CN107691877A - A kind of preparation method of the fresh-water fishes microcapsules opening material of zero starch - Google Patents
A kind of preparation method of the fresh-water fishes microcapsules opening material of zero starch Download PDFInfo
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- CN107691877A CN107691877A CN201710600401.4A CN201710600401A CN107691877A CN 107691877 A CN107691877 A CN 107691877A CN 201710600401 A CN201710600401 A CN 201710600401A CN 107691877 A CN107691877 A CN 107691877A
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- Prior art keywords
- raw material
- preparation
- microcapsules
- fresh
- opening material
- Prior art date
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- 239000003094 microcapsule Substances 0.000 title claims abstract description 85
- 239000000463 material Substances 0.000 title claims abstract description 72
- 241000251468 Actinopterygii Species 0.000 title claims abstract description 55
- 239000013505 freshwater Substances 0.000 title claims abstract description 52
- 238000002360 preparation method Methods 0.000 title claims abstract description 32
- 229920002472 Starch Polymers 0.000 title claims abstract description 18
- 235000019698 starch Nutrition 0.000 title claims abstract description 18
- 239000008107 starch Substances 0.000 title claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 67
- UYXTWWCETRIEDR-UHFFFAOYSA-N Tributyrin Chemical compound CCCC(=O)OCC(OC(=O)CCC)COC(=O)CCC UYXTWWCETRIEDR-UHFFFAOYSA-N 0.000 claims abstract description 50
- 102000004169 proteins and genes Human genes 0.000 claims abstract description 45
- 108090000623 proteins and genes Proteins 0.000 claims abstract description 45
- 239000002131 composite material Substances 0.000 claims abstract description 30
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 30
- 239000011707 mineral Substances 0.000 claims abstract description 30
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 claims abstract description 27
- 229930003944 flavone Natural products 0.000 claims abstract description 27
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- 235000011949 flavones Nutrition 0.000 claims abstract description 27
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 claims abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000005507 spraying Methods 0.000 claims abstract description 15
- -1 B B-complex Substances 0.000 claims abstract description 10
- 239000003595 mist Substances 0.000 claims abstract description 10
- 238000000227 grinding Methods 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 8
- 238000004513 sizing Methods 0.000 claims abstract description 8
- 238000001035 drying Methods 0.000 claims abstract description 5
- 239000000843 powder Substances 0.000 claims description 41
- 235000019733 Fish meal Nutrition 0.000 claims description 23
- 239000004467 fishmeal Substances 0.000 claims description 23
- 241001481656 Stratiomyidae Species 0.000 claims description 21
- 239000005862 Whey Substances 0.000 claims description 20
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- 241000195493 Cryptophyta Species 0.000 claims description 18
- 235000011803 sesame oil Nutrition 0.000 claims description 18
- 239000008159 sesame oil Substances 0.000 claims description 18
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- 238000001816 cooling Methods 0.000 abstract description 6
- 102000008186 Collagen Human genes 0.000 abstract description 4
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- 108010010803 Gelatin Proteins 0.000 abstract description 4
- 229920001436 collagen Polymers 0.000 abstract description 4
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- 235000019322 gelatine Nutrition 0.000 abstract description 4
- 235000011852 gelatine desserts Nutrition 0.000 abstract description 4
- 239000005667 attractant Substances 0.000 abstract description 3
- 230000031902 chemoattractant activity Effects 0.000 abstract description 3
- 235000008935 nutritious Nutrition 0.000 abstract description 3
- 239000002699 waste material Substances 0.000 abstract description 3
- 230000015572 biosynthetic process Effects 0.000 abstract 1
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- 239000002253 acid Substances 0.000 description 3
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- 230000001488 breeding effect Effects 0.000 description 3
- 239000002775 capsule Substances 0.000 description 3
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- 235000016709 nutrition Nutrition 0.000 description 3
- 230000035764 nutrition Effects 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 239000006054 starter diet Substances 0.000 description 3
- YBJHBAHKTGYVGT-ZKWXMUAHSA-N (+)-Biotin Chemical compound N1C(=O)N[C@@H]2[C@H](CCCCC(=O)O)SC[C@@H]21 YBJHBAHKTGYVGT-ZKWXMUAHSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 241000755266 Kathetostoma giganteum Species 0.000 description 2
- PVNIIMVLHYAWGP-UHFFFAOYSA-N Niacin Chemical compound OC(=O)C1=CC=CN=C1 PVNIIMVLHYAWGP-UHFFFAOYSA-N 0.000 description 2
- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 description 2
- 150000001336 alkenes Chemical class 0.000 description 2
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- 235000009508 confectionery Nutrition 0.000 description 2
- 238000012258 culturing Methods 0.000 description 2
