CN107956155A - A kind of new dye for being used to spin and preparation method thereof - Google Patents
A kind of new dye for being used to spin and preparation method thereof Download PDFInfo
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- CN107956155A CN107956155A CN201711348431.7A CN201711348431A CN107956155A CN 107956155 A CN107956155 A CN 107956155A CN 201711348431 A CN201711348431 A CN 201711348431A CN 107956155 A CN107956155 A CN 107956155A
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- new dye
- defoamer
- spin
- dispersant
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- D06P1/525—Polymers of unsaturated carboxylic acids or functional derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- D06P1/525—Polymers of unsaturated carboxylic acids or functional derivatives thereof
- D06P1/5257—(Meth)acrylic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5264—Macromolecular compounds obtained otherwise than by reactions involving only unsaturated carbon-to-carbon bonds
- D06P1/5271—Polyesters; Polycarbonates; Alkyd resins
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5264—Macromolecular compounds obtained otherwise than by reactions involving only unsaturated carbon-to-carbon bonds
- D06P1/5292—Macromolecular compounds obtained otherwise than by reactions involving only unsaturated carbon-to-carbon bonds containing Si-atoms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65125—Compounds containing ester groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of new dye for being used to spin, it is related to spinning field, including each component that weight proportion is following：70 90 parts of acrylic emulsion；1 part of nano silver or nanometer titanium dioxide；5 10 parts of dispersant；12 parts of defoamer；12 parts of emulsifying agent；10 20 parts of mill base.The program can effectively suppress the bacteriums such as Escherichia coli, staphylococcus aureus, Candida albicans because containing antiseptic in formula.Therefore there is certain antibiotic effect.The dyestuff of this programme is added in spinning process can make obtained yarn material more healthy, and can have broader practice prospect in medicine and sphere of life.
Description
Technical field
The present invention relates to textile manufacturing process field, more particularly to a kind of new dye for being used to spin and its preparation
Method.
Background technology
Textile dyestuff is a kind of stain for textile dyeing, is divided into natural dye and synthetic dyestuffs, it, which contains, makes fibre
Dimension dyes the distinct and organic compound of fast color, so as to carry out operation dyeing on yarn fabric.The general character with dyestuff：
1. there is color；
2. form dispersion with being dissolved in water or water；
3. fiber can be contaminated above；
4. there is certain fastness.
With the increasingly raising of people's living standard, the demands of different textile dyestuffs is also come it is bigger, with antibacterial functions
Textile dyestuff be increasingly subject to the concern of people.
Natural antibacterial agent such as chitin, horseradish etc., using simplicity, but antibacterial action is limited, it is impossible to broad-spectrum long-acting；It is organic anti-
Microbial inoculum such as quaternary ammonium salt, sulfurous cyanogen acid compounds, sorbic acid etc., their sterilization speed is fast, exploitation and using technology maturation,
But stability and long-term effect are poor；Inorganic metal, such as mercury, silver, copper, chromium, zinc have microorganism different degrees of killing effect, people
Pulverulent material of these metals on carrier is usually used, using these antibacterial metal ions, slowly discharged from carrier,
The harmful bacteria for being attached to its surface is killed long-term effectively.
The content of the invention
The shortcomings that present invention is directed to above-mentioned technical problem, overcomes the prior art, proposes a kind of new dye for being used to spin,
The dyestuff enriches textile dyestuff species, because containing antiseptic in formula, the dyestuff to Escherichia coli, staphylococcus aureus,
Candida albicans can effectively suppress for the bacterium of representative, and inhibiting rate is up to 90%.
In order to solve the above technical problems, the present invention provides a kind of new dye for being used to spin, including weight proportion is such as
Under each component：
60-90 parts of acrylic emulsion；
1-5 parts of nano silver or nano-titanium dioxide；
5-10 parts of dispersant；
1-3 parts of defoamer；
1-3 parts of emulsifying agent；
10-20 parts of mill base.
Technique effect：
The technical solution that further limits of the present invention is：
Further, a kind of new dye for being used to spin, it is characterised in that including the following each component of weight proportion：
70-9 parts of acrylic emulsion；
1-5 parts of nano silver and/or nano-titanium dioxide；
8-10 parts of dispersant；
1-2 parts of defoamer；
1-2 parts of emulsifying agent；
15-20 parts of mill base.
A kind of preceding new dye for being used to spin, dispersant is polyester resin and/or butyl acetate.
A kind of preceding new dye for being used to spin, the weight proportion of acrylic emulsion is 70 parts.
A kind of preceding new dye for being used to spin, defoamer is organic silicon defoamer.
A kind of preceding new dye for being used to spin, defoamer is dimethyl silicone polymer.
