CN107898749B - A topical composition with skin caring effect and its preparation method - Google Patents
A topical composition with skin caring effect and its preparation method Download PDFInfo
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Classifications
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
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Abstract
The invention provides an external composition with skin care effect and a preparation method thereof, wherein the external composition is prepared from the following raw materials in parts by weight: 5-15 parts of safflower, 20-40 parts of ginseng, 5-15 parts of rhodiola rosea, 10-30 parts of hemsleya amabilis, 10-30 parts of liquorice, 20-40 parts of poria cocos, 10-30 parts of astragalus membranaceus, 10-30 parts of snow lotus herb, 30-50 parts of propolis and 350-500 parts of honey. The experimental result proves that the external composition has multiple effects of whitening, removing freckles, moisturizing, removing acnes, smoothing wrinkles, delaying aging and the like, solves the problem of single effect of the existing skin care product, and has wide market application prospect.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to an external composition with a skin care effect and a preparation method thereof.
Background
With the development of science and technology and the continuous improvement of the living standard of people, cosmetics take an increasingly important position in the life of people. In recent years, the variety of cosmetics is increasing, the functionality of the cosmetics is becoming stronger, and the technological content is becoming higher. Skin care products have also been developed to a great extent as one of representative products of cosmetics.
At present, skin care products on the market mainly comprise two types, one type is a chemical synthetic substance which is used as a main component, although the efficacy is obvious, harmful components such as heavy metal or fluorescent powder can be contained, and certain side effect can be generated on the skin after long-term use; the other is a traditional Chinese medicine skin care product, which has mild effect and small toxic and side effect.
However, the traditional Chinese medicine skin care product has single effect at present, and the skin problem can be solved only by using a plurality of skin care products with different effects at the same time. For example: CN107049838A discloses a facial mask consisting of orange essential oil, cinnamon essential oil, rose essential oil, red wine polyphenol, radix Arnebiae extract, radix Rhodiolae extract, Poria, semen Persicae, and rhizoma Typhonii for removing wrinkle; CN107375155A discloses a facial mask which only has the effects of moisturizing and preserving moisture and consists of coix seed powder, blueberry extract, chamomile extract, aloe juice, momordica grosvenori, trehalose, honeysuckle, liquorice, rose, cotinus coggygria leaves and lysimachia foenum-graecum; CN104922011A discloses a skin care lotion with skin whitening effect, which is composed of aloe, lilac, white pharbitis, chinaroot greenbrier rhizome, white ginkgo seed, bletilla striata, angelica dahurica, bighead atractylodes rhizome, bird's nest, coix seed, gentian, angelica and ginkgo.
Therefore, there is an urgent need for a skin care product with multiple effects.
Disclosure of Invention
The technical scheme of the invention is to provide an external composition with a skin care effect. The invention also provides a preparation method and application of the external composition.
The invention provides an external composition with skin care effect, which is prepared from the following raw materials in parts by weight:
5-15 parts of safflower, 20-40 parts of ginseng, 5-15 parts of rhodiola rosea, 10-30 parts of hemsleya amabilis, 10-30 parts of liquorice, 20-40 parts of poria cocos, 10-30 parts of astragalus membranaceus, 10-30 parts of snow lotus herb, 30-50 parts of propolis and 350-500 parts of honey.
Further preferably, the composition is prepared from the following raw materials in parts by weight:
10 parts of safflower, 30 parts of ginseng, 10 parts of rhodiola rosea, 20 parts of hemsleya amabilis, 20 parts of liquorice, 30 parts of tuckahoe, 20 parts of astragalus, 20 parts of snow lotus herb, 40 parts of propolis and 400 parts of honey.
The composition is a preparation prepared by taking the original powder of safflower, ginseng, rhodiola rosea, hemsleya amabilis, liquorice, tuckahoe, astragalus and snow lotus herb, water or organic solvent extract as active ingredients and adding propolis, honey and auxiliary materials or auxiliary ingredients acceptable in medicines and cosmetics.