- 238000004945 emulsification Methods 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 241000894007 species Species 0.000 description 2
- 241001519451 Abramis brama Species 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 206010003210 Arteriosclerosis Diseases 0.000 description 1
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- 241001609213 Carassius carassius Species 0.000 description 1
- 241000252185 Cobitidae Species 0.000 description 1
- 235000019750 Crude protein Nutrition 0.000 description 1
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 description 1
- 241000252210 Cyprinidae Species 0.000 description 1
- AUNGANRZJHBGPY-UHFFFAOYSA-N D-Lyxoflavin Natural products OCC(O)C(O)C(O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-UHFFFAOYSA-N 0.000 description 1
- ZAKOWWREFLAJOT-CEFNRUSXSA-N D-alpha-tocopherylacetate Chemical compound CC(=O)OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-CEFNRUSXSA-N 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- SQUHHTBVTRBESD-UHFFFAOYSA-N Hexa-Ac-myo-Inositol Natural products CC(=O)OC1C(OC(C)=O)C(OC(C)=O)C(OC(C)=O)C(OC(C)=O)C1OC(C)=O SQUHHTBVTRBESD-UHFFFAOYSA-N 0.000 description 1
- FFEARJCKVFRZRR-BYPYZUCNSA-N L-methionine Chemical compound CSCC[C@H](N)C(O)=O FFEARJCKVFRZRR-BYPYZUCNSA-N 0.000 description 1
- JLVVSXFLKOJNIY-UHFFFAOYSA-N Magnesium ion Chemical compound [Mg+2] JLVVSXFLKOJNIY-UHFFFAOYSA-N 0.000 description 1
- 241000361919 Metaphire sieboldi Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 241001275898 Mylopharyngodon piceus Species 0.000 description 1
- 241000700141 Rotifera Species 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- 241000207961 Sesamum Species 0.000 description 1
- 235000003434 Sesamum indicum Nutrition 0.000 description 1
- PTFCDOFLOPIGGS-UHFFFAOYSA-N Zinc dication Chemical compound [Zn+2] PTFCDOFLOPIGGS-UHFFFAOYSA-N 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 235000021120 animal protein Nutrition 0.000 description 1
- 208000011775 arteriosclerosis disease Diseases 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 229960002685 biotin Drugs 0.000 description 1
- 235000020958 biotin Nutrition 0.000 description 1
- 239000011616 biotin Substances 0.000 description 1
- FAPWYRCQGJNNSJ-UBKPKTQASA-L calcium D-pantothenic acid Chemical compound [Ca+2].OCC(C)(C)[C@@H](O)C(=O)NCCC([O-])=O.OCC(C)(C)[C@@H](O)C(=O)NCCC([O-])=O FAPWYRCQGJNNSJ-UBKPKTQASA-L 0.000 description 1
- 229960002079 calcium pantothenate Drugs 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 229910001429 cobalt ion Inorganic materials 0.000 description 1
- XLJKHNWPARRRJB-UHFFFAOYSA-N cobalt(2+) Chemical compound [Co+2] XLJKHNWPARRRJB-UHFFFAOYSA-N 0.000 description 1
- AGVAZMGAQJOSFJ-WZHZPDAFSA-M cobalt(2+);[(2r,3s,4r,5s)-5-(5,6-dimethylbenzimidazol-1-yl)-4-hydroxy-2-(hydroxymethyl)oxolan-3-yl] [(2r)-1-[3-[(1r,2r,3r,4z,7s,9z,12s,13s,14z,17s,18s,19r)-2,13,18-tris(2-amino-2-oxoethyl)-7,12,17-tris(3-amino-3-oxopropyl)-3,5,8,8,13,15,18,19-octamethyl-2 Chemical compound [Co+2].N#[C-].[N-]([C@@H]1[C@H](CC(N)=O)[C@@]2(C)CCC(=O)NC[C@@H](C)OP(O)(=O)O[C@H]3[C@H]([C@H](O[C@@H]3CO)N3C4=CC(C)=C(C)C=C4N=C3)O)\C2=C(C)/C([C@H](C\2(C)C)CCC(N)=O)=N/C/2=C\C([C@H]([C@@]/2(CC(N)=O)C)CCC(N)=O)=N\C\2=C(C)/C2=N[C@]1(C)[C@@](C)(CC(N)=O)[C@@H]2CCC(N)=O AGVAZMGAQJOSFJ-WZHZPDAFSA-M 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
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- 239000013078 crystal Substances 0.000 description 1
- ZAKOWWREFLAJOT-UHFFFAOYSA-N d-alpha-Tocopheryl acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-UHFFFAOYSA-N 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 235000008242 dietary patterns Nutrition 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 210000002969 egg yolk Anatomy 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000009313 farming Methods 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 235000021393 food security Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000003862 health status Effects 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 229960000367 inositol Drugs 0.000 description 1
- CDAISMWEOUEBRE-GPIVLXJGSA-N inositol Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@H](O)[C@@H]1O CDAISMWEOUEBRE-GPIVLXJGSA-N 0.000 description 1
- XMBWDFGMSWQBCA-UHFFFAOYSA-M iodide Chemical compound [I-] XMBWDFGMSWQBCA-UHFFFAOYSA-M 0.000 description 1
- 229940006461 iodide ion Drugs 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910001425 magnesium ion Inorganic materials 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 229930182817 methionine Natural products 0.000 description 1
- 238000000386 microscopy Methods 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 229960003512 nicotinic acid Drugs 0.000 description 1
- 235000001968 nicotinic acid Nutrition 0.000 description 1
- 239000011664 nicotinic acid Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 235000020777 polyunsaturated fatty acids Nutrition 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- ZUFQODAHGAHPFQ-UHFFFAOYSA-N pyridoxine hydrochloride Chemical compound Cl.CC1=NC=C(CO)C(CO)=C1O ZUFQODAHGAHPFQ-UHFFFAOYSA-N 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000001846 repelling effect Effects 0.000 description 1
- 229960002477 riboflavin Drugs 0.000 description 1
- 235000019192 riboflavin Nutrition 0.000 description 1
