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CN107714555A - A kind of pure plant moisture-keeping crease-shedding eye cream and preparation method thereof - Google Patents

A kind of pure plant moisture-keeping crease-shedding eye cream and preparation method thereof Download PDF

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CN107714555A
CN107714555A CN201711189922.1A CN201711189922A CN107714555A CN 107714555 A CN107714555 A CN 107714555A CN 201711189922 A CN201711189922 A CN 201711189922A CN 107714555 A CN107714555 A CN 107714555A
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extract solution
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储成玲
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a kind of pure plant moisture-keeping crease-shedding eye cream and preparation method thereof, is related to Chinese medicine cosmetic technical field, includes the raw material of following parts by weight:20 30 parts of orchid, 22 30 parts of the fruit of Chinese magnoliavine, 20 30 parts of chamomile, 20 30 parts of eclipta, 17 25 parts of the root of kudzu vine, 17 25 parts of pseudo-ginseng, 14 22 parts of radix glycyrrhizae, 20 30 parts of the fleece-flower root, 17 25 parts of cactus, 25 35 parts of rhodiola root, 36 parts of Sweet Almond Oil, appropriate amount of water.The present invention is formulated using pure plant raw material, through reasonable compatibility, acted synergistically between each composition, the effect of playing the promoting flow of qi and blood circulation, clearing heat for detumescence, tonify the liver and kidney, eye circumference skin blood circulation can be promoted, strengthen cell viability, repair damaged cell and abundant nutritional ingredient is provided for it, deep layer moistens eye circumference skin, the problems such as improving eye dryness, edema, relaxation, desalinate microgroove, go wrinkle effect good, suitable for any skin.

Description

A kind of pure plant moisture-keeping crease-shedding eye cream and preparation method thereof
Technical field
The present invention relates to Chinese medicine cosmetic technical field, more particularly to a kind of pure plant moisture-keeping crease-shedding eye cream and its preparation side Method.
Background technology
Many women can make up daily, and especially eye is emphasis cosmetic position, in cosmetics containing many chemistry into Point, it is easy to eyelid health is influenceed, causes eye skin to dry aging.Research shows the especially soft and fine fibre of skin around eyes It is thin, and have the gauffer of many, therefore muscles around eyes skin water evaporation rate is most fast, meanwhile, the sebaceous glands point of the sweat gland of periocualr skin Cloth is less, is particularly easy to dry water shortage, so as to easily produce wrinkle.Eye circumference skin begins to go down hill after general 25 years old, There is the problems such as livid ring around eye, crow's feet, pouch, granulation, edema, so, prevention and nursing are highly important, existing market eyes White quality is very different, and multipair greatly to improve effect of the eye skin without reality, anti-wrinkle effect is general, or added with variousization Medicine is learned, although quick, dependence is strong, is not suitable for long-term use.Therefore, under the increasing market demand, if Count a gentle non-stimulated, being capable of long-term use of eye cream is extremely necessary.
The content of the invention
Based on technical problem existing for background technology, the present invention proposes a kind of pure plant moisture-keeping crease-shedding eye cream and its preparation Method, the problems such as eye dryness, edema can be improved, relaxed, desalinate microgroove, go wrinkle effect good, suitable for any skin.
A kind of pure plant moisture-keeping crease-shedding eye cream proposed by the present invention, include the raw material of following parts by weight:Orchid 20-30 parts, Fruit of Chinese magnoliavine 22-30 parts, chamomile 20-30 parts, eclipta 20-30 parts, root of kudzu vine 17-25 parts, pseudo-ginseng 17-25 parts, radix glycyrrhizae 14-22 Part, fleece-flower root 20-30 parts, cactus 17-25 parts, rhodiola root 25-35 parts, Sweet Almond Oil 3-6 parts, appropriate amount of water.
Preferably, the raw material of following parts by weight is included:25 parts of orchid, 27 parts of the fruit of Chinese magnoliavine, 25 parts of chamomile, eclipta 22 Part, 22 parts of the root of kudzu vine, 20 parts of pseudo-ginseng, 18 parts of radix glycyrrhizae, 25 parts of the fleece-flower root, 22 parts of cactus, 30 parts of rhodiola root, 5 parts of Sweet Almond Oil, water In right amount.