Wherein the preparation is emulsion, film agent or gel. Specific products may include a facial cleanser, mask, lotion, cream or eye cream.
The invention also provides a preparation method of the external composition, which comprises the following steps:
(1) weighing propolis and honey according to the weight ratio, uniformly stirring, and hermetically fermenting for 1-3 days at the temperature of 25-40 ℃ and the humidity of 75% to obtain propolis honey;
(2) breaking cell wall of other materials, and pulverizing into superfine powder;
(3) weighing the superfine powder and the propolis honey according to the weight ratio, uniformly stirring, hermetically fermenting for 5-15 days at the temperature of 25-30 ℃ and the humidity of 75%, and adding auxiliary materials or auxiliary components acceptable in medicines and cosmetics to prepare the preparation.
Wherein, in the step (1), the fermentation temperature is 30 ℃, and the fermentation time is 2 days.
Wherein, in the step (2), the temperature for breaking the wall is 10 +/-2 ℃.
Wherein, in the step (3), the fermentation temperature is 25 ℃, and the fermentation time is 10 days.
Wherein, in the step (3), the fermentation process also comprises stirring for 10 minutes every day, and the stirring speed is 20 revolutions per minute; preferably, the stirring is clockwise for 5 minutes and counterclockwise for 5 minutes.
The invention also provides application of the external composition in preparing medicines or cosmetics for whitening, removing freckles, moisturizing, removing acnes, smoothing wrinkles or delaying senescence.
In the invention, the safflower has the functions of promoting blood circulation and dredging channels, and eliminating stasis and relieving pain; ginseng, which greatly supplements primordial qi, recovers the pulse, relieves exhaustion, tonifies spleen, benefits lung, promotes production of body fluid, nourishes blood, soothes nerves and benefits intelligence; rhodiola rosea has the effects of tonifying qi, activating blood, promoting blood circulation and relieving asthma; hemsleya amabilis has the effects of clearing away heat and toxic materials, and relieving swelling and pain; the liquorice has the effects of tonifying spleen and qi, clearing away heat and toxic materials, eliminating phlegm and stopping cough, relieving spasm and pain and harmonizing the medicines; tuckahoe, Poria promotes diuresis and eliminates dampness, invigorates the spleen and calms the heart; astragalus root, radix astragali, invigorating qi and raising yang, consolidating superficial resistance and arresting sweating, inducing diuresis and reducing edema, promoting the production of body fluid and nourishing blood, activating stagnancy and removing obstruction of qi, expelling toxin and pus, healing sore and promoting granulation; snow lotus herb, herba saussureae involucratae, for clearing away heat and toxic materials, and relieving swelling and pain; propolis has effects in tonifying asthenia, eliminating turbid pathogen, quenching thirst, removing toxic materials, relieving swelling, astringing, and promoting granulation; honey has the effects of tonifying middle-jiao, moistening dryness, relieving pain, removing toxicity, promoting granulation and healing wound.
The external composition of the invention skillfully uses the functions of various traditional Chinese medicines to exert respective effects, and simultaneously skillfully uses pure natural honey and propolis, and is a pure natural skin care product without adding any additive. The skin care product disclosed by the invention can exert respective effects to the maximum extent by fermentation of various traditional Chinese medicines, and is more exquisite and more moist in use in the fermentation process.
The experimental result proves that the external composition has multiple effects of whitening, removing freckles, moisturizing, removing acnes, smoothing wrinkles, delaying aging and the like, solves the problem of single effect of the existing skin care product, and has wide market application prospect.
Obviously, many modifications, substitutions, and variations are possible in light of the above teachings of the invention, without departing from the basic technical spirit of the invention, as defined by the following claims.
The present invention will be described in further detail with reference to the following examples. This should not be understood as limiting the scope of the above-described subject matter of the present invention to the following examples. All the technologies realized based on the above contents of the present invention belong to the scope of the present invention.
Drawings
FIG. 1 shows propolis honey after fermentation.
Fig. 2 is the mixed wall-broken traditional Chinese medicine powder of the invention.
FIG. 3 is a paste mixture of the present invention before fermentation.