- 239000002151 riboflavin Substances 0.000 description 1
- CDAISMWEOUEBRE-UHFFFAOYSA-N scyllo-inosotol Natural products OC1C(O)C(O)C(O)C(O)C1O CDAISMWEOUEBRE-UHFFFAOYSA-N 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 229940042585 tocopherol acetate Drugs 0.000 description 1
- 239000011691 vitamin B1 Substances 0.000 description 1
- 239000011715 vitamin B12 Substances 0.000 description 1
- 239000011647 vitamin D3 Substances 0.000 description 1
- QYSXJUFSXHHAJI-YRZJJWOYSA-N vitamin D3 Chemical compound C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C\C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-YRZJJWOYSA-N 0.000 description 1
- 239000011652 vitamin K3 Substances 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/10—Animal feeding-stuffs obtained by microbiological or biochemical processes
- A23K10/16—Addition of microorganisms or extracts thereof, e.g. single-cell proteins, to feeding-stuff compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/20—Animal feeding-stuffs from material of animal origin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/20—Animal feeding-stuffs from material of animal origin
- A23K10/22—Animal feeding-stuffs from material of animal origin from fish
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/116—Heterocyclic compounds
- A23K20/121—Heterocyclic compounds containing oxygen or sulfur as hetero atom
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/142—Amino acids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/142—Amino acids; Derivatives thereof
- A23K20/147—Polymeric derivatives, e.g. peptides or proteins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/158—Fatty acids; Fats; Products containing oils or fats
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/174—Vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/24—Compounds of alkaline earth metals, e.g. magnesium
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/30—Oligoelements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K40/00—Shaping or working-up of animal feeding-stuffs
- A23K40/30—Shaping or working-up of animal feeding-stuffs by encapsulating; by coating
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/80—Feeding-stuffs specially adapted for particular animals for aquatic animals, e.g. fish, crustaceans or molluscs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Zoology (AREA)
- Animal Husbandry (AREA)
- Biomedical Technology (AREA)
- Physiology (AREA)
- Health & Medical Sciences (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Biotechnology (AREA)
- Molecular Biology (AREA)
- Microbiology (AREA)
- Marine Sciences & Fisheries (AREA)
- Inorganic Chemistry (AREA)
- Biochemistry (AREA)
- Insects & Arthropods (AREA)
- Birds (AREA)
- Feed For Specific Animals (AREA)
- Fodder In General (AREA)
Abstract
The invention discloses a kind of preparation method of the fresh-water fishes microcapsules opening material of zero starch, the raw material that the microcapsules opening material is made up of following mass percent component is prepared：Protein sources raw material 75%~85%, fat source raw material 11~23%, B B-complex 0.5~1%, composite mineral matter 0.5~1%, tributyrin 0.5~1%, vine tea flavone 0.5~1%；By protein sources raw material ultramicro grinding into after the micro mist of 325~450 mesh, it is sufficiently mixed with fat source raw material, B B-complex, composite mineral matter, tributyrin, vine tea flavone；Add water to emulsify 10~20min after sizing mixing, be prepared into 20~35% underflow, homogeneous under the conditions of 10~20MPa；Microcapsules opening material is obtained after spraying, drying, sub-sieve, cooling.The present invention need not additionally add any wall material（Such as starch or gelatin）, but it is wrapped in other raw materials formation microcapsule granule by the colloid of collagen in protein sources raw material.Moreover, obtained opening material is not only nutritious, attractant is good, and feed waste will not be produced so as to polluted-water and environment.
Description
Technical field
The present invention relates to aquatic feeds field, in particular it relates to aquatic products opening material technical field, more particularly, to one
The preparation method of the fresh-water fishes microcapsules opening material of zero starch of kind.
Background technology
In a broad sense, the fish that meaning can live in the fresh water that salinity is 3/1000ths just can be described as fresh water to fresh-water fishes
Fish.Narrow sense says, means in its history of life part stage such as only young stage or adult fish phase, or throughout one's life all must be
The fish tided in fresh water.Known fish there are about kind more than 26000 in the world, and fresh-water fishes there are about more than 8600 and plant.China fresh-water fishes
Class there are about more than 800 and plant.Wherein, Cyprinidae category kind is most, has more than 400 to plant, accounts for the half of whole fresh-water fishes, Nian sections and Cobitidae
Category kind it is quite a few, two sections share more than 200 and planted, and account for a quarter of whole fresh-water fishes, and the gill closes in other sections such as Xia Hu sections, murrel section
Ke Deng sections share more than 200 and planted, and account for a quarter of whole fresh-water fishes.
