CN107603456A - A kind of UV solidifies anti-paste light diffusion coating and preparation method thereof - Google Patents
A kind of UV solidifies anti-paste light diffusion coating and preparation method thereof Download PDFInfo
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- CN107603456A CN107603456A CN201611011191.7A CN201611011191A CN107603456A CN 107603456 A CN107603456 A CN 107603456A CN 201611011191 A CN201611011191 A CN 201611011191A CN 107603456 A CN107603456 A CN 107603456A
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- light diffusion
- diffusion coating
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- silane coupler
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- 238000000576 coating method Methods 0.000 title claims abstract description 60
- 239000011248 coating agent Substances 0.000 title claims abstract description 57
- 238000009792 diffusion process Methods 0.000 title claims abstract description 55
- 238000002360 preparation method Methods 0.000 title abstract description 12
- 238000007711 solidification Methods 0.000 claims abstract description 27
- 230000008023 solidification Effects 0.000 claims abstract description 27
- 239000011347 resin Substances 0.000 claims abstract description 19
- 229920005989 resin Polymers 0.000 claims abstract description 19
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000003085 diluting agent Substances 0.000 claims abstract description 17
- 239000002245 particle Substances 0.000 claims abstract description 17
- 229910000077 silane Inorganic materials 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 14
- 239000012752 auxiliary agent Substances 0.000 claims description 15
- 239000000463 material Substances 0.000 claims description 11
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 10
- BPSIOYPQMFLKFR-UHFFFAOYSA-N trimethoxy-[3-(oxiran-2-ylmethoxy)propyl]silane Chemical group CO[Si](OC)(OC)CCCOCC1CO1 BPSIOYPQMFLKFR-UHFFFAOYSA-N 0.000 claims description 10
- 239000004593 Epoxy Substances 0.000 claims description 9
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 9
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical group FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 claims description 9
- 238000012986 modification Methods 0.000 claims description 9
- 230000004048 modification Effects 0.000 claims description 9
- 229920003229 poly(methyl methacrylate) Polymers 0.000 claims description 9
- 239000004926 polymethyl methacrylate Substances 0.000 claims description 9
- 229920005573 silicon-containing polymer Polymers 0.000 claims description 9
- 239000011521 glass Substances 0.000 claims description 7
- 229920000058 polyacrylate Polymers 0.000 claims description 5
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 239000011737 fluorine Substances 0.000 claims description 4
- 229910052731 fluorine Inorganic materials 0.000 claims description 4
- 238000012545 processing Methods 0.000 claims description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical class OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 2
- 239000012788 optical film Substances 0.000 claims description 2
- 239000011856 silicon-based particle Substances 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims 1
- 150000002148 esters Chemical class 0.000 claims 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims 1
- 125000004805 propylene group Polymers [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims 1
- 238000002525 ultrasonication Methods 0.000 abstract description 6
- 238000000016 photochemical curing Methods 0.000 abstract description 2
- 239000002904 solvent Substances 0.000 abstract description 2
- 238000003756 stirring Methods 0.000 description 7
- 238000013019 agitation Methods 0.000 description 5
- 230000002045 lasting effect Effects 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 239000010408 film Substances 0.000 description 4
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 230000003287 optical effect Effects 0.000 description 3
- -1 poly dimethyl silicon Oxygen alkane Chemical class 0.000 description 3
- 238000002834 transmittance Methods 0.000 description 3
- 239000004925 Acrylic resin Substances 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 238000001723 curing Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- 238000005286 illumination Methods 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000003595 mist Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 239000004814 polyurethane Substances 0.000 description 2
- 238000012827 research and development Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229920000178 Acrylic resin Polymers 0.000 description 1
- 239000004820 Pressure-sensitive adhesive Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 230000003670 easy-to-clean Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 238000003384 imaging method Methods 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
Abstract
The invention belongs to technical field of coatings, more particularly to a kind of UV solidification light diffusion coating and preparation method thereof.The raw materials by weight portion proportioning of UV solidification light diffusion coating is as follows：15 40 parts of resin, 30 60 parts of diluent, 2 10 parts of light trigger, 13 parts of silane coupler, 5 15 parts of light diffusion particle.Preparation method is to weigh raw material：Each raw material is weighed by required number；30% diluent and silane coupler of light diffusion particle parts by weight, carry out ultrasonication 30 minutes, pre-dispersed；70% diluent of resin, light trigger and parts by weight is added into obtained solution, is stirred, is stirred, that is, UV solidification light diffusion coating is made.Light diffusion coating does not contain volatile solvent, belongs to environment-friendly type coating, and uses ultraviolet photo-curing, and hardening time is short.
