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CN107504910A - White light reflection dynamic measurement film thickness method based on threshold value wavelet transformation - Google Patents

White light reflection dynamic measurement film thickness method based on threshold value wavelet transformation Download PDF

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CN107504910A
CN107504910A CN201710705416.7A CN201710705416A CN107504910A CN 107504910 A CN107504910 A CN 107504910A CN 201710705416 A CN201710705416 A CN 201710705416A CN 107504910 A CN107504910 A CN 107504910A
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signal
white light
film thickness
wavelet
threshold
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郑永军
卫银杰
顾海洋
柳滨
孔明
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China Jiliang University
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China Jiliang University
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01BMEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS; MEASURING ANGLES; MEASURING AREAS; MEASURING IRREGULARITIES OF SURFACES OR CONTOURS
    • G01B11/00Measuring arrangements characterised by the use of optical techniques
    • G01B11/02Measuring arrangements characterised by the use of optical techniques for measuring length, width or thickness
    • G01B11/06Measuring arrangements characterised by the use of optical techniques for measuring length, width or thickness for measuring thickness ; e.g. of sheet material

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  • General Physics & Mathematics (AREA)
  • Length Measuring Devices By Optical Means (AREA)

Abstract

The invention discloses a kind of white light reflection dynamic measurement film thickness method based on threshold value wavelet transformation.White light reflectance spectrum signal is carried out three layers of wavelet decomposition by this method, then extract and carry out denoising with default threshold after each layer approximation coefficient and detail coefficients, finally by the characteristic value for asking for white light reflectance spectrum, i.e. the minimum value of reflectivity quickly judge so as to obtain film thickness.Invention enhances the degree of accuracy to film thickness measuring to be measured and speed.

Description

基于阈值小波变换的白光反射动态测量薄膜厚度方法Thin Film Thickness Measuring Method Based on Threshold Wavelet Transform

技术领域technical field

本发明属于光学精密测量和信号处理领域,具体涉及一种利用阈值小波变换对白光反射率谱信号进行处理从而判断薄膜厚度的方法。The invention belongs to the field of optical precision measurement and signal processing, and in particular relates to a method for judging film thickness by processing white light reflectance spectrum signals by using threshold wavelet transform.

背景技术Background technique

随着制造技术的飞速发展,薄膜成为满足一些设备性能指标的重要部件。薄膜广泛应用于许多领域,如光学、信息学、生物学和航空航天等。因此准确地测量薄膜的厚度,对于判断薄膜是否工作正常显得非常重要。With the rapid development of manufacturing technology, thin films have become an important component to meet some equipment performance indicators. Thin films are widely used in many fields, such as optics, informatics, biology, and aerospace. Therefore, it is very important to accurately measure the thickness of the film to judge whether the film is working properly.

本发明提出了使用白光反射率谱(white light reflectance spectroscopy,WLRS)对薄膜厚度进行测量。这种方法具有响应快,精度高以及测量结果准确度高等优点。WLRS测量膜厚的具体原理如下:如附图1所示,白光由点A垂直进入待测薄膜,在S1和S2表面经过数次折射及反射后,其相位发生变化,由此可以得到其WLRS。并且,WLRS与待测薄膜的厚度之间存在着一一对应关系。由此,可根据上述原理对基层表面的薄膜厚度进行非接触式的测量。由于在薄膜厚度的动态测量过程中,其精度可达到纳米级,因此不可避免地会引入大量噪声。这些噪声直接影响到了薄膜膜厚测量的精度。由此,如何快速地处理测量过程中由于各种原因而引入的噪声就成为一个重要课题。The present invention proposes to use white light reflectance spectroscopy (WLRS) to measure the film thickness. This method has the advantages of fast response, high precision and high accuracy of measurement results. The specific principle of WLRS measurement of film thickness is as follows: As shown in Figure 1, white light enters the film to be tested vertically from point A, and after several times of refraction and reflection on the surfaces of S1 and S2, its phase changes, and thus its WLRS can be obtained . Moreover, there is a one-to-one correspondence between the WLRS and the thickness of the film to be measured. Thus, the film thickness on the surface of the base layer can be measured in a non-contact manner according to the above principle. Since the precision can reach the nanometer level during the dynamic measurement of film thickness, a lot of noise will inevitably be introduced. These noises directly affect the accuracy of film thickness measurement. Therefore, how to quickly deal with the noise introduced by various reasons in the measurement process has become an important issue.

