CN107686774A - A kind of extracting method of Peppermint essential oil - Google Patents
A kind of extracting method of Peppermint essential oil Download PDFInfo
- Publication number
- CN107686774A CN107686774A CN201710997921.3A CN201710997921A CN107686774A CN 107686774 A CN107686774 A CN 107686774A CN 201710997921 A CN201710997921 A CN 201710997921A CN 107686774 A CN107686774 A CN 107686774A
- Authority
- CN
- China
- Prior art keywords
- essential oil
- peppermint essential
- filter residue
- extracting method
- peppermint
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000341 volatile oil Substances 0.000 title claims abstract description 40
- 235000016257 Mentha pulegium Nutrition 0.000 title claims abstract description 29
- 235000004357 Mentha x piperita Nutrition 0.000 title claims abstract description 29
- 241001479543 Mentha x piperita Species 0.000 title claims abstract description 29
- 235000001050 hortel pimenta Nutrition 0.000 title claims abstract description 29
- 238000000034 method Methods 0.000 title claims abstract description 19
- 238000000605 extraction Methods 0.000 claims abstract description 13
- 108090000790 Enzymes Proteins 0.000 claims abstract description 10
- 102000004190 Enzymes Human genes 0.000 claims abstract description 10
- 239000000284 extract Substances 0.000 claims abstract description 9
- 239000012530 fluid Substances 0.000 claims description 17
- 229940088598 enzyme Drugs 0.000 claims description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 108010059892 Cellulase Proteins 0.000 claims description 4
- 229940106157 cellulase Drugs 0.000 claims description 4
- 238000009833 condensation Methods 0.000 claims description 4
- 230000005494 condensation Effects 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 4
- 229940059442 hemicellulase Drugs 0.000 claims description 4
- 108010002430 hemicellulase Proteins 0.000 claims description 4
- 239000012535 impurity Substances 0.000 claims description 4
- 239000001771 mentha piperita Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 229920002678 cellulose Polymers 0.000 abstract description 4
- 239000001913 cellulose Substances 0.000 abstract description 4
- 238000007796 conventional method Methods 0.000 abstract description 4
- 229920005610 lignin Polymers 0.000 abstract description 4
- 239000003921 oil Substances 0.000 abstract description 4
- 229920002488 Hemicellulose Polymers 0.000 abstract description 3
- 238000002474 experimental method Methods 0.000 abstract description 3
- 239000003960 organic solvent Substances 0.000 abstract description 3
- 238000000746 purification Methods 0.000 abstract description 3
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 2
- 239000000287 crude extract Substances 0.000 abstract description 2
- 230000009849 deactivation Effects 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 8
- 235000006679 Mentha X verticillata Nutrition 0.000 description 1
- 235000002899 Mentha suaveolens Nutrition 0.000 description 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention relates to a kind of extracting method of Peppermint essential oil, comprise the following steps：（1）Organic solvent extracts；（2）Extraction is squeezed after filter residue enzymolysis；（3）Secondary purification.A kind of extracting method of Peppermint essential oil provided by the invention, the Peppermint essential oil high purity more than 98.8% of extraction, extracted by organic solvent, the higher essential oil of purity can be obtained, then filter residue is digested, remove the cellulose in filter residue, hemicellulose, lignin, help improves oil yield, distilled again after finally crude extract is mixed, play enzyme deactivation bactericidal action, secondary purification is played again, substantially increase the purity of Peppermint essential oil, more market value, by experiment, extraction of essential oil amount adds 21% than conventional method, substantially increase economic benefit, it is worth of widely use.
Description
Technical field
The invention belongs to extraction of essential oil field, and in particular to a kind of extracting method of Peppermint essential oil.
Background technology
Peppermint essential oil is a kind of king-sized essential oil species of market demand, because its mint flavored having refreshes the mind, clearly
It is fragrant pleasant, offset eliminate the unusual smell, throat-clearing throat-moistening, body and mind of releiving have unique curative effect, but the extracting method of Peppermint essential oil is more at present
It is single, it is not high enough to the utilization rate of raw material.
The content of the invention
In order to overcome problem above, the invention provides a kind of extracting method of Peppermint essential oil.
The present invention is achieved through the following technical solutions：
A kind of extracting method of Peppermint essential oil, comprises the following steps：
（1）Dried peppermint leaf is dried to water content below 5%, is crushed to 80 mesh, 75% alcohol is added and extraction 180 is shaken at 15 DEG C
Minute, filter residue and extract solution are filtered to obtain, extract solution is centrifuged in 240r/min, takes upper strata fluid A；
（2）By step（1）The filter residue is digested 90 minutes using complex enzyme at 30 DEG C, and the filter residue is dried after filtering, is used
Mechanical expression, obtain pressed liquor, by the pressed liquor it is closed stand 2 days, take upper strata fluid B；
（3）By step（1）The fluid A and step（2）After the fluid B mixing, it is heated to seething with excitement, is gone after collecting steam condensation
Except a small amount of impurity, the very high Peppermint essential oil of purity is produced.
