CN107627226B - A kind of elasticity concretion abrasive and its preparation method and application - Google Patents
A kind of elasticity concretion abrasive and its preparation method and application Download PDFInfo
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- CN107627226B CN107627226B CN201710835212.5A CN201710835212A CN107627226B CN 107627226 B CN107627226 B CN 107627226B CN 201710835212 A CN201710835212 A CN 201710835212A CN 107627226 B CN107627226 B CN 107627226B
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- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 238000005498 polishing Methods 0.000 claims abstract description 55
- 239000010432 diamond Substances 0.000 claims abstract description 48
- 229910003460 diamond Inorganic materials 0.000 claims abstract description 46
- 239000000843 powder Substances 0.000 claims abstract description 36
- 239000000463 material Substances 0.000 claims abstract description 34
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000010445 mica Substances 0.000 claims abstract description 32
- 229910052618 mica group Inorganic materials 0.000 claims abstract description 32
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 19
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 19
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000008117 stearic acid Substances 0.000 claims abstract description 19
- 238000000227 grinding Methods 0.000 claims abstract description 14
- 238000002156 mixing Methods 0.000 claims description 34
- 239000011812 mixed powder Substances 0.000 claims description 28
- 238000000034 method Methods 0.000 claims description 19
- 229920003225 polyurethane elastomer Polymers 0.000 claims description 3
- 229920001971 elastomer Polymers 0.000 abstract description 25
- 229920002803 thermoplastic polyurethane Polymers 0.000 abstract description 20
- 239000004433 Thermoplastic polyurethane Substances 0.000 abstract description 19
- 230000000694 effects Effects 0.000 abstract description 9
- 239000000806 elastomer Substances 0.000 abstract description 4
- 239000003082 abrasive agent Substances 0.000 description 9
- 239000000919 ceramic Substances 0.000 description 8
- 238000012360 testing method Methods 0.000 description 8
- 238000001125 extrusion Methods 0.000 description 7
- 239000003292 glue Substances 0.000 description 7
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 6
- 239000012530 fluid Substances 0.000 description 5
- 230000003746 surface roughness Effects 0.000 description 5
- 238000007596 consolidation process Methods 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 229910052594 sapphire Inorganic materials 0.000 description 4
- 239000010980 sapphire Substances 0.000 description 4
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 229920001169 thermoplastic Polymers 0.000 description 3
- 239000004416 thermosoftening plastic Substances 0.000 description 3
- 229910000838 Al alloy Inorganic materials 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000013065 commercial product Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 238000005422 blasting Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 229920006332 epoxy adhesive Polymers 0.000 description 1
- 238000013003 hot bending Methods 0.000 description 1
- 230000001795 light effect Effects 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 230000001050 lubricating effect Effects 0.000 description 1
- 239000011859 microparticle Substances 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 238000007517 polishing process Methods 0.000 description 1
- -1 poly ammonia Ester Chemical class 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- TUTLDIXHQPSHHQ-UHFFFAOYSA-N tin(iv) sulfide Chemical compound [S-2].[S-2].[Sn+4] TUTLDIXHQPSHHQ-UHFFFAOYSA-N 0.000 description 1
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- Polishing Bodies And Polishing Tools (AREA)
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
Abstract
The invention belongs to polishing material technical field, a kind of elastic concretion abrasive and its preparation method and application is provided.Elasticity concretion abrasive provided by the invention comprises the following components in parts by weight: 8~10 parts of diamond, 5~50 parts of thermoplastic polyurethane rubber, 20~25 parts of talcum powder, 15~20 parts of mica powder, 5~10 parts of stearic acid；The hardness of elasticity concretion abrasive provided by the invention is 35~45HD, the elastic concretion abrasive of material can be with the cambered surface Full connected of hard brittle material based on thermoplastic polyurethane rubber, make stress surface pressure stable and uniform, compares the polishing effect of free type cambered surface polishing more evenly；And diamond abrasive is evenly dispersed in thermoplastic polyurethane rubber main body, so that surface of elastomer exposes many equally distributed diamonds protrusions, polishing effect and polishing efficiency when grinding and polishing are all significantly improved.