Fig. 4 is a mask fermented for 2 days.
Fig. 5 is a mask after 10 days of fermentation.
Detailed Description
Example 1 preparation of mask of the invention
The formula is as follows: 10g of safflower, 30g of ginseng, 10g of rhodiola rosea, 20g of hemsleya amabilis, 20g of liquorice, 30g of poria cocos, 20g of astragalus membranaceus, 20g of snow lotus herb, 40g of propolis and 400g of honey.
The preparation method comprises the following steps:
weighing honey and propolis according to the formula, uniformly stirring, sealing in an environment with the temperature of 30 ℃ and the humidity of 75%, and fermenting for 2 days to prepare the propolis honey as shown in figure 1.
Secondly, breaking the walls of all the raw materials except the propolis honey in the formula at 10 ℃ respectively, crushing the raw materials into superfine powder, sieving the superfine powder with a 200-mesh sieve, weighing all the raw material powder except the propolis honey according to the formula amount, and uniformly mixing the raw material powder and the propolis honey, wherein the formula is shown in figure 2.
Thirdly, adding the fermented propolis honey into the mixed raw material powder, fully and uniformly stirring the mixture to prepare a paste, and the picture is shown in figure 3.
Fourthly, the paste obtained in the third step is sealed in an environment with the temperature of 25 ℃ and the humidity of 75 percent, the paste is stirred once a day after being uncovered, the mixture is stirred for 5 minutes in a counterclockwise way at the speed of 20 revolutions per minute, then the mixture is stirred for 5 minutes in a clockwise way, and the mixture is fermented for 10 days, as shown in the figure 4 and the figure 5.
The using method comprises the following steps: after the face is fully cleaned, the face is directly applied to the face and cleaned after 20-30 minutes, 2-3 times per week.
Example 2 preparation of an emulsion according to the invention
The formula is as follows: 5g of safflower, 20g of ginseng, 15g of rhodiola rosea, 10g of hemsleya amabilis, 30g of liquorice, 20g of poria cocos, 30g of astragalus membranaceus, 10g of snow lotus herb, 50g of propolis and 350g of honey.
The preparation method comprises the following steps:
weighing honey and propolis according to the formula, uniformly stirring, sealing in an environment with the temperature of 30 ℃ and the humidity of 75%, and fermenting for 2 days to prepare the propolis honey.
Secondly, weighing all the raw materials except the propolis honey according to the formula, adding 10 times of water, decocting for 30min, filtering, adding 8 times of water into filter residues, decocting for 20min, filtering, combining the two filtrates, and concentrating.
And thirdly, adding the propolis honey into the concentrated solution, and uniformly mixing.
Example 3 preparation of a facial cleanser of the invention
The formula is as follows: 15g of safflower, 40g of ginseng, 5g of rhodiola rosea, 30g of hemsleya amabilis, 10g of liquorice, 40g of poria cocos, 10g of astragalus membranaceus, 30g of snow lotus herb, 30g of propolis and 500g of honey.
The preparation method comprises the following steps:
weighing honey and propolis according to the formula, uniformly stirring, sealing in an environment with the temperature of 30 ℃ and the humidity of 75%, and fermenting for 2 days to prepare the propolis honey.
Secondly, breaking the walls of all the raw materials except the propolis honey in the formula at 10 ℃ respectively, crushing the raw materials into superfine powder, sieving the superfine powder with a 200-mesh sieve, weighing all the raw materials except the propolis honey according to the formula amount, and uniformly mixing.
Mixing the raw material powder, the propolis honey and 2g of sodium lauryl polyether sulfate uniformly.