Large freshwater fish mainly includes 7 black carp, grass carp, silver carp, flathead, carp, crucian carp, triangular bream kinds, and this seven big kind is China
Main aquaculture kind, its cultured output account for the larger specific gravity of inland aquaculture yield, are the important sets of China's food security
Into part, and one of main source of animal protein, important position is occupied in the eating patterns of our people.According to
Statistics is shown within 2008, and national freshwater aquiculture total output is 20,720,000 tons, and the total output of above-mentioned seven kinds of fishes is 14,450,000
Ton, accounts for the 70% of national freshwater aquiculture total output.Wherein, grass carp, silver carp, carp and flathead yield occupy me respectively more than 2,200,000 tons
First four of state's fish culture kind.Silver carp, bighead are the important kinds of freshwater aquiculture, and it is required to contain substantial amounts of n-6 in its muscle
The n-3 series fatty acids of aliphatic acid and anti arteriosclerosis.Silver carp, bighead are rich in the olefin(e) acid of 20 carbon 5 and the olefin(e) acid of 22 carbon 6, and grass carp, carp are rich
Polyunsaturated fatty acid containing n-3.Experiment proves：It is beneficial to health to often eat silver carp, bighead, can prevention of arterial hardening, it is especially right
Cardiovascular patient has good effect.
Because fresh-water fishes generally inhabit inland waters, its living environment is easily by the shadow of outside environmental elements
Ring, such as economic development, population increase, environmental pollution, estrepement, build excessively, build a dam, arbitrarily introduce non-local kind, excessive capture
Problem.So high density, intensive fresh-water fishes artificial farming industry are in the ascendant, and still, high density, intensive marine fish culture
The drawbacks of, cause the bearing capacity of breeding water body to greatly exceed its natural bearing capacity, thus cause the immunity function of fresh-water fishes
Decline with anti-stress ability, the death rate remains high in breeding process.In order to reduce the death rate in breeding process, scholars from
Each stage start strengthen fresh-water fishes immunity function and anti-stress ability, picked up since fry be freshwater fish culturing pass
Key.
The health status of fry and the opening material nutrient of early stage are closely bound up, when opening material is that animal seed ingests for the first time
The bait eaten, at present in freshwater fish culturing industry, the opening material of fry is generally wheel animalcule, water silk earthworm powder, yolk, soya-bean milk and microalgae
Deng bait, because water repelling property of these bait in water is poor, spread rapidly after putting into water, most of bait can not be by
Fresh-water fishes predation is arrived, and is caused that bait utilization is low, nutritive loss is big, is made food nutrition incomplete, influence the fresh-water fishes speed of growth, reach
Less than the purpose of fast long high yield；Simultaneously because the composition of bait is substantially organic matter, the easy contaminant water of the bait being so lost in
Matter, deteriorate aquifer cultivation environment.Therefore, for crayfish culture industry, it is badly in need of a kind of comprehensive and environmentally friendly commercialization fresh water of nutrition
Fish opening material.
The content of the invention
In order to overcome the above-mentioned deficiency of prior art, the present invention provides a kind of fresh-water fishes microcapsules opening material of zero starch
Preparation method, this method need not additionally add any wall material（Such as starch or gelatin）, but by glue in protein sources raw material
The colloid of former albumen is wrapped in other raw materials and forms microcapsule granule.Moreover, obtained opening material is not only nutritious, attractant
It is good, and feed waste will not be produced so as to polluted-water and environment.
In order to solve the above technical problems, the technical solution adopted by the present invention is：
A kind of preparation method of the fresh-water fishes microcapsules opening material of zero starch, the microcapsules opening material is by following mass percent
The raw material of component composition is prepared：Protein sources raw material 75%~85%, fat source raw material 11~23%, B B-complex 0.5~
1%, composite mineral matter 0.5~1%, tributyrin 0.5~1%, vine tea flavone 0.5~1%；Wherein, the protein sources are former
Material is made up of fish meal, PURE WHEY, dephenolization cottonseed protein, black soldier flies larva powder；
The preparation method of the microcapsules opening material comprises the following steps：By protein sources raw material ultramicro grinding into 325~450 purposes
After micro mist, it is sufficiently mixed with fat source raw material, B B-complex, composite mineral matter, tributyrin, vine tea flavone；Add water
10~20min is emulsified after sizing mixing, is prepared into 20~35% underflow, homogeneous under the conditions of 10~20MPa；It is spraying, drying, sub-sieve, cold
But microcapsules opening material is obtained afterwards.
The present invention by the grinding particle size of the accurate content and protein sources raw material for controlling protein sources raw material, then in conjunction with
Suitable granulating process（Emulsification times, underflow concentration, homogenization pressure etc.）, it is possible to achieve it need not additionally add wall material（As formed sediment
Powder or gelatin etc.）, but rely on the colloid in protein sources raw material to be wrapped in other raw materials and form microcapsule granule.
If the dosage of protein sources raw material cannot be guaranteed at least 75%, the glue of protein sources raw material self collagen albumen
Matter content cannot just be wrapped in other raw materials and form microcapsule granule, therefore, granulation would not succeed with regard to inadequate.But pelletize
While must also consider demand of the fresh-water fishes fry opening for nutrition, so, the species of protein sources raw material and fat source and
Dosage must be integrated to determine.
