CN107686375A - A kind of quartz sand medium temperature coloring process - Google Patents
A kind of quartz sand medium temperature coloring process Download PDFInfo
- Publication number
- CN107686375A CN107686375A CN201710913009.5A CN201710913009A CN107686375A CN 107686375 A CN107686375 A CN 107686375A CN 201710913009 A CN201710913009 A CN 201710913009A CN 107686375 A CN107686375 A CN 107686375A
- Authority
- CN
- China
- Prior art keywords
- quartz sand
- coloring process
- medium temperature
- stove
- temperature coloring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 24
- 238000004040 coloring Methods 0.000 title claims abstract description 16
- 239000006004 Quartz sand Substances 0.000 title claims abstract description 14
- 238000000034 method Methods 0.000 title claims abstract description 14
- 239000000049 pigment Substances 0.000 claims abstract description 8
- 239000000654 additive Substances 0.000 claims abstract description 7
- 230000000996 additive effect Effects 0.000 claims abstract description 7
- 150000008064 anhydrides Chemical class 0.000 claims abstract description 5
- 229910052809 inorganic oxide Inorganic materials 0.000 claims abstract description 5
- 239000004094 surface-active agent Substances 0.000 claims abstract description 5
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000004327 boric acid Substances 0.000 claims abstract description 4
- 238000007873 sieving Methods 0.000 claims abstract description 4
- QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical group [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 claims description 6
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 4
- 229960004643 cupric oxide Drugs 0.000 claims description 3
- MPPQGYCZBNURDG-UHFFFAOYSA-N 2-propionyl-6-dimethylaminonaphthalene Chemical compound C1=C(N(C)C)C=CC2=CC(C(=O)CC)=CC=C21 MPPQGYCZBNURDG-UHFFFAOYSA-N 0.000 claims description 2
- YOPKGUUNMWGPCZ-UHFFFAOYSA-N phosphoric acid;propane Chemical compound CCC.OP(O)(O)=O YOPKGUUNMWGPCZ-UHFFFAOYSA-N 0.000 claims description 2
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 claims 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical group [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims 1
- 229910052698 phosphorus Inorganic materials 0.000 claims 1
- 239000011574 phosphorus Substances 0.000 claims 1
- 238000005516 engineering process Methods 0.000 abstract description 7
- 230000006750 UV protection Effects 0.000 abstract description 2
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 239000004576 sand Substances 0.000 description 6
- 238000000576 coating method Methods 0.000 description 5
- 239000011248 coating agent Substances 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000005245 sintering Methods 0.000 description 3
- 241001062009 Indigofera Species 0.000 description 2
- IRERQBUNZFJFGC-UHFFFAOYSA-L azure blue Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[S-]S[S-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-] IRERQBUNZFJFGC-UHFFFAOYSA-L 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- ZSFDBVJMDCMTBM-UHFFFAOYSA-N ethane-1,2-diamine;phosphoric acid Chemical compound NCCN.OP(O)(O)=O ZSFDBVJMDCMTBM-UHFFFAOYSA-N 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- VLCQZHSMCYCDJL-UHFFFAOYSA-N tribenuron methyl Chemical compound COC(=O)C1=CC=CC=C1S(=O)(=O)NC(=O)N(C)C1=NC(C)=NC(OC)=N1 VLCQZHSMCYCDJL-UHFFFAOYSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 150000002927 oxygen compounds Chemical class 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000004224 protection Effects 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 238000003746 solid phase reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5072—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with oxides or hydroxides not covered by C04B41/5025
- C04B41/5074—Copper oxide or solid solutions thereof
- C04B41/5075—Copper oxide
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses a kind of quartz sand medium temperature coloring process, comprise the following steps：（1）Glaze slip configures, and takes boric acid 50g/L, basic anhydride 100g/L, additive 5g/L, surfactant 0.05g/L to be well mixed；（2）Take 50mL glaze slips to be added in 100g ores in sand form to be well mixed, then be separately added into inorganic oxide pigments and be sufficiently mixed；（3）It is placed in stove and is sintered 30 minutes at a temperature of 800 DEG C；（4）Come out of the stove, crush, sieving.The beneficial effect of the invention is：The bright-coloured of its product color is rich and varied, water-fast, acidproof, alkaline-resisting, ultraviolet resistance.Do not influenceed by environment, weather, time.Not only there is the characteristics of high heat colouring but also the cheap new technology of cost, the easy convenient for production that construct have good application value.