Further, step（2）The complex enzyme, by cellulase, hemicellulase, lignoenzyme in mass ratio 3:1:
3 mix.
Beneficial effects of the present invention：A kind of extracting method of Peppermint essential oil provided by the invention, the Peppermint essential oil of extraction are pure
Degree up to more than 98.8%, is extracted by organic solvent, can obtain the higher essential oil of purity, then digest filter residue, removed in filter residue
Cellulose, hemicellulose, lignin, help improve oil yield, distilled again after finally crude extract is mixed, that is, play enzyme deactivation
Bactericidal action, secondary purification being played again, substantially increasing the purity of Peppermint essential oil, more market value, by experiment, essential oil carries
Taken amount adds 21% than conventional method, substantially increases economic benefit, is worth of widely use.
Embodiment
Embodiment 1
A kind of extracting method of Peppermint essential oil, comprises the following steps：
（1）Dried peppermint leaf is dried to water content below 5%, is crushed to 80 mesh, 75% alcohol is added and extraction 180 is shaken at 15 DEG C
Minute, Peppermint essential oil is completely dissolved in alcohol, filter to obtain filter residue and extract solution, by extract solution in 240r/min centrifugations point
From taking upper strata fluid A；
（2）By step（1）The filter residue is digested 90 minutes using complex enzyme at 35 DEG C, makes cellulose in filter residue, hemicellulose
Element, lignin fully digest, and help improves oil yield, and the filter residue is dried after filtering, using mechanical expression, obtains pressed liquor, will
The pressed liquor is closed to stand 3 days, takes upper strata fluid B；
（3）By step（1）The fluid A and step（2）After the fluid B mixing, it is heated to seething with excitement, is gone after collecting steam condensation
Except a small amount of impurity, the very high Peppermint essential oil of purity is produced.
Further, step（2）The complex enzyme, by cellulase, hemicellulase, lignoenzyme in mass ratio 3:1:
3 mix.
Embodiment 2
A kind of extracting method of Peppermint essential oil, comprises the following steps：
（1）Dried peppermint leaf is dried to water content below 5%, is crushed to 80 mesh, 75% alcohol is added and extraction 180 is shaken at 15 DEG C
Minute, Peppermint essential oil is completely dissolved in alcohol, filter to obtain filter residue and extract solution, extract solution is centrifuged in 200-240r/min
Separation, takes upper strata fluid A；
（2）By step（1）The filter residue is digested 90 minutes using complex enzyme at 30-35 DEG C, makes cellulose, half fibre in filter residue
Dimension element, lignin fully digest, and help improves oil yield, and the filter residue is dried after filtering, using mechanical expression, obtains pressed liquor,
By the pressed liquor it is closed stand 2-3 days, take upper strata fluid B；
（3）By step（1）The fluid A and step（2）After the fluid B mixing, it is heated to seething with excitement, is gone after collecting steam condensation
Except a small amount of impurity, the very high Peppermint essential oil of purity is produced.
Further, step（2）The complex enzyme, by cellulase, hemicellulase, lignoenzyme in mass ratio 3:1:
3 mix.
Comparative example 1
This comparative example 1 compared with Example 1, without using step（2）The obtained fluid B, method and step in addition
All same.
Comparative example 2
This comparative example 2 compared with Example 2, without step（3）The operation, method and step all same in addition.
Control group
The extracting method of conventional Peppermint essential oil.
What five kinds of methods that embodiment 1, embodiment 2, comparative example 1, comparative example 2, control group are provided were extracted
Peppermint essential oil carries out chemical composition analysis, calculates the purity and extracted amount of Peppermint essential oil, statistical result such as table 1：
Table 1
| Essential oil purity（%） | Extraction of essential oil amount（ml/100gFW） | |
| Embodiment 1 | 98.8 | 0.40 |
| Embodiment 2 | 99.0 | 0.41 |
| Comparative example 1 | 99.1 | 0.28 |
| Comparative example 2 | 78.5 | 0.40 |
| Control group | 95.6 | 0.33 |
As shown in Table 1, a kind of extracting method of the Peppermint essential oil provided using the inventive method is high by experiment, essential oil purity
Up to 99.0%, the Peppermint essential oil purity than the extraction of conventional method of extraction of essential oil is higher, more market value, meanwhile, extraction of essential oil amount
21% is added than conventional method, substantially increases economic benefit, is worth of widely use.
