CN107446721A - A kind of fruits and vegetables and tableware powder detergent and preparation method thereof - Google Patents
A kind of fruits and vegetables and tableware powder detergent and preparation method thereof Download PDFInfo
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- CN107446721A CN107446721A CN201710825713.5A CN201710825713A CN107446721A CN 107446721 A CN107446721 A CN 107446721A CN 201710825713 A CN201710825713 A CN 201710825713A CN 107446721 A CN107446721 A CN 107446721A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/28—Sulfonation products derived from fatty acids or their derivatives, e.g. esters, amides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The present invention relates to a kind of fruits and vegetables and tableware powder detergent and preparation method thereof, are specifically mixed by 7 15 parts of first surface activating agent, 11.5 20 parts of second surface activating agent, 20 30 parts of food-grade sodium carbonate, 20 60 parts of food grade sodium chloride；The first surface activating agent is DBSA, or is made up of DBSA and neopelex；The second surface activating agent is methyl sodiosul foaliphatate, or is made up of a sodium olefin sulfonates and APG compounding.It is powder shaped that a kind of fruits and vegetables and tableware of the present invention are washed with powder detergent, and clean result is good and Environmental Safety；A kind of fruits and vegetables and tableware preparation method of powder detergent of the present invention, preparation process is simple and easy to control, is easy to implement efficient automation, continuous production, and production cost is reduced.
Description
Technical field
The present invention relates to a kind of fruits and vegetables and tableware powder detergent and preparation method thereof, belong to daily chemical product technology
Field.
Background technology
Relative to clothing detergent, fruits and vegetables and tableware detergent have higher requirement to environmental safety.No matter
It is detergent product, powder Betengent product or solid block detergent product, all right and wrong in clothing detergent
It is often universal.And the existing fruits and vegetables of in the market and tableware detergent are all fluid product mostly, the unit such as all multiple enterprises is universal
In the more preferable detergent product that can improve environmental safety simultaneously of research and development clean result.Such as prior art
CN104479931A discloses a kind of preparation method for residues of pesticides vegetable and fruit washing agent of dispelling, and utilizes washing made from the preparation method
Although agent can effectively clean fruit surface residues of pesticides, dirt and various pathogenic bacteria, stable performance is free from environmental pollution, this
Commercially like product is widely present kind liquid detergent, and the market competitive pressure is big, and its packaging, storage, transportation
It is more troublesome relative to powder product, wherein it prevents that detergent is rotten by adding the preservatives such as nipagin esters in terms of storage
Lose rotten.
The content of the invention
The first object of the present invention is to provide that a kind of clean result is good and the fruits and vegetables of Environmental Safety and tableware are washed with powder
Wash agent.
The first object of the present invention is achieved through the following technical solutions：
A kind of fruits and vegetables and tableware powder detergent, it is characterised in that the fruits and vegetables and tableware are with powder detergent by following original
The formula for expecting to form by weight ratio is made：The first surface activating agent of 7-15 parts, the second surface activity of 11.5-20 parts
Agent, the food-grade sodium carbonate of 20-30 parts, the food grade sodium chloride of 20-60 parts；The first surface activating agent is detergent alkylate
Sulfonic acid, or be made up of DBSA and neopelex；The second surface activating agent is fatty acid methyl ester
Sodium sulfonate, or be made up of a- sodium olefin sulfonates and APG compounding.
A kind of fruits and vegetables and tableware of the present invention are powder shaped with powder detergent, relative to liquid detergent, it is not necessary to add
Adding preservative agent, packaging, storage, in transportation it is all more convenient, and the fruits and vegetables and tableware are each with powder detergent
Component is evenly distributed in powder, has good decontamination, removes the ability of residues of pesticides.Due to the fruits and vegetables and tableware powder
Body detergent is mainly used in the washing of fruits and vegetables and tableware, high to security requirement, so sodium carbonate and sodium chloride all use food
Level, the food-grade sodium carbonate and the food grade sodium chloride improve the removal ability to residues of pesticides.
A kind of preferably, described fruits and vegetables and tableware powder detergent, it is characterised in that the first of described 7-15 parts
Surfactant is made up of the DBSA of 5-10 parts and the neopelex of 2-5 parts.
The DBSA meeting generated reactive gas and heat in mixed process with the food-grade sodium carbonate,
Inventor has found that caused gas has the function that fluffy particle and takes away heat, and caused heat, which has, promotes raw material
Mix and promote the effect of moisture evaporation.Inventor has found that DBSA accounts for described in the first surface activating agent
During than excessive or all DBSAs, on the one hand need to increase the food when preparing the detergent of the present invention
The dosage of grade sodium carbonate, the another aspect DBSA react with the food-grade sodium carbonate in mixed process
Will excessively acutely, the generation of excessive gas and heat increases control difficulty of the inventor to preparation technology.Inventor's discovery,
The first surface activating agent of described 7-15 parts is by the DBSA of 5-10 parts and the neopelex group of 2-5 parts
Cheng Shi, with the food-grade sodium carbonate hybrid reaction of described 20-30 parts caused by gas and heat it is more suitable, mixed process technique
It is easy to control, and the powder detergent clean result finally prepared is good.