传统的去噪方法,如傅立叶信号分析法等是对信号全局的分析,而不能很好的对信号的微细部分进行处理。小波变换(wavelet transform,WT)可通过对时频的局部变换达到有效地提取信息的目的。它不用进行傅立叶变换,使用更方便。WT处理的是信号的细节,且可对时域和频域信号自适应,因此能做到对信号的精细处理。Traditional denoising methods, such as Fourier signal analysis, analyze the overall signal, but cannot deal with the subtle parts of the signal well. Wavelet transform (wavelet transform, WT) can achieve the purpose of effectively extracting information through local transformation of time and frequency. It does not need Fourier transform and is more convenient to use. WT processes the details of the signal, and can adapt to the time domain and frequency domain signals, so it can achieve fine processing of the signal.

通常情况下,将一段含噪信号在频域上进行分解,低频为有用信号,高频为噪声信号。因此,在去噪时的理想状态是将信号高频部分去除的同时保留其低频部分。而小波变换是对信号的时频分析,具有高分辨率的优点,可以很轻松地区分信号的高低频部分从而达到去除噪声的目的。Usually, a segment of noisy signal is decomposed in the frequency domain, the low frequency is the useful signal, and the high frequency is the noise signal. Therefore, the ideal state in denoising is to remove the high frequency part of the signal while retaining its low frequency part. The wavelet transform is a time-frequency analysis of the signal, which has the advantage of high resolution, and can easily distinguish the high and low frequency parts of the signal to achieve the purpose of removing noise.

小波去噪的基本原理为:先选定要对信号分解的层次数,然后将含有噪声的信号小波分解(噪声通常在高频部分)。接着计算阈值,对信号已分解出的各层细节进行处理,以去除噪声。最后根据分解层数及相应细节对其进行重构,恢复真实的信号。The basic principle of wavelet denoising is: first select the number of layers to be decomposed on the signal, and then decompose the signal containing noise by wavelet (the noise is usually in the high frequency part). Then the threshold is calculated, and the details of each layer that have been decomposed from the signal are processed to remove noise. Finally, it is reconstructed according to the number of decomposition layers and corresponding details to restore the real signal.

发明内容Contents of the invention

本发明提出一种利用小波变换对WLRS信号进行快速去噪处理从而对薄膜厚度进行测量的方法。The invention proposes a method for quickly denoising the WLRS signal by using wavelet transform so as to measure the thickness of the film.

本发明有以下步骤:The present invention has following steps:

1)令白光的光源近垂直地入射待测薄膜,以获取WLRS原始信号;1) Make the light source of white light incident on the film to be tested nearly vertically to obtain the original signal of WLRS;

2)将步骤1所得的WLRS原始信号进行小波分解;2) carrying out wavelet decomposition to the WLRS original signal gained in step 1;

3)对步骤2中小波分解的信号抽取近似系数及细节系数;3) extract approximate coefficient and detail coefficient to the signal of wavelet decomposition in step 2;

4)对步骤3中的各层系数进行阈值处理;4) Threshold processing is carried out to each layer coefficient in step 3;

5)重建WLRS信号;5) Reconstruct the WLRS signal;

6)对步骤5得到的去噪后的WLRS信号提取特征值,通过特征值求得待测薄膜的膜厚。6) Extract eigenvalues from the denoised WLRS signal obtained in step 5, and obtain the film thickness of the film to be measured through the eigenvalues.

本发明的有益效果:去噪效果好,处理速度较快,能够较好地区分有用信号和噪声,较好地提高了使用特征值判断薄膜厚度的准确率。The beneficial effect of the present invention is that the denoising effect is good, the processing speed is fast, the useful signal and the noise can be better distinguished, and the accuracy rate of judging the thickness of the film by using the characteristic value is better improved.