Description
Technical field
The present invention relates to quartz sand processing technology field, specially a kind of quartz sand medium temperature coloring process.
Background technology
Architectural chemistries industry in recent years emerges rapidly, and to continue to bring out building coatings be even more five light to various building decoratives
Ten colors, and sand wall-like wall covering is because its distinctive abundant texture and serious surface three-dimensional sense are increasingly by people's
Pay attention to and like.Important component of the color sand as sand wall-like exterior coating, play regulation coating form and aspect, lightness and chroma
Effect makes the designs and varieties of coating varied.Therefore the quality of coloured silk sand directly influences the performance of exterior coating.Originally grind
Study carefully according to solid phase reaction principle, by experimental analysis and compare and finally develop a kind of brand-new intermediate sintering temperature quartz sand coloring
Technology has good economic benefit and social benefit.
The content of the invention
It is an object of the invention to provide a kind of quartz sand medium temperature coloring process, to solve what is proposed in above-mentioned background technology
Problem.
To achieve the above object, the present invention provides following technical scheme：One kind, comprise the following steps：
（1）Glaze slip configures, and takes boric acid 50g/L, basic anhydride 100g/L, additive 5g/L, surfactant 0.05g/L mixing
Uniformly；
（2）Take 50mL glaze slips to be added in 100g ores in sand form to be well mixed, then be separately added into inorganic oxide pigments and be sufficiently mixed；
（3）It is placed in stove and is sintered 30 minutes at a temperature of 800 DEG C；
（4）Come out of the stove, crush, sieving.
Preferably, the step（2）Inorganic oxide pigments be cupric oxide.
Preferably, the surfactant is one kind in ethylenediamine phosphate, phosphoric acid propane diamine, dimethylbenzene, prodan.
Preferably, the additive includes pinecone oil.
Compared with prior art, the beneficial effects of the invention are as follows：And this color sand coloring process is former using ceramic glaze sintering
Reason is different from conventional method, and the technique includes glaze slurry formula and technological parameter.Kind has blue sea indigo plant, ultramarine, purplish red, purplish blue, green
Color, cameo brown etc..The bright-coloured of its product color is rich and varied, water-fast, acidproof, alkaline-resisting, ultraviolet resistance.Not by environment, weather, when
Between influence.Not only there is the characteristics of high heat colouring but also the cheap new technology of cost, the easy convenient for production that construct have good
Good application value.
Embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all
Belong to the scope of protection of the invention.
The present invention provides a kind of technical scheme：A kind of quartz sand medium temperature coloring process, to solve to carry in above-mentioned background technology
The problem of going out.
To achieve the above object, the present invention provides following technical scheme：One kind, comprise the following steps：
（1）Glaze slip configures, and takes boric acid 50g/L, basic anhydride 100g/L, additive 5g/L, ethylenediamine phosphate 0.05g/L mixing
Uniformly；
（2）Take 50mL glaze slips to be added in 100g ores in sand form to be well mixed, then be separately added into cupric oxide and be sufficiently mixed；
（3）It is placed in stove and is sintered 30 minutes at a temperature of 800 DEG C；
（4）Come out of the stove, crush, sieving.
Wherein, additive includes pinecone oil.
This color sand coloring process using ceramic glaze sintering theory it is different from conventional method, the technique including glaze slurry formula with
Technological parameter, kind have blue sea indigo plant, ultramarine, purplish red, purplish blue, green, cameo brown etc..It is characterized in that provide suitable inorganic oxygen
Compound pigment and basic anhydride fluxing agent.It is inner in 800 1 900 DEG C when pigment and fluxing agent are evenly distributed on quartz sand surface
When being sintered in stove, the melt of fluxing agent interpenetrates pigment with the quartz sand top layer softened and also penetrated into therewith, and solid phase occurs
React face colouring.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (4)
- A kind of 1. quartz sand medium temperature coloring process, it is characterised in that：Comprise the following steps：（1）Glaze slip configures, and takes boric acid 50g/L, basic anhydride 100g/L, additive 5g/L, surfactant 0.05g/L mixing Uniformly；（2）Take 50mL glaze slips to be added in 100g ores in sand form to be well mixed, then be separately added into inorganic oxide pigments and be sufficiently mixed；（3）It is placed in stove and is sintered 30 minutes at a temperature of 800 DEG C；（4）Come out of the stove, crush, sieving.
- A kind of 2. quartz sand medium temperature coloring process according to claim 1, it is characterised in that：The step（2）It is inorganic Oxide pigment is cupric oxide.
