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CN108117301A - A kind of non-sintered filled type vacuum stone preparation process - Google Patents

A kind of non-sintered filled type vacuum stone preparation process Download PDF

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Publication number
CN108117301A
CN108117301A CN201611075153.8A CN201611075153A CN108117301A CN 108117301 A CN108117301 A CN 108117301A CN 201611075153 A CN201611075153 A CN 201611075153A CN 108117301 A CN108117301 A CN 108117301A
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China
Prior art keywords
aggregate
solid
liquid
preparation process
unit body
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CN201611075153.8A
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Chinese (zh)
Inventor
杨绍良
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Anhui Province Environmental Protection Mstar Technology Ltd Lee Teuk Amtt
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Anhui Province Environmental Protection Mstar Technology Ltd Lee Teuk Amtt
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Application filed by Anhui Province Environmental Protection Mstar Technology Ltd Lee Teuk Amtt filed Critical Anhui Province Environmental Protection Mstar Technology Ltd Lee Teuk Amtt
Priority to CN201611075153.8A priority Critical patent/CN108117301A/en
Priority to PCT/CN2017/107213 priority patent/WO2018099204A1/en
Publication of CN108117301A publication Critical patent/CN108117301A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B26/00Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
    • C04B26/02Macromolecular compounds
    • C04B26/04Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C04B26/06Acrylates
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B26/00Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
    • C04B26/02Macromolecular compounds
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B26/00Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
    • C04B26/02Macromolecular compounds
    • C04B26/10Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C04B26/14Polyepoxides
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B40/00Processes, in general, for influencing or modifying the properties of mortars, concrete or artificial stone compositions, e.g. their setting or hardening ability
    • C04B40/0028Aspects relating to the mixing step of the mortar preparation
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/54Substitutes for natural stone, artistic materials or the like

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention discloses a kind of non-sintered filled type vacuum stone preparation processes, comprise the following steps, and prepare fills unit body, fine grain solid particle filler material is mixed with liquid filler, and the surface of the solid particle filler material is made to form flexible liquid filling film;The granulated aggregate of different-grain diameter with the fills unit body is mixed, mixture is made by batch mixing;Shaping, granulated aggregate movement filling, and the fills unit body is filled into the gap of each granulated aggregate mutually under vacuum power and the force action of weight slap power, forms vacuum tightness body.The present invention uses a kind of brand-new preparation process, using the mutual filling between size particles, will have the gap and tamps as far as possible, and the air in the gap between granulated aggregate is discharged, and forms vacuum tightness body, i.e., using Magdeburg hemispheres principle, forms vacuum stone.

Description

A kind of non-sintered filled type vacuum stone preparation process
Technical field
The present invention relates to a kind of non-sintered filled type vacuum stone preparation processes.
Background technology
Pith of the lithotome as construction material, because its color is diversified, exploitation is easy, always since ancient times It is widely used by people.But with the excessive increase of its yield, the reasons such as exploitation utilization rate is low, the exploitation of lithotome is progressively It is restricted, particularly European countries, has prohibited the exploitation of lithotome.And the product in each mineral products area, pattern, Kind is all only one, further increases the difficulty in its use.People always search for its substitute.With the development of economy, Building and ornament materials are maked rapid progress, and compound stone obtains very big opportunity to develop as a kind of new ornament materials.But existing skill Compound stone in art usually has granulated aggregate and binding agent mixing to suppress, such as China Patent No. is CN200910215153.7 patents of invention, publication date are on May 11st, 2011, disclose a kind of system of artificial quartz stone plate Standby technique, which is characterized in that it is comprised the technical steps that:A, dispensing, by automatic batching system by quartz sand, silica flour, Glass, marble particle, unsaturated-resin, toner, curing agent and coupling agent mix in proportion, and are sent into planetary mixer at a high speed Stirring, be sufficiently stirred will directly expect to drop afterwards it is preset it is framed in, material cloth is put down, is then covered with leatheroid;B, multilayer lamination is passed through Machine stacks multiple plates;C, compacting, intermediate temperature setting, by multi-laminate plate pressing machine compression moulding, using lift curing oven, using three The curing mode of block iron plate folder plus two plates, conduction is evenly heated by constant temperature conduction oil, cures plate uniform shrinkage;d、 Polishing, cutting, packaging.During the processing step a, the primary raw material and ratio of adjuvant (calculating by weight percentage) of use Including quartz sand 10~40%, silica flour 28~36%, glass 5~45%, marble particle 5~15%, unsaturated-resin 8~ 12%th, toner 0.1~0.4%, curing agent and coupling agent 0.04~0.5%.It can be seen that in the prior art by above-mentioned patent Blending process in be to be mixed together binding agent (resin) with aggregate, essence is to be bonded in each aggregate by binding agent Together, the intensity of compound stone is determined by binding agent.But this adhesive bond mode is limited by adhesion strength, compound stone Intensity be difficult improve.In addition, in order to which all aggregates are bonded together, it is necessary to using more resin, tree is added The usage amount of fat, the increase of resin usage amount not only reduces the intensity of compound stone, but also brings environmental issue.