Preferably, the raw material that the microcapsules opening material is made up of following mass percent component is prepared：Protein sources
Raw material 80%, fat source raw material 16%, B B-complex 1%, composite mineral matter 1%, tributyrin 1%, vine tea flavone 1%.
Preferably, the fish meal：PURE WHEY：Dephenolization cottonseed protein：The mass ratio of black soldier flies larva powder is 1：1~2：
1：1~2.
It is highly preferred that the fish meal：PURE WHEY：Dephenolization cottonseed protein：The mass ratio of black soldier flies larva powder is 1：2：
1：1.
Preferably, the fat source raw material is formed by splitting kettle algae powder and sesame oil.
It is highly preferred that it is described split kettle algae powder and account for microcapsules opening material feedstuff quality 6~12%, sesame oil accounts for micro- glue
The 5~11% of capsule opening material feedstuff quality.
Preferably, EAT is 180~230 DEG C during the spraying, and leaving air temp is 100~120 DEG C.
Preferably, the temperature of the drying is 100~150 DEG C.
The composition composition of the B B-complex is by weight generally：Vitamin B10.025wt%, riboflavin 0.1wt%,
Vitamin B6Hydrochloride 0.075wt%, nicotinic acid 0.25wt%, inositol 39.9wt%, calcium pantothenate 0.5wt%, biotin 0.25wt%, leaf
Sour 0.025wt%, vitamin K30.5wt%, vitamin B12 0.25wt%, vitamine A acetate 0.25wt%, vitamin D3
0.625wt%, vitamin E acetate 7.25wt%, media fibers element 50wt%.
Composite mineral matter of the present invention is the conventional use of composite mineral salt in aquatic feeds field, the composite mineral salt
Composition composition by weight generally：Magnesium ion >=1wt%, iron ion >=0.2wt%, iodide ion >=0.08wt%, copper ion >=
0.3wt%, zinc ion >=2wt%, plasma selenium >=0.004wt%, cobalt ions >=0.022wt%.
Compared with prior art, the beneficial effects of the invention are as follows：
The present invention need not additionally add any wall material（Such as starch or gelatin）, but by collagen in protein sources raw material
Colloid be wrapped in other raw materials formed microcapsule granule.Moreover, obtained opening material is not only nutritious, attractant is good, and
And feed waste will not be produced so as to polluted-water and environment.
Embodiment
Further elaborated with reference to saying that specific embodiment is made to the present invention, the embodiment is served only for explaining
The present invention, it is not intended to limit the scope of the present invention.Test method used in following embodiments is unless otherwise specified
Conventional method；Used material, reagent etc., unless otherwise specified, for the reagent and material commercially obtained.
Embodiment 1
A kind of fresh-water fishes microcapsules opening material of zero starch, the microcapsules opening material are made up of following mass percent component
Raw material is prepared：Fish meal 15%, PURE WHEY 30%, dephenolization cottonseed protein 15%, black soldier flies larva powder 15%, split kettle algae powder
11%th, sesame oil 10%, B B-complex 1%, composite mineral matter 1%, tributyrin 1%, vine tea flavone 1%.
The preparation method of the microcapsules opening material comprises the following steps：By protein sources raw material ultramicro grinding into 400 purposes
After micro mist, it is sufficiently mixed with fat source raw material, B B-complex, composite mineral matter, tributyrin, vine tea flavone；Add water
15min is emulsified after sizing mixing, is prepared into 30% underflow, homogeneous under the conditions of 15MPa；(EAT is 210 DEG C during spraying, is gone out for spraying
Air temperature is 110 DEG C), dry (dry temperature be 120 DEG C), sub-sieve, microcapsules opening material obtained after cooling.The yield of microcapsules
For 83%, microcapsule embedded rate is 82%.
Embodiment 2
A kind of fresh-water fishes microcapsules opening material of zero starch, the microcapsules opening material are made up of following mass percent component
Raw material is prepared：Fish meal 16%, PURE WHEY 32%, dephenolization cottonseed protein 16%, black soldier flies larva powder 16%, split kettle algae powder
8%th, sesame oil 8%, B B-complex 1%, composite mineral matter 1%, tributyrin 1%, vine tea flavone 1%.
The preparation method of the microcapsules opening material comprises the following steps：By protein sources raw material ultramicro grinding into 400 purposes
After micro mist, it is sufficiently mixed with fat source raw material, B B-complex, composite mineral matter, tributyrin, vine tea flavone；Add water
15min is emulsified after sizing mixing, is prepared into 30% underflow, homogeneous under the conditions of 15MPa；(EAT is 210 DEG C during spraying, is gone out for spraying
Air temperature is 110 DEG C), dry (dry temperature be 120 DEG C), sub-sieve, microcapsules opening material obtained after cooling.The yield of microcapsules
For 94%, microcapsule embedded rate is 94%.