Description
Technical field
The invention belongs to technical field of coatings, more particularly to a kind of UV to solidify anti-paste light diffusion coating and its preparation side
Method.
Background technology
Light diffusion coating is a kind of material with special optical characteristic, by adding light diffusion particle, forms surface
Microlens structure, reach optics diffusion effect.Spot light can be converted into area source by optical diffusion film, form light unrestrained anti-
Penetrate, reach the effect of even light.Therefore, the optical material has important in the systems such as FPD, laser, LED illumination and imaging
Application, be widely used in LCD TV, liquid crystal display, tablet personal computer, laptop computer, mobile phone, light fixture, indoor lamp source with
And the application such as advertising lamp box.
UV is coating material solidified, be by the use of ultraviolet light energy trigger coating in low molecule performed polymer or oligomer and as work
Property diluent monomer molecule between polymerization and cross-linking reaction, obtain hardening paint film, it is real essentially by forming chemical bond
Existing chemical seasoning.The advantages of curing system coating material solidified due to UV, protrudes, and turns into very active research and development field in recent years,
Research and development and accreditation of the people to it are also more and more deep, and application in the industry is more and more extensive.
The content of the invention
The invention provides a kind of UV to solidify anti-paste light diffusion coating and preparation method thereof.Light diffusion coating does not contain
Volatile solvent, belong to environment-friendly type coating, and use ultraviolet photo-curing, hardening time is short.Coating has light diffusion simultaneously
With anti-paste dual-use function.
To achieve these goals, UV solidifications light diffusion coating provided by the invention, raw materials by weight portion proportioning are as follows：
Resin 15-40 parts, diluent 30-60 parts, light trigger 2-10 parts, silane coupler 1-3 parts, light diffusion particle 5-15 parts, prevent
Scribble auxiliary agent 1-3 parts.
To achieve these goals, the present invention also provides the preparation method that above-mentioned UV solidifies anti-paste light diffusion coating, tool
Body comprises the following steps.
Step 1, weigh raw material：Each raw material is weighed by required number, the wherein particle diameter of light diffusion particle is 0.5-3um.
Step 2, decentralized processing：30% diluent and silane coupler of light diffusion particle and parts by weight, carry out ultrasonic wave
Processing, it is pre-dispersed；70% diluent, the anti-graffiti auxiliary agent of resin, light trigger and parts by weight are added into obtained solution,
It is stirred, that is, UV solidification light diffusion coating is made.
Described resin is polyurethane-modified polyacrylate resin or epoxy modified acrylic resin.
Described diluent is one kind in IBOA or EOEOEA.
Described light trigger is light trigger 184.
Described silane coupler is one kind in silane coupler KH560 or silane coupler KH570.
Described light diffusion particle is organic silicon particle, one kind in PMMA particles or glass microballoon.
Described anti-graffiti auxiliary agent is organosilicon auxiliary agent or fluorine auxiliary agent；Described organosilicon auxiliary agent is preferably poly dimethyl silicon
Oxygen alkane, described fluorine auxiliary agent is preferably fluorocarbon resin.
Described UV solidification light diffusion coating is used for optical film material and sheet material field.
Beneficial effects of the present invention.