The content of the invention
The technical problems to be solved by the invention are the deficiency for overcoming the above-mentioned prior art, provide a kind of intensity height, ring A kind of non-sintered filled type vacuum stone preparation process protected.
According to a kind of non-sintered filled type vacuum stone preparation process provided by the invention, comprise the following steps, preparation is filled out Cell cube is filled, fine grain solid particle filler material with liquid filler is mixed, makes the surface shape of the solid particle filler material Into flexible liquid filling film;The granulated aggregate of different-grain diameter with the fills unit body is mixed, mixture is made by batch mixing;Into Type, granulated aggregate movement filling, and by the fills unit mutually under vacuum power and the force action of weight slap power Body is filled into the gap of each granulated aggregate, forms vacuum tightness body.
Also there is following attached technology spy according to a kind of non-sintered filled type vacuum stone preparation process provided by the invention Sign:
Further comprise, the dosage of the solid particle filler material and the liquid filler is determined by the following conditions:
QLiquid=(ρSolidParticle is compacted)/ρSolid×1cm3×ρLiquid
QSolidParticle is compacted×1cm3
In formula:QLiquidTo be pressed with 1 ton of pressure to the fills unit body of a square centimeters area, one is finally obtained Liquid filler benchmark dosage unit g in the fills unit body of cubic centimetre
QSolidIt is final to obtain one cube li to be pressed with 1 ton of pressure to the fills unit body of a square centimeters area Solid particle filler material benchmark dosage unit g in the fills unit body of rice
ρSolidFor the actual density unit g/cm of solid particle filler material3
ρParticle is compactedTo be pressed with 1 ton of pressure to a square centimeters area solid granule filling material, final acquisition one is vertical The mass unit g/cm of square centimetre of solid particle filler material3
ρLiquidFor the actual density unit g/cm of liquid filler3
Further comprise, the dosage of the granulated aggregate and the fills unit body is determined by the following conditions:
QCell cube=(ρAggregateAggregate is compacted)/ρAggregate×1cm3×ρCell cube
QAggregateAggregate is compacted×1cm3
In formula:QCell cubeFor the fills unit body benchmark dosage unit g in one cubic centimetre of vacuum stone
QAggregateFor the granulated aggregate benchmark dosage unit g in one cubic centimetre of vacuum stone
ρAggregateFor the actual density unit g/cm of granulated aggregate3
ρAggregate is compactedIt is final to obtain one cube li to be pressed with 1 ton of pressure to the granulated aggregate of a square centimeters area The mass unit g/cm of the granulated aggregate of rice3
ρCell cubeFor the actual density unit g/cm of fills unit body3
ρCell cube=(QLiquid+QSolid)/1cm3
Further comprise, with the liquid filler by being stirred, weight ratio is the solid particle filler material 2-6:1.
Further comprise, cloth has been further included before forming step, the mixture is arranged to platy structure.
Further comprise, further included curing after the conformation step, the liquid filler is become into solid-state from liquid.
Further comprise, the grain size of the solid particle filler material is 0.1mm-0.01mm, the grain size of the granulated aggregate For more than 0.1mm.
Further comprise, the liquid filler, which can have from liquid, becomes solid characteristic, including organic resinoid With inorganic resinoid.
