CN107541341A - Fragrant line fructus amomi essence and its application in a kind of ramuscule filter stick - Google Patents
Fragrant line fructus amomi essence and its application in a kind of ramuscule filter stick Download PDFInfo
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- CN107541341A CN107541341A CN201710846804.7A CN201710846804A CN107541341A CN 107541341 A CN107541341 A CN 107541341A CN 201710846804 A CN201710846804 A CN 201710846804A CN 107541341 A CN107541341 A CN 107541341A
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Abstract
The invention belongs to ramuscule cigarette filter rod production technical field, and in particular to fragrant line fructus amomi essence and its patent application of application in a kind of ramuscule filter stick.It is calculated in mass percent, it is composed of the following components：2.0 ~ 4.0% Bronyl acetate, 0.05 ~ 0.1% linalool, 0.1 ~ 0.2% linalool oxide, 0.05 ~ 0.1% nerolidol, 0.2 ~ 0.5% borneol, 0.05 ~ 0.1% lemon oil, 0.1 ~ 0.2% folium eucalypti absolute oil, 0.05 ~ 0.1% carvol, 94.7 ~ 97.4% Glycerin, mixed triester with caprylic acid capric acid.The application coordinates the improvement of ramuscule cigarette filter rod structure while fragrant line is with fructus amomi essence in providing a kind of ramuscule cigarette with peat-reek, can preferably improve the effect of sucking of ramuscule cigarette, and improvement effect is obvious, has preferable practical value.
Description
Technical field
The invention belongs to ramuscule cigarette filter rod production technical field, and in particular to fragrant line is fragrant with fructus amomi in a kind of ramuscule filter stick
Essence and its patent application of application.
Background technology
With the continuous improvement of people's living standards, the cigarette kind on cigarette market is also increasingly abundanter, also it is consumption
Person provides more choices, and ramuscule cigarette is exactly typical case therein.From the point of view of effective sale effect, ramuscule cigarette is unique with it
Glamour conquered increasing consumer.
From the point of view of cigarette quality, the tar content of ramuscule cigarette is more general than regular-size cigarette low, and suction taste is also thin, thus comparison operators
The demand of particular consumer is closed, the urban woman for being particularly subject to follow the fashion, graceful, fashion is lived consumes the especially blue or green of family
Look at.And as the fast development of low-coke tar cigarette, advantage of the ramuscule cigarette in terms of " tar reduction is protected fragrant " just seem especially noticeable.
Due to occupying the relatively small number of innate advantage of cigarette small volume, releasing content of coke tar, ramuscule cigarette also goes out simultaneously
The problems such as smoke is light, fragrance is insufficient is showed, thus it is promoted the crowd of being applicable and certain limitation be present.Therefore, existing cigarette
Manufacturing enterprise is also cracking this technical barrier by reducing many technological means such as filter stick pressure drop, optimization tobacco structure.
In terms of the ramuscule cigarette flavouring, in prior art thinking, mainly using the forms such as perfume particles, essence capsule come
Supplement or increase cigarette fragrance, but this release of several ramuscule cigarette flavouring mode generally existing fragrance is uneven, the resting period is short,
The defects of with flue gas inaccurate coordination, so that improving fragrance effect is not obvious enough.Thus pole is necessary in existing flavouring mode
On the basis of, comprehensive means are further improved etc. by composition, flavouring mode, further to improve the uniformity of flavouring, steady
Qualitative and harmony.
The content of the invention
Present invention aims at a kind of fructus amomi essence for fragrant line in ramuscule filter stick of offer, while coordinate ramuscule filter stick
The improvement of configuration aspects, while abundant ramuscule cigarette type, further improve the flavouring effect of ramuscule cigarette.
Details are as follows for the technical scheme that the application is taken.
Fragrant line fructus amomi essence, is calculated in mass percent in a kind of ramuscule filter stick, composed of the following components：
2.0 ~ 4.0% Bronyl acetate, 0.05 ~ 0.1% linalool, 0.1 ~ 0.2% linalool oxide,
0.05 ~ 0.1% nerolidol, 0.2 ~ 0.5% borneol, 0.05 ~ 0.1% lemon oil, 0.1 ~ 0.2% folium eucalypti absolute oil,
0.05 ~ 0.1% carvol, 94.7 ~ 97.4% Glycerin, mixed triester with caprylic acid capric acid.
