CN107778859A - A kind of preparation method of high-performance rubber composition - Google Patents
A kind of preparation method of high-performance rubber composition Download PDFInfo
- Publication number
- CN107778859A CN107778859A CN201610749186.XA CN201610749186A CN107778859A CN 107778859 A CN107778859 A CN 107778859A CN 201610749186 A CN201610749186 A CN 201610749186A CN 107778859 A CN107778859 A CN 107778859A
- Authority
- CN
- China
- Prior art keywords
- parts
- curing accelerator
- rubber composition
- preparation
- agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 229920006247 high-performance elastomer Polymers 0.000 title claims abstract description 11
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 13
- 229920001971 elastomer Polymers 0.000 claims abstract description 13
- 229920001577 copolymer Polymers 0.000 claims abstract description 7
- HIHIPCDUFKZOSL-UHFFFAOYSA-N ethenyl(methyl)silicon Chemical compound C[Si]C=C HIHIPCDUFKZOSL-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229920001721 polyimide Polymers 0.000 claims abstract description 7
- 239000009719 polyimide resin Substances 0.000 claims abstract description 7
- 229920002379 silicone rubber Polymers 0.000 claims abstract description 7
- 239000004945 silicone rubber Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 5
- 238000004040 coloring Methods 0.000 claims abstract description 4
- 239000003063 flame retardant Substances 0.000 claims abstract description 4
- 239000000463 material Substances 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 4
- 239000003292 glue Substances 0.000 claims description 3
- 239000012943 hotmelt Substances 0.000 claims description 3
- 238000002844 melting Methods 0.000 claims description 3
- 230000008018 melting Effects 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 239000004952 Polyamide Substances 0.000 claims description 2
- 229920002647 polyamide Polymers 0.000 claims description 2
- 230000032683 aging Effects 0.000 abstract description 2
- 238000004806 packaging method and process Methods 0.000 abstract description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/92—Measuring, controlling or regulating
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L101/00—Compositions of unspecified macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L79/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen with or without oxygen or carbon only, not provided for in groups C08L61/00 - C08L77/00
- C08L79/04—Polycondensates having nitrogen-containing heterocyclic rings in the main chain; Polyhydrazides; Polyamide acids or similar polyimide precursors
- C08L79/08—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C2948/00—Indexing scheme relating to extrusion moulding
- B29C2948/92—Measuring, controlling or regulating
- B29C2948/92504—Controlled parameter
- B29C2948/92514—Pressure
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C2948/00—Indexing scheme relating to extrusion moulding
- B29C2948/92—Measuring, controlling or regulating
- B29C2948/92504—Controlled parameter
- B29C2948/92704—Temperature
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Laminated Bodies (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a kind of preparation method of high-performance rubber composition, and it includes the raw material of following weight parts：4 parts of 50 120 parts of polyimide resin, 20 160 parts of high molecular weight copolymer rubber, 40 80 parts of methyl vinyl silicone rubber, 36 parts of curing agent, 25 parts of curing accelerator, 28 parts of fire retardant, 5 10 parts of releasing agent and colouring agent.The high-performance rubber composition that the present invention makes has an excellent mechanical property and packaging appearance yield, and high temperature resistant, ageing-resistant, while also tool makees good mouldability, anti-flammability and reliability.
Description
Technical field
The present invention relates to a kind of preparation method of high-performance rubber composition, is related specifically to a kind of high-performance rubber group
The preparation method of compound.
Background technology
The preparation method of building rubber compound generally includes raw material mixing, extrusion is kneaded, tabletting cooling, crush, rear mixing, into
The process such as type.Rubber composition is fully kneaded to form certain limitation to material, and then to the mechanical property of rubber composition
Yield and can be encapsulated and cause negative limitation.
The content of the invention
The technical problem to be solved in the present invention is to overcome above-mentioned deficiency, there is provided a kind of making side of high-performance rubber composition
Method.