Embodiment 3
A kind of fresh-water fishes microcapsules opening material of zero starch, the microcapsules opening material are made up of following mass percent component
Raw material is prepared：Fish meal 17%, PURE WHEY 34%, dephenolization cottonseed protein 17%, black soldier flies larva powder 17%, split kettle algae powder
6%th, sesame oil 5%, B B-complex 1%, composite mineral matter 1%, tributyrin 1%, vine tea flavone 1%.
The preparation method of the microcapsules opening material comprises the following steps：By protein sources raw material ultramicro grinding into 400 purposes
After micro mist, it is sufficiently mixed with fat source raw material, B B-complex, composite mineral matter, tributyrin, vine tea flavone；Add water
15min is emulsified after sizing mixing, is prepared into 30% underflow, homogeneous under the conditions of 15MPa；(EAT is 210 DEG C during spraying, is gone out for spraying
Air temperature is 110 DEG C), dry (dry temperature be 120 DEG C), sub-sieve, microcapsules opening material obtained after cooling.The yield of microcapsules
For 85%, microcapsule embedded rate is 86%.
Embodiment 4
A kind of fresh-water fishes microcapsules opening material of zero starch, the microcapsules opening material are made up of following mass percent component
Raw material is prepared：Fish meal 20%, PURE WHEY 20%, dephenolization cottonseed protein 20%, black soldier flies larva powder 20%, split kettle algae powder
9%th, sesame oil 8%, B B-complex 1%, composite mineral matter 1%, tributyrin 0.5%, vine tea flavone 0.5%.
The preparation method of the microcapsules opening material comprises the following steps：By protein sources raw material ultramicro grinding into 325 purposes
After micro mist, it is sufficiently mixed with fat source raw material, B B-complex, composite mineral matter, tributyrin, vine tea flavone；Add water
10min is emulsified after sizing mixing, is prepared into 25% underflow, homogeneous under the conditions of 10MPa；(EAT is 230 DEG C during spraying, is gone out for spraying
Air temperature is 120 DEG C), dry (dry temperature be 120 DEG C), sub-sieve, microcapsules opening material obtained after cooling.The yield of microcapsules
For 81%, microcapsule embedded rate is 80%.
Embodiment 5
A kind of fresh-water fishes microcapsules opening material of zero starch, the microcapsules opening material are made up of following mass percent component
Raw material is prepared：Fish meal 20%, PURE WHEY 20%, dephenolization cottonseed protein 20%, black soldier flies larva powder 20%, split kettle algae powder
9%th, sesame oil 8%, B B-complex 0.5%, composite mineral matter 0.5%, tributyrin 1%, vine tea flavone 1%.
The preparation method of the microcapsules opening material comprises the following steps：By protein sources raw material ultramicro grinding into 450 purposes
After micro mist, it is sufficiently mixed with fat source raw material, B B-complex, composite mineral matter, tributyrin, vine tea flavone；Add water
20min is emulsified after sizing mixing, is prepared into 35% underflow, homogeneous under the conditions of 20MPa；(EAT is 180 DEG C during spraying, is gone out for spraying
Air temperature is 100 DEG C), dry (dry temperature be 110 DEG C), sub-sieve, microcapsules opening material obtained after cooling.The yield of microcapsules
For 88%, microcapsule embedded rate is 87%.
Comparative example 1
A kind of fresh-water fishes microcapsules opening material of zero starch, preparation method with embodiment 2, it is unique from embodiment 2 unlike raise
Expect that the composition of raw material is different.This comparative example sets the formula that two kinds of raw materials form.
Formula 1 is made up of the raw material of following mass percent：Fish meal 14%, PURE WHEY 28%, dephenolization cottonseed protein
14%th, black soldier flies larva powder 14%, split kettle algae powder 14%, sesame oil 14%, B B-complex 1%, composite mineral matter 1%, three butyric acid are sweet
Grease 1%, vine tea flavone 1%.The yield for the microcapsules that formula 1 is prepared is 61%, and microcapsule embedded rate is 60%.Because match somebody with somebody
The dosage of the protein sources raw material of side 1 is only 70%, and the gum level of protein sources raw material self collagen albumen is insufficient, Wu Fachong
Divide and other raw materials are wrapped to form microcapsule granule, therefore, prepare the poor effect of microcapsules.
Formula 2 is made up of the raw material of following mass percent：Fish meal 10%, PURE WHEY 20%, dephenolization cottonseed protein
10%th, black soldier flies larva powder 10%, split kettle algae powder 24%, sesame oil 22%, B B-complex 1%, composite mineral matter 1%, three butyric acid are sweet
Grease 1%, vine tea flavone 1%.Microcapsule granule can not be prepared in formula 2 at all.
Comparative example 2
A kind of fresh-water fishes microcapsules opening material of zero starch, the composition of feedstuff are uniquely different from embodiment 2 with embodiment 2
The preparation method for being microcapsules, this comparative example set 4 kinds of different preparation methods.
Processing 1：Basic preparation process is to surpass protein sources raw material with embodiment 2 from the unique different place of embodiment 2
Micro mist is broken into the micro mist of 300 mesh；The yield for the microcapsules that processing 1 is prepared is 70%, and microcapsule embedded rate is 70%.
Processing 2：Basic preparation process is that the concentration of slurries is with embodiment 2 from the unique different place of embodiment 2
15%；The yield for the microcapsules that processing 2 is prepared is 79%, and microcapsule embedded rate is 78%.