Claims (2)
1. a kind of extracting method of Peppermint essential oil, it is characterised in that comprise the following steps：
（1）Dried peppermint leaf is dried to water content below 5%, is crushed to 80 mesh, 75% alcohol is added and extraction 180 is shaken at 15 DEG C
Minute, filter residue and extract solution are filtered to obtain, extract solution is centrifuged in 240r/min, takes upper strata fluid A；
（2）By step（1）The filter residue is digested 90 minutes using complex enzyme at 30 DEG C, and the filter residue is dried after filtering, is used
Mechanical expression, obtain pressed liquor, by the pressed liquor it is closed stand 2 days, take upper strata fluid B；
（3）By step（1）The fluid A and step（2）After the fluid B mixing, it is heated to seething with excitement, is gone after collecting steam condensation
Except a small amount of impurity, the very high Peppermint essential oil of purity is produced.
A kind of 2. extracting method of Peppermint essential oil according to claim 1, it is characterised in that：Step（2）The complex enzyme,
By cellulase, hemicellulase, lignoenzyme in mass ratio 3:1:3 mix.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710997921.3A CN107686774A (en) | 2017-10-24 | 2017-10-24 | A kind of extracting method of Peppermint essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710997921.3A CN107686774A (en) | 2017-10-24 | 2017-10-24 | A kind of extracting method of Peppermint essential oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107686774A true CN107686774A (en) | 2018-02-13 |
Family
ID=61153973
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710997921.3A Pending CN107686774A (en) | 2017-10-24 | 2017-10-24 | A kind of extracting method of Peppermint essential oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107686774A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109809969A (en) * | 2019-03-15 | 2019-05-28 | 黑龙江阳光工业大麻研究院 | A kind of method that enzyme process combination embrane method extracts cannabidiol |
| CN111234270A (en) * | 2020-03-18 | 2020-06-05 | 百事基材料（青岛）股份有限公司 | Mint terylene master batch and preparation method thereof |
| WO2025133943A1 (en) * | 2023-12-20 | 2025-06-26 | Jonas MACULLO | Working and recycling process of plants of the picea family or other varieties, and products obtained therefrom |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003253292A (en) * | 2002-03-01 | 2003-09-10 | Ogawa & Co Ltd | Sustained releasability-giving agent and sustained- release mint flavor |
| CN1721512A (en) * | 2004-07-16 | 2006-01-18 | 厦门今润医药科学开发有限公司 | Process for heating-free extraction of fresh peppermint essential oil |
| CN103614230A (en) * | 2013-11-20 | 2014-03-05 | 徐州黎明食品有限公司 | Preparation method of garlic oil |
| CN104560400A (en) * | 2014-12-26 | 2015-04-29 | 江苏省中国科学院植物研究所 | Method for extracting peppermint oil |
| CN105886122A (en) * | 2014-12-08 | 2016-08-24 | 陈亚海 | Lucid ganoderma essential oil and preparation method thereof |
-
2017
- 2017-10-24 CN CN201710997921.3A patent/CN107686774A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003253292A (en) * | 2002-03-01 | 2003-09-10 | Ogawa & Co Ltd | Sustained releasability-giving agent and sustained- release mint flavor |
| CN1721512A (en) * | 2004-07-16 | 2006-01-18 | 厦门今润医药科学开发有限公司 | Process for heating-free extraction of fresh peppermint essential oil |
| CN103614230A (en) * | 2013-11-20 | 2014-03-05 | 徐州黎明食品有限公司 | Preparation method of garlic oil |
| CN105886122A (en) * | 2014-12-08 | 2016-08-24 | 陈亚海 | Lucid ganoderma essential oil and preparation method thereof |
| CN104560400A (en) * | 2014-12-26 | 2015-04-29 | 江苏省中国科学院植物研究所 | Method for extracting peppermint oil |
Non-Patent Citations (1)
| Title |
|---|
| 高燕: "野生薄荷精油的提取分离及其抗氧化活性研究", 《中国优秀硕士学位论文全文数据库 基础科学辑》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109809969A (en) * | 2019-03-15 | 2019-05-28 | 黑龙江阳光工业大麻研究院 | A kind of method that enzyme process combination embrane method extracts cannabidiol |
| CN111234270A (en) * | 2020-03-18 | 2020-06-05 | 百事基材料（青岛）股份有限公司 | Mint terylene master batch and preparation method thereof |
| WO2025133943A1 (en) * | 2023-12-20 | 2025-06-26 | Jonas MACULLO | Working and recycling process of plants of the picea family or other varieties, and products obtained therefrom |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20180213 |