The invention also provides the preparation method of above-mentioned pure plant moisture-keeping crease-shedding eye cream, comprise the following steps:
S1, fresh orchid, chamomile smashed to pieces, add 60-70% alcohol solution dippings, cold pressing is squeezed, pressed liquor is subtracted Pressure concentration removes ethanol, obtains extract solution A;
S2, cactus added water to cook into extraction, filtered, add papain and cellulase into filtrate, hydrolysis, from The heart, obtain extract solution B;
S3, by the fruit of Chinese magnoliavine, pseudo-ginseng, the fleece-flower root mix, crush, add 70% ethanol solution refluxing extraction, filtering, reclaim second Alcohol, it is dissolved in water, filters, obtain filter residue and extract solution C;
S4, by eclipta, the root of kudzu vine, radix glycyrrhizae, rhodiola root mix, crush, add S3 in filter residue, add water to cook extraction, mistake Filter, obtains extract solution D;
S5, extract solution A, extract solution B, extract solution C, extract solution D be well mixed, it is quiet that activated carbon is added into mixed liquor Put, filter, concentrate filtrate to the clear cream (60-70 DEG C) that relative density is 1.02-1.04, clear cream is cooled to 40-50 DEG C, Sweet Almond Oil is added, is stirred, cooling bottling, sealing, is produced.
Preferably, in the S1, fresh orchid, chamomile are smashed to pieces, according to 1g:(3-4) mL solid-liquid ratio adds 60- 70% ethanol solution, soak 5-7 days, cold pressing is squeezed, and pressed liquor is concentrated under reduced pressure and removes ethanol, obtains extract solution A.
Preferably, in the S2, cactus is added water to cook into extraction 1-2h, amount of water is cactus raw material initial mass 5-8 times, filtering, it is 6.0-6.5 to add papain and cellulase, regulation pH into filtrate, and 3- is hydrolyzed at 40-50 DEG C 5h, centrifuged with 3000-3500r/min rotating speed, obtain extract solution B.
Preferably, the addition of the papain be cactus quality 0.2-0.5%, the addition of cellulase For the 0.2-0.5% of cactus quality.
Preferably, in the S3, the fruit of Chinese magnoliavine, pseudo-ginseng, the fleece-flower root is mixed, crushed, adds the initial gross mass of 5-8 times of material 70% ethanol solution refluxing extraction 2-3h, filtering, reclaim ethanol, be dissolved in water, filter, obtain filter residue and extract solution C.
Preferably, in the S4, eclipta, the root of kudzu vine, radix glycyrrhizae, rhodiola root is mixed, crushed, the filter residue added in S3, is added Enter the water boiling and extraction 2-3h of the initial gross mass of 5-8 times of material, filter, obtain extract solution D.
Preferably, in the S5, extract solution A, extract solution B, extract solution C, extract solution D are well mixed, into mixed liquor The activated carbon for adding the 2-4% of its quality stands 3-5h, filtering.
It is as follows the effect of each raw material in the present invention:
Orchid:Acrid flavour, mild-natured, return lung warp, the spleen channel, Liver Channel, there is the effect of regulating the qi flowing in the channels is with, cough-relieving improving eyesight;It is rich in orchid Containing the several mineral materials needed for skin, oligosaccharides and flavonoid class active ingredient, moisturizing is effectively played, anti-oxidant, enhancing skin is exempted from Epidemic disease power and the effect for reducing microgroove, and its reparation power is very strong, and the elite extracted from orchid is used in around eyes and compared On fragile skin, the injury that eyes are subject to can be repaired, so as to Vitamin K, restoring ocular skin.
The fruit of Chinese magnoliavine:It is warm-natured, sour, sweet, return lung warp, the heart channel of Hang-Shaoyin, kidney channel, have and restrain astringent or styptic treatment for spontaneous sweating, nourishing generate fluid, kidney calming Effect;Contain lignanoids, volatile ingredient, glycoside, organic acid, chlorophyll, vitamin, tannin etc. in the fruit of Chinese magnoliavine.With anti- Oxidation, anti-aging effects, there is significant protective effect to damage caused by oxygen radical.The intellection of people can be improved, eliminated Fatigue, operating efficiency is improved, can strengthen defence capability of the body to nonspecific stimulation, and with antiulcer, antiviral, anti- Cancer acts on.