The folium eucalypti absolute oil, finished product can be used, or be prepared with reference to following preparation method：
（1）After folium eucalypti leaf crushes after drying, 45-55 mesh sieves are crossed, obtain folium eucalypti leaf powder；
（2）A certain amount of folium eucalypti leaf powder is taken to insert in distilling flask, after adding a certain amount of distilled water, 4 ~ 5h of steam distillation obtains oily
The distillate of water stratification；
（3）With the oil phase in dichloromethane extractive distillation liquid, and use anhydrous sodium sulfate drying；
（4）By step（3）Rotation evaporates solvent under 50 DEG C of water bath conditions after middle gained finish filtering, obtains folium eucalypti leaf essence
Oil；
（5）A certain amount of folium eucalypti leaf essential oil is added in extraction flask, the ethanol for adding 10-20 times of volume carries out solvent extraction；
（6）Alcohol layer is taken after balance to be extracted, and ethanol extractant is collected in repeated multiple times extraction；
（7）Then ethanol evaporation is fallen into obtain folium eucalypti absolute oil by being evaporated under reduced pressure under the conditions of 0.1MPa.
The lemon oil, finished product can be used, or be prepared with reference to following preparation method：
（1）After lemon crushes after drying, 45-55 mesh sieves are crossed, obtain bergamot powder；
（2）A certain amount of lemon powder is taken to insert in distilling flask, after adding a certain amount of distilled water, 4 ~ 5h of steam distillation obtains profit point
The distillate of layer；
（3）With the oil phase in dichloromethane extractive distillation liquid, and use anhydrous sodium sulfate drying；
（4）By step（3）Rotation evaporates solvent under 50 DEG C of water bath conditions after middle gained finish filtering, obtains lemon.
Fragrant line fructus amomi essence, specific formula are, for example, in the ramuscule filter stick：3.0% Bronyl acetate, 0.08%
Linalool, 0.15% linalool oxide, 0.08% nerolidol, 0.35% borneol, 0.07% lemon oil, 0.15% eucalyptus
Leaf absolute oil, 0.08% carvol, 96.04% Glycerin, mixed triester with caprylic acid capric acid.
Application of the fragrant line with fructus amomi essence in cigarette in the ramuscule filter stick, for fragrant line in ramuscule cigarette filter rod.
A kind of ramuscule composite filter of built-in fructus amomi essence perfume (or spice) line, the composite filter outer wrap has forming paper, internal
It is combined by common vinegar fibre filter rod segments and built-in fructus amomi essence perfume (or spice) line vinegar fibre filter rod segments, wherein built-in fructus amomi essence perfume (or spice) line vinegar is fine
Filter rod segments are close to pipe tobacco section；
Common vinegar fibre filter rod segments and built-in fructus amomi essence perfume (or spice) line vinegar fibre filter rod segments, the cross sectional shape of diacetate fiber used are Y types, silk
Beam specification requires：Single-strand is 6.0den ~ 11.0den, and total denier is 15000den ~ 17000den；
Common vinegar fibre filter rod segments and the length ratio of built-in fructus amomi essence perfume (or spice) line vinegar fibre filter rod segments, can be according to resistance to suction or flavouring demand
It is adjusted, length ratio is, for example, specifically 1:1；
The built-in fructus amomi essence perfume (or spice) line vinegar fibre filter rod segments, its middle part are built-in with fragrant line, and fragrant line is adsorbed with fructus amomi essence；It is prepared
Process is prepared by prior art, is specially：Before fragrant line enters filter-stick forming device after being come out from line roller, by equipped with certain dense
The flavoring system for spending fructus amomi essence applies essence；
The The concrete specification of the composite filter, it is, for example,：Length is 120mm, a length of 16.90mm of circumference, pressure drop be 2600Pa ~
4200Pa。
The essence applied amount of the ramuscule perfume (or spice) line filter stick list branch filter stick is 10mg ~ 30mg.
Utilize ramuscule cigarette prepared by the ramuscule composite filter of the built-in fructus amomi essence perfume (or spice) line.
The present invention prepares a kind of savory essence of the fructus amomi with peat-reek first by autonomous Design composition, will
It has prepared the ramuscule composite filter with fructus amomi fragrance as the flavouring additive in ramuscule perfume (or spice) line filter stick.Fructus amomi taste
Pungent warm-natured, returns spleen, stomach, kidney channel, because fructus amomi has dampness elimination appetizing, warming spleen and stopping diarrha, regulating the flow of vital energy antiabortive and other effects, thus the application exists
Existing essence product type is enriched meanwhile, it is capable to which part reduces harmfulness of the tobacco product to human body.