The particle diameter of a kind of preceding new dye for being used to spin, nano silver and/or nano-titanium dioxide is 50-
90nm。
A kind of preparation method for the new dye that spins, it is characterised in that comprise the following steps：Mixing, acrylic emulsion 70
Part, nano silver and/or 3 parts of nano-titanium dioxide, 8-10 parts of dispersant, 1 part of defoamer, by above-mentioned material according to setting
Fixed quality is ready to add in the container specified plus water mixing, is aided with mixed process and stirs and obtain mixed solution；
Ultrasonic disperse, the mixed solution is carried out ultrasonic disperse processing using ultrasonic wave, the speed of ultrasonic disperse for 300 turns/
Minute, the time is not less than 30 minutes, and temperature is no more than 50 DEG C；
Colour, addition mass fraction is 15 parts of mill base and is stirred in the solution after supersound process, by mixed solution
Infusion is heated, heating-up temperature is 150 DEG C, and heating time is 7 minutes；
Preliminary sedimentation, sediment is filtered out in 10 minutes by the solution left standstill after coloring；
Deeply precipitation, the emulsifying agent that mass fraction is 1 point is added into the solution after preliminary sedimentation, is then stood again, and mistake
Filter sediment；
Steam, mixture obtained in the previous step is evaporated, obtains dyestuff.
A kind of preparation method of preceding spinning new dye, needs with shank when steaming periodically into the mixture
Into and out, and hole is formed on the mixture, hole is evenly distributed on the surface of mixture.
The beneficial effects of the invention are as follows：
（1）The new dye production cost that the present invention is used to spin in the present invention is low, to Escherichia coli, staphylococcus aureus,
Candida albicans can effectively suppress for the bacterium of representative, and inhibiting rate is up to 90%；
（2）New dye color power that the present invention is used to spin, thickness, heat-resisting cold resistance are attained by a certain degree, to adult and
Child does not stimulate.It is widely used, the growth and breeding of various bacteriums are can effectively prevent, can be applied to special trade work clothes
In printing and dyeing, such as environmental sanitation is for people's clothes dye system.
Embodiment
Embodiment 1
Present embodiment discloses a kind of new dye for being used to spin that can apply to field of textiles, including weight proportion is following
Each component：
70 parts of acrylic emulsion；
5 parts of nano silver and nano-titanium dioxide；
10 parts of dispersant；
2 parts of defoamer；
1 part of emulsifying agent；
20 parts of mill base.
Wherein dispersant is polyester resin, and defoamer is organic silicon defoamer, and fluorescer selects nontoxic fluorescer.
Embodiment 2
Present embodiment discloses a kind of new dye for being used to spin that can apply to field of textiles, including weight proportion is following
Each component：
80 parts of acrylic emulsion；
4 parts of nano silver；
5-10 parts of dispersant；
2 parts of defoamer；
1 part of emulsifying agent；
18 parts of mill base.
Wherein, dispersant is polyester resin and the mixture of person's butyl acetate, and preservative is sodium propionate, and defoamer is poly- two
Methylsiloxane, has the advantages that antifoaming speed is fast, suds effect is good at normal temperatures, and fluorescer selects nontoxic fluorescer.
Embodiment 3
Present embodiment discloses a kind of new dye for being used to spin that can apply to field of textiles, including weight proportion is following
Each component：
90 parts of acrylic emulsion；
5 parts of nano-titanium dioxide；
5 parts of dispersant；
2 parts of defoamer；
2 parts of emulsifying agent；
20 parts of mill base.
Wherein, dispersant is butyl acetate, and defoamer is organic silicon defoamer, and fluorescer selects nontoxic fluorescence
Agent.
This law invention is not limited to the new dye for being used to spin described in above-described embodiment, and wherein each component weight is matched somebody with somebody
The change of ratio, the change of dispersant, the change of mill base species is within protection scope of the present invention.
Embodiment 4
Present embodiment discloses a kind of new dye for being used to spin that can apply to field of textiles, including weight proportion is following
Each component：
60 parts of acrylic emulsion；
5 parts of nano silver and nano-titanium dioxide；
10 parts of dispersant；
2 parts of defoamer；
1 part of emulsifying agent；
20 parts of mill base.
Wherein dispersant is polyester resin, and defoamer is organic silicon defoamer, and fluorescer selects nontoxic fluorescer.
A kind of preparation method for preparing the new dye that spins in above-mentioned any embodiment：
Mixing, 3 parts of 70 parts of acrylic emulsion, nano silver or nano-titanium dioxide, 8-10 parts of dispersant, 1 part of defoamer,
Above-mentioned material is ready to add in the container specified according to the quality of setting plus water mixes, is aided with mixed process and is stirred and obtain
To mixed solution；
Ultrasonic disperse, the mixed solution is carried out ultrasonic disperse processing using ultrasonic wave, the speed of ultrasonic disperse for 300 turns/
Minute, the time is not less than 30 minutes, and temperature is no more than 50 DEG C；
Colour, addition mass fraction is 15 parts of mill base and is stirred in the solution after supersound process, by mixed solution
Infusion is heated, heating-up temperature is 150 DEG C, and heating time is 7 minutes；
Preliminary sedimentation, sediment is filtered out in 10 minutes by the solution left standstill after coloring；
Deeply precipitation, the emulsifying agent that mass fraction is 1 point is added into the solution after preliminary sedimentation, is then stood again, and mistake
Filter sediment；
Steam, mixed liquor obtained in the previous step is evaporated, obtains dyestuff.Needed when steaming with shank periodically into the mixture
Into and out, and hole is formed on the mixture, hole is evenly distributed on the surface of mixture.