Chamomile:It is famous with refrigerant, calm, sleeping effect, have it is clearing heat and detoxicating, clear liver and improve vision, blood circulation promoting and enriching, dispelling wind Radiating, anti-inflammatory sterilization, fatigue of releiving, mood placating, the function for improving sleep, the beauty functions of chamomile depend on chamomile temperature With, the characteristic releived, it is allowed to turn into good companion of combination of various plants maintenance composition;Chamomile can Lavender Extract, skin of releiving Sensitiveness, anti-inflammatory of subsiding a swelling, receives thin fine vascular, reduces chemical substance or the too high injury to skin of essential oil concentration, can make flesh Skin produces protection, can improve skin water shortage, sensitivity phenomenon, skin health is full of gloss, to the reparation work(of skin after solarization Effect is more notable.
Mo Liancao:It is cold in nature, it is sweet, sour, return kidney channel, Liver Channel, there is the effect of nourishing liver and kidney, cooling blood and hemostasis;Modern age pharmacology Research thinks that the immune organ weight that Mo Liancao can make animal degenerate returns to normally, and then raising cellular immunity and body fluid are exempted from Epidemic disease function, and the main reason for the reduction of immunologic function is body ill, aging, influence of the Eclipta prostrata to immunologic function is probably Its body-building, nourishing, the pharmacological basis of macrobiosis.
The root of kudzu vine:It is cool in nature, it is sweet, pungent, returns spleen warp, stomach, have expelling pathogenic factors from muscles and skin bring down a fever, promote the production of body fluid, promoting eruption, Shengyang Zhixie the effect of; The flavone compound contained in the root of kudzu vine, such as Puerarin, peanut element etc., have and remove oxygen radical excessive in vivo, be advantageous to Beautifying face and moistering lotion, anti-aging;Also containing elements necessary to skin such as abundant protein, amino acid, carbohydrates in the root of kudzu vine, it is also There is enhancing Abwehrkraft des Koepers, improve the function of cutaneous immunisation power, excite macrophage M4 foreign matter phagocytic function, remove poison in vivo Element, blood clean, there is certain spot-removal function.
Pseudo-ginseng:It is warm-natured, sweet, slight bitter, return liver warp, stomach, there is the effect of dissipate stasis of blood hemostasis, detumescence ding-tong;It is main in pseudo-ginseng Contain saponin(e, flavones, volatile oil, amino acid, polysaccharide, starch, protein and Inorganic chemical composition, there is good beauty and skin care to imitate Fruit, active ingredient arasaponin PNS and notoginseng diol glycosides PDS has Green Tea Extract, anti-oxidant, anti-aging work in pseudo-ginseng With flavone compound has the effect such as very strong removing free radical, anti-lipid peroxidation, anti-oxidant, in addition, containing in pseudo-ginseng A variety of essential amino acids and protein component, nutrition can be provided for skin, reduce the generation of wrinkle, skin whitening, dispel Except color spot, skin blood circulation can also be promoted, skin dark sore of releiving growth, the immunity of raising skin itself.
Radix glycyrrhizae:It is mild-natured, sweet, thoughts of returning home warp, stomach, the spleen channel, lung channel, have invigorate the spleen and benefit qi, cough-relieving apophlegmatic, emergency analgesic therapy, The effect of mediation property of medicine;The licoflavone extracted in radix glycyrrhizae has multiple efficacies in cosmetics, can uvioresistant, energy Suppressing the activity of tyrosinase, can also improve coarse, water shortage, the skin of inflammation, enoxolone can adjust the immunologic function of skin, Strengthen the resistance against diseases of skin, also acted on anti-oxidant, antiallergy, anti-inflammatory etc., effectively suppress the activation of tyrosinase, prevent The generation of melanin.
The fleece-flower root:It is warm-natured, bitter, sweet, puckery, return liver warp, kidney channel, the heart channel of Hang-Shaoyin, there is the effect of removing toxic substances, carbuncle that disappears, relax bowel; The fleece-flower root mainly contains three effective constituents:Stibene glucoside type compound, anthraquinone analog compound agent polymerization OPC, additionally Containing lecithin and various trace elements, wherein, Stibene-glucoside is distinctive active component in the fleece-flower root, is had anti-oxidant clear Except free radical, anti-aging, the effect of anti-lipid peroxidation, also enhancing is immunized, promotes adrenocortical effect.
Cactus:It is cold in nature, bitter, return stomach, there is the effect of promoting flow of qi and blood circulation, cooling blood and hemostasis, removing toxicity for detumescence;Cactus contains There are abundant protein, mineral matter, cellulose and vitamin C etc., it is also a variety of containing abundant SOD, flavonoids and polysaccharide etc. Active functional component, and aminoacid ingredient, it can remove and suppress free radical, apply it in cosmetics, can play The effects such as moisturizing, antiallergy, anti-aging and increase skin elasticity.