A kind of preparation method of high-performance rubber composition of the present invention, it includes the raw material of following weight parts：Polyamides is sub-
Polyimide resin 50-120 parts, high molecular weight copolymer rubber 20-160 parts, methyl vinyl silicone rubber 40-80 parts, curing agent 3-6
4 parts of part, curing accelerator 2-5 parts, fire retardant 2-8 parts, releasing agent 5-10 parts and colouring agent, its preparation method include following step
Suddenly：
First step：Reserved curing accelerator；
Second step：By homogenizer by the polyimide resin in addition to curing accelerator, high molecular weight copolymer rubber
Glue and methyl vinyl silicone rubber are well mixed, and speed of agitator 150-200 turns/min, mixing time 2-2.5h, and is sent to
In next step；
Third step：Material hot-melt extruded as obtained by double screw extruder by second step, hot melting temperature are 150-200 DEG C,
And it is sent in next step；
Four steps：Curing accelerator is added with 4kg/h rate of addition in muller feed zone or contains curing accelerator
Solution, and having passed through muller makes material uniform；
5th step：Molecule is made by blanking, tabletting, cooling, crushing, sub-sieve in material, after mixed after it is scattered equal
It is even, through being cooled to solid fraction rubber composition.
Beneficial effects of the present invention are that a kind of high-performance rubber composition tool that the present invention makes makees excellent mechanical property
Can and packaging appearance yield, it is and high temperature resistant, ageing-resistant, while also tool makees good mouldability, anti-flammability and reliability.
Embodiment
The present invention is further illustrated with reference to embodiments, but this is only citing, is not limitation of the present invention.
A kind of preparation method of high-performance rubber composition, it includes the raw material of following weight parts：Polyimide resin 50-
120 parts, high molecular weight copolymer rubber 20-160 parts, methyl vinyl silicone rubber 40-80 parts, curing agent 3-6 parts, solidification promote
4 parts of agent 2-5 parts, fire retardant 2-8 parts, releasing agent 5-10 parts and colouring agent, its preparation method comprises the following steps：
First step：Reserved curing accelerator；
Second step：By homogenizer by the polyimide resin in addition to curing accelerator, high molecular weight copolymer rubber
Glue and methyl vinyl silicone rubber are well mixed, and speed of agitator 150-200 turns/min, mixing time 2-2.5h, and is sent to
In next step；
Third step：Material hot-melt extruded as obtained by double screw extruder by second step, hot melting temperature are 150-200 DEG C,
And it is sent in next step；
Four steps：Curing accelerator is added with 4kg/h rate of addition in muller feed zone or contains curing accelerator
Solution, and having passed through muller makes material uniform；
5th step：Molecule is made by blanking, tabletting, cooling, crushing, sub-sieve in material, after mixed after it is scattered equal
It is even, through being cooled to solid fraction rubber composition.
Preferred embodiments of the present invention are these are only, therefore the scope that the present invention is implemented can not be limited according to this, i.e., according to the present invention
The equivalence changes and decoration that description is made, it should all belong in the range of present invention covering.