Preliminary Applications show, after the ramuscule perfume (or spice) line composite filter is used for ramuscule cigarette, not only increase the equal of essence application
Even property and the stability of release, also improve the harmony of fragrance and product sensory quality.By the fructus amomi essence applied is
Natural materials allotment obtains, therefore these aroma substances, after cigarette smoke is entered, " the roasting sweet tea " that can more highlight cigarette is fragrant
Rhythm, lifts the fragrance richness and plumpness of ramuscule cigarette, and then improves its sucking quality and sense organ comfort level.
Compared with existing perfuming technology, main advantages of the present invention have：
(1) simple process：Preparation technology of the present invention is simple, without making notable adjustment to current production technology and equipment, without
Large-scale instrument and equipment and expensive reagent, it is simple to operate, it is easily controllable；
(2) safety and sanitation：Raw and auxiliary material of the present invention is widely used in food processing field, in the absence of toxic reagent
Residue problem, thus securely and reliably；
（3）Release is stable：Built-in fragrant line composite filter form of the present invention, the same of fragrant line is directly contacted avoiding oral cavity
When, help to slow down the loss of fragrance.
In general, a kind of the application fragrant line in the ramuscule cigarette with peat-reek is provided is same with fructus amomi essence
When, coordinate the improvement of ramuscule cigarette filter rod structure, can preferably improve the effect of sucking of ramuscule cigarette, and improvement effect is obvious,
With preferable practical value, while abundant cigarette product type, design, exploitation and production for new ramuscule cigarette
Sale has preferable Demonstration And Extension application value.
Brief description of the drawings
Fig. 1 is the ramuscule composite filter structural representation of built-in fructus amomi essence perfume (or spice) line provided by the present invention；
Fig. 2 is ramuscule cigarette structure schematic diagram prepared by the ramuscule composite filter of fructus amomi essence perfume (or spice) line built in utilization.
Embodiment
Explanation is further explained to the application with reference to embodiment., it is necessary to illustrate before specific embodiment is introduced
, Bronyl acetate, linalool, linalool oxide, nerolidol, borneol, lemon oil, folium eucalypti employed in following embodiments
The materials such as absolute oil, carvol are Shanghai Huabao Biotechnology Co., Ltd.'s Products；Fragrant line, ramuscule filter stick etc. are also by existing
Technology production is carried out.
Embodiment 1
The present embodiment provides fragrant line fructus amomi essence in ramuscule filter stick, is calculated in mass percent, composed of the following components：
2.0% Bronyl acetate, 0.05% linalool, 0.1% linalool oxide, 0.05% nerolidol, 0.2% dragon
Brain, 0.05% lemon oil, 0.1% folium eucalypti absolute oil, 0.05% carvol, 97.4% Glycerin, mixed triester with caprylic acid capric acid.
By prior art, the ramuscule composite filter of fructus amomi essence perfume (or spice) line built in preparation is as shown in Figure 1, 2, prepared compound
Filter stick 3, outer wrap has forming paper, internal compound by common vinegar fibre filter rod segments 2 and built-in fructus amomi essence perfume (or spice) line vinegar fibre filter rod segments 1
Form, wherein built-in fructus amomi essence perfume (or spice) line vinegar fibre filter rod segments 1 are close to pipe tobacco section 4；
Common vinegar fibre filter rod segments 2, the cross sectional shape of diacetate fiber used is Y types, and strand specification requirement is：6.0Y/17000
（den/den）；
Built-in fructus amomi essence perfume (or spice) line vinegar fibre filter rod segments 2, the cross sectional shape of diacetate fiber used is Y types, and strand specification requirement is：
8.0Y/15000（den/den）；
The length ratio of common vinegar fibre filter rod segments and built-in fructus amomi essence perfume (or spice) line vinegar fibre filter rod segments, it is 1:1；The composite filter
The concrete specification is：Length is 120mm, a length of 16.90mm of circumference（In Fig. 2, during actual use, filter length 30mm（That is Fig. 2
Middle 1+2 part-structures length））.
When preparing the ramuscule composite filter of the built-in fructus amomi essence perfume (or spice) line, carry out by existing filter stick production technology, pass through first
The fragrant line for being applied with fructus amomi essence is inserted filter stick center and fragrant line filter stick is made by filter-stick forming device, then passes through filter stick compounding machine again
It is ramuscule perfume (or spice) line binary compound filter candle with common vinegar fibre filter stick formation（State the ramuscule composite filter of built-in fructus amomi essence perfume (or spice) line）.Into
After type, measurement result shows, fragrant line is 20mg or so with fructus amomi essence applied amount in every composite filter（That is the long filter sticks of 120mm
Dosage be 20mg）.