Rhodiola root:It is mild-natured, it is sweet, bitter, return lung warp, the heart channel of Hang-Shaoyin, there is the effect of qi and activate blood circulation, promotes blood circulation and relievings asthma.Rhodiola root Chemical composition mainly containing rhodioside, tyrosol, dendrolasin, Zang Honghua aldehyde, caffeic acid, Kaempferol, progallin A, β- Sitosterol, dibutyl phthalate, palmitic acid, cumarin, rhodiola glycosides, human body need 17 kinds of amino acid, 21 kinds Trace element and the composition such as multivitamin, volatile oil, flavones, sterol, organic acid.Rhodiola root also contains substantial amounts of manganese ion, Have the function that to promote polysaccharide polymerase activity;Rhodiola essence and rhodioloside, which have, suppresses internal collagen decomposition, makes urine Interior hydroxyproline discharge is reduced, and suppresses the effect of wrinkle generates;Also suppress the effect of tyrosine kinase activity, it is black so as to prevent The calm generation with dark brown spot of brown pigment.
Sweet Almond Oil:Pale yellow, smell delicate fragrance, quality is relaxed and comfortable soft, moist and non-greasy, extremely gently, rich in more The materials such as first unrighted acid, vitamin D, E and protein, it can relax, soft skin, moisturizing, specially control skin and itch, be red Swollen, dry and pimples.
Beneficial effect:The present invention is formulated using pure plant raw material, through reasonable compatibility, is acted synergistically between each composition, The effect of playing the promoting flow of qi and blood circulation, clearing heat for detumescence, tonifying the liver and kidney, eye circumference skin blood circulation can be promoted, strengthen cell viability, repair Multiple damaged cell simultaneously provides abundant nutritional ingredient for it, and deep layer moistens eye circumference skin, is effectively improved eye dryness, edema, pine The problems such as relaxation, desalinate microgroove, go wrinkle effect good, suitable for any skin.
Embodiment
Below, technical scheme is described in detail by specific embodiment.
Embodiment 1
A kind of pure plant moisture-keeping crease-shedding eye cream proposed by the present invention, include the raw material of following parts by weight:20 parts of orchid, the five tastes 30 parts of son, 20 parts of chamomile, 30 parts of eclipta, 17 parts of the root of kudzu vine, 25 parts of pseudo-ginseng, 14 parts of radix glycyrrhizae, 30 parts of the fleece-flower root, cactus 17 Part, 35 parts of rhodiola root, 3 parts of Sweet Almond Oil, appropriate amount of water.
The invention also provides the preparation method of above-mentioned pure plant moisture-keeping crease-shedding eye cream, comprise the following steps:
S1, fresh orchid, chamomile smashed to pieces, add 60-70% alcohol solution dippings, cold pressing is squeezed, pressed liquor is subtracted Pressure concentration removes ethanol, obtains extract solution A;
S2, cactus added water to cook into extraction, filtered, add papain and cellulase into filtrate, hydrolysis, from The heart, obtain extract solution B;
S3, by the fruit of Chinese magnoliavine, pseudo-ginseng, the fleece-flower root mix, crush, add 70% ethanol solution refluxing extraction, filtering, reclaim second Alcohol, it is dissolved in water, filters, obtain filter residue and extract solution C;
S4, by eclipta, the root of kudzu vine, radix glycyrrhizae, rhodiola root mix, crush, add S3 in filter residue, add water to cook extraction, mistake Filter, obtains extract solution D;
S5, extract solution A, extract solution B, extract solution C, extract solution D be well mixed, it is quiet that activated carbon is added into mixed liquor Put, filter, concentrate filtrate to the clear cream (60-70 DEG C) that relative density is 1.02-1.04, clear cream is cooled to 40-50 DEG C, Sweet Almond Oil is added, is stirred, cooling bottling, sealing, is produced.
Embodiment 2
A kind of pure plant moisture-keeping crease-shedding eye cream proposed by the present invention, include the raw material of following parts by weight:22 parts of orchid, the five tastes 25 parts of son, 24 parts of chamomile, 24 parts of eclipta, 20 parts of the root of kudzu vine, 18 parts of pseudo-ginseng, 20 parts of radix glycyrrhizae, 26 parts of the fleece-flower root, cactus 20 Part, 32 parts of rhodiola root, 4 parts of Sweet Almond Oil, appropriate amount of water.