Processing 3：Basic preparation process is that emulsification times are with embodiment 2 from the unique different place of embodiment 2
25min；The yield for the microcapsules that processing 3 is prepared is 86%, and microcapsule embedded rate is 85%.
Processing 4：Basic preparation process is under the conditions of 25MPa with embodiment 2 from the unique different place of embodiment 2
Matter；The yield for the microcapsules that processing 4 is prepared is 89%, and microcapsule embedded rate is 89%.
Comparative example 3
A kind of fresh-water fishes microcapsules opening material of zero starch, preparation method with embodiment 2, it is unique from embodiment 2 unlike raise
Expect that the composition of raw material is different.This comparative example sets the formula that 7 kinds of raw materials form.
Formula 1：It is made up of the raw material of following mass percent：Fish meal 32%, PURE WHEY 32%, dephenolization cottonseed protein
16%th, kettle algae powder 8%, sesame oil 8%, B B-complex 1%, composite mineral matter 1%, tributyrin 1%, vine tea flavone are split
1%。
The yield for the microcapsules that formula 1 is prepared is 89%, and microcapsule embedded rate is 88%.Can be with by the result of formula 1
Find out, it is micro- if black soldier flies larva powder is replaced with into fish meal although the crude protein content of fish meal is more than black soldier flies larva powder
The yield and embedding rate of capsule can be reduced accordingly, may is that the reason for reduction amino acid classes that black soldier flies larva powder contains and
The species of amino acid contained by fish meal is dramatically different, and the amino acid in black soldier flies larva powder is more suitable for the crosslinking during coating
Reaction, so as to cause the two difference occur in the yield of microcapsules and embedding rate.
Formula 2：Fish meal 32%, PURE WHEY 32%, black soldier flies larva powder 16%, split kettle algae powder 8%, be sesame oil 8%, compound
Vitamin 1%, composite mineral matter 1%, tributyrin 1%, vine tea flavone 1%.
The yield and embedding rate for the microcapsules that formula 2 is prepared do not have difference compared with Example 2, but respectively with real
The microcapsules opening material for applying example 2 and the preparation of this comparative example formula 2 goes to feed fresh-water fishes seedling, comprises the following steps that：To fully it expose
The running water of gas is added in 10 1000ml beaker.First every group of thermohaline is all adjusted in preset level before the test,
Micro- inflation.The salinity of each test combinations is regulated and controled with sea crystal, and since 6ppt, 4ppt was raised and lowered every 2 hours, until
The salinity setting reached needed for each combination is horizontal.To ensure temperature controllable precise, all test combinations are set up in salinity levels
Illumination box (MGC types) progress is placed on after.Temperature reduces by 2.0 DEG C since 20 DEG C, every 2 hours.By seedling according to this
It is put into the 1000ml of combinations thereof beaker, 100 tails is put in each beaker, altogether 1000 tails or so, the light intensity cycle is 24L:
0D.It is 7.5~8.0 to measure other factors pH in water body environment simultaneously, dissolved oxygen amount 6.0mg/L.The measure of aperture opening ratio, from the 4th
My god feed micro-capsule starter diet (seedling is open on the 4th day typically after the membrane), feed within one day 8 times, 1 hour after feeding every time
Start to measure each group aperture opening ratio, 30 tail prelarvas are taken from each beaker, its situation of ingesting of microscopy, calculate aperture opening ratio.Aperture opening ratio is surveyed
Fixed (to be all open within the 6th day) for final statistical result with the 5th day, result of the test takes its average value.（Aperture opening ratio（%）=opening
Total mantissa × 100% of mantissa/measure）；As a result the aperture opening ratio for finding the opening material nursing fresh-water fishes of embodiment 2 is 97%, and is formulated 2
Opening material feed fresh-water fishes aperture opening ratio be 91%.Reason is that dephenolization cottonseed protein amino acid composition is reasonable, it is necessary to amino acid
High and balance, wherein methionine content is of a relatively high, can promote the initial feeding of fresh-water fishes seedling.
Formula 3：Fish meal 16%, PURE WHEY 32%, dephenolization cottonseed protein 16%, black soldier flies larva powder 16%, fish oil 6%, sesame
Sesame oil 8%, B B-complex 1%, composite mineral matter 1%, tributyrin 1%, vine tea flavone 1%.What formula 3 was prepared
The yield and embedding rate of microcapsules do not have difference compared with Example 2, but respectively with embodiment 2 and the system of this comparative example formula 3
Standby microcapsules opening material goes to feed fresh-water fishes, and specific feeding step is same as above, as a result found, the opening material nursing of embodiment 2 is light
The aperture opening ratio of water fish is 97%, and the aperture opening ratio for being formulated 3 opening material nursing fresh-water fishes is 94%.