Further comprise, organic resinoid includes acryl resin, unsaturated-resin, propylene resin or asphalt mixtures modified by epoxy resin Fat.
Further comprise, the inorganic resinoid includes soybean-based resin or rubber resin.
Have compared with prior art such as according to a kind of non-sintered filled type vacuum stone preparation process provided by the invention Lower advantage:The present invention uses a kind of brand-new preparation process, and small size particle aggregate is filled into the seam of large-size particles aggregate In gap, then fine particle size granulated aggregate is filled into the gap of small size particle aggregate, the gap of fine particle aggregate then by Liquid filler is filled, and using the mutual filling between size particles, will be had the gap and is tamped as far as possible, will be between granulated aggregate Air discharge in gap, forms vacuum tightness body, i.e., using Magdeburg hemispheres principle, forms vacuum stone, vacuum of the invention Stone intensity is not dependent on the adhesion strength of binding agent, but the compaction rate by filling determines, can effectively improve vacuum stone Intensity.Liquid filler in the present invention is only mixed with fine grain solid particle, therefore usage amount is smaller, not only environmentally friendly, and And facilitate stirring and processing.
Description of the drawings
Fig. 1 is the structure diagram of the present invention.
Specific embodiment
Clearly to illustrate the scheme in the present invention, preferred embodiment is given below and being described with reference to the accompanying drawings.With Under illustrative in nature on be merely exemplary and be not intended to limitation the disclosure application or purposes.It should be appreciated that In whole attached drawings, corresponding reference numeral represents identical or corresponding component and feature.
Referring to Fig. 1, a kind of non-sintered filled type vacuum stone preparation process provided by the invention comprises the following steps,
Fills unit body 1 is prepared, fine grain solid particle filler material 11 with liquid filler is mixed, makes the solid The surface of grain filler material 11 forms flexible liquid filling film 12;Fine grain solid particle filler material 11 in the present invention is most granule Footpath fills unit, the flexible liquid filling film 12 have shape deformability characteristics, in the filling process can be according to the big of gap Small changes shape, it is so as to be applicable in gap of different sizes, gap filling is closely knit.
The granulated aggregate 2 of different-grain diameter with the fills unit body 1 is mixed, mixture is made by batch mixing;
Shaping, the granulated aggregate 2 movement filling, and by institute mutually under vacuum power and the force action of weight slap power It states fills unit body 1 to be filled into the gap of each granulated aggregate 2, forms vacuum tightness body.Vacuum power and again in the present invention Hammer slap power is that the weight slap type compound stone shaping machine possessed by inventor is realized, referring to Chinese Patent Application No. For 201510026692.1 application for a patent for invention.The granulated aggregate of different-grain diameter can mutually be filled using the equipment, greatly The fitting close to each other of particles aggregate, small size particle aggregate fill the gap between large-size particles aggregate, each grain size Gap between grain aggregate is filled by fills unit body, and the fills unit body is during filling, the flexible hydraulic on surface Body filling film deforms according to the size shape in gap, so as to will have the gap as far as possible fill it is closely knit, discharge gap in Air.The present invention prepares vacuum stone using the principle of Magdeburg hemispheres, and the vacuum stone is closer to natural stone in nature Material, the overall performance of vacuum stone is also close to lithotome.
Compound stone of the prior art is to be bonded together the granulated aggregate of each grain size using binding agent, is not only synthesized The intensity of stone is not high, and not environmentally friendly enough.The vacuum stone of the present invention is that each particles aggregate is pressed in one using atmospheric pressure It rises, intensity higher is also more environmentally friendly.Filling concept proposed by the present invention refers to that each particles aggregate mutually moves fitting, and by The granulated aggregate of secondary level-one grain size fills the granulated aggregate gap of big level-one grain size, is finally had the gap by the completion of fills unit body Filling.The fill process of the present invention is different from pressing process of the prior art.The present invention is in order to realize filling purpose, each grain Footpath granulated aggregate is not mixed with liquid filler, and each particles aggregate can be preferably bonded to each other, and also reduced liquid and filled out Fill the usage amount of agent.The liquid filler is only mixed with fine grain solid particle filler material, and the filling list of minimum grain size is made First body, the fills unit body for preparing completion are used further to the mixing of granulated aggregate, and the fills unit body is made to wrap up each grain size Granulated aggregate, the granulated aggregate of package fills unit body preferably can be filled mutually in forming process, between them Gap is then filled by fills unit body, ultimately forms vacuum tightness body.If each particles aggregate surface wraps up binding agent, In pressing process, fine grain granulated aggregate is difficult to be filled into the gap of granulated aggregate.Binding agent is used excessively, in pressing process In, extra binding agent be difficult from compound stone discharge, it is finally formed be exactly bonded by binding agent formed synthesize stone structure, glue The adhesion strength of knot agent determines the intensity of compound stone.Meanwhile the present invention is sintered without to vacuum stone, is a kind of unburned Preparation process is tied, it is more environmentally-friendly.Therefore, preparation process proposed by the present invention is a kind of brand-new technique.