In the present invention, the coating material solidified coating with light diffusion function of UV has superelevation light transmittance, and the light of injection occurs
After diffraction, diffraction, refraction, reflection or the efficient combination of scattering, the light for making injection by the micro-structural of material spreads, and forms light
Line is uniform, the shadow surface that briliancy improves, improves light source luminous point problem；The anti-scribble auxiliary agent added, greatly improves coating
The smooth degree on surface, adhesive sticker pressure sensitive adhesive is set not paste, the pollutant such as dust easily cleans.Avoided in technical scheme using big
The volatile organic solvent of amount, environment will not be polluted, greatly reduce VOC discharge capacity, improve the peace of the present invention
Quan Xing；The coating of the present invention need not add substantial amounts of curing agent, the double bond in resin by ultraviolet light irradiation be it is curable,
Hardening time is short, and effect is good, the addition of various auxiliary agents, coating is had good adhesive force to a variety of base materials, into film hardness height；
As outdoor advertising more and more employs LED illumination mode to requirement more and more higher attractive in appearance and environmentally friendly, outdoor lamp house.Lamp
Case needs to fall apart using the light with diffusion function.Coating is spread using anti-paste light easy to clean, the effect of even light can be reached,
And can effectively prevents lamp box from being stuck small advertisement and dust, is highly susceptible to cleaning.The coating of the present invention belongs to comprehensive coating,
Existing light diffusion function, and can avoids coating from being scribbled after coating, and coating is convenient；Technique is simple, easy to operate, is easy to give birth to
Production and use.
Embodiment
With specific embodiment, the present invention will be further described below.
Embodiment 1.
35 parts of polyurethane-modified polyacrylate, 48 parts of IBOA, 184 3 parts of light trigger, 12 parts of organosilicon, silane are even
Join 2 parts of agent KH570,3 parts of dimethyl silicone polymer.
The preparation method of above-mentioned UV solidifications light diffusion coating, specifically includes following steps：First by organosilicon spread powder（Particle diameter
For 0.8um）With it is a small amount of（30%）IBOA, silane coupler KH570, carry out ultrasonication 30 minutes, pre-dispersed, add poly-
Urethane modified acrylate ester, light trigger 184 and remaining diluent IBOA, dimethyl silicone polymer, lasting stirring, during stirring
Between 1 hour, agitation revolution 800rmp, until each composition is uniformly dispersed, that is, UV solidification light diffusion coating is made.
Embodiment 2.
38 parts of epoxy modification acrylate, 46 parts of IBOA, 184 3 parts of light trigger, 10 parts of PMMA, silane coupler
3 parts of KH560,1 part of dimethyl silicone polymer.
The preparation method of above-mentioned UV solidifications light diffusion coating, specifically includes following steps：First by PMMA spread powders（Particle diameter is
2um）IBOA, silane coupler KH560 with 30%, carry out ultrasonication 30 minutes, and progress is pre-dispersed, adds epoxy and changes
Property acrylate, light trigger 184 and remaining diluent IBOA, dimethyl silicone polymer, lasting stirring, mixing time 1 is small
When, agitation revolution 800rmp, until each composition is uniformly dispersed, that is, UV solidification light diffusion coating is made.
Embodiment 3.
35 parts of polyurethane-modified polyacrylate, 48 parts of IBOA, 184 3 parts of light trigger, 12 parts of glass microballoon, silane are even
Join 2 parts of agent KH570,2 parts of dimethyl silicone polymer.
The preparation method of above-mentioned UV solidifications light diffusion coating, specifically includes following steps：First by glass microballoon spread powder（Grain
Footpath is 2um）IBOA, silane coupler KH560 with 30%, carry out ultrasonication 30 minutes, and progress is pre-dispersed, adds poly-
Urethane modified acrylate ester, light trigger 184 and remaining diluent IBOA, dimethyl silicone polymer, lasting stirring, during stirring
Between 1 hour, agitation revolution 800rmp, until each composition is uniformly dispersed, that is, UV solidification light diffusion coating is made.
Embodiment 4.
15 parts of epoxy modification acrylate, 30 parts of EOEOEA, 184 2 parts of light trigger, 3 parts of silane coupler KH560,
5 parts of PMMA, 3 parts of fluorocarbon resin.