Formula 4：Fish meal 16%, PURE WHEY 32%, dephenolization cottonseed protein 16%, black soldier flies larva powder 16%, split kettle algae powder
8%th, fish oil 8%, B B-complex 1%, composite mineral matter 1%, tributyrin 1%, vine tea flavone 1%.Formula 4 is prepared
Microcapsules yield and embedding rate there is no difference compared with Example 2, but respectively with embodiment 2 and this comparative example formula 4
The microcapsules opening material of preparation is gone to feed fresh-water fishes, and specific feeding step is same as above, as a result found, the opening material of embodiment 2 is fed
The aperture opening ratio of fresh-water fishes is 97%, and the aperture opening ratio for being formulated 4 opening material nursing fresh-water fishes is 94%.
Formula 5：Fish meal 16%, PURE WHEY 32%, dephenolization cottonseed protein 16%, black soldier flies larva powder 16%, fish oil 16%,
B B-complex 1%, composite mineral matter 1%, tributyrin 1%, vine tea flavone 1%.The microcapsules that formula 5 is prepared
Yield and embedding rate do not have difference compared with Example 2, but respectively with embodiment 2 and micro- glue of the preparation of this comparative example formula 5
Capsule opening material goes to feed fresh-water fishes, and specific feeding step is same as above, as a result found, the opening material of embodiment 2 feeds opening for fresh-water fishes
Mouth rate is 97%, and the aperture opening ratio for being formulated 5 opening material nursing fresh-water fishes is 89%.It can be seen that and split by the result of formula 3,4,5
Kettle algae powder and sesame oil split kettle algae powder and sesame oil in terms of the food calling opening of fresh-water fishes in addition to it can provide fat source raw material
Play a part of Synergistic.
Formula 6：It is made up of the raw material of following mass percent：Fish meal 32%, PURE WHEY 32%, dephenolization cottonseed protein
16%th, kettle algae powder 8%, sesame oil 8%, B B-complex 1%, composite mineral matter 1%, tributyrin 2% are split.
Formula 7：It is made up of the raw material of following mass percent：Fish meal 32%, PURE WHEY 32%, dephenolization cottonseed protein
16%th, kettle algae powder 8%, sesame oil 8%, B B-complex 1%, composite mineral matter 1%, vine tea flavone 2% are split.
The yield and embedding rate for the microcapsules that formula 6 and 7 is prepared do not have difference compared with Example 2, but respectively
The microcapsules opening material prepared with embodiment 2 and this comparative example formula 6,7 is gone to feed fresh-water fishes, and specific feeding step is same as above, fish
After seedling opening, fry is put into fish pond and cultivated, tested the low-temperature resistance stress respond of fry, as a result find, with formula 6
The low-temperature resistance stress respond of the fry of the starter diet feeding prepared with formula 7 is substantially lower than what is prepared with embodiment 2
The fry of starter diet feeding, analysis reason are that tributyrin and vine tea flavone are in terms of the immunity of fry is improved
With collaboration mutual assistance effect, the immunity of fry improves, so as to which low-temperature resistance stress ability is also correspondingly improved.
Claims (8)
- A kind of 1. preparation method of the fresh-water fishes microcapsules opening material of zero starch, it is characterised in that the microcapsules opening material by The raw material of following mass percent component composition is prepared：Protein sources raw material 75%~85%, fat source raw material 11~23%, answer Close vitamin 0.5~1%, composite mineral matter 0.5~1%, tributyrin 0.5~1%, vine tea flavone 0.5~1%；Wherein, The protein sources raw material is made up of fish meal, PURE WHEY, dephenolization cottonseed protein, black soldier flies larva powder；The preparation method of the microcapsules opening material comprises the following steps：By protein sources raw material ultramicro grinding into 325~450 purposes After micro mist, it is sufficiently mixed with fat source raw material, B B-complex, composite mineral matter, tributyrin, vine tea flavone；Add water 10~20min is emulsified after sizing mixing, is prepared into 20~35% underflow, homogeneous under the conditions of 10~20MPa；It is spraying, drying, sub-sieve, cold But microcapsules opening material is obtained afterwards.
- 2. preparation method according to claim 1, it is characterised in that the microcapsules opening material is by following mass percent The raw material of component composition is prepared：Protein sources raw material 80%, fat source raw material 16%, B B-complex 1%, composite mineral matter 1%th, tributyrin 1%, vine tea flavone 1%.
- 3. preparation method according to claim 1, it is characterised in that the fish meal：PURE WHEY：Dephenolization cottonseed egg In vain：The mass ratio of black soldier flies larva powder is 1：1~2：1：1~2.
- 4. preparation method according to claim 3, it is characterised in that the fish meal：PURE WHEY：Dephenolization cottonseed egg In vain：The mass ratio of black soldier flies larva powder is 1：2：1：1.
- 5. preparation method according to claim 1, it is characterised in that the fat source raw material is by splitting kettle algae powder and sesame oil Composition.
- 6. preparation method according to claim 5, it is characterised in that the kettle algae powder that splits accounts for microcapsules opening material feed original Expect the 6~12% of quality, sesame oil accounts for the 5~11% of microcapsules opening material feedstuff quality.
- 7. preparation method according to claim 1, it is characterised in that EAT is 180~230 DEG C during the spraying, Leaving air temp is 100~120 DEG C.
- 8. preparation method according to claim 1, it is characterised in that the temperature of the drying is 100~150 DEG C.
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