Description
Technical field
The present invention relates to polishing material technical field more particularly to a kind of elastic concretion abrasive and preparation method thereof and answer
With.
Background technique
Currently, mobile phone hard brittle material, as the plane polishing technology of sapphire, zirconia ceramics and glass has compared into
It is ripe, but cambered surface polishing technology is still in the technical bottleneck phase.In the prior art, cambered surface component processing mainly passes through CNC or hot bending skill
Art processes arc-shaped curved surface to the edge of workpiece.However, the arc-shaped curved surface rough surface that the above method processes, is in dumb light shape
State needs further to be processed by shot blasting cambered surface, the coarse striped on cambered surface surface and fluctuating is removed, and cambered surface is made to have one
Fixed brightness and finish.
Existing cambered surface polishing method is mainly free type chemically mechanical polishing, and this method is mainly using flexible mill skin or hair
Brush is used as abrasive material loading material, cooperates the polishing fluid containing polishing particles abrasive material, polishes to cambered surface workpiece.Due to carrying material
Material has elasticity and flexibility, can preferably coat cambered surface, act on cambered surface can with polishing particles abrasive material sufficiently, be finally reached side
Edge is bright.
For example, patent 201320885994.0 provides a kind of globoidal glass burnishing device, felt cloth and sponge are attached to
The polishing fluid of panel surface on polishing machine, cooperation polishing powder configuration makes to polish using the elastic telescopic characteristic of upper disk pressure and sponge
Powder is applied in the cambered surface of workpiece, plane and cambered surface edge is swept bright；Patent 201120347925.5 provides a kind of silicon single crystal rod
Arc-surface polishing wheel, carrying out brush to cambered surface using hairbrush and polishing fluid makes cambered surface be finally reached light；Patent
201510138283.0 disclose a kind of polishing mill skin and the small ceramic product cambered surface polishing method using this mill skin, wherein
Polishing is made of sponge, adhesive and resin from bottom to top with mill skin, cooperates silicon dioxide microparticle polishing fluid using this mill skin, right
Small ceramic product with cambered surface is polished.
The above polishing is all made of free type chemical mechanical polishing method and processes to cambered surface, due to abrasive material carrier and polishing fluid
It is separation, need to be used cooperatively when being polished, abrasive material is caused to be unevenly distributed during the polishing process, cambered surface stress is smaller, throws
Light effect and efficiency are all lower, polish particularly with the cambered surface of the hard brittle materials such as the biggish sapphire of hardness or zirconia ceramics,
Polishing effect is very poor, is unable to satisfy its demand.
Summary of the invention
For deficiency present in existing free type CMP process, the object of the present invention is to provide one kind
The higher integrated elastic concretion abrasive of hardness can significantly improve the uniformity and polishing efficiency of the polishing of hard brittle material cambered surface.
In order to achieve the above-mentioned object of the invention, the present invention is the following technical schemes are provided: a kind of elasticity concretion abrasive, including following
The component of parts by weight:
Preferably, the elastic concretion abrasive, comprises the following components in parts by weight:
Preferably, the partial size of the diamond is 0.5~50 μm.
Preferably, the partial size of the talcum powder is 1~30 μm.
Preferably, the partial size of the mica powder is 30~50 μm.
The present invention also provides the preparation methods of above-mentioned elastic concretion abrasive, include the following steps:
Diamond, talcum powder, mica powder, stearic acid and thermoplastic polyurethane rubber are kneaded to obtain elasticity consolidation mill
Material.
Preferably, the temperature of the mixing is 70~230 DEG C.
Preferably, the time of the mixing is 1~2h.
Preferably, the rate of the mixing is 30~120r/min.