By prior art, the ramuscule composite filter of the built-in fructus amomi essence perfume (or spice) line and tobacco sample cigarette are rolled up for ramuscule
Cigarette sample sets blank control sample as test sample（Blank perfume (or spice) line is added at filter stick same position）As control sample,
By 7 professional sensory evaluation personnel evaluation is detected and is aspirated respectively to test sample and control sample.Specific flue gas inspection result
With specific suction evaluation score value referring to form hereinafter.
Suction evaluation result shows that after it with the addition of fructus amomi essence, " fructus amomi " fragrance of cigarette sample is obvious, the perfume (or spice) of flue gas
Gas is rich certain lifting, and excitant is reduced, and miscellaneous gas is reduced, and flue gas sophistication improves, and pleasant impression makes moderate progress.
Embodiment 2
The present embodiment provides fragrant line fructus amomi essence in ramuscule filter stick, is calculated in mass percent, composed of the following components：
3.0% Bronyl acetate, 0.08% linalool, 0.15% linalool oxide, 0.08% nerolidol, 0.35%
Borneol, 0.07% lemon oil, 0.15% folium eucalypti absolute oil, 0.08% carvol, 96.04% Glycerin, mixed triester with caprylic acid capric acid
With the filter stick specification of embodiment 1, the ramuscule composite filter of fructus amomi essence perfume (or spice) line built in preparation.After shaping, measurement result table
Bright, fragrant line is 20mg or so with fructus amomi essence applied amount in every composite filter.
Using the ramuscule composite filter of the built-in fructus amomi essence perfume (or spice) line and tobacco sample cigarette be ramuscule cigarette sample as
Test sample, carry out suction evaluation.
Suction evaluation result shows, after it with the addition of fructus amomi essence, " fructus amomi is fragrant " of cigarette sample is obvious, and flue gas is fragrant
Gas is rich to be dramatically increased, and excitant significantly reduces, and miscellaneous gas is reduced, and flue gas sophistication is significantly improved, and pleasant impression is obviously improved.
Embodiment 3
The present embodiment provides fragrant line fructus amomi essence in ramuscule filter stick, is calculated in mass percent, composed of the following components：
4.0% Bronyl acetate, 0.1% linalool, 0.2% linalool oxide, 0.1% nerolidol, 0.5% borneol,
0.1% lemon oil, 0.2% folium eucalypti absolute oil, 0.1% carvol, 94.7% Glycerin, mixed triester with caprylic acid capric acid
With the filter stick specification of embodiment 1, the ramuscule composite filter of fructus amomi essence perfume (or spice) line built in preparation.After shaping, measurement result table
Bright, fragrant line is 20mg or so with fructus amomi essence applied amount in every composite filter.
Using the ramuscule composite filter of the built-in fructus amomi essence perfume (or spice) line and tobacco sample cigarette be ramuscule cigarette sample as
Test sample, carry out suction evaluation.
Suction evaluation result shows, after it with the addition of fructus amomi essence, " fructus amomi is fragrant " of cigarette sample is fairly obvious, and flue gas is fragrant
Gas harmony is reduced, and excitant increase, miscellaneous gas is reduced, and flue gas inaccurate coordination and has uncomfortable sweet sense, and pleasant impression is not so good as
Normal cigarette（Compared with control sample cigarette）.
Composite filter prepared by different embodiments is detected, further according to《The cigarette of GB/T 19609-2004
TPM and tar are determined with conventional analysis smoking machine》Method measure cigarette mainstream flue gas in TPM, tar, cigarette
The index such as alkali and moisture is detected, and concrete outcome is as shown in the table.
Table 1, the testing result of the ramuscule composite filter of built-in fructus amomi essence perfume (or spice) line prepared by different embodiments：
；
Table 2, the physical index and main flume testing result of kinds of cigarettes sample：
；
Be can be seen that from the above-mentioned data of table 1 compared with normal diacetate fiber filter stick, place fructus amomi perfume (or spice) line filter stick physical index without
Significant difference.As can be seen from Table 2, compared with the normal cigarette of reference examples, the main flume of fructus amomi perfume (or spice) coil of wire cigarette is without obvious
Change, the key index tar and nicotine for influenceing cigarette sense organ do not have significant changes.