Preferably, described a kind of fruits and vegetables and tableware powder detergent, it is characterised in that described 11.5-20 parts
Second surface activating agent is made up of the a- sodium olefin sulfonates of 10-15 parts and the APG compounding of 1.5-5 parts.
The APG is a kind of green safe, comprehensive nonionic surfactant of performance, and a- sodium olefin sulfonates can
Surface-active is effectively increased, reduces surface tension.Compounded by the APG and the a- sodium olefin sulfonates described in forming
Second surface activating agent has more comprehensively performance and the more feature of environmental protection.
Preferably, described a kind of fruits and vegetables and tableware powder detergent, it is characterised in that described 11.5-20 parts
Second surface activating agent is the methyl sodiosul foaliphatate of 11.5-20 parts.
The methyl sodiosul foaliphatate is a kind of green surfactant, the methyl sodiosul foaliphatate of powdery
It is very beneficial for preparing powder detergent by the method being stirred.
The second object of the present invention be to provide it is a kind of it is simple and easy to control, cost is low, the fruits and vegetables of efficiency high and tableware powder
The preparation method of detergent.
The second object of the present invention is achieved through the following technical solutions：
A kind of preparation method of fruits and vegetables and tableware powder detergent, it is characterised in that including following [MS1]：
A. the first mixing：Described first surface activating agent in the formula, the second surface activating agent are matched somebody with somebody as described
The ratio of side is well mixed, and the first mixture is made；
B. the second mixing：By ratio of the food-grade sodium carbonate in the formula in the formula and institute made from step A
State the first mixture to be well mixed, the second mixture is made；
C. the 3rd mixing：By ratio of the food grade sodium chloride in the formula in the formula and institute made from step B
State the second mixture to be well mixed, fruits and vegetables and tableware powder detergent is made.
The first surface activating agent dirt-removing power is good, and cost is low.The second surface activating agent enhances surface-active,
Improve dirt-removing power.The first surface activating agent is with the second surface activating agent at normal temperatures by stirring each component
Well mixed, the process is simple and easy to control, and cost is low.The DBSA is liquid, mixes each component
Be more uniformly distributed, avoid between simple different solid particles because between particle the difference of itself can not effectively mix under gravity
Close uniformly, and then laid the foundation for the next step.
When the food-grade sodium carbonate and first mixture are stirred, described ten in first mixture
Dialkyl benzene sulfonic acids can react with the food-grade sodium carbonate produces gas and heat, gas pair caused by inventor's utilization
Each component in stirring serves the effect of fluffy particle, and the evaporation of moisture content is promoted using caused heat.
The food grade sodium chloride can effectively improve the removal ability and dirt-removing power to residues of pesticides, and inventor has found institute
State that food grade sodium chloride is very few significantly to weaken pesticides removal ability and dirt-removing power, crossing at most can not only improve pesticides removal
Ability and dirt-removing power, or even salting-out phenomenon can be produced, so the dosage of the food grade sodium chloride must be controlled.Inventor
The heat and gas of step B process residues are also made full use of, is promoted uniform between the food grade sodium chloride and other components
Mixing.
A kind of preferably, preparation method of described fruits and vegetables and tableware powder detergent, it is characterised in that step B
In the second described mixed processes, material mixt system temperature control is 40-50 DEG C.
Inventor has found, at room temperature will be anti-in the DBSA and the food-grade sodium carbonate mixed process
Heat and gas should be produced, heat caused by reaction causes the temperature of material mixt system to rise, is very beneficial for each component
Mixing, is advantageous to the evaporation of the moisture content in system, but need the temperature control of mixed process simultaneously no more than 50 DEG C again.Through
Inventor's repetition test finds that the material mixt system temperature control of second mixed processes is preferred at 40-50 DEG C.
A kind of preferably, preparation method of described fruits and vegetables and tableware powder detergent, it is characterised in that step A
Described in first mixing the speed that is stirred be 100-200r/min, it is 8-12min to be stirred the time.
Inventor find, it is described first mixing during, be stirred excessive velocities or it is excessively slow, be stirred time mistake
It is long or too short, it can all influence the first surface activating agent, the mixed effect and efficiency of the second surface activating agent, Jin Erying
Ring subsequent step.
A kind of preferably, preparation method of described fruits and vegetables and tableware powder detergent, it is characterised in that step B
Described in second mixing the speed that is stirred be 100-200r/min, it is 12-18min to be stirred the time；Described in step C
The speed that is stirred of 3rd mixing is 100-200r/min, and it is 12-18min to be stirred the time.