Example 4 screening of fermentation conditions for mask of the present invention
1. Screening of fermentation temperature
By adopting the formula and the preparation method of the example 1, the influence of the fermentation temperature in the step (iv) on the facial mask paste is examined, the temperature variation range is 20-30 ℃, and the experimental results are shown in table 1:
TABLE 1 screening of fermentation temperature of mask paste
2. Screening of fermentation humidity
By adopting the formula and the preparation method of the example 1, the influence of the fermentation humidity in the step (iv) on the facial mask paste is examined, the humidity change range is 60-90%, and the experimental results are shown in table 2:
TABLE 2 screening of mask paste fermentation humidity
3. Screening of fermentation time
By adopting the formula and the preparation method of the example 1, the influence of the fermentation time in the step (iv) on the facial mask paste is examined, the time variation range is 1-15 days, and the experimental results are shown in table 3:
TABLE 3 screening of mask paste fermentation time
The experimental result shows that the optimal fermentation temperature of the mask paste is 30 ℃, the fermentation humidity is 75%, and the fermentation time is 10 days.
The advantageous effects of the present invention are described below by way of test examples.
Test example 1
1. Test material
Example 1 the resulting mask was prepared; the herborist new seven-white whitening and skin tendering mask (new edition) contains seven Chinese herbal medicines such as radix paeoniae alba, radix ampelopsis, bletilla striata, tribulus terrestris and the like, and is a new seven-white upgrading essence.
2. Test object
45 volunteers, female, age 22-60 years, 15 people in one group.
3. Test methods and results
3.1 test method:
during the test period, 45 female volunteers with the age of 22-60 years are selected and randomly divided into a test group, a positive control group and a blank control group of 3 groups, wherein each group comprises 15 female volunteers. The facial mask prepared in example 1 was used by volunteers in the test group, a herborist new seven-white whitening and skin-tendering facial mask (rejuvenation) was used by volunteers in the positive control group, no product was used by volunteers in the blank control group, both the test group and the positive control group were used normally according to the respective methods of use of the facial masks, and the test period was 1 month. The respective numbers of volunteers in each group were observed before and after the test.
3.2 test standards and results
3.2.1 moisture test
And (4) testing standard: the skin is dry when it is easy to peel and tighten, and wet when it is moist and elastic, the two are normal. The test results are shown in Table 4.
Table 4 moisture retention test
The experimental result shows that compared with a blank control group, the test group has obvious moisturizing effect, and compared with a positive control group, the moisturizing effect of the test group is superior to that of the positive control group.
3.2.2 whitening test
And (4) testing standard: the complexion of the face changes before and after the mask is used, and the complexion of the face is brighter and becomes white when the mask is not dark yellow any more after the mask is used than before the mask is used. The test results are shown in Table 5.
TABLE 5 whitening test
The test result shows that compared with a blank control group, the test group has obvious whitening effect, and compared with a positive control group, the whitening effect of the test group is superior to that of the positive control group.
3.2.3 Spot lightening test
And (4) testing standard: aiming at people with facial spots, the facial spots change before and after the facial mask is used, and the facial spots fade or even disappear after the facial mask is used compared with before the facial mask is used. The test results are shown in Table 6.
TABLE 6 Spot lightening test
| Group of | Number of spotted persons before testing | Number of mottles after testing |
| Test set | 6 | 4 |
| Positive control group | 5 | 1 |
| Blank control group | 8 | 0 |
The experimental result shows that compared with a blank control group, the test group has obvious spot-fading effect, and compared with a positive control group, the spot-fading effect of the test group is superior to that of the positive control group.
3.2.4 acne removal test
And (4) testing standard: aiming at the crowd with acne on the face, the acne on the face before and after the mask is used is changed, and the acne on the face is reduced or even eliminated after the mask is used compared with before the mask is used. The test results are shown in Table 7.
Table 7 acne removal test
| Group of | The number of people with acne before testing | Number of people who removed acne after test |
| Test set | 5 | 5 |
| Positive control group | 6 | 0 |
| Blank control group | 3 | 0 |
The experimental result shows that compared with a blank control group, the test group has obvious acne removing effect, and compared with a positive control group, the acne removing effect of the test group is superior to that of the positive control group.
3.2.5 wrinkle removal test
And (4) testing standard: aiming at the people with wrinkles on the face, the wrinkles on the face are changed before and after the facial mask is used, and the wrinkles on the face are reduced or even eliminated after the facial mask is used compared with before the facial mask is used. The test results are shown in Table 8.