- A kind of 3. quartz sand medium temperature coloring process according to claim 1, it is characterised in that：The surfactant is phosphorus One kind in sour ethylenediamine, phosphoric acid propane diamine, dimethylbenzene, prodan.
- A kind of 4. quartz sand medium temperature coloring process according to claim 1, it is characterised in that：The additive includes the pinecone Oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710913009.5A CN107686375A (en) | 2017-09-30 | 2017-09-30 | A kind of quartz sand medium temperature coloring process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710913009.5A CN107686375A (en) | 2017-09-30 | 2017-09-30 | A kind of quartz sand medium temperature coloring process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107686375A true CN107686375A (en) | 2018-02-13 |
Family
ID=61153794
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710913009.5A Pending CN107686375A (en) | 2017-09-30 | 2017-09-30 | A kind of quartz sand medium temperature coloring process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107686375A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108341598A (en) * | 2018-03-08 | 2018-07-31 | 福建工程学院 | A kind of production method of color sand vitreous brick |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1133267A (en) * | 1995-11-23 | 1996-10-16 | 庞德春 | Vitreous jewel colour sand and preparation method |
| CN102531688A (en) * | 2011-12-14 | 2012-07-04 | 刘锐浩 | Creamy white frit and preparation method thereof |
| CN106145733A (en) * | 2015-03-27 | 2016-11-23 | 山西亮龙涂料有限公司 | A kind of burning colorful sand and preparation technology thereof |
-
2017
- 2017-09-30 CN CN201710913009.5A patent/CN107686375A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1133267A (en) * | 1995-11-23 | 1996-10-16 | 庞德春 | Vitreous jewel colour sand and preparation method |
| CN102531688A (en) * | 2011-12-14 | 2012-07-04 | 刘锐浩 | Creamy white frit and preparation method thereof |
| CN106145733A (en) * | 2015-03-27 | 2016-11-23 | 山西亮龙涂料有限公司 | A kind of burning colorful sand and preparation technology thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108341598A (en) * | 2018-03-08 | 2018-07-31 | 福建工程学院 | A kind of production method of color sand vitreous brick |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP3604258A1 (en) | Semi-transparent ceramic sheet decorated with ink light-absorbance and preparation method thereof | |
| CN101372422B (en) | In-glaze decoration method for bright red glazed ceramic | |
| CN103613409B (en) | Clay glaze and production method of red soil pottery product | |
| CN103588507B (en) | White-dotted stereoscopic decorative glazed ceramic product and preparation method thereof | |
| CN106365694B (en) | Ceramic tile with three-dimensional pattern and combined ceramic ink and production method thereof | |
| CN105647287A (en) | Ceramic ink with glaze separating function, and preparation method and production method thereof | |
| CN104386933A (en) | Colored glazed quartz colorful sand and preparation method thereof | |
| WO2015054805A1 (en) | High whiteness underglaze multicolored low-temperature porcelain and preparation method | |
| CN105820692A (en) | Sand wall like coating containing water-based dyeing colored sand and preparation method of sand wall like coating | |
| CN104496415A (en) | Mud filling method for Nixing pottery | |
| CN107954602A (en) | Unglazed argentine crystal glaze and preparation method thereof | |
| CN110937814A (en) | Matte color transmutation glaze and preparation method thereof | |
| CN106046939A (en) | Novel ceramic ink-jet ink and production process thereof | |
| CN109081591A (en) | The art pottery and preparation method thereof with regular contracting glaze texture | |
| CN107686375A (en) | A kind of quartz sand medium temperature coloring process | |
| CN104478258B (en) | Preparation method of resin coated color quartz sand | |
| CN111689768A (en) | Co-firing method of whole-body ink-jet black golden flower fully-polished brick and common archaized brick | |
| CN104761286A (en) | Sintered color sand | |
| CN101962301B (en) | Method used for underglaze transfer-printing and quick-glazing of ceramics | |
| CN110713393B (en) | Blended ceramic pigment glaze and production method thereof, stone-like glazed tile and production method thereof | |
| CN104402278A (en) | Preparation method of glazed colored sand | |
| CN104176977A (en) | Stone like coating prepared by using waste ceramic, and its preparation method | |
| CN106116157B (en) | A kind of preparation method of Suzhou soil low fever terracotta glaze | |
| CN108069609A (en) | Reddish brown rust coloured glaze and preparation method thereof | |
| CN111548011B (en) | Purple-color green-point kiln-changing porcelain and preparation process thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180213 |