CN107794761A - A kind of preparation method embroidered with natural disinfection finishing agent - Google Patents
A kind of preparation method embroidered with natural disinfection finishing agent Download PDFInfo
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- CN107794761A CN107794761A CN201711237343.XA CN201711237343A CN107794761A CN 107794761 A CN107794761 A CN 107794761A CN 201711237343 A CN201711237343 A CN 201711237343A CN 107794761 A CN107794761 A CN 107794761A
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- parts
- embroidery
- finishing agent
- good
- natural disinfection
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- 238000004659 sterilization and disinfection Methods 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- LWIHDJKSTIGBAC-UHFFFAOYSA-K tripotassium phosphate Chemical compound [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 claims abstract description 34
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 28
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 17
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 229910000160 potassium phosphate Inorganic materials 0.000 claims abstract description 17
- 235000011009 potassium phosphates Nutrition 0.000 claims abstract description 17
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims abstract description 17
- 229910021642 ultra pure water Inorganic materials 0.000 claims abstract description 17
- 239000012498 ultrapure water Substances 0.000 claims abstract description 17
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 12
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 12
- 239000003292 glue Substances 0.000 claims abstract description 12
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 12
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 claims abstract description 12
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 12
- 229920005989 resin Polymers 0.000 claims abstract description 12
- 239000011347 resin Substances 0.000 claims abstract description 12
- 239000008117 stearic acid Substances 0.000 claims abstract description 12
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims description 18
- 238000010792 warming Methods 0.000 claims description 10
- 239000002994 raw material Substances 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 6
- 238000009413 insulation Methods 0.000 claims description 5
- 239000004576 sand Substances 0.000 claims description 5
- KMNUDJAXRXUZQS-UHFFFAOYSA-L zinc;n-ethyl-n-phenylcarbamodithioate Chemical compound [Zn+2].CCN(C([S-])=S)C1=CC=CC=C1.CCN(C([S-])=S)C1=CC=CC=C1 KMNUDJAXRXUZQS-UHFFFAOYSA-L 0.000 claims description 5
- -1 alkene nitrile Chemical class 0.000 claims description 4
- 230000000694 effects Effects 0.000 abstract description 11
- 238000001035 drying Methods 0.000 abstract description 6
- 241000222122 Candida albicans Species 0.000 abstract description 5
- 241000588724 Escherichia coli Species 0.000 abstract description 5
- 241000191967 Staphylococcus aureus Species 0.000 abstract description 5
- 238000005299 abrasion Methods 0.000 abstract description 5
- 230000000845 anti-microbial effect Effects 0.000 abstract description 5
- 229940095731 candida albicans Drugs 0.000 abstract description 5
- 238000005260 corrosion Methods 0.000 abstract description 5
- 230000007797 corrosion Effects 0.000 abstract description 5
- 231100000252 nontoxic Toxicity 0.000 abstract description 5
- 230000003000 nontoxic effect Effects 0.000 abstract description 5
- 230000035699 permeability Effects 0.000 abstract description 4
- 239000000463 material Substances 0.000 description 10
- 239000004744 fabric Substances 0.000 description 8
- 230000000844 anti-bacterial effect Effects 0.000 description 6
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 238000004078 waterproofing Methods 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
- 239000005864 Sulphur Substances 0.000 description 3
- 239000003599 detergent Substances 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 3
- 238000000227 grinding Methods 0.000 description 3
- 239000012188 paraffin wax Substances 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229910052731 fluorine Inorganic materials 0.000 description 2
- 239000011737 fluorine Substances 0.000 description 2
- 239000010985 leather Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000009941 weaving Methods 0.000 description 2
- 241000208340 Araliaceae Species 0.000 description 1
- 241001108921 Asclepias asperula Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000009956 embroidering Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 125000001153 fluoro group Chemical group F* 0.000 description 1