The invention also provides the preparation method of above-mentioned pure plant moisture-keeping crease-shedding eye cream, comprise the following steps:
S1, fresh orchid, chamomile smashed to pieces, according to 1g:3mL solid-liquid ratio adds 60% ethanol solution, immersion 5 My god, cold pressing is squeezed, and pressed liquor is concentrated under reduced pressure and removes ethanol, obtains extract solution A;
S2, cactus is added water to cook to extraction 1h, amount of water is 5 times of cactus raw material initial mass, is filtered, to filtrate In be separately added into 0.2% papain and 0.2% cellulase for accounting for cactus quality, regulation pH is 6.0, the water at 40 DEG C 3h is solved, is centrifuged with 3000r/min rotating speed, obtains extract solution B;
S3, by the fruit of Chinese magnoliavine, pseudo-ginseng, the fleece-flower root mix, crush, add 5 times of initial gross masses of material 70% ethanol solution Refluxing extraction 2h, filtering, ethanol is reclaimed, is dissolved in water, filtered, obtain filter residue and extract solution C;
S4, by eclipta, the root of kudzu vine, radix glycyrrhizae, rhodiola root mix, crush, add S3 in filter residue, add 5 times of materials it is initial The water boiling and extraction 2h of gross mass, filtering, obtains extract solution D;
S5, extract solution A, extract solution B, extract solution C, extract solution D be well mixed, its quality is added into mixed liquor 2% activated carbon stands 3h, filtering, concentrates filtrate to the clear cream (60-70 DEG C) that relative density is 1.02, clear cream is dropped Temperature adds Sweet Almond Oil, stirred to 40 DEG C, cooling bottling, sealing, produces.
Embodiment 3
A kind of pure plant moisture-keeping crease-shedding eye cream proposed by the present invention, include the raw material of following parts by weight:28 parts of orchid, the five tastes 28 parts of son, 26 parts of chamomile, 27 parts of eclipta, 22 parts of the root of kudzu vine, 18 parts of pseudo-ginseng, 16 parts of radix glycyrrhizae, 22 parts of the fleece-flower root, cactus 20 Part, 28 parts of rhodiola root, 5 parts of Sweet Almond Oil, appropriate amount of water.
The invention also provides the preparation method of above-mentioned pure plant moisture-keeping crease-shedding eye cream, comprise the following steps:
S1, fresh orchid, chamomile smashed to pieces, according to 1g:3.5mL solid-liquid ratio adds 65% ethanol solution, immersion 6 My god, cold pressing is squeezed, and pressed liquor is concentrated under reduced pressure and removes ethanol, obtains extract solution A;
S2, cactus is added water to cook to extraction 1.5h, amount of water is 7 times of cactus raw material initial mass, is filtered, to filter 0.3% papain and 0.3% cellulase for accounting for cactus quality are separately added into liquid, regulation pH is 6.5, at 45 DEG C 4h is hydrolyzed, is centrifuged with 3300r/min rotating speed, obtains extract solution B;
S3, by the fruit of Chinese magnoliavine, pseudo-ginseng, the fleece-flower root mix, crush, add 7 times of initial gross masses of material 70% ethanol solution Refluxing extraction 2.5h, filtering, ethanol is reclaimed, is dissolved in water, filtered, obtain filter residue and extract solution C;
S4, by eclipta, the root of kudzu vine, radix glycyrrhizae, rhodiola root mix, crush, add S3 in filter residue, add 7 times of materials it is initial The water boiling and extraction 2.5h of gross mass, filtering, obtains extract solution D;
S5, extract solution A, extract solution B, extract solution C, extract solution D be well mixed, its quality is added into mixed liquor 3% activated carbon stands 4h, filtering, concentrates filtrate to the clear cream (60-70 DEG C) that relative density is 1.03, clear cream is dropped Temperature adds Sweet Almond Oil, stirred to 45 DEG C, cooling bottling, sealing, produces.
Embodiment 4
A kind of pure plant moisture-keeping crease-shedding eye cream proposed by the present invention, include the raw material of following parts by weight:25 parts of orchid, the five tastes 27 parts of son, 25 parts of chamomile, 22 parts of eclipta, 22 parts of the root of kudzu vine, 20 parts of pseudo-ginseng, 18 parts of radix glycyrrhizae, 25 parts of the fleece-flower root, cactus 22 Part, 30 parts of rhodiola root, 5 parts of Sweet Almond Oil, appropriate amount of water.