附图说明Description of drawings

图1原理图;Figure 1 schematic diagram;

图2整体框图;Figure 2 overall block diagram;

图3去噪前不同膜厚的WLRS动态测量结果图(300-345nm);Figure 3 WLRS dynamic measurement results of different film thicknesses before denoising (300-345nm);

图4去噪前特征参数分布图(300-350nm);Fig. 4 Distribution diagram of characteristic parameters before denoising (300-350nm);

图5小波去噪分解三层近似图(膜厚:300nm);Figure 5 wavelet denoising decomposition three-layer approximation diagram (film thickness: 300nm);

图6小波去噪分解一层细节(膜厚:300nm);Figure 6 Wavelet denoising decomposes a layer of details (film thickness: 300nm);

图7小波去噪分解二层细节(膜厚:300nm);Figure 7 Wavelet denoising decomposition of the second layer details (film thickness: 300nm);

图8小波去噪分解三层细节(膜厚:300nm);Figure 8 Wavelet denoising decomposes three-layer details (film thickness: 300nm);

图9去噪后不同膜厚的WLRS动态测量结果图(300-345nm);Figure 9 WLRS dynamic measurement results of different film thickness after denoising (300-345nm);

图10去噪后特征参数分布图(300-350nm)。Fig. 10 Distribution diagram of characteristic parameters after denoising (300-350nm).

具体实施方式detailed description

下面将结合附图2对本发明作进一步说明。The present invention will be further described in conjunction with accompanying drawing 2 below.

1)令白光的光源近垂直地入射待测薄膜,以获取WLRS原始信号;1) Make the light source of white light incident on the film to be tested nearly vertically to obtain the original signal of WLRS;

具体为:具体原理如附图1所示,白光由点A近垂直(最大角度不超过±5°)进入待测薄膜,在S1和S2表面经过数次折射及反射后,其相位发生变化。通过采集B1、B2、…、Bn,可以得到WLRS原始信号。设原始信号的模型为:Specifically: the specific principle is shown in Figure 1. White light enters the film to be tested from point A near vertical (the maximum angle does not exceed ±5°). After several times of refraction and reflection on the surfaces of S1 and S2, its phase Variety. By collecting B 1 , B 2 , . . . , B n , the original WLRS signal can be obtained. Let the model of the original signal be:

S(x)=f(x)+n1(x)×n2(x) (1)S(x)=f(x)+n 1 (x)×n 2 (x) (1)

其中,S(x)为含噪信号,f(x)为真实信号,n1(x)为加性噪声,n2(x)为乘性噪声。在本实施例中,信号模型可简化为:Among them, S(x) is a noisy signal, f(x) is a real signal, n 1 (x) is additive noise, and n 2 (x) is multiplicative noise. In this embodiment, the signal model can be simplified as:

S(x)=f(x)+n(x) (2)S(x)=f(x)+n(x) (2)

其中,S(x)为含噪信号,f(x)为真实信号,n(x)为噪声。Among them, S(x) is the noisy signal, f(x) is the real signal, and n(x) is the noise.

2)将步骤1所得的WLRS原始信号进行小波分解;2) carrying out wavelet decomposition to the WLRS original signal gained in step 1;

具体为:将WLRS进行小波分解后,其低频为有用信号,而高频为噪声信号。因此,可对WLRS进行一定层数的分解,然后在每层上使用不同的阈值进行处理,达到去噪的目的。分解层数越多,其高频部分被去除得越多,但层数过多会将部分有用信号一起剔除,即分解过度。因此选取层数为3的小波对WLRS原始信号f(x)进行小波分解。Specifically: After WLRS is decomposed by wavelet, its low frequency is a useful signal, while its high frequency is a noise signal. Therefore, WLRS can be decomposed into a certain number of layers, and then processed with different thresholds on each layer to achieve the purpose of denoising. The more the number of decomposition layers, the more the high-frequency part is removed, but too many layers will remove some useful signals together, that is, the decomposition is excessive. Therefore, the wavelet with 3 layers is selected to decompose the WLRS original signal f(x) by wavelet.

