Mild and efficient surfactant composition for cleaning |
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| CN1186255A (en) * | 1996-12-27 | 1998-07-01 | 刘伟中 | All functional lotion |
| CN1326106A (en) * | 2000-05-26 | 2001-12-12 | 盛岩 | Special nursing liquid |
| JP2007256969A (en) * | 2007-05-11 | 2007-10-04 | Rohto Pharmaceut Co Ltd | Liquid agent for cleaning and storing contact lens |
| JP2014088534A (en) * | 2012-10-31 | 2014-05-15 | Sanyo Chem Ind Ltd | Liquid detergent composition |
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- 2018-01-29 CN CN201810084007.4A patent/CN108130222A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1186255A (en) * | 1996-12-27 | 1998-07-01 | 刘伟中 | All functional lotion |
| CN1326106A (en) * | 2000-05-26 | 2001-12-12 | 盛岩 | Special nursing liquid |
| JP2007256969A (en) * | 2007-05-11 | 2007-10-04 | Rohto Pharmaceut Co Ltd | Liquid agent for cleaning and storing contact lens |
| JP2014088534A (en) * | 2012-10-31 | 2014-05-15 | Sanyo Chem Ind Ltd | Liquid detergent composition |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110527602A (en) * | 2019-08-30 | 2019-12-03 | 合肥学院 | A kind of portable computer impregnated wipe |
| CN112080353A (en) * | 2020-09-02 | 2020-12-15 | 广东丽臣奥威实业有限公司 | Mild and efficient surfactant composition for cleaning |
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