The invention also provides the preparation method of above-mentioned pure plant moisture-keeping crease-shedding eye cream, comprise the following steps:
S1, fresh orchid, chamomile smashed to pieces, according to 1g:4mL solid-liquid ratio adds 65% ethanol solution, immersion 7 My god, cold pressing is squeezed, and pressed liquor is concentrated under reduced pressure and removes ethanol, obtains extract solution A;
S2, cactus is added water to cook to extraction 1.5h, amount of water is 8 times of cactus raw material initial mass, is filtered, to filter 0.3% papain and 0.4% cellulase for accounting for cactus quality are separately added into liquid, regulation pH is 6.0, at 50 DEG C 4h is hydrolyzed, is centrifuged with 3500r/min rotating speed, obtains extract solution B;
S3, by the fruit of Chinese magnoliavine, pseudo-ginseng, the fleece-flower root mix, crush, add 8 times of initial gross masses of material 70% ethanol solution Refluxing extraction 2.5h, filtering, ethanol is reclaimed, is dissolved in water, filtered, obtain filter residue and extract solution C;
S4, by eclipta, the root of kudzu vine, radix glycyrrhizae, rhodiola root mix, crush, add S3 in filter residue, add 8 times of materials it is initial The water boiling and extraction 2.5h of gross mass, filtering, obtains extract solution D;
S5, extract solution A, extract solution B, extract solution C, extract solution D be well mixed, its quality is added into mixed liquor 2.5% activated carbon stands 5h, filtering, the clear cream (60-70 DEG C) that relative density is 1.03 is concentrated filtrate to, by clear cream 50 DEG C are cooled to, Sweet Almond Oil is added, stirs, cooling bottling, sealing, is produced.
Embodiment 5
A kind of pure plant moisture-keeping crease-shedding eye cream proposed by the present invention, include the raw material of following parts by weight:30 parts of orchid, the five tastes 22 parts of son, 30 parts of chamomile, 20 parts of eclipta, 25 parts of the root of kudzu vine, 17 parts of pseudo-ginseng, 22 parts of radix glycyrrhizae, 20 parts of the fleece-flower root, cactus 25 Part, 25 parts of rhodiola root, 6 parts of Sweet Almond Oil, appropriate amount of water.
The invention also provides the preparation method of above-mentioned pure plant moisture-keeping crease-shedding eye cream, comprise the following steps:
S1, fresh orchid, chamomile smashed to pieces, according to 1g:4mL solid-liquid ratio adds 70% ethanol solution, immersion 7 My god, cold pressing is squeezed, and pressed liquor is concentrated under reduced pressure and removes ethanol, obtains extract solution A;
S2, cactus is added water to cook to extraction 2h, amount of water is 8 times of cactus raw material initial mass, is filtered, to filtrate In be separately added into 0.5% papain and 0.5% cellulase for accounting for cactus quality, regulation pH is 6.5, the water at 50 DEG C 5h is solved, is centrifuged with 3500r/min rotating speed, obtains extract solution B;
S3, by the fruit of Chinese magnoliavine, pseudo-ginseng, the fleece-flower root mix, crush, add 8 times of initial gross masses of material 70% ethanol solution Refluxing extraction 3h, filtering, ethanol is reclaimed, is dissolved in water, filtered, obtain filter residue and extract solution C;
S4, by eclipta, the root of kudzu vine, radix glycyrrhizae, rhodiola root mix, crush, add S3 in filter residue, add 8 times of materials it is initial The water boiling and extraction 3h of gross mass, filtering, obtains extract solution D;
S5, extract solution A, extract solution B, extract solution C, extract solution D be well mixed, its quality is added into mixed liquor 4% activated carbon stands 5h, filtering, concentrates filtrate to the clear cream (60-70 DEG C) that relative density is 1.04, clear cream is dropped Temperature adds Sweet Almond Oil, stirred to 50 DEG C, cooling bottling, sealing, produces.
Performance detection is carried out to pure plant moisture-keeping crease-shedding eye cream prepared by 2-5 of the embodiment of the present invention.
First, safety evaluatio
The pure plant moisture-keeping crease-shedding eye cream prepared using 2-5 of the embodiment of the present invention carries out small white mouse safety testing.
Experimental procedure:The small white mouse 20 of health is chosen, is randomly divided into 4 groups, every group 5, using androgynous left and right sides itself Method of comparison is evaluated.Small white mouse back spinal both sides hair is shaved off with battery powered shaver first, it is 2cmx2cm to shave off area, Pure plant moisture-keeping crease-shedding eye cream prepared by embodiment 2-5 is applied to small white mouse left dorsal on plucked skin respectively, it is right Side is untreated to be compareed as self-blank, smears around area skin whether have the allergy such as redness per observation left side every other hour Phenomenon, eye cream is washed away with warm water after 24h, observe small white mouse mental status and skin appearance.
