CN107604647A - A kind of antibiotic ultraviolet-resistant brocade cotton - Google Patents
A kind of antibiotic ultraviolet-resistant brocade cotton Download PDFInfo
- Publication number
- CN107604647A CN107604647A CN201710932151.4A CN201710932151A CN107604647A CN 107604647 A CN107604647 A CN 107604647A CN 201710932151 A CN201710932151 A CN 201710932151A CN 107604647 A CN107604647 A CN 107604647A
- Authority
- CN
- China
- Prior art keywords
- parts
- cotton
- bright
- dressing liquid
- quaternary ammonium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920000742 Cotton Polymers 0.000 title claims abstract description 23
- 230000003115 biocidal effect Effects 0.000 title claims abstract description 8
- 239000007788 liquid Substances 0.000 claims abstract description 12
- -1 quaternary ammonium salt modified nano-titanium dioxide Chemical class 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims abstract description 8
- 238000001035 drying Methods 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 4
- OBFQBDOLCADBTP-UHFFFAOYSA-N aminosilicon Chemical compound [Si]N OBFQBDOLCADBTP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000000839 emulsion Substances 0.000 claims abstract description 4
- 239000000203 mixture Substances 0.000 claims abstract description 4
- 239000003921 oil Substances 0.000 claims abstract description 4
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 4
- 238000005096 rolling process Methods 0.000 claims abstract description 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 9
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 6
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 6
- 239000000243 solution Substances 0.000 claims description 4
- 235000019270 ammonium chloride Nutrition 0.000 claims description 3
- 235000019441 ethanol Nutrition 0.000 claims description 3
- 125000005909 ethyl alcohol group Chemical group 0.000 claims description 3
- 239000012065 filter cake Substances 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 239000011259 mixed solution Substances 0.000 claims description 3
- 235000006408 oxalic acid Nutrition 0.000 claims description 3
- ONJQDTZCDSESIW-UHFFFAOYSA-N polidocanol Chemical compound CCCCCCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO ONJQDTZCDSESIW-UHFFFAOYSA-N 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 3
- 239000000758 substrate Substances 0.000 claims description 3
- 239000000725 suspension Substances 0.000 claims description 3
- PZJJKWKADRNWSW-UHFFFAOYSA-N trimethoxysilicon Chemical compound CO[Si](OC)OC PZJJKWKADRNWSW-UHFFFAOYSA-N 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims 3
- 229920000728 polyester Polymers 0.000 claims 3
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical class [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 claims 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 claims 1
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 3
- 241000894006 Bacteria Species 0.000 description 3
- 125000000217 alkyl group Chemical group 0.000 description 2
- 230000000845 anti-microbial effect Effects 0.000 description 2
- 238000009395 breeding Methods 0.000 description 2
- 230000001488 breeding effect Effects 0.000 description 2
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 230000003071 parasitic effect Effects 0.000 description 2
- 230000002411 adverse Effects 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000000644 propagated effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of antibiotic ultraviolet-resistant brocade cotton, prepared by following finishing technique：A, bright and beautiful cotton is immersed into dressing liquid 15min；B, an immersing and rolling；C, 120 DEG C of drying 3min, 170 DEG C 190 DEG C bake 4min.The composition of described dressing liquid is：22 parts of organosilicon quaternary ammonium salt modified nano-titanium dioxide, 3 parts of polyvinyl alcohol, 92 parts of AEO, 5 parts of amino silicon oil emulsion, 318 parts of water.In step a, the bath raio of bright and beautiful cotton and dressing liquid is 1: 10.In step b, the pick-up rate of bright and beautiful cotton 80% 100%.Bright and beautiful cotton of the present invention has good antibacterial and uvioresistant effect, also with good flexibility, smooth feeling.
Description
Technical field
The invention belongs to textile yarn technical field, and specifically, the present invention relates to a kind of antibiotic ultraviolet-resistant brocade cotton yarn
Line.
Background technology
Yarn, the fabric being made up of fiber, due to the chemical constitution of its porous type body form and high molecular polymer profit
Adhere in microorganism, turn into microbe survival, the good parasitic body of breeding.Parasitic body can also be dirty in addition to the harm to human body
Fiber is contaminated, thus the main purpose of antimicrobial yarn is exactly to eliminate these adverse effects.
Antimicrobial yarn has good antibacterial action, can eliminate because of bacterium and caused by peculiar smell, fabric is kept clean and tidy,
Avoiding the breeding of bacterium to play simultaneously reduces the risk propagated again.
The content of the invention
It is an object of the present invention to provide a kind of antibiotic ultraviolet-resistant brocade cotton, by padding finishing liquid, possesses yarn anti-
Bacterium anti-ultraviolet function.
To achieve the above object, the technical solution adopted by the present invention is：
A kind of antibiotic ultraviolet-resistant brocade cotton, is prepared by following finishing technique：
A, bright and beautiful cotton is immersed into dressing liquid 15min；
B, an immersing and rolling；
C, 120 DEG C of drying 3min, 170 DEG C -190 DEG C bake 4min.
The composition of described dressing liquid is：
22 parts of organosilicon quaternary ammonium salt modified nano-titanium dioxide
3 parts of polyvinyl alcohol
2 parts of AEO-9
5 parts of amino silicon oil emulsion
318 parts of water.
The preparation method of described organosilicon quaternary ammonium salt modified nano-titanium dioxide is：
50 parts of nano titanium oxide is added in the mixed solution that 500mL volume ratios are 3: 1 absolute ethyl alcohols/water,
Make its fully dispersed under 3000r/min high speed shears, when 70 DEG C or so of reaction temperature, addition mass fraction is 10 parts of dimethyl ten
Eight alkyl [3- (trimethoxy silicon substrate) propyl group] ammonium chloride, with oxalic acid solution regulation system pH value to 4 or so.Reacting 60min will
Nano titanium oxide suspension filters, and filter cake produces organosilicon quaternary ammonium salt modified nano-titanium dioxide powder through drying, grinding.