Further comprise in above-described embodiment that the present invention provides, the solid particle filler material is filled with the liquid The dosage of agent is determined by the following conditions:
QLiquid=(ρSolidParticle is compacted)/ρSolid×1cm3×ρLiquid
QSolidParticle is compacted×1cm3
In formula:QLiquidTo be pressed with 1 ton of pressure to the fills unit body of a square centimeters area, one is finally obtained Liquid filler benchmark dosage unit g in the fills unit body of cubic centimetre, which is as liquid filler institute accounting The referential data of example, i.e. optimised quantity.For reality in preparation process, which provides reference value for sorting, passes through above-mentioned formula The numerical value of the parameter is determined, according to the volume conversion phase application amount for preparing fills unit body.The dosage can be in reference value On the basis of be adjusted, so as to simplify the proportioning work of each material, reduce material loss.
QSolidIt is final to obtain one cube li to be pressed with 1 ton of pressure to the fills unit body of a square centimeters area The solid particle filler material benchmark dosage unit g parameters in the fills unit body of rice are as solid particle filler material institute accounting The referential data of example, i.e. optimised quantity.For reality in preparation process, which provides reference value for sorting, passes through above-mentioned formula The numerical value of the parameter is determined, according to the volume conversion phase application amount for preparing fills unit body.The dosage can be in reference value On the basis of be adjusted, so as to simplify the proportioning work of each material, reduce material loss.
ρSolidFor the actual density unit g/cm of solid particle filler material3, which is determined by the material of used solid particle It is fixed, according to the solid particle of a variety of unlike materials, then calculated by variant material solid particle proportion, finally It draws.For example the actual density of quartz is 2.65g/cm3
ρParticle is compactedTo be pressed with 1 ton of pressure to a square centimeters area solid granule filling material, final acquisition one is vertical The mass unit g/cm of square centimetre of solid particle filler material3, the parameter can by test obtain, take consolidating for unlike material Body granule filling material is suppressed respectively, then weighs to obtain.
ρLiquidFor the actual density unit g/cm of liquid filler3, which is determined by used liquid filler, For example the density of unsaturated-resin is in 1.4-2.2g/cm3
In the above-described embodiment provided in the present invention, if adopted using quartz as fine grain solid particle filler material By the use of unsaturated-resin as liquid filler.First, to fine grain quartz according to a square centimeters with 1 ton of pressure criteria into Row compacting, after the completion of compacting, takes one cubic centimetre to weigh, and the final parameter that obtains is ρParticle is compacted=1.91g/cm3.Therefore, QSolidParticle is compacted×1cm3=1.91g.QLiquid=(ρSolidParticle is compacted)/ρSolid×1cm3×ρLiquid=(2.65-1.91)/2.65 × 1 × 2=0.56g.I.e. reference value is that the fills unit body of one cubic centimetre of compacting needs quartz 1.91g, unsaturated-resin 0.56g is matched according to the proportionate relationship.
Referring to Fig. 1, further comprise in above-described embodiment that the present invention provides, the granulated aggregate and the filling are single The dosage of first body is determined by the following conditions:
QCell cube=(ρAggregateAggregate is compacted)/ρAggregate×1cm3×ρCell cube
QAggregateAggregate is compacted×1cm3
In formula:QCell cubeFor the fills unit body benchmark dosage unit g in one cubic centimetre of vacuum stone, which is conduct The referential data of fills unit body proportion, i.e. optimised quantity.For reality in preparation process, which provides reference for sorting Value determines the numerical value of the parameter by above-mentioned formula, according to the volume conversion phase application amount for preparing vacuum stone.The dosage can be with It is adjusted on the basis of reference value, so as to simplify the proportioning work of each material, reduces material loss.