- 239000010437 gem Substances 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000002706 hydrostatic effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- YFSUTJLHUFNCNZ-UHFFFAOYSA-N perfluorooctane-1-sulfonic acid Chemical compound OS(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F YFSUTJLHUFNCNZ-UHFFFAOYSA-N 0.000 description 1
- SNGREZUHAYWORS-UHFFFAOYSA-N perfluorooctanoic acid Chemical compound OC(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F SNGREZUHAYWORS-UHFFFAOYSA-N 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 230000032258 transport Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/327—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
- D06M15/333—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/46—Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic Table; Titanates; Zirconates; Stannates; Plumbates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
- D06M11/71—Salts of phosphoric acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/30—Flame or heat resistance, fire retardancy properties
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
A kind of preparation method this application discloses embroidery with natural disinfection finishing agent, weigh ultra-pure water, vinyl acetate, accelerator, 107 glue, neopelex, polyvinyl butyral resin, nano titanium oxide, acrylonitrile, potassium phosphate, polyethylene glycol and stearic acid；Natural disinfection, anti-mold effect is good, the 3.5MPa of tensile strength 2.8, and resistance to moisture is excellent；It is nontoxic, increase gloss, adhesion 1 grade, good corrosion resistance, abrasion resistance 300 500 times；Good permeability, 80 90 acarids of water-wash resistance walk quickly and keep away rate 97 99%, pliability 1mm, and glossiness is good；Cost is cheap, extends embroidery service life, fast drying, fire resistance is good, and anti-microbial property is good, to Escherichia coli bacteriostasis rate 99.4 99.8%, to Candida albicans bacteriostasis rate 99.85 99.95%, to staphylococcus aureus bacteriostasis rate 99.6 99.8%.
Description
Technical field
The application belongs to embroidery material field, more particularly to a kind of preparation method embroidered with natural disinfection finishing agent.
Background technology
Usually used Nano Silver particle diameter is 2-5nm in fabric nano-silver antibacterial finishing agent, and colorless and odorless transparency liquid is
Main antibacterial raw material, the efficient fabric antibacterial finishing agent formed through NEW TYPE OF COMPOSITE mode, is widely used in various textiles, nonwoven
Each kind fabric such as cloth, leather.Antibacterial effect is more than 99%.
The advantages of without fluoro water proofing agent：Do not protected and perplexed by Environmental security, APEO, PFOA involved by completely without environmental protection,
PFOS；It can be used alone, and there is good waterproof effect；Price material benefit, it is suitable with existing C8 fluorine systems waterproofing agent, than C6 fluorine
It is that waterproofing agent is cheap；There is waterproof, washable effect simultaneously；With anti-siphon, resistance to hydrostatic pressure and permeation-proof slurry and other effects；Individually
Using or addition use, all with good washing-resistant effect.
Aluminium soap, paraffin/metallic salt finishing agent（Paraffin-aluminum salt, paraffin-zirconates etc.）：Utilize paraffin wax emulsions and metal salt
Aqueous dispersions dipping fabric, generate metal salts thing or hydroxide, the mixture with paraffin after drying and heat treatment
It is deposited on fabric, assigns the water proofing property of fabric.
Staple line is embroidered to be also known as disk stalk embroidery or paste line and embroidered, and is that various silk ribbons, cotton rope are embroidered on clothes or weaving by certain pattern nail
A kind of embroidering method on product.Conventional staple line method has bright two kinds of nail and blind nail, and on the former the online stalk of needle tracking exposure, the latter is then
It is hidden in line stalk.Staple line embroider embroidery method it is simple, with a long history, its decorated style is elegant and graceful, in recent years in kimonos apply compared with
It is more.Sequin embroidery, also referred to as pearl embroidery, it is that embroidery is sewed in dress ornament for material with hollow bead, pearl pipe, synthetic cut stone, flash of light sequin etc.
On, to produce bedecked with jewels, dazzling brilliant effect, it is generally used on stage performance clothes, to increase the aesthetic feeling of clothes and suction
Gravitation, while it is also widely used in vamp, bag, casket etc. above.