The elastic concretion abrasive obtained the present invention also provides a kind of above-mentioned elastic grinding material and above-mentioned preparation method is in arc
Application in the polishing of face, comprising: grinding and polishing is carried out to hard brittle material cambered surface with the elastic concretion abrasive.
The present invention provides a kind of elastic concretion abrasives, comprise the following components in parts by weight: 8~10 parts of diamond, thermoplastic
5~50 parts of polyurethane rubber, 20~25 parts of talcum powder, 15~20 parts of mica powder, 5~10 parts of stearic acid of property.It is provided by the invention
In elastic concretion abrasive, it is excellent that thermoplastic polyurethane rubber as the material of main part of elastic concretion abrasive can be such that concretion abrasive has
Fine diamond thermoplastic polyurethane rubber consolidation is got up, is formed containing the elasticity for being uniformly distributed abrasive material by different elasticity
Body, the diamond of surface microprotrusion can play the role of material digging quarter；Talcum powder and mica powder are a kind of fillers, can be effective
It adjusts the hardness of elastic concretion abrasive and improves the distributing homogeneity of diamond；Stearic acid is as a kind of lubricant and softening plasticising
Material can effectively control the plasticity of elastic concretion abrasive.The experimental results showed that elasticity concretion abrasive provided by the invention is hard
Degree is 35~45HD, can satisfy the cambered surface polishing to the biggish sapphire of hardness or zirconia ceramics material.
Elasticity concretion abrasive provided by the invention, grinds hard brittle material surface by the diamond microprotrusion particle on surface
Grinding and polishing light, elastic grinding material can make stress surface pressure stable and uniform, the polishing with separate type with the cambered surface Full connected of hard brittle material
Liquid phase is more more excellent than polishing effect.In addition, making since diamond abrasive is evenly dispersed in thermoplastic polyurethane rubber main body
Surface of elastomer exposes many equally distributed diamonds protrusions, when carrying out grinding and polishing to hard brittle material, polishing effect with
And polishing efficiency is all significantly improved.
Detailed description of the invention
The elastic concretion abrasive of Fig. 1 embodiment 1 with plane to the schematic diagram of hard brittle material cambered surface grinding and polishing, wherein 11 be potsherd
Sample, 12 be the aluminum alloy round mill tool for being adhesive with plain film elasticity concretion abrasive；
The elastic concretion abrasive of Fig. 2 embodiment 8 with end face to the schematic diagram of hard brittle material cambered surface grinding and polishing, wherein 21 be potsherd
Sample, 22 be cylinder body elasticity concretion abrasive.
Specific embodiment
The present invention provides a kind of elastic concretion abrasives, comprise the following components in parts by weight: 8~10 parts of diamond, thermoplastic
5~50 parts of polyurethane rubber, 20~25 parts of talcum powder, 15~20 parts of mica powder, 5~10 parts of stearic acid of property.
It include 8~10 parts by weight of diamond, preferably 9 parts by weight in elasticity concretion abrasive provided by the invention；In this hair
In bright, the partial size of the diamond is preferably 0.5~50 μm, more preferably 1~30 μm, most preferably 2~10 μm；In the present invention
In, main component of the diamond as elastic concretion abrasive, extreme hardness can play the role of digging quarter, improve polishing effect；?
In the embodiment of the present invention, diamond is preferably polycrystalline diamond.
In the present invention, diamond partial size determines the surface roughness of final processing resulting materials, and partial size is smaller, obtains thick
Rugosity is lower, and therefore, the diamond partial size in the present invention is preferably 2~4 μm, and the surface roughness for processing resulting materials can drop
It is extremely minimum.
It include thermoplastic polyurethane rubber 5 in elasticity concretion abrasive provided by the invention on the basis of the quality of diamond
~50 parts by weight, preferably 10~45 parts by weight, more preferably 20~40 parts by weight；In the present invention, due to thermoplastic poly ammonia
Ester rubber has elastically-deformable characteristic, can increase the forced area of material with the cambered surface Full connected of material in polishing, make
The pressure stable and uniform of stress surface.