QAggregateFor the granulated aggregate benchmark dosage unit g in one cubic centimetre of vacuum stone, which is as granulated aggregate The referential data of proportion, i.e. optimised quantity.Reality is in preparation process, which provides reference value for sorting, by upper The numerical value that formula determines the parameter is stated, according to the volume conversion phase application amount for preparing vacuum stone.The dosage can be in reference value On the basis of be adjusted, so as to simplify the proportioning work of each material, reduce material loss.
ρAggregateFor the actual density unit g/cm of granulated aggregate3, which is determined by the material of used granulated aggregate, if Using a variety of unlike materials granulated aggregate when, then calculated by variant material granulated aggregate proportion, it is final Go out.For example the actual density of quartz is 2.65g/cm3
ρAggregate is compactedIt is final to obtain one cube li to be pressed with 1 ton of pressure to the granulated aggregate of a square centimeters area The mass unit g/cm of the granulated aggregate of rice3, the parameter can by test obtain, the granulated aggregate of unlike material be taken to distinguish Compacting, then weighs to obtain.
ρCell cubeFor the actual density unit g/cm of fills unit body3The parameter is that the following formula determines:
ρCell cube=(QLiquid+QSolid)/1cm3
.Wherein QLiquidAnd QSolidIt is consistent with the above.
In the above-described embodiment provided in the present invention, if using quartz as granulated aggregate.First, by different-grain diameter Granulated aggregate mixing suppressed according to one square centimeter with 1 ton of pressure criteria, after the completion of compacting, take one cubic centimetre Granulated aggregate is weighed, and finally obtains parameter ρAggregate is compacted=2.0g/cm3。QAggregateAggregate is compacted×1cm3=2.0g.ρCell cube= (0.56g+1.91)/1=2.47g/cm3,QCell cube=(ρAggregateAggregate is compacted)/ρAggregate×1cm3×ρCell cube=(2.65-2.0)/2.65 × 1 × 2.47=0.60g.I.e. reference value is that the vacuum stone of one cubic centimetre of compacting needs fills unit body 0.60g, quartz Grain aggregate 2.0g, is matched according to the proportionate relationship.
Further comprise in above-described embodiment that the present invention provides, the solid particle filler material is filled with the liquid Agent is by being stirred, weight ratio 2-6:1.Reference value, Ke Yi are obtained by above-mentioned fills unit body each component formula It is adjusted in the proportionate relationship, it can be with as long as meeting the proportionate relationship.The ginseng that the proportionate relationship can also calculate formula It examines value to be verified, it is determined whether meet the requirements.The ratio that the present embodiment is determined by above-mentioned formula is 3.4:1.
Further comprise in above-described embodiment that the present invention provides, cloth has been further included before forming step, by institute It states mixture and is arranged to platy structure.Cloth can be carried out cloth by material distributing machine, and when cloth will cause fills unit body and particle Aggregate is evenly distributed, beneficial to the filling campaign of forming step.
Further comprise in above-described embodiment that the present invention provides, curing has been further included after the conformation step, by institute It states liquid filler and solid-state is become from liquid.Liquid filler of the present invention refers to have is converted into solid-state properties by liquid Liquid, this liquid also needs to keep solid-state for a long time in normality, so as to eliminate the air in gap, is not easy air Into in gap, such as resin etc..
Further comprise in above-described embodiment that the present invention provides, the grain size of the solid particle filler material is 0.1mm- 0.01mm, the present embodiment use 0.05mm, and the grain size of the granulated aggregate is more than 0.1mm.Granulated aggregate in the present invention Grain size is the granulated aggregate for selecting different-grain diameter as required, and more than 0.1mm is not without limitation, the granulated aggregate grain The selection in footpath is suitable for the various unlike material aggregate sizes in this field, and those skilled in the art can be according to the specific knot of vacuum stone Structure makes choice.