3)对步骤2中小波分解的信号抽取近似系数及细节系数;3) extract approximate coefficient and detail coefficient to the signal of wavelet decomposition in step 2;

具体为:对步骤2得到的3层分解中抽取出信号的三层近似ck及其1、2、3层细节dj,k,其中j表示分解层数,k表示第k个数据。Specifically: extract the three-layer approximation c k of the signal from the three-layer decomposition obtained in step 2 and its details d j,k of layers 1, 2, and 3, where j represents the number of decomposition layers, and k represents the kth data.

4)对步骤3中的小波系数进行阈值处理;4) Threshold processing is carried out to the wavelet coefficient in step 3;

具体为:使用计算出的阈值δj用公式(3)对第j层的细节部分dj,k进行处理。处理公式如下:Specifically: use the calculated threshold δ j to process the detail part d j, k of the jth layer with formula (3). The processing formula is as follows:

即当|dj,k|>δj时,令dj,k=dj,k;当|dj,k|≤δj时,令dj,k=0。以此对dj,k进行筛选处理。That is, when |d j,k |>δ j , set d j,k =d j,k ; when |d j,k |≤δ j , set d j,k =0. In this way, d j, k are screened.

一般来说,阈值是由原信号的信噪比选定的。本实施例采用固定阈值。阈值δj由下式确定:In general, the threshold is selected by the signal-to-noise ratio of the original signal. This embodiment adopts a fixed threshold. The threshold δ j is determined by the following formula:

式中n为信号的长度。Where n is the length of the signal.

5)重建WLRS信号;5) Reconstruct the WLRS signal;

具体为:将3层近似和1-3层细节dj,k利用算法进行重构,得到真实信号。Specifically: the 3-layer approximation and the 1-3 layer details d j,k are reconstructed using an algorithm to obtain the real signal.

6)对步骤4得到的去噪后的WLRS信号提取特征值,通过特征值求得待测薄膜的膜厚。6) Extract eigenvalues from the denoised WLRS signal obtained in step 4, and obtain the film thickness of the film to be measured through the eigenvalues.

具体为:求去噪后的WLRS信号的反射率的最小值为特征值,特征值与膜厚存在着一定的线性关系,可通过此线性关系求出待测膜厚。Specifically, the minimum value of the reflectivity of the denoised WLRS signal is calculated as the eigenvalue, and there is a certain linear relationship between the eigenvalue and the film thickness, and the film thickness to be measured can be obtained through this linear relationship.