Described finishing technique, in step a, the bath raio of bright and beautiful cotton and dressing liquid is 1: 10.
Described finishing technique, in step b, the pick-up rate 80%-100% of bright and beautiful cotton.
Bright and beautiful cotton of the present invention has good antibacterial and uvioresistant effect, also with good flexibility,
Smooth feeling.
Embodiment
Embodiment 1：
A kind of antibiotic ultraviolet-resistant brocade cotton, specification are 50/50 40s/2, are prepared by following finishing technique：
A, bright and beautiful cotton is immersed into dressing liquid 15min, bath raio 1: 10；
B, an immersing and rolling, pick-up rate 80%-100%；
C, 120 DEG C of drying 3min, 170 DEG C -190 DEG C bake 4min.
The composition of described dressing liquid is：
22 parts of organosilicon quaternary ammonium salt modified nano-titanium dioxide
3 parts of polyvinyl alcohol
2 parts of AEO-9
5 parts of amino silicon oil emulsion
318 parts of water.
The preparation method of described organosilicon quaternary ammonium salt modified nano-titanium dioxide is：
50 parts of nano titanium oxide is added in the mixed solution that 500mL volume ratios are 3: 1 absolute ethyl alcohols/water,
Make its fully dispersed under 3000r/min high speed shears, when 70 DEG C or so of reaction temperature, addition mass fraction is 10 parts of dimethyl ten
Eight alkyl [3- (trimethoxy silicon substrate) propyl group] ammonium chloride, with oxalic acid solution regulation system pH value to 4 or so.Reacting 60min will
Nano titanium oxide suspension filters, and filter cake produces organosilicon quaternary ammonium salt modified nano-titanium dioxide powder through drying, grinding.
Claims (4)
1. a kind of antibiotic ultraviolet-resistant brocade cotton, is prepared by following finishing technique：
A, bright and beautiful cotton is immersed into dressing liquid 15min；
B, an immersing and rolling；
C, 120 DEG C of drying 3min, 170 DEG C -190 DEG C bake 4min,
The composition of described dressing liquid is：
22 parts of organosilicon quaternary ammonium salt modified nano-titanium dioxide
3 parts of polyvinyl alcohol
2 parts of AEO-9
5 parts of amino silicon oil emulsion
318 parts of water.
A kind of 2. Antistatic polyester cotton blending yarn according to claim 1, it is characterised in that：Described organosilicon quaternary ammonium salt
The preparation method of modified nano-titanium dioxide is：
50 parts of nano titanium oxide is added in the mixed solution that 500mL volume ratios are 3: 1 absolute ethyl alcohols/water, in 3000r/
Make its fully dispersed under min high speed shears, when 70 DEG C or so of reaction temperature, addition mass fraction is 10 parts of dimethyl stearyls
[3- (trimethoxy silicon substrate) propyl group] ammonium chloride, with oxalic acid solution regulation system pH value to 4 or so.60min is reacted by nanometer two
Titanium oxide suspension filters, and filter cake produces organosilicon quaternary ammonium salt modified nano-titanium dioxide powder through drying, grinding.
A kind of 3. Antistatic polyester cotton blending yarn according to claim 1, it is characterised in that：Described finishing technique, step
In rapid a, the bath raio of bright and beautiful cotton and dressing liquid is 1: 10.
A kind of 4. Antistatic polyester cotton blending yarn according to claim 1, it is characterised in that：Described finishing technique, step
In rapid b, the pick-up rate 80%-100% of bright and beautiful cotton.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710932151.4A CN107604647A (en) | 2017-09-29 | 2017-09-29 | A kind of antibiotic ultraviolet-resistant brocade cotton |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710932151.4A CN107604647A (en) | 2017-09-29 | 2017-09-29 | A kind of antibiotic ultraviolet-resistant brocade cotton |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107604647A true CN107604647A (en) | 2018-01-19 |
Family
ID=61068705
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710932151.4A Pending CN107604647A (en) | 2017-09-29 | 2017-09-29 | A kind of antibiotic ultraviolet-resistant brocade cotton |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107604647A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109295734A (en) * | 2018-10-10 | 2019-02-01 | 五邑大学 | Water- and oil-repellent fabric finishing agent, preparation method of water- and oil-repellent fabric, water- and oil-repellent fabric and application thereof |
| CN114318855A (en) * | 2022-01-18 | 2022-04-12 | 苍南县合帮纺织有限公司 | Blended regenerated cotton yarn and preparation method thereof |
-
2017
- 2017-09-29 CN CN201710932151.4A patent/CN107604647A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109295734A (en) * | 2018-10-10 | 2019-02-01 | 五邑大学 | Water- and oil-repellent fabric finishing agent, preparation method of water- and oil-repellent fabric, water- and oil-repellent fabric and application thereof |
| CN109295734B (en) * | 2018-10-10 | 2021-06-08 | 五邑大学 | Water- and oil-repellent fabric finishing agent, preparation method of water- and oil-repellent fabric, water- and oil-repellent fabric and application thereof |
| CN114318855A (en) * | 2022-01-18 | 2022-04-12 | 苍南县合帮纺织有限公司 | Blended regenerated cotton yarn and preparation method thereof |
| CN114318855B (en) * | 2022-01-18 | 2024-01-26 | 苍南县合帮纺织有限公司 | Blending regenerated cotton yarn and preparation method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180119 |