The preparation method of above-mentioned UV solidifications light diffusion coating, specifically includes following steps：First by glass microballoon spread powder (grain
Footpath is 1um) EOEOEA, silane coupler KH560 with 30%, ultrasonication 30 minutes is carried out, carries out pre-dispersed, is added
Epoxy modification acrylate, light trigger 184 and remaining diluent IBOA, fluorocarbon resin, lasting stirring, mixing time 1 are small
When, agitation revolution 800rmp, until each composition is uniformly dispersed, that is, UV solidification light diffusion coating is made.
Embodiment 5.
40 parts of epoxy modification acrylate, 60 parts of IBOA, 184 10 parts of light trigger, 1 part of PMMA, silane coupler
15 parts of KH560,1 part of fluorocarbon resin.
The preparation method of above-mentioned UV solidifications light diffusion coating, specifically includes following steps：First by glass microballoon spread powder (grain
Footpath is 2u) IBOA, silane coupler KH560 with 30%, ultrasonication 30 minutes is carried out, carries out pre-dispersed, adds ring
Oxygen modification acrylate, light trigger 184 and remaining diluent IBOA, fluorocarbon resin, lasting stirring, mixing time 1 hour,
Agitation revolution 800rmp, until each composition is uniformly dispersed, that is, UV solidification light diffusion coating is made.
Polyurethane-modified polyacrylate described in above-described embodiment 1 to 5 is purchased in Sartomer Guangzhou Chemical Co., Ltd.；Ring
Oxygen modification acrylate is purchased in Changxing synthetic resin（Changshu）Co., Ltd；Fluorocarbon resin is purchased limited in group of China of Du Pont
Company.
The light diffusion coating of certain manufacturer production to being bought in above-described embodiment 1 to 5 and market carries out performance detection, detection
As a result it is as shown in table 1.
The embodiment 1 to 5 of table 1 and the results of performance analysis of commercially available light diffusion coating.
| Performance | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Commercially available light spreads coating |
| Light transmittance（%） | 89.35 | 89.31 | 89.27 | 89.23 | 90.15 | 88.54 |
| Mist degree（%） | 91.05 | 89.32 | 92.33 | 89.12 | 88.39 | 82.31 |
| Case hardness | 2H | 2H | 2H | 2H | 2H | H |
| Adhesive force（PC films） | 0 grade | 0 grade | 0 grade | 0 grade | 0 grade | 0 grade |
| VOC content（%） | 0 | 0 | 0 | 0 | 0 | 42 |
As can be seen here, coating light transmittance of the invention and mist are all preferable, are above commercially available light diffusion coating, and VOC
Content is 0, belongs to Environmentally friendly coatings.
Claims (10)
1. a kind of UV solidifications light diffusion coating, it is characterised in that its raw material is included by number proportioning：Resin 15-40 parts, diluent
30-60 parts, light trigger 2-10 parts, silane coupler 1-3 parts, light diffusion particle 5-15 parts, anti-graffiti auxiliary agent 1-3 parts.
2. UV solidifications light diffusion coating as claimed in claim 1, it is characterised in that described resin is polyurethane-modified propylene
Acid esters resin or epoxy-modified acrylic acid resin.
3. UV as claimed in claim 1 solidification light diffusion coating, it is characterised in that described diluent include IBOA and
EOEOEA；Described light trigger is light trigger 184；Described silane coupler is silane coupler KH560 and silane is even
Join agent KH570；Described light diffusion particle includes organic silicon particle, PMMA particles and glass microballoon；Described anti-graffiti auxiliary agent
For organosilicon auxiliary agent and fluorine auxiliary agent；Described organosilicon auxiliary agent is preferably dimethyl silicone polymer, and described fluorine auxiliary agent is preferably
Fluorocarbon resin.
4. UV solidifications light diffusion coating as claimed in claim 1, it is characterised in that its raw materials by weight portion proportioning is as follows：
35 parts of polyurethane-modified polyacrylate, 48 parts of IBOA, 184 3 parts of light trigger, 12 parts of organosilicon, silane coupler KH570
2 parts, 3 parts of dimethyl silicone polymer.