The present invention gets up the diamond thermoplastic polyurethane elastic rubber consolidation of uniform particle sizes, forms uniform mosaic gold
The elastomer of hard rock abrasive material presses to cambered surface when grinding and polishing, so that elastic concretion abrasive and cambered surface is carried out Full connected, leans on elastomer
The diamond abrasive of surface bulge carries out grinding and polishing to cambered surface, not only increases the polishing effect of cambered surface, and reduces polishing institute
It takes time, polishing efficiency is also promoted.
It include 20~25 weight of talcum powder in elasticity concretion abrasive provided by the invention on the basis of the quality of diamond
Part, preferably 22~24 parts by weight；In the present invention, the partial size of the talcum powder is preferably 1~30 μm, more preferably 3~20 μ
M, most preferably 5~10 μm.The present invention does not have particular/special requirement for the source of talcum powder, using commercial product.
It include 15~20 weight of mica powder in elasticity concretion abrasive provided by the invention on the basis of the quality of diamond
Part, preferably 16~18 parts by weight；In the present invention, the partial size of the mica powder is preferably 30~50 μm, more preferably 35~
45 μm, most preferably 40 μm.The present invention does not have particular/special requirement for the source of mica powder, using commercial product.In this hair
In bright, talcum powder and mica powder are a kind of fillers, are mainly used for adjusting point of the hardness of elastic concretion abrasive and diamond abrasive
Cloth uniformity can adjust and stablize the hardness of elastic concretion abrasive using the synergistic effect of talcum powder and mica powder.
It include 5~10 parts by weight of stearic acid in elasticity concretion abrasive provided by the invention on the basis of the quality of diamond,
Preferably 6~8 parts by weight；The present invention does not have particular/special requirement for stearic partial size, can uniformly incorporate elasticity in mixing process
In body；In the present invention, stearic acid has the function of lubricating and softening plasticising, can control the modeling of material in mixing process
Property, so that each component is uniformly mixed, while improving abrasive hardness, plastic property is also guaranteed.
The present invention also provides a kind of preparation methods of elastic concretion abrasive, comprising:
Diamond, talcum powder, mica powder, stearic acid and thermoplastic polyurethane rubber are kneaded to obtain elasticity consolidation mill
Material.
Diamond, talcum powder, mica powder and stearic acid are preferably first mixed to get mixed powder by the present invention, then will be mixed again
Powder is closed to be kneaded with thermoplastic polyurethane rubber.In the present invention, above-mentioned mixing order enables to diamond, talcum
Powder, mica powder and stearic acid are dispersed in elastomeric thermoplastic's polyurethane rubber, improve the equal of elastic concretion abrasive performance
Even property prevents product Local Property deviation larger, reduces the generation of product quality and yield rate.
The present invention when diamond, talcum powder, mica powder and stearic acid are mixed, to the diamond, talcum powder,
Mica powder and the not special requirement of stearic hybrid manipulation sequence, prepare mixed powder using well known to those skilled in the art
The technical solution of body.
The present invention is preferably dried obtained mixed powder after obtaining mixed powder；The temperature of the drying
Preferably 80~120 DEG C of degree, more preferably 90~110 DEG C, most preferably 100 DEG C；The time of the drying is preferably 4~6h,
More preferably 5h.In the present invention, the moisture in powder can be sufficiently discharged in the drying process process, ensure that material has and stablize
Preparation repeatability.
After drying process, the present invention preferably is kneaded obtained mixed powder and thermoplastic polyurethane rubber to obtain bullet
Property concretion abrasive；In the present invention, the temperature of the mixing is preferably 70~230 DEG C, and more preferably 100~220 DEG C, most preferably
It is 150~200 DEG C；The time of the mixing is preferably 1~2h, more preferably 1.5h；The rate of the mixing is preferably 30~
120r/min, more preferably 35~60r/min, most preferably 45r/min.