下面将通过实例进行进一步的说明。在膜厚300nm-350nm的区间上,每隔1nm进行一次动态测量,共得到50条WLRS。从这50条WLRS中选取300nm、315nm、330nm和345nm这4条,如附图3所示。在进行高精度的动态测量过程中会引入一些噪声,使得在使用特征值计算其实际膜厚时产生一些偏差,如附图4所示,不难看出特征值与膜厚之间具有一定的相关性,即随着膜厚的增加,其特征值在总体上是随之减小的,然而想要更准确地由特征值计算出膜厚,还需要对其进行一定的处理。故使用小波变换对其进行去噪处理。以对膜厚为300nm的WLRS小波变换为例,首先根据公式(2)建立一个原始信号的模型对WLRS原始信号进行三层小波分解,然后从中抽取出信号的三层近似及其1、2、3层细节,信号的三层近似如附图5所示,1层细节如附图6所示,2层细节如附图7所示,3层细节如附图8所示。由公式(4)计算出的总阈值为0.0277,由公式(3)对1-3层细节进行处理(当|dj,k|>δj时,令dj,k=dj,k;当|dj,k|≤δj时,令dj,k=0)。最后重建WLRS信号,得到真实的WLRS曲线。对300-350nm的信号都做上述处理,结果如附图9所示。对去噪后的WLRS求其反射率的最小值,绘制特征值-膜厚曲线,即附图10。可看出,特征值与膜厚基本呈线性相关。此时,即可根据特征值来计算出薄膜厚度,达到动态测量的目的。Further description will be given below through examples. In the range of film thickness 300nm-350nm, a dynamic measurement is performed every 1nm, and a total of 50 WLRSs are obtained. Select 4 WLRSs of 300nm, 315nm, 330nm and 345nm from the 50 WLRSs, as shown in Figure 3. During the high-precision dynamic measurement process, some noise will be introduced, which will cause some deviations when using the eigenvalues to calculate the actual film thickness. As shown in Figure 4, it is not difficult to see that there is a certain correlation between the eigenvalues and the film thickness. In other words, as the film thickness increases, its eigenvalues generally decrease. However, if we want to calculate the film thickness more accurately from the eigenvalues, we need to do some processing. Therefore, wavelet transform is used to denoise it. Taking the WLRS wavelet transform with a film thickness of 300nm as an example, firstly, a model of the original signal is established according to the formula (2) to decompose the WLRS original signal by three-layer wavelet, and then the three-layer approximation of the signal and its 1, 2, 3-layer details, the three-layer signal approximation is shown in Figure 5, the 1-layer details are shown in Figure 6, the 2-layer details are shown in Figure 7, and the 3-layer details are shown in Figure 8. The total threshold value calculated by the formula (4) is 0.0277, and the 1-3 layer details are processed by the formula (3) (when |d j,k |>δ j , let d j,k =d j,k ; When |d j,k |≤δ j , set d j,k =0). Finally, the WLRS signal is reconstructed to obtain the real WLRS curve. The above-mentioned processing is performed on the 300-350nm signal, and the result is shown in Fig. 9 . Find the minimum value of the reflectance of the denoised WLRS, and draw the characteristic value-film thickness curve, which is shown in Figure 10. It can be seen that the eigenvalues are basically linearly correlated with the film thickness. At this time, the film thickness can be calculated according to the characteristic value, so as to achieve the purpose of dynamic measurement.

Claims (7)