5. UV solidifications light diffusion coating as claimed in claim 1, it is characterised in that its raw materials by weight portion proportioning is as follows：
Epoxy modification acrylate 38, IBOA 46, light trigger 184 3, PMMA 10, silane coupler KH560 3, poly dimethyl
Siloxanes 1.
6. UV solidifications light diffusion coating as claimed in claim 1, it is characterised in that its raw materials by weight portion proportioning is as follows：
35 parts of polyurethane-modified polyacrylate, 48 parts of IBOA, 184 3 parts of light trigger, 12 parts of glass microballoon, silane coupler
2 parts of KH570,2 parts of dimethyl silicone polymer.
7. UV solidifications light diffusion coating as claimed in claim 1, it is characterised in that its raw materials by weight portion proportioning is as follows：
15 parts of epoxy modification acrylate, 30 parts of EOEOEA, 184 2 parts of light trigger, 3 parts of silane coupler KH560, PMMA 5
Part, 3 parts of fluorocarbon resin.
8. UV solidifications light diffusion coating as claimed in claim 1, it is characterised in that its raw materials by weight portion proportioning is as follows：
40 parts of epoxy modification acrylate, 60 parts of IBOA, 184 10 parts of light trigger, 1 part of PMMA, silane coupler KH560 15
Part, 1 part of fluorocarbon resin.
9. the UV solidification light diffusion coating as described in claim 1-8, it is characterised in that specifically include following steps：
Step 1, weigh raw material：Each raw material is weighed by required number, the wherein particle diameter of light diffusion particle is 0.5-3um；
Step 2, decentralized processing：30% diluent and silane coupler of light diffusion particle parts by weight, carry out at ultrasonic wave
Reason, it is pre-dispersed；70% diluent of resin, light trigger and parts by weight is added into obtained solution, is stirred,
UV solidification light diffusion coating is made.
10. the UV solidification light diffusion coating as described in claim 1-9 is any, it is characterised in that for optical film material and sheet material
Field.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611011191.7A CN107603456A (en) | 2016-11-17 | 2016-11-17 | A kind of UV solidifies anti-paste light diffusion coating and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611011191.7A CN107603456A (en) | 2016-11-17 | 2016-11-17 | A kind of UV solidifies anti-paste light diffusion coating and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107603456A true CN107603456A (en) | 2018-01-19 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611011191.7A Pending CN107603456A (en) | 2016-11-17 | 2016-11-17 | A kind of UV solidifies anti-paste light diffusion coating and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110908234A (en) * | 2018-08-28 | 2020-03-24 | 深圳光峰科技股份有限公司 | Curing glue and its projection screen |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103044996A (en) * | 2012-12-24 | 2013-04-17 | 东莞上海大学纳米技术研究院 | A kind of solvent-free UV curing light diffusion coating material, preparation method and application thereof |
| CN105585917A (en) * | 2015-12-18 | 2016-05-18 | 李小鹏 | Water-based light diffusion coating and preparation method thereof |
| CN105802398A (en) * | 2016-03-15 | 2016-07-27 | 盘锦凯米特新材料有限公司 | Environment-friendly water-based photodiffusion coating and preparation method and application thereof |
-
2016
- 2016-11-17 CN CN201611011191.7A patent/CN107603456A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103044996A (en) * | 2012-12-24 | 2013-04-17 | 东莞上海大学纳米技术研究院 | A kind of solvent-free UV curing light diffusion coating material, preparation method and application thereof |
| CN105585917A (en) * | 2015-12-18 | 2016-05-18 | 李小鹏 | Water-based light diffusion coating and preparation method thereof |
| CN105802398A (en) * | 2016-03-15 | 2016-07-27 | 盘锦凯米特新材料有限公司 | Environment-friendly water-based photodiffusion coating and preparation method and application thereof |
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| Title |
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| CN110908234A (en) * | 2018-08-28 | 2020-03-24 | 深圳光峰科技股份有限公司 | Curing glue and its projection screen |
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Application publication date: 20180119 |