After mixing, the present invention will preferably be kneaded obtained elastic concretion abrasive and squeeze out shape or cylinder in blocks, obtain
Sheet or columned elastic concretion abrasive.
The present invention also provides a kind of application of elastic concretion abrasive in cambered surface polishing, comprising: with the elasticity
Concretion abrasive carries out grinding and polishing to hard brittle material cambered surface；
Elastic concretion abrasive is preferably pasted and is carried out on disk clamp or pole fixture to hard brittle material cambered surface by the present invention
Grinding and polishing；In the present invention, the hard brittle material includes potsherd, sapphire and glass.
In the present invention, the rate of the grinding and polishing preferably 1000~12000rpm, more preferable 1000~3000rpm, it is optimal
It is selected as 2000rpm.
Elastic concretion abrasive provided by the invention and the preparation method and application thereof is carried out below with reference to embodiment detailed
Illustrate, but they cannot be interpreted as limiting the scope of the present invention.
Embodiment 1
Step 1 weighs 10 parts of diamond, 24 parts of talcum powder, 15 parts of mica powder, 5 parts of stearic acid progress in parts by weight
It is mixed to get mixed powder, obtaining mixed powder, that 4h is dried under conditions of 100 DEG C of temperature is spare；
Wherein, diamond partial size is 2~4 μm,
10~15 μm of talcum powder partial size,
30~35 μm of mica powder partial size.
Step 2 weighs thermoplastic polyurethane elastic rubber under conditions of temperature is 180 DEG C, mixing rate is 45r/min
It is added in mixer together with mixed powder obtained in 45 parts of glue and step 1 and is kneaded 2h；
Mixing is obtained elastic concretion abrasive and is transferred quickly to extruder, squeezed out with a thickness of 3mm, breadth is by step 3
The plain film elasticity concretion abrasive of 150mm, is cut to disk for the plain film of extrusion, pastes on disk clamp, such as 12 institutes in attached drawing 1
Show.
Embodiment 2
Step 1 weighs 8 parts of diamond, 20 parts of talcum powder, 17 parts of mica powder, 10 parts of stearic acid progress in parts by weight
It is mixed to get mixed powder, obtaining mixed powder, that 6h is dried under conditions of 100 DEG C of temperature is spare；
Wherein, diamond partial size is 0.5~50 μm,
10~20 μm of talcum powder partial size,
30~35 μm of mica powder partial size.
Step 2 weighs thermoplastic polyurethane elastic rubber under conditions of temperature is 190 DEG C, mixing rate is 45r/min
It is added in mixer together with mixed powder obtained in 50 parts of glue and step 1 and is kneaded 1h；
Mixing is obtained elastic concretion abrasive and is transferred quickly to extruder, squeezed out with a thickness of 3mm, breadth is by step 3
The plain film elasticity concretion abrasive of 150mm, is cut to disk for the plain film of extrusion, pastes on disk clamp.
Embodiment 3
Step 1 weighs 9 parts of diamond, 20 parts of talcum powder, 15 parts of mica powder, 10 parts of stearic acid progress in parts by weight
It is mixed to get mixed powder, obtaining mixed powder, that 4h is dried under conditions of 100 DEG C of temperature is spare；
Wherein, diamond partial size is 5~10 μm,
10~15 μm of talcum powder partial size,
30~35 μm of mica powder partial size.
Step 2 weighs thermoplastic polyurethane elastic rubber under conditions of temperature is 200 DEG C, mixing rate is 45r/min
It is added in mixer together with mixed powder obtained in 45 parts of glue and step 1 and is kneaded 2h；
Mixing is obtained elastic concretion abrasive and is transferred quickly to extruder, squeezed out with a thickness of 3mm, breadth is by step 3
The plain film elasticity concretion abrasive of 150mm, is cut to disk for the plain film of extrusion, pastes on disk clamp.