Inventor has found, described in step B during the second mixing, the speed and time that are stirred mix to material
The temperature of system has a direct impact, and directly affects mixed effect and efficiency；Inventor is made by being stirred the control of speed
The temperature of material mixt system keeps in the reasonable scope, enabling the fluffy effect of gas to play, in as far as possible short time model
Reach good mixed effect in enclosing.Inventor is carried out in time by being stirred the control of time after step B is well mixed
Step C, to make full use of heat that step B not yet distributes and gas to promote the 3rd mixing.Inventor is in step C
In, by being stirred the control of speed, make step C material mixt tie up to be stirred during temperature be down to room naturally
Temperature.
A kind of preferably, preparation method of described fruits and vegetables and tableware powder detergent, it is characterised in that the step
Rapid A, step B, step C are continuous.
It need not pause and be stirred after step A is well mixed, directly be added while stirring into first mixture
The food-grade sodium carbonate；It need not pause and be stirred after step B is well mixed, directly while stirring to the described second mixing
The food grade sodium chloride is added in thing.The step A, step B, step C continuitys are good, are easy to Automated condtrol, production effect
Rate is high.
A kind of preferably, preparation method of described fruits and vegetables and tableware powder detergent, it is characterised in that step A
Described in first mixing the speed that is stirred be 160-180r/min, it is 8-10min to be stirred the time；Described in step B
The speed that is stirred of second mixing is 110-140r/min, and it is 12-15min to be stirred the time；The 3rd is mixed described in step C
The speed that is stirred closed is 130-170r/min, and it is 12-14min to be stirred the time.
Inventor has found, is made up of the DBSA of described 5-10 parts and the neopelex of 2-5 parts
The first surface activating agent and the second surface activating agent of described 7-15 parts there is good mixed effect in step,
Inventor with 160-180r/min be stirred speed stirring 8-10min can be well mixed；The dodecane of described 5-10 parts
Hybrid reaction produces gas and heat to the food-grade sodium carbonate of base benzene sulfonic acid and described 20-30 parts in stepb, inventor with
110-140r/min be stirred speed can both make full use of caused by gas play fluffy effect, and can makes heat
Produce and distribute and reach balance, even if without using extra temperature adjustment control device（Such as constant temperature ring is provided with constant temperature jacket pot
Border）, mixed process is only controlled by 110-140r/min mixing speed can make the temperature of material mixt system maintain 40-
50 DEG C of reasonable interval.On this condition, step B, which is stirred 12-15min, can add the food grade sodium chloride, and with
130-170r/min be stirred speed be stirred 12-14min can complete step C be prepared the present invention a seed pod
Vegetable and tableware powder detergent.Inventor has found that the preparation process is relatively more simple and easy to control, cost is lower, more efficient,
A kind of fruits and vegetables and tableware the powder detergent of the invention being prepared simultaneously has good clean result.
Beneficial effects of the present invention：
1. a kind of fruits and vegetables and tableware of the present invention with powder detergent are powder shaped, relative in the market generally existing fruits and vegetables and
Tableware washes agent by liquid, and similar powder shaped competing product is few, and it need not add preservative, in packaging, storage, transportation
In it is all more convenient；A kind of fruits and vegetables and tableware of the present invention are evenly distributed with each component of powder detergent in powder, are had
Good decontamination, the ability for removing residues of pesticides；The powder detergent environmental protection of a kind of fruits and vegetables and tableware of the present invention, safety, can
Fully meet that fruits and vegetables and dishwashing detergent use.
2. a kind of fruits and vegetables and tableware preparation method of powder detergent of the present invention, preparation process is simple and easy to control, is easy to
Efficient automation, continuous production are realized, and production cost is reduced.
Embodiment
Form by the following examples, the above of the present invention is described in further detail again, but should not be by this
The scope for being interpreted as the above-mentioned theme of the present invention is only limitted to following example, and all technologies for being realized based on the above of the present invention are equal
Belong to the scope of the present invention.
Formula 1 is formed by following raw material by weight ratio：1100g first surface activating agent, 1550g second surface
Activating agent, 2500g food-grade sodium carbonate, 4850g food grade sodium chloride；The first surface activating agent of the 1100g by
800g DBSA and 300g neopelex composition；The second surface activating agent of the 1550g by
1200g a- sodium olefin sulfonates and 350g APG compounding composition.
Formula 2 is formed by following raw material by weight ratio：1000g first surface activating agent, 1150g second surface
Activating agent, 2000g food-grade sodium carbonate, 5850g food grade sodium chloride；The first surface activating agent of the 1000g by
500g DBSA and 500g neopelex composition；The second surface activating agent of the 1150g by
1000g a- sodium olefin sulfonates and 150g APG compounding composition.
Formula 3 is formed by following raw material by weight ratio：1200g first surface activating agent, 2000g second surface
Activating agent, 3000g food-grade sodium carbonate, 3800g food grade sodium chloride；The first surface activating agent of the 1200g by
1000g DBSA and 200g neopelex composition；The second surface activating agent of the 2000g by
1500g a- sodium olefin sulfonates and 500g APG compounding composition.
Formula 4 is formed by following raw material by weight ratio：700g first surface activating agent, 1150g second surface
Activating agent, 2150g food-grade sodium carbonate, 6000g food grade sodium chloride；The