In addition to the implementation, the present invention can also have other embodiment.It is all to use equivalent substitution or equivalent transformation shape
Into technical solution, all fall within the protection domains of application claims.
Claims (9)
1. a kind of new dye for being used to spin, it is characterised in that including the following each component of weight proportion：
60-90 parts of acrylic emulsion；
1-5 parts of nano silver or nano-titanium dioxide；
5-10 parts of dispersant；
1-3 parts of defoamer；
1-3 parts of emulsifying agent；
10-20 parts of mill base.
A kind of 2. new dye for being used to spin according to claim 1, it is characterised in that following including weight proportion
Each component：
70-9 parts of acrylic emulsion；
1-5 parts of nano silver and/or nano-titanium dioxide；
8-10 parts of dispersant；
1-2 parts of defoamer；
1-2 parts of emulsifying agent；
15-20 parts of mill base.
3. a kind of new dye for being used to spin according to claim 2, it is characterised in that the dispersant is polyester tree
Fat and/or butyl acetate.
A kind of 4. new dye for being used to spin according to claim 3, it is characterised in that the weight of the acrylic emulsion
Amount proportioning is 70 parts.
5. a kind of new dye for being used to spin according to claim 1, it is characterised in that the defoamer is organosilicon
Class defoamer.
6. a kind of new dye for being used to spin according to claim 1, it is characterised in that the defoamer is poly- diformazan
Radical siloxane.
7. a kind of new dye for being used to spin according to claim 1, it is characterised in that the nano silver and/or receive
The particle diameter of rice titanium dioxide is 50-90nm.
8. a kind of preparation method for being used to prepare a kind of spinning new dye described in claim 1~7 any one, its feature
It is, comprises the following steps：Mixing, 70 parts of acrylic emulsion, nano silver and/or 3 parts of nano-titanium dioxide, dispersant 8-
10 parts, 1 part of defoamer, above-mentioned material is ready to add in the container specified according to the quality of setting plus water mixes, mixing
During be aided with and stir and obtain mixed solution；
Ultrasonic disperse, the mixed solution is carried out ultrasonic disperse processing using ultrasonic wave, the speed of ultrasonic disperse for 300 turns/
Minute, the time is not less than 30 minutes, and temperature is no more than 50 DEG C；
Colour, addition mass fraction is 15 parts of mill base and is stirred in the solution after supersound process, by mixed solution
Infusion is heated, heating-up temperature is 150 DEG C, and heating time is 7 minutes；
Preliminary sedimentation, sediment is filtered out in 10 minutes by the solution left standstill after coloring；
Deeply precipitation, the emulsifying agent that mass fraction is 1 point is added into the solution after preliminary sedimentation, is then stood again, and mistake
Filter sediment；
Steam, mixture obtained in the previous step is evaporated, obtains dyestuff.
A kind of 9. preparation method of new dye that spins according to claim 8, it is characterised in that：Need to use pin when steaming
Bar periodically into the mixture into and out and forming hole, hole is evenly distributed on the table of mixture on the mixture
On face.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711348431.7A CN107956155A (en) | 2017-12-15 | 2017-12-15 | A kind of new dye for being used to spin and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711348431.7A CN107956155A (en) | 2017-12-15 | 2017-12-15 | A kind of new dye for being used to spin and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107956155A true CN107956155A (en) | 2018-04-24 |
Family
ID=61959083
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711348431.7A Pending CN107956155A (en) | 2017-12-15 | 2017-12-15 | A kind of new dye for being used to spin and preparation method thereof |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105113293A (en) * | 2015-08-20 | 2015-12-02 | 浙江百德纺织有限公司 | Fluorescent textile dye |
| CN105113299A (en) * | 2015-08-20 | 2015-12-02 | 浙江百德纺织有限公司 | Antibacterial textile dye |
-
2017
- 2017-12-15 CN CN201711348431.7A patent/CN107956155A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105113293A (en) * | 2015-08-20 | 2015-12-02 | 浙江百德纺织有限公司 | Fluorescent textile dye |
| CN105113299A (en) * | 2015-08-20 | 2015-12-02 | 浙江百德纺织有限公司 | Antibacterial textile dye |
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Application publication date: 20180424 |