Embodiment 4
Step 1 weighs 10 parts of diamond, 20 parts of talcum powder, 20 parts of mica powder, 5 parts of stearic acid progress in parts by weight
It is mixed to get mixed powder, obtaining mixed powder, that 4h is dried under conditions of 100 DEG C of temperature is spare；
Wherein, 2~10 μm of diamond partial size,
10~15 μm of talcum powder partial size,
30~35 μm of mica powder partial size.
Step 2 weighs thermoplastic polyurethane elastic rubber under conditions of temperature is 210 DEG C, mixing rate is 45r/min
It is added in mixer together with mixed powder obtained in 45 parts of glue and step 1 and is kneaded 2h；
Mixing is obtained elastic concretion abrasive and is transferred quickly to extruder, squeezed out with a thickness of 3mm, breadth is by step 3
The plain film elasticity concretion abrasive of 150mm, is cut to disk for the plain film of extrusion, pastes on disk clamp.
Embodiment 5
Step 1 weighs 8 parts of diamond, 20 parts of talcum powder, 15 parts of mica powder, 10 parts of stearic acid progress in parts by weight
It is mixed to get mixed powder, obtaining mixed powder, that 4h is dried under conditions of 100 DEG C of temperature is spare；
Wherein, diamond partial size is 1~30 μm,
10~20 μm of talcum powder partial size,
30~35 μm of mica powder partial size.
Step 2 weighs thermoplastic polyurethane elastic rubber under conditions of temperature is 205 DEG C, mixing rate is 45r/min
It is added in mixer together with mixed powder obtained in 47 parts of glue and step 1 and is kneaded 2h；
Mixing is obtained elastic concretion abrasive and is transferred quickly to extruder, squeezed out with a thickness of 3mm, breadth is by step 3
The plain film elasticity concretion abrasive of 150mm, is cut to disk for the plain film of extrusion, pastes on disk clamp.
Embodiment 6
Step 1 weighs 10 parts of diamond, 20 parts of talcum powder, 15 parts of mica powder, 5 parts of stearic acid progress in parts by weight
It is mixed to get mixed powder, obtaining mixed powder, that 4h is dried under conditions of 100 DEG C of temperature is spare；
Wherein, diamond partial size is 0.5~50 μm,
10~20 μm of talcum powder partial size,
30~35 μm of mica powder partial size.
Step 2 weighs thermoplastic polyurethane elastic rubber under conditions of temperature is 210 DEG C, mixing rate is 45r/min
It is added in mixer together with mixed powder obtained in 10 parts of glue and step 1 and is kneaded 2h；
Mixing is obtained elastic concretion abrasive and is transferred quickly to extruder, squeezed out with a thickness of 3mm, breadth is by step 3
The plain film elasticity concretion abrasive of 150mm, is cut to disk for the plain film of extrusion, pastes on disk clamp.
Embodiment 7
Step 1, in parts by weight, weigh 9 parts of diamond, 21 parts of talcum powder, 17 parts of mica powder, 5 parts of stearic acid mixed
Conjunction obtains mixed powder, and obtaining mixed powder, that 4h is dried under conditions of 100 DEG C of temperature is spare；
Wherein, diamond partial size is 0.5~50 μm,
10~20 μm of talcum powder partial size,
30~35 μm of mica powder partial size.
Step 2 weighs thermoplastic polyurethane elastic rubber under conditions of temperature is 220 DEG C, mixing rate is 45r/min
It is added in mixer together with mixed powder obtained in 45 parts of glue and step 1 and is kneaded 2h；
Mixing is obtained elastic concretion abrasive and is transferred quickly to extruder, squeezed out with a thickness of 3mm, breadth is by step 3
The plain film elasticity concretion abrasive of 150mm, is cut to disk for the plain film of extrusion, pastes on disk clamp.