At the beginning of the late Qing Dynasty people, gradually, there are innovation works in Suzhou embroidery in Western learning east.During the time ruled by Emperor Guang Xu, the wife Shen rainbow conk of remaining feel embroiders skill exquisiteness,
Well-known Suzhou Xiu Tan.During Shen Shi 30 years old, the birthday of the Empress Dowager 70 is met, the eight frame works that Shen Shi has embroidered " Eight Immortals celebrate the longevity " are offered birthday congratulations, obtained
Bestow " good fortune " " longevity " two word, thus the Shen Shou that renames.Shen is embroidered transports old law with new meaning, shows light and does color, and ginseng is imitated western drawing Xiao god with realistic
Genuine feature is found expression among embroidery, new to create " emulational embroidery ", or " artistic embroidery ", and the skill of handling needles is changeable, rich third dimension.
Fabric nano-silver antibacterial finishing agent has used new technology silver（Ag）Nanometer (Nano) level is fabricated to, is fully demonstrated
Silver-colored original advantageous characteristic, therefore application field also constantly expands.Such as：Weaving, coating, plastic cement, medical treatment, leather, environmental protection etc..
The content of the invention
The technical problem of solution：
The application is directed to above-mentioned technical problem, there is provided a kind of preparation method embroidered with natural disinfection finishing agent, solves existing thorn
Embroider with natural disinfection finishing agent anti-mold effect is poor, glossiness is low and the technical problems such as bactericidal properties are poor.
Technical scheme：
A kind of preparation method embroidered with natural disinfection finishing agent, comprises the following steps：
The first step：According to parts by weight proportioning weigh 100 parts of ultra-pure water, vinyl acetate 30-40 parts, accelerator 1.5-5.5 parts,
107 glue 10-30 parts, neopelex 10-20 parts, polyvinyl butyral resin 5-9 parts, nano titanium oxide 15-35 parts,
Acrylonitrile 4-8 parts, potassium phosphate 7-9 parts, polyethylene glycol 10-30 parts and stearic acid 1-5 parts；
Second step：Neopelex, nano titanium oxide and potassium phosphate are put into grinder and grind 30-50min, is ground
After the completion of mill in reactor of the input with thermometer, mixer and heater, mixer mixing is opened, is warming up to 50-70
DEG C, mixing velocity 300-400r/min, mix 40-80min；
3rd step：Ultra-pure water and vinyl acetate are sequentially added, regulation mixing velocity to 400-500 r/min, mixes 20-60min,
Surplus stock is added, 100-120 DEG C is warming up to, well mixed product is put into sand mill after insulation reaction 4-6h, is sanded 2
It is secondary, after crossing cleaner liquid, produced after standing 2-4h.
As a preferred technical solution of the present invention：Embroidery is pressed with the raw material of natural disinfection finishing agent in the first step
Parts by weight proportioning is as follows：100 parts of ultra-pure water, 30 parts of vinyl acetate, 1.5 parts of accelerator, 10 parts of 107 glue, detergent alkylate sulphur
Sour 10 parts of sodium, 5 parts of polyvinyl butyral resin, 15 parts of nano titanium oxide, 4 parts of acrylonitrile, 7 parts of potassium phosphate, 10 parts of polyethylene glycol
With 1 part of stearic acid.
As a preferred technical solution of the present invention：Embroidery is pressed with the raw material of natural disinfection finishing agent in the first step
Parts by weight proportioning is as follows：100 parts of ultra-pure water, 40 parts of vinyl acetate, 5.5 parts of accelerator, 30 parts of 107 glue, detergent alkylate sulphur
Sour 20 parts of sodium, 9 parts of polyvinyl butyral resin, 35 parts of nano titanium oxide, 8 parts of acrylonitrile, 9 parts of potassium phosphate, 30 parts of polyethylene glycol
With 5 parts of stearic acid.