1.基于阈值小波变换的白光反射动态测量薄膜厚度方法,其特征在于,包括如下步骤:1. The white light reflection dynamic measurement film thickness method based on threshold wavelet transform, is characterized in that, comprises the steps: 1)令白光的光源近垂直地入射待测薄膜,以获取白光反射率谱原始信号;1) Make the light source of white light incident on the film to be tested nearly vertically to obtain the original signal of white light reflectance spectrum; 2)将步骤1)所得的白光反射率谱原始信号进行小波分解;2) performing wavelet decomposition on the original signal of the white light reflectance spectrum obtained in step 1); 3)对步骤2)中小波分解的信号抽取近似系数及细节系数;3) extract approximate coefficient and detail coefficient to the signal of wavelet decomposition in step 2); 4)对步骤3)中的各层系数进行阈值处理;4) carry out threshold value processing to each layer coefficient in step 3); 5)重建白光反射率谱信号;5) Reconstruct the white light reflectance spectrum signal; 6)对步骤5)得到的去噪后的白光反射率谱信号提取特征值,通过特征值求得待测薄膜的膜厚。6) Extract eigenvalues from the denoised white light reflectance spectrum signal obtained in step 5), and obtain the film thickness of the film to be measured through the eigenvalues. 2.根据权利要求1所述的基于阈值小波变换的白光反射动态测量薄膜厚度方法,其特征在于,所述步骤1具体为:白光由点A近垂直进入待测薄膜,在S1和S2表面经过数次折射及反射后,其相位发生变化;通过采集反复折射反射后的光线B1、B2、…、Bn,得到WLRS原始信号;设原始信号的模型为:2. The white light reflection dynamic method for measuring film thickness based on threshold wavelet transform according to claim 1, characterized in that, said step 1 is specifically: white light enters the film to be measured from point A nearly vertically, at S 1 and S 2 After several times of refraction and reflection on the surface, its phase changes; the original signal of WLRS is obtained by collecting the light rays B 1 , B 2 , ..., B n after repeated refraction and reflection; the model of the original signal is set as: S(x)=f(x)+n1(x)×n2(x)S(x)=f(x)+n1(x)×n2(x) 其中,S(x)为含噪信号,f(x)为真实信号,n1(x)为加性噪声,n2(x)为乘性噪声;则信号模型可简化为:Among them, S(x) is a noisy signal, f(x) is a real signal, n1(x) is an additive noise, and n2(x) is a multiplicative noise; then the signal model can be simplified as: S(x)=f(x)+n(x)S(x)=f(x)+n(x) 其中,S(x)为含噪信号,f(x)为真实信号,n(x)为噪声。Among them, S(x) is the noisy signal, f(x) is the real signal, and n(x) is the noise. 3.据权利要求1所述的基于阈值小波变换的白光反射动态测量薄膜厚度方法,其特征在于,所述步骤2具体为:选取层数为3的小波对WLRS原始信号f(x)进行小波分解。3. according to the white light reflection dynamic measurement film thickness method based on threshold value wavelet transform according to claim 1, it is characterized in that, described step 2 is specially: choose the wavelet that number of layers is 3 to carry out wavelet to WLRS original signal f (x) break down. 4.据权利要求3所述的基于阈值小波变换的白光反射动态测量薄膜厚度方法,其特征在是,所述步骤3具体为:对步骤2得到的3层分解中抽取出信号的三层近似ck及其1、2、3层细节dj,k,其中j表示分解层数,k表示第k个数据。4. according to claim 3 based on the white light reflection dynamic measurement film thickness method of threshold value wavelet transform, it is characterized in that, described step 3 is specifically: extract the three-layer approximation of signal in the 3-layer decomposition that step 2 obtains c k and its level 1, 2, and 3 details d j,k , where j represents the number of decomposition layers, and k represents the kth data. 5.据权利要求4所述的基于阈值小波变换的白光反射动态测量薄膜厚度方法,其特征在于,所述步骤4具体为:取出第j层的细节dj,k,根据选定的阈值δj处理;公式如下:5. The method for dynamically measuring film thickness based on threshold wavelet transform according to claim 4, wherein the step 4 is specifically: taking out the details d j,k of the jth layer, and according to the selected threshold δ j processing; the formula is as follows: 阈值δj由下式确定:The threshold δ j is determined by the following formula: <mrow> <msub> <mi>&amp;delta;</mi> <mi>j</mi> </msub> <mo>=</mo> <msqrt> <mrow> <mn>2</mn> <mi>l</mi> <mi>o</mi> <mi>g</mi> <mrow> <mo>(</mo> <mi>n</mi> <mo>)</mo> </mrow> </mrow> </msqrt> </mrow> <mrow><msub><mi>&amp;delta;</mi><mi>j</mi></msub><mo>=</mo><msqrt><mrow><mn>2</mn><mi>l</mi><mi>o</mi><mi>g</mi><mrow><mo>(</mo><mi>n</mi><mo>)</mo></mrow></mrow></msqrt></mrow> 式中n为信号的长度。Where n is the length of the signal. 6.据权利要求5所述的基于阈值小波变换的白光反射动态测量薄膜厚度方法,其特征在于,所述步骤5具体为:将三层近似ck和1-3层细节dj,k进行重构,得到真实信号。6. according to claim 5, based on the white light reflection dynamic measurement film thickness method of threshold value wavelet transform, it is characterized in that, described step 5 is specifically: three-layer approximation c k and 1-3 layer details d j, k are carried out Refactor to get the real signal. 7.据权利要求6所述的基于阈值小波变换的白光反射动态测量薄膜厚度方法,其特征在于,所述步骤6具体为:求去噪后的白光反射率谱信号的反射率的最小值为特征值,特征值与膜厚存在着一定的线性关系,通过此线性关系求出待测膜厚。7. according to claim 6 based on the white light reflection dynamic measurement film thickness method of threshold value wavelet transform, it is characterized in that, described step 6 is specifically: seek the minimum value of the reflectivity of the white light reflectance spectrum signal after denoising There is a certain linear relationship between the eigenvalue and the film thickness, and the film thickness to be measured is obtained through this linear relationship.
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