TABLE 8 wrinkle removal test
| Group of | Number of people with wrinkles before testing | Number of people who removed wrinkles after testing |
| Test set | 3 | 2 |
| Positive control group | 2 | 0 |
| Blank control group | 3 | 0 |
The experimental result shows that compared with a blank control group and a positive control group, the test group has obvious wrinkle removing effect.
In conclusion, the pure natural skin care product which is prepared by skillfully using the functions of various traditional Chinese medicines and exerting the respective effects and simultaneously skillfully using the pure natural honey and the propolis and does not contain any additive has multiple effects of whitening, removing freckles, moisturizing, removing acnes, smoothing wrinkles, delaying aging and the like, solves the problem of single effect of the existing skin care product, and has wide market application prospect.
Claims (9)
1. A composition for external use having skin care effect, characterized in that: the traditional Chinese medicine is prepared from the following raw materials in parts by weight:
10 parts of safflower, 30 parts of ginseng, 10 parts of rhodiola rosea, 20 parts of hemsleya amabilis, 20 parts of liquorice, 30 parts of poria cocos, 20 parts of astragalus membranaceus, 20 parts of snow lotus herb, 40 parts of propolis and 400 parts of honey;
the preparation method comprises the following steps:
(1) weighing propolis and honey according to the weight ratio, uniformly stirring, and hermetically fermenting for 1-3 days at the temperature of 25-40 ℃ and the humidity of 75% to obtain propolis honey;
(2) breaking cell wall of other materials, and pulverizing into superfine powder;
(3) weighing the superfine powder and the propolis honey according to the weight ratio, uniformly stirring, carrying out sealed fermentation for 5-15 days at the temperature of 25-30 ℃ and the humidity of 75%, and adding auxiliary materials acceptable in cosmetics to prepare the preparation.
2. The composition for external use according to claim 1, wherein: the preparation is emulsion, film agent or gel.
3. A process for producing the composition for external use according to claim 1 or 2, characterized in that: it comprises the following steps:
(1) weighing propolis and honey according to the weight ratio, uniformly stirring, and hermetically fermenting for 1-3 days at the temperature of 25-40 ℃ and the humidity of 75% to obtain propolis honey;
(2) breaking cell wall of other materials, and pulverizing into superfine powder;
(3) weighing the superfine powder and the propolis honey according to the weight ratio, uniformly stirring, carrying out sealed fermentation for 5-15 days at the temperature of 25-30 ℃ and the humidity of 75%, and adding auxiliary materials acceptable in cosmetics to prepare the preparation.
4. The production method according to claim 3, characterized in that: in the step (1), the fermentation temperature is 30 ℃, and the fermentation time is 2 days.
5. The production method according to claim 3 or 4, characterized in that: in the step (2), the temperature for breaking the wall is 10 +/-2 ℃.
6. The production method according to claim 3, characterized in that: in the step (3), the fermentation temperature is 25 ℃, and the fermentation time is 10 days.
7. The production method according to claim 3, characterized in that: in the step (3), the fermentation process further comprises stirring for 10 minutes every day, wherein the stirring speed is 20 revolutions per minute.
8. The method of claim 7, wherein: the stirring time of 10 minutes is 5 minutes clockwise and 5 minutes counterclockwise.
9. Use of the composition for external use according to claim 1 or 2 for preparing a cosmetic for whitening, removing freckles, moisturizing, removing acne, smoothing wrinkles or delaying aging.
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| CN115804741B (en) * | 2022-12-10 | 2023-06-20 | 广州腾麟生物科技有限公司 | Anti-aging active composition for promoting absorption and preparation method and application thereof |
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Application publication date: 20180413 Assignee: SICHUAN FUZHENG PHARMACEUTICAL CO.,LTD. Assignor: CHENGDU FUZHENG BIOLOGY TECHNOLOGY Co.,Ltd. Contract record no.: X2021510000055 Denomination of invention: The invention relates to an external composition with skin care effect and a preparation method thereof Granted publication date: 20211015 License type: Common License Record date: 20211214 |
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