As a preferred technical solution of the present invention：Embroidery is pressed with the raw material of natural disinfection finishing agent in the first step
Parts by weight proportioning is as follows：100 parts of ultra-pure water, 35 parts of vinyl acetate, 3.5 parts of accelerator, 20 parts of 107 glue, detergent alkylate sulphur
Sour 15 parts of sodium, 7 parts of polyvinyl butyral resin, 25 parts of nano titanium oxide, 6 parts of acrylonitrile, 8 parts of potassium phosphate, 20 parts of polyethylene glycol
With 3 parts of stearic acid.
As a preferred technical solution of the present invention：The accelerator uses zinc-ethylphenyl dithiocarbamate.
Beneficial effect：
A kind of embroider of the present invention uses above technical scheme and prior art phase with the preparation method of natural disinfection finishing agent
Than having following technique effect：1st, preparation method is simple, natural disinfection, and anti-mold effect is good, tensile strength 2.8-3.5MPa, resists
Moisture is excellent；2nd, it is nontoxic, increase gloss, adhesion 1 grade, good corrosion resistance, abrasion resistance 300-500 times；3rd, breathe freely
Property is good, and 80-90 acarid of water-wash resistance walks quickly and keeps away rate 97-99%, pliability 1mm, and glossiness is good；4th, cost is cheap, and extending embroidery makes
Good with life-span, fast drying, fire resistance, anti-microbial property is good, and to Escherichia coli bacteriostasis rate 99.4-99.8%, Candida albicans is pressed down
Bacterium rate 99.85-99.95%, to staphylococcus aureus bacteriostasis rate 99.6-99.8%, it can extensively produce and constantly replace existing
Material.
Embodiment
Embodiment 1:
100 parts of ultra-pure water, 30 parts of vinyl acetate, zinc-ethylphenyl dithiocarbamate 1.5 are weighed according to parts by weight proportioning
Part, 10 parts of 107 glue, 10 parts of neopelex, 5 parts of polyvinyl butyral resin, 15 parts of nano titanium oxide, acrylonitrile 4
Part, 7 parts of potassium phosphate, 10 parts of polyethylene glycol and 1 part of stearic acid.
Neopelex, nano titanium oxide and potassium phosphate are put into grinder and grind 30min, grinding is completed
Afterwards in reactor of the input with thermometer, mixer and heater, mixer mixing is opened, is warming up to 50 DEG C, mixing speed
Spend for 300r/min, mixing 40min.
Ultra-pure water and vinyl acetate are sequentially added, regulation mixing velocity to 400 r/min, mixes 20min, is added remaining former
Material, 100 DEG C are warming up to, well mixed product is put into sand mill after insulation reaction 4h, is sanded 2 times, it is quiet after crossing cleaner liquid
Produced after putting 2h.
Preparation method is simple, natural disinfection, and anti-mold effect is good, tensile strength 2.8MPa, and resistance to moisture is excellent；Nontoxic nothing
Evil, increase gloss, adhesion 1 grade, good corrosion resistance, abrasion resistance 300 times；Good permeability, 80 acarids of water-wash resistance are walked quickly and kept away
Rate 97%, pliability 1mm, glossiness are good；Cost is cheap, extends embroidery service life, fast drying, fire resistance is good, anti-microbial property
It is good, to Escherichia coli bacteriostasis rate 99.4%, to Candida albicans bacteriostasis rate 99.85%, to staphylococcus aureus bacteriostasis rate
99.6%, it can extensively produce and constantly replace current material.
Embodiment 2:
100 parts of ultra-pure water, 40 parts of vinyl acetate, zinc-ethylphenyl dithiocarbamate 5.5 are weighed according to parts by weight proportioning
Part, 30 parts of 107 glue, 20 parts of neopelex, 9 parts of polyvinyl butyral resin, 35 parts of nano titanium oxide, acrylonitrile 8
Part, 9 parts of potassium phosphate, 30 parts of polyethylene glycol and 5 parts of stearic acid.