Table 3, kinds of cigarettes sample sensory quality assessment result：
。
As can be seen from Table 3, it can be shown cigarette sensory quality by using fructus amomi essence perfume (or spice) line composite filter
Writing improves, and its sensory evaluation scores highest can improve 0.40 point, and fragrance significantly improves, and pleasant impression improves, and excitant and miscellaneous gas also have larger
Reduce.
To sum up, by targetedly designing the fragrant line filter stick composition of specific fragrance, after being applied to cigarette, energy
Odor characteristic during smoking property of cigarette is enough obviously improved, impression is sucked in abundant and raising, simultaneously because the present invention uses special construction
Fragrant line filter stick, conventional fragrant line filter stick can be avoided quickly to be lost in, while safety and sanitation.Therefore the application highlights cigarette as one kind
" fructus amomi " note, the new fructus amomi taste ramuscule perfume (or spice) line composite filter for improving sucking quality, in industry have definitely to promote and answer
With value.
Claims (5)
- A kind of 1. fragrant line fructus amomi essence in ramuscule filter stick, it is characterised in that it is calculated in mass percent, it is composed of the following components：2.0 ~ 4.0% Bronyl acetate, 0.05 ~ 0.1% linalool, 0.1 ~ 0.2% linalool oxide,0.05 ~ 0.1% nerolidol, 0.2 ~ 0.5% borneol, 0.05 ~ 0.1% lemon oil, 0.1 ~ 0.2% folium eucalypti absolute oil,0.05 ~ 0.1% carvol, 94.7 ~ 97.4% Glycerin, mixed triester with caprylic acid capric acid.
- 2. fragrant line fructus amomi essence in ramuscule filter stick as claimed in claim 1, it is characterised in that specific formula is：4.0% second Sour borneol acetate, 0.1% linalool, 0.2% linalool oxide, 0.1% nerolidol, 0.5% borneol, 0.1% lemon Oil, 0.2% folium eucalypti absolute oil, 0.1% carvol, 94.7% Glycerin, mixed triester with caprylic acid capric acid；Or it is：3.0% Bronyl acetate, 0.08% linalool, 0.15% linalool oxide, 0.08% nerolidol, 0.35% borneol, 0.07% lemon oil, 0.15% folium eucalypti absolute oil, 0.08% carvol, 96.04% Glycerin, mixed triester with caprylic acid capric acid；Or it is：2.0% Bronyl acetate, 0.05% linalool, 0.1% linalool oxide, 0.05% nerolidol, 0.2% borneol, 0.05% lemon oil, 0.1% folium eucalypti absolute oil, 0.05% carvol, 97.4% Glycerin, mixed triester with caprylic acid capric acid.
- 3. application of the fragrant line with fructus amomi essence in cigarette in the ramuscule filter stick of claim 1 or 2, it is characterised in that be used for Fragrant line in ramuscule cigarette filter rod.
- 4. a kind of ramuscule composite filter of built-in fructus amomi essence perfume (or spice) line, it is characterised in that the composite filter outer wrap has into Type paper, inside is combined by common vinegar fibre filter rod segments and built-in fructus amomi essence perfume (or spice) line vinegar fibre filter rod segments, wherein built-in fructus amomi is fragrant The fragrant line vinegar fibre filter rod segments of essence are close to pipe tobacco section；Common vinegar fibre filter rod segments and built-in fructus amomi essence perfume (or spice) line vinegar fibre filter rod segments, the cross sectional shape of diacetate fiber used are Y types, silk Beam specification requires：Single-strand is 6.0den ~ 11.0den, and total denier is 15000den ~ 17000den；The length ratio of common vinegar fibre filter rod segments and built-in fructus amomi essence perfume (or spice) line vinegar fibre filter rod segments is 1:1；The built-in fructus amomi essence perfume (or spice) line vinegar fibre filter rod segments, its middle part are built-in with fragrant line, and fragrant line is adsorbed with fructus amomi essence.
- 5. existed using ramuscule cigarette, its feature prepared by the ramuscule composite filter of built-in fructus amomi essence perfume (or spice) line described in claim 4 In the essence applied amount of single branch filter stick is 10mg ~ 30mg.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710846804.7A CN107541341A (en) | 2017-09-19 | 2017-09-19 | Fragrant line fructus amomi essence and its application in a kind of ramuscule filter stick |
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|---|---|---|---|
| CN201710846804.7A CN107541341A (en) | 2017-09-19 | 2017-09-19 | Fragrant line fructus amomi essence and its application in a kind of ramuscule filter stick |
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Application publication date: 20180105 |