Claims (1)
1. a kind of preparation method of high-performance rubber composition, it is characterised in that it includes the raw material of following weight parts：Polyamides is sub-
Polyimide resin 50-120 parts, high molecular weight copolymer rubber 20-160 parts, methyl vinyl silicone rubber 40-80 parts, curing agent 3-6
4 parts of part, curing accelerator 2-5 parts, fire retardant 2-8 parts, releasing agent 5-10 parts and colouring agent, its preparation method include following step
Suddenly：
First step：Reserved curing accelerator；
Second step：By homogenizer by the polyimide resin in addition to curing accelerator, high molecular weight copolymer rubber
Glue and methyl vinyl silicone rubber are well mixed, and speed of agitator 150-200 turns/min, mixing time 2-2.5h, and is sent to
In next step；
Third step：Material hot-melt extruded as obtained by double screw extruder by second step, hot melting temperature are 150-200 DEG C,
And it is sent in next step；
Four steps：Curing accelerator is added with 4kg/h rate of addition in muller feed zone or contains curing accelerator
Solution, and having passed through muller makes material uniform；
5th step：Molecule is made by blanking, tabletting, cooling, crushing, sub-sieve in material, after mixed after it is scattered equal
It is even, through being cooled to solid fraction rubber composition.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610749186.XA CN107778859A (en) | 2016-08-30 | 2016-08-30 | A kind of preparation method of high-performance rubber composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610749186.XA CN107778859A (en) | 2016-08-30 | 2016-08-30 | A kind of preparation method of high-performance rubber composition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107778859A true CN107778859A (en) | 2018-03-09 |
Family
ID=61440704
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610749186.XA Pending CN107778859A (en) | 2016-08-30 | 2016-08-30 | A kind of preparation method of high-performance rubber composition |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107778859A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117801520A (en) * | 2023-12-28 | 2024-04-02 | 东莞市高酷纳米科技有限公司 | A method for preparing high-performance flame-retardant and thermally conductive compound rubber for the electronics industry |
-
2016
- 2016-08-30 CN CN201610749186.XA patent/CN107778859A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117801520A (en) * | 2023-12-28 | 2024-04-02 | 东莞市高酷纳米科技有限公司 | A method for preparing high-performance flame-retardant and thermally conductive compound rubber for the electronics industry |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102336989A (en) | Polyvinyl chloride (PVC) wood-plastic foaming wood grain section and preparation method thereof | |
| WO2008135529A3 (en) | Process for making polyolefin compositions | |
| CN105419142B (en) | A kind of plating PC/ABS alloy materials and preparation method thereof | |
| CN105348746B (en) | A kind of plastic filler parent granule and preparation method thereof | |
| CN107540920A (en) | Metallocene PE composition and preparation method thereof | |
| CN108690315A (en) | A kind of Heat resistance ABS material of matt and preparation method thereof | |
| CN103419373B (en) | A kind of preparation method of CSM/NBR compound rubber pipe | |
| CN103709493A (en) | High-concentration anti-static master batch for polyolefin and preparation method thereof | |
| CN103937124A (en) | High-speed extrusion matte polyvinyl chloride cable material and preparation method thereof | |
| CN103113709A (en) | Special high-filling master batch for acrylonitrile butadiene styrene and preparation method thereof | |
| CN107778859A (en) | A kind of preparation method of high-performance rubber composition | |
| CN108219260A (en) | A kind of halogen-free flameproof EVA thermoplastic elastic materials and preparation method thereof | |
| CN105400053B (en) | A kind of micro- permeability low viscosity PE alloy materials and preparation method thereof | |
| CN106633411A (en) | Polypropylene composite material capable of realizing 3D (three-dimensional) printing and preparation method thereof | |
| CN109575446A (en) | A kind of high-performance polypropylene material and preparation method thereof | |
| CN104098866A (en) | Raw material formula and preparation method of thermoplastic elastomer wood-plastic material | |
| CA3012086C (en) | Masterbatch for pvc | |
| CN104761862A (en) | Preparation method of high-polymer packaging material | |
| CN110157101A (en) | A kind of 3D printing modified poly propylene composition and preparation method thereof | |
| CN105602272A (en) | Novel environment-friendly TPR plastic flooring material, and preparation method thereof | |
| CN102485791A (en) | Masterbatch | |
| CN106479209A (en) | A kind of composite for making fungus-proof antisepsis door pocket and preparation method thereof | |
| CN104497488A (en) | Preparation method of environment-friendly epoxy resin composition for semiconductor package | |
| CN105566678A (en) | Talcum powder nucleation masterbatch and producing process thereof | |
| CN102286175A (en) | Flame retardant masterbatch and manufacturing process thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180309 |
|
| WD01 | Invention patent application deemed withdrawn after publication |