Neopelex, nano titanium oxide and potassium phosphate are put into grinder and grind 50min, grinding is completed
Afterwards in reactor of the input with thermometer, mixer and heater, mixer mixing is opened, is warming up to 70 DEG C, mixing speed
Spend for 400r/min, mixing 80min.
Ultra-pure water and vinyl acetate are sequentially added, regulation mixing velocity to 500 r/min, mixes 60min, is added remaining former
Material, 120 DEG C are warming up to, well mixed product is put into sand mill after insulation reaction 6h, is sanded 2 times, it is quiet after crossing cleaner liquid
Produced after putting 4h.
Preparation method is simple, natural disinfection, and anti-mold effect is good, tensile strength 3MPa, and resistance to moisture is excellent；It is nontoxic,
Increase gloss, adhesion 1 grade, good corrosion resistance, abrasion resistance 400 times；Good permeability, 85 acarids of water-wash resistance walk quickly and keep away rate
98%, pliability 1mm, glossiness are good；Cost is cheap, extends embroidery service life, fast drying, fire resistance is good, anti-microbial property
It is good, to Escherichia coli bacteriostasis rate 99.6%, to Candida albicans bacteriostasis rate 99.9%, to staphylococcus aureus bacteriostasis rate 99.7%,
It can extensively produce and constantly replace current material.
Embodiment 3:
100 parts of ultra-pure water, 35 parts of vinyl acetate, zinc-ethylphenyl dithiocarbamate 3.5 are weighed according to parts by weight proportioning
Part, 20 parts of 107 glue, 15 parts of neopelex, 7 parts of polyvinyl butyral resin, 25 parts of nano titanium oxide, acrylonitrile 6
Part, 8 parts of potassium phosphate, 20 parts of polyethylene glycol and 3 parts of stearic acid.
Neopelex, nano titanium oxide and potassium phosphate are put into grinder and grind 40min, grinding is completed
Afterwards in reactor of the input with thermometer, mixer and heater, mixer mixing is opened, is warming up to 60 DEG C, mixing speed
Spend for 350r/min, mixing 60min.
Ultra-pure water and vinyl acetate are sequentially added, regulation mixing velocity to 450 r/min, mixes 40min, is added remaining former
Material, 110 DEG C are warming up to, well mixed product is put into sand mill after insulation reaction 5h, is sanded 2 times, it is quiet after crossing cleaner liquid
Produced after putting 3h.
Preparation method is simple, natural disinfection, and anti-mold effect is good, tensile strength 3.5MPa, and resistance to moisture is excellent；Nontoxic nothing
Evil, increase gloss, adhesion 1 grade, good corrosion resistance, abrasion resistance 500 times；Good permeability, 90 acarids of water-wash resistance are walked quickly and kept away
Rate 99%, pliability 1mm, glossiness are good；Cost is cheap, extends embroidery service life, fast drying, fire resistance is good, anti-microbial property
It is good, to Escherichia coli bacteriostasis rate 99.8%, to Candida albicans bacteriostasis rate 99.95%, to staphylococcus aureus bacteriostasis rate
99.8%, it can extensively produce and constantly replace current material.
Claims (5)
1. a kind of preparation method embroidered with natural disinfection finishing agent, it is characterised in that comprise the following steps：
The first step：According to parts by weight proportioning weigh 100 parts of ultra-pure water, vinyl acetate 30-40 parts, accelerator 1.5-5.5 parts,
107 glue 10-30 parts, neopelex 10-20 parts, polyvinyl butyral resin 5-9 parts, nano titanium oxide 15-35 parts,
Acrylonitrile 4-8 parts, potassium phosphate 7-9 parts, polyethylene glycol 10-30 parts and stearic acid 1-5 parts；
Second step：Neopelex, nano titanium oxide and potassium phosphate are put into grinder and grind 30-50min, is ground
After the completion of mill in reactor of the input with thermometer, mixer and heater, mixer mixing is opened, is warming up to 50-70
DEG C, mixing velocity 300-400r/min, mix 40-80min；
3rd step：Ultra-pure water and vinyl acetate are sequentially added, regulation mixing velocity to 400-500 r/min, mixes 20-60min,
Surplus stock is added, 100-120 DEG C is warming up to, well mixed product is put into sand mill after insulation reaction 4-6h, is sanded 2
It is secondary, after crossing cleaner liquid, produced after standing 2-4h.