Experimental result:It is observed that small white mouse spirit is normal, without restless or depressed phenomenon, diet is normal, the skin of recipient site Skin is consistent with color and luster with right side control group skin appearance without the allergic phenomena such as erythema and oedema, illustrates that the pure plant of the present invention is protected Wet anti-wrinkle eye cream is nonirritant to mouse skin.
2nd, anti-wrinkle effect is evaluated
Pure plant moisture-keeping crease-shedding eye cream is prepared using the embodiment of the present invention 4 and carries out anti-wrinkle effect evaluation.
The women of selection 30-60 year, exclude with serious systemic disease, immune deficiency, the crowd of autoimmune disease, and Hormone medicine and immunodepressant are not used in nearly one month, selects volunteer 50 altogether, average age is early daily at 43 years old After the clean eye skin of late Qing Dynasty, appropriate eye cream is taken with finger pulp is viscous, eyes surrounding is applied to, skin is gently massaged into finger pulp and is inhaled completely Receive, be used continuously 4 weeks.High pixel phase is used using the obvious wrinkle and fine wrinkles at the canthus position before and after eye cream to subject Machine is taken pictures, and subject combines photo and using effect carries out registration scoring to the change using front and rear wrinkle, and invalid is 0 point, is gone The better score value of effect that wrinkles is higher, and highest score is 10 points.
Use result:There are 27 people very satisfied, feel and substantially desalinated using rear eye microgroove and livid ring around eye, and clearly Non-greasy, the soft and moist eye circumference of moisturizing, eye circumference of compacting skin, provide 10 points of score value;There are 11 people to feel more satisfied, provide 9 points Score value;There is the appearance that 10 people are regarded to prevent very well dry line microgroove, improve livid ring around eye, can preferably keep eye circumference position water Divide, provide 8 points of score value;Also 1 people provides 5 points of score value, and 1 is thought invalid;Evaluation is divided equally and reaches 9 points, and effect makes us full Meaning, and tested volunteer does not have a people allergic phenomena occur.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.

Claims (9)

1. a kind of pure plant moisture-keeping crease-shedding eye cream, it is characterised in that include the raw material of following parts by weight:Orchid 20-30 parts, the five tastes Sub- 22-30 parts, chamomile 20-30 parts, eclipta 20-30 parts, root of kudzu vine 17-25 parts, pseudo-ginseng 17-25 parts, radix glycyrrhizae 14-22 parts, what Tuber of multiflower knotweed 20-30 parts, cactus 17-25 parts, rhodiola root 25-35 parts, Sweet Almond Oil 3-6 parts, appropriate amount of water.
2. pure plant moisture-keeping crease-shedding eye cream according to claim 1, it is characterised in that include the raw material of following parts by weight: 25 parts of orchid, 27 parts of the fruit of Chinese magnoliavine, 25 parts of chamomile, 22 parts of eclipta, 22 parts of the root of kudzu vine, 20 parts of pseudo-ginseng, 18 parts of radix glycyrrhizae, the fleece-flower root 25 Part, 22 parts of cactus, 30 parts of rhodiola root, 5 parts of Sweet Almond Oil, appropriate amount of water.
A kind of 3. preparation method of the pure plant moisture-keeping crease-shedding eye cream based on described in claim 1 or 2, it is characterised in that including Following steps:
S1, fresh orchid, chamomile smashed to pieces, add 60-70% alcohol solution dippings, cold pressing is squeezed, pressed liquor depressurized dense Contracting removes ethanol, obtains extract solution A;
S2, cactus added water to cook into extraction, filtered, papain and cellulase are added into filtrate, hydrolyzed, centrifugation, Obtain extract solution B;
S3, by the fruit of Chinese magnoliavine, pseudo-ginseng, the fleece-flower root mix, crush, add 70% ethanol solution refluxing extraction, filtering, reclaim ethanol, It is dissolved in water, filters, obtain filter residue and extract solution C;
S4, by eclipta, the root of kudzu vine, radix glycyrrhizae, rhodiola root mix, crush, add S3 in filter residue, add water to cook extraction, filtering, obtain Extract solution D;
S5, extract solution A, extract solution B, extract solution C, extract solution D be well mixed, activated carbon is added into mixed liquor and is stood, mistake Filter, the clear cream (60-70 DEG C) that relative density is 1.02-1.04 is concentrated filtrate to, clear cream is cooled to 40-50 DEG C, added Enter Sweet Almond Oil, stir, cooling bottling, sealing, produce.