Embodiment 8
The difference of embodiment 8 and embodiment 1 is only that: step 3, and mixing is obtained elastic concretion abrasive and is transferred quickly to
Extruder squeezes out the cylindrical pole that cylindrical diameter is 25mm；Cylindrical pole is cut into high 30mm, the circle of diameter 25mm
Cylinder elasticity concretion abrasive, as shown in 22 in attached drawing 2.
Embodiment 9
The difference of embodiment 9 and embodiment 2 is only that: step 3, and mixing is obtained elastic concretion abrasive and is transferred quickly to
Extruder squeezes out the cylindrical pole that cylindrical diameter is 25mm；Cylindrical pole is cut into high 30mm, the circle of diameter 25mm
Cylinder elasticity concretion abrasive.
Embodiment 10
The difference of embodiment 10 and embodiment 3 is only that: step 3, and mixing is obtained elastic concretion abrasive and is transferred quickly to
Extruder squeezes out the cylindrical pole that cylindrical diameter is 25mm；Cylindrical pole is cut into high 30mm, the circle of diameter 25mm
Cylinder elasticity concretion abrasive.
Embodiment 11
The difference of embodiment 11 and embodiment 4 is only that: step 3, and mixing is obtained elastic concretion abrasive and is transferred quickly to
Extruder squeezes out the cylindrical pole that cylindrical diameter is 25mm；Cylindrical pole is cut into high 30mm, the circle of diameter 25mm
Cylinder elasticity concretion abrasive.
Embodiment 12
The difference of embodiment 12 and embodiment 5 is only that: step 3, and mixing is obtained elastic concretion abrasive and is transferred quickly to
Extruder squeezes out the cylindrical pole that cylindrical diameter is 25mm；Cylindrical pole is cut into high 30mm, the circle of diameter 25mm
Cylinder elasticity concretion abrasive.
Embodiment 13
The difference of embodiment 13 and embodiment 6 is only that: step 3, and mixing is obtained elastic concretion abrasive and is transferred quickly to
Extruder squeezes out the cylindrical pole that cylindrical diameter is 25mm；Cylindrical pole is cut into high 30mm, the circle of diameter 25mm
Cylinder elasticity concretion abrasive.
Embodiment 14
The difference of embodiment 14 and embodiment 7 is only that: step 3, and mixing is obtained elastic concretion abrasive and is transferred quickly to
Extruder squeezes out the cylindrical pole that cylindrical diameter is 25mm；Cylindrical pole is cut into high 30mm, the circle of diameter 25mm
Cylinder elasticity concretion abrasive.
Test experiments 1:
Test method the following steps are included:
Step 1: the aluminum alloy round mill for being adhesive with plain film elasticity concretion abrasive in Examples 1 to 7 tool is mounted on always
It flows on magneto, motor is fixed on three axis shifting axle of an x, y, z by motor rated power 50W, rated speed 3000rpm
On；
Step 2: processed potsherd sample is vertically fixed on fixture (as shown in Figure 1), potsherd thickness
5mm, long 125mm, wide 60mm；
Step 3: adjustment is moved along x, y, z direction by motor, the disk in the outer circle region of elastic concretion abrasive is made to be located at quilt
The surface of the side of the potsherd of processing；
Step 4: starting direct current permanent magnet motor, is adjusted to 100rpm for motor speed, motor is made to be less than rated moment
Under the conditions of operate, motor is moved to (direction z in Fig. 1) straight down, elastic concretion abrasive is contacted with ceramic side and makes to rub
Power gradually increases, until motor shuts down, records the height and position (Z0) in the direction z at this time, closes motor power；
Step 5: first making elastic concretion abrasive move back and forth the (side y along the side of potsherd on the height and position of Z0
To), restart motor, and run motor under rated speed (3000rpm) and rated power (50w), is used in operational process
Recycle the blade edges water spray of hydraulic giant alignment rotation, water flow 1L/min, milling time 15min；
Ceramic surface roughness test: BRUKER (Dektak XT) step instrument
Ceramic surface depth of lines test: BRUKER (Dektak XT) step instrument
1. Examples 1 to 7 elasticity concretion abrasive of table and the existing hairbrush technique that clears off are to the quick milled processed in potsherd surface
The Comparative result of 15min:
It is handled from 1 test result of table it is found that doing quick fine gtinding to potsherd surface with plain film elasticity concretion abrasive,
The surface roughness of potsherd and surface pattern depth significantly reduce after 15min, and polishing effect is significantly improved, and with existing
Brush plate process is cleared off, the variation of potsherd surface is unobvious.