2. the preparation method of embroidery natural disinfection finishing agent according to claim 1, it is characterised in that：The first step
Middle embroidery is as follows with the raw materials by weight portion proportioning of natural disinfection finishing agent：100 parts of ultra-pure water, 30 parts of vinyl acetate, promote
1.5 parts of agent, 10 parts of 107 glue, 10 parts of neopelex, 5 parts of polyvinyl butyral resin, 15 parts of nano titanium oxide, third
1 part of 4 parts of alkene nitrile, 7 parts of potassium phosphate, 10 parts of polyethylene glycol and stearic acid.
3. the preparation method of embroidery natural disinfection finishing agent according to claim 1, it is characterised in that：The first step
Middle embroidery is as follows with the raw materials by weight portion proportioning of natural disinfection finishing agent：100 parts of ultra-pure water, 40 parts of vinyl acetate, promote
5.5 parts of agent, 30 parts of 107 glue, 20 parts of neopelex, 9 parts of polyvinyl butyral resin, 35 parts of nano titanium oxide, third
5 parts of 8 parts of alkene nitrile, 9 parts of potassium phosphate, 30 parts of polyethylene glycol and stearic acid.
4. the preparation method of embroidery natural disinfection finishing agent according to claim 1, it is characterised in that：The first step
Middle embroidery is as follows with the raw materials by weight portion proportioning of natural disinfection finishing agent：100 parts of ultra-pure water, 35 parts of vinyl acetate, promote
3.5 parts of agent, 20 parts of 107 glue, 15 parts of neopelex, 7 parts of polyvinyl butyral resin, 25 parts of nano titanium oxide, third
3 parts of 6 parts of alkene nitrile, 8 parts of potassium phosphate, 20 parts of polyethylene glycol and stearic acid.
5. the preparation method of embroidery natural disinfection finishing agent according to claim 1, it is characterised in that：The accelerator
Using zinc-ethylphenyl dithiocarbamate.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108691203A (en) * | 2018-05-07 | 2018-10-23 | 贵州西江阿幼民族文化博物馆有限公司 | A kind of preparation method of embroidery sterilization and insect prevention finishing agent |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1566512A (en) * | 2003-07-02 | 2005-01-19 | 北京化大天瑞纳米材料技术有限公司 | Antibacterial fabric and its preparation method and application |
| CN103437144A (en) * | 2013-07-22 | 2013-12-11 | 苏州三和开泰花线织造有限公司 | Preparation method for nanometer titanium dioxide finishing agent |
| CN106700831A (en) * | 2016-12-14 | 2017-05-24 | 南京悠谷知识产权服务有限公司 | Corrosion-resistant paint for aviation materials and preparation method thereof |
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2017
- 2017-11-30 CN CN201711237343.XA patent/CN107794761A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1566512A (en) * | 2003-07-02 | 2005-01-19 | 北京化大天瑞纳米材料技术有限公司 | Antibacterial fabric and its preparation method and application |
| CN103437144A (en) * | 2013-07-22 | 2013-12-11 | 苏州三和开泰花线织造有限公司 | Preparation method for nanometer titanium dioxide finishing agent |
| CN106700831A (en) * | 2016-12-14 | 2017-05-24 | 南京悠谷知识产权服务有限公司 | Corrosion-resistant paint for aviation materials and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108691203A (en) * | 2018-05-07 | 2018-10-23 | 贵州西江阿幼民族文化博物馆有限公司 | A kind of preparation method of embroidery sterilization and insect prevention finishing agent |
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Application publication date: 20180313 |