4. the preparation method of pure plant moisture-keeping crease-shedding eye cream according to claim 3, it is characterised in that, will in the S1 Fresh orchid, chamomile are smashed to pieces, according to 1g:(3-4) mL solid-liquid ratio adds 60-70% ethanol solutions, soaks 5-7 days, cold Squeezing, pressed liquor is concentrated under reduced pressure and removes ethanol, obtains extract solution A.
5. the preparation method of pure plant moisture-keeping crease-shedding eye cream according to claim 3, it is characterised in that, will in the S2 Cactus adds water to cook extraction 1-2h, and amount of water is 5-8 times of cactus raw material initial mass, filtering, wood is added into filtrate Melon protease and cellulase, regulation pH are 6.0-6.5,3-5h are hydrolyzed at 40-50 DEG C, with 3000-3500r/min rotating speed Centrifugation, obtains extract solution B.
6. the preparation method of pure plant moisture-keeping crease-shedding eye cream according to claim 5, it is characterised in that the Papain The addition of enzyme is the 0.2-0.5% of cactus quality, and the addition of cellulase is the 0.2-0.5% of cactus quality.
7. the preparation method of pure plant moisture-keeping crease-shedding eye cream according to claim 3, it is characterised in that, will in the S3 The fruit of Chinese magnoliavine, pseudo-ginseng, fleece-flower root mixing, crush, add 70% ethanol solution refluxing extraction 2- of the initial gross mass of 5-8 times of material 3h, filtering, ethanol is reclaimed, is dissolved in water, filtered, obtain filter residue and extract solution C.
8. the preparation method of pure plant moisture-keeping crease-shedding eye cream according to claim 3, it is characterised in that, will in the S4 Eclipta, the root of kudzu vine, radix glycyrrhizae, rhodiola root mixing, crush, the filter residue added in S3, add the decocting of the initial gross mass of 5-8 times of material Extraction 2-3h is boiled, filtering, obtains extract solution D.
9. the preparation method of pure plant moisture-keeping crease-shedding eye cream according to claim 3, it is characterised in that, will in the S5 Extract solution A, extract solution B, extract solution C, extract solution D are well mixed, and the activated carbon that the 2-4% of its quality is added into mixed liquor is quiet 3-5h is put, is filtered.
CN201711189922.1A 2017-11-24 2017-11-24 A kind of pure plant moisture-keeping crease-shedding eye cream and preparation method thereof Withdrawn CN107714555A (en)

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CN108272683A (en) * 2018-03-30 2018-07-13 深圳市芭格美生物科技有限公司 A kind of biological enzyme processing and corrosion-resistant moisturizing plant extraction liquid and the preparation method and application thereof

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CN104771347A (en) * 2015-03-19 2015-07-15 苏州谷力生物科技有限公司 Eye cream and preparation method thereof
CN105534854A (en) * 2015-12-30 2016-05-04 殷志杰 Eye cream for removing crow's feet and under-eye bags and preparation method thereof
CN106852760A (en) * 2016-12-08 2017-06-16 长沙协浩吉生物工程有限公司 A kind of compound method of nti-freckle eye cream
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Publication number Priority date Publication date Assignee Title
CN1931125A (en) * 2006-09-20 2007-03-21 蔡世珍 Eye cream and its prepn process
CN104688645A (en) * 2013-12-09 2015-06-10 吴胜 Wrinkle reducing eye cream
CN104688643A (en) * 2013-12-09 2015-06-10 吴胜 Pure nature plant eye cream
CN104771347A (en) * 2015-03-19 2015-07-15 苏州谷力生物科技有限公司 Eye cream and preparation method thereof
CN105534854A (en) * 2015-12-30 2016-05-04 殷志杰 Eye cream for removing crow's feet and under-eye bags and preparation method thereof
CN106852760A (en) * 2016-12-08 2017-06-16 长沙协浩吉生物工程有限公司 A kind of compound method of nti-freckle eye cream
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108272683A (en) * 2018-03-30 2018-07-13 深圳市芭格美生物科技有限公司 A kind of biological enzyme processing and corrosion-resistant moisturizing plant extraction liquid and the preparation method and application thereof

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Application publication date: 20180223