Test experiments 2:
The difference of test experiments 2 and test experiments 1 is only that step 1: cylinder body elasticity prepared by embodiment 8~14
Concretion abrasive epoxy adhesive is connected (as shown in Fig. 2) with round steel bar, is prepared into cylindrical bistrique, then pole is mounted on
On one direct current permanent magnet motor, motor rated power 50W, rated speed 3000rpm, then motor is fixed on an x, y, z three
On axis shifting axle.
2. embodiment of the present invention of table, 8~14 cylinder body elasticity concretion abrasive and the existing hairbrush technique that clears off are to potsherd surface
The Comparative result of quick milled processed 15min:
It is handled from 2 test result of table it is found that doing quick fine gtinding to potsherd surface with cylinder body elasticity concretion abrasive,
The surface roughness of potsherd and surface pattern depth significantly reduce after 15min, and polishing effect is significantly improved, and with existing
Brush plate process is cleared off, the variation of potsherd surface is unobvious.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered
It is considered as protection scope of the present invention.
Claims (7)
1. a kind of elasticity concretion abrasive, comprises the following components in parts by weight:
The partial size of the diamond is 0.5~50 μm；
The partial size of the talcum powder is 1~30 μm；
The partial size of the mica powder is 30~50 μm.
2. elasticity concretion abrasive according to claim 1, which is characterized in that comprise the following components in parts by weight:
3. the preparation method of elasticity concretion abrasive, includes the following steps: described in claim 1~2 any one
Diamond, talcum powder, mica powder and stearic acid are first mixed to get mixed powder, then again by mixed powder and thermoplasticity
Polyurethane rubber is kneaded.
4. the preparation method of elasticity concretion abrasive according to claim 3, which is characterized in that the temperature of the mixing is 70
~230 DEG C.
5. the preparation method of elasticity concretion abrasive according to claim 3, which is characterized in that the time of the mixing is 1
~2h.
6. according to the preparation method of elastic concretion abrasive described in claim 3,4 or 5, which is characterized in that the speed of the mixing
Rate is 30~120r/min.
7. preparation side described in any one of elasticity concretion abrasive or claim 3~6 described in claim 1~2 any one
Application of the elastic concretion abrasive that method obtains in cambered surface polishing, comprising: with the elastic concretion abrasive to hard brittle material cambered surface
Carry out grinding and polishing.
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| CN110387213B (en) * | 2019-04-02 | 2022-01-07 | 深圳市鑫意晟科技有限公司 | Method for manufacturing soft elastic abrasive, cutting tool and method for processing die |
| CN110861236A (en) * | 2019-11-21 | 2020-03-06 | 深圳兰品科技有限公司 | Production method of precise elastic abrasive particles |
| CN112536733B (en) * | 2020-12-03 | 2022-03-22 | 郑州磨料磨具磨削研究所有限公司 | Ultra-precise grinding wheel and preparation method and application thereof |
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Address after: 8 / F, 53 fofu Road, foziao village, Dalang Town, Dongguan City, Guangdong Province 523000 Patentee after: Dongguan Zhongwei Lihe Semiconductor Technology Co.,Ltd. Address before: 8 / F, 53 fofu Road, foziao village, Dalang Town, Dongguan City, Guangdong Province 523000 Patentee before: DONGGUAN CITY ZONEWE NANO TECHNOLOGY Co.,Ltd. |