Further comprise referring to Fig. 1 in above-described embodiment for providing of the present invention, the liquid filler can have by Liquid becomes solid characteristic, including organic resinoid and inorganic resinoid.Organic resinoid includes acryl resin, no Saturated resin, propylene resin or epoxy resin, inorganic resinoid include soybean-based resin or rubber resin.These liquid are filled out Filling agent has from liquid to solid state transformed characteristic, and disclosure satisfy that the needs of vacuum stone.Liquid filler of the present invention Referring to that there is the liquid that solid-state properties are converted by liquid, this liquid also needs to keep solid-state for a long time in normality, from And eliminate the air in gap, air is made to be not easily accessible in gap, than various resins described above etc., these resins itself or Solid-state is converted by liquid under the action of catalyst.
In conclusion above said content is only the embodiment of the present invention, the principle of the present invention is merely to illustrate, is not used In restriction protection scope of the present invention.Within the spirit and principles of the invention, any modification for being made, equivalent substitution change Into etc., it should all be included in the protection scope of the present invention.

Claims (10)

1. a kind of non-sintered filled type vacuum stone preparation process, it is characterised in that:Comprise the following steps,
Fills unit body is prepared, fine grain solid particle filler material is mixed with liquid filler, fills the solid particle The surface of material forms flexible liquid filling film;
The granulated aggregate of different-grain diameter with the fills unit body is mixed, mixture is made by batch mixing;
Shaping, granulated aggregate movement filling, and being filled out described mutually under vacuum power and the force action of weight slap power It fills cell cube to be filled into the gap of each granulated aggregate, forms vacuum tightness body.
2. a kind of non-sintered filled type vacuum stone preparation process as described in claim 1, it is characterised in that:The solid The dosage of grain filler material and the liquid filler is determined by the following conditions:
QLiquid=(ρSolidParticle is compacted)/ρSolid×1cm3×ρLiquid
QSolidParticle is compacted×1cm3
In formula:QLiquidIt is final to obtain one cube to be pressed with 1 ton of pressure to the fills unit body of a square centimeters area Centimetre fills unit body in liquid filler benchmark dosage unit g
QSolidTo be pressed with 1 ton of pressure to the fills unit body of a square centimeters area, final one cubic centimetre of acquisition Solid particle filler material benchmark dosage unit g in fills unit body
ρSolidFor the actual density unit g/cm of solid particle filler material3
ρParticle is compactedIt is final to obtain one cube li to be pressed with 1 ton of pressure to a square centimeters area solid granule filling material The mass unit g/cm of the solid particle filler material of rice3
ρLiquidFor the actual density unit g/cm of liquid filler3
3. a kind of non-sintered filled type vacuum stone preparation process as claimed in claim 2, it is characterised in that:The particulate cancellous bone Expect to be determined by the following conditions with the dosage of the fills unit body:
QCell cube=(ρAggregateAggregate is compacted)/ρAggregate×1cm3×ρCell cube
QAggregateAggregate is compacted×1cm3
In formula:QCell cubeFor the fills unit body benchmark dosage unit g in one cubic centimetre of vacuum stone
QAggregateFor the granulated aggregate benchmark dosage unit g in one cubic centimetre of vacuum stone
ρAggregateFor the actual density unit g/cm of granulated aggregate3
ρAggregate is compactedTo be pressed with 1 ton of pressure to the granulated aggregate of a square centimeters area, final one cubic centimetre of acquisition The mass unit g/cm of granulated aggregate3
ρCell cubeFor the actual density unit g/cm of fills unit body3
ρCell cube=(QLiquid+QSolid)/1cm3
4. a kind of non-sintered filled type vacuum stone preparation process as described in claim 1, it is characterised in that:The solid Grain filler material with the liquid filler by being stirred, weight ratio 2-6:1.
5. a kind of non-sintered filled type vacuum stone preparation process as described in claim 1, it is characterised in that:In forming step Cloth has been further included before, and the mixture is arranged to platy structure.
6. a kind of non-sintered filled type vacuum stone preparation process as described in claim 1, it is characterised in that:In forming step Curing has been further included afterwards, and the liquid filler is become into solid-state from liquid.
7. a kind of non-sintered filled type vacuum stone preparation process as described in claim 1, it is characterised in that:The solid The grain size of grain filler material is 0.1mm-0.01mm, and the grain size of the granulated aggregate is more than 0.1mm.
8. a kind of non-sintered filled type vacuum stone preparation process as described in claim 1, it is characterised in that:The liquid is filled out Fill agent can be with solid characteristic be become, including organic resinoid and inorganic resinoid from liquid.
9. a kind of non-sintered filled type vacuum stone preparation process as claimed in claim 8, it is characterised in that:The organic Resin includes acryl resin, unsaturated-resin, propylene resin or epoxy resin.
10. a kind of non-sintered filled type vacuum stone preparation process as claimed in claim 8, it is characterised in that:It is described inorganic Resinoid includes soybean-based resin or rubber resin.
CN201611075153.8A 2016-11-29 2016-11-29 A kind of non-sintered filled type vacuum stone preparation process Pending CN108117301A (en)

Priority Applications (2)

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CN201611075153.8A CN108117301A (en) 2016-11-29 2016-11-29 A kind of non-sintered filled type vacuum stone preparation process
PCT/CN2017/107213 WO2018099204A1 (en) 2016-11-29 2017-10-23 Non-sintered filled vacuum stone and preparation process

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Application Number Priority Date Filing Date Title
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109049281A (en) * 2018-09-27 2018-12-21 安徽省安美利特环保材料科技有限公司 A kind of vacuum stone and preparation process with multicolor patterns
CN109176826A (en) * 2018-09-27 2019-01-11 安徽省安美利特环保材料科技有限公司 A kind of vacuum stone and preparation process with convex-concave surface
CN109466080A (en) * 2018-09-27 2019-03-15 安徽省安美利特环保材料科技有限公司 A kind of vacuum stone and preparation process with decorative pattern
CN109972803A (en) * 2017-12-27 2019-07-05 安徽省安美利特环保材料科技有限公司 A kind of vacuum stone of embedded installation part
CN109972810A (en) * 2017-12-27 2019-07-05 安徽省安美利特环保材料科技有限公司 A kind of vacuum stone installation system and mounting process
CN113651561A (en) * 2021-07-16 2021-11-16 清远金谷智联环保产业研究院有限公司 Method for preparing sintering-free artificial synthetic plate by adopting nickel smelting furnace slag

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CN105856382A (en) * 2015-01-20 2016-08-17 上海安美利特环保材料科技有限公司 Counterweight slapping type synthetic stone forming machine and processing technology
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CN104230214A (en) * 2014-09-17 2014-12-24 常州明清新材料技术有限公司 Method for manufacturing artificial colorized quartz composite stone with colorized quartz sand
CN104261727A (en) * 2014-09-17 2015-01-07 常州明清新材料技术有限公司 Method for preparing high-gloss high-permeability artificial colored quartz plate
CN105856382A (en) * 2015-01-20 2016-08-17 上海安美利特环保材料科技有限公司 Counterweight slapping type synthetic stone forming machine and processing technology
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Publication number Priority date Publication date Assignee Title
CN109972803A (en) * 2017-12-27 2019-07-05 安徽省安美利特环保材料科技有限公司 A kind of vacuum stone of embedded installation part
CN109972810A (en) * 2017-12-27 2019-07-05 安徽省安美利特环保材料科技有限公司 A kind of vacuum stone installation system and mounting process
CN109049281A (en) * 2018-09-27 2018-12-21 安徽省安美利特环保材料科技有限公司 A kind of vacuum stone and preparation process with multicolor patterns
CN109176826A (en) * 2018-09-27 2019-01-11 安徽省安美利特环保材料科技有限公司 A kind of vacuum stone and preparation process with convex-concave surface
CN109466080A (en) * 2018-09-27 2019-03-15 安徽省安美利特环保材料科技有限公司 A kind of vacuum stone and preparation process with decorative pattern
CN113651561A (en) * 2021-07-16 2021-11-16 清远金谷智联环保产业研究院有限公司 Method for preparing sintering-free artificial synthetic plate by adopting nickel smelting furnace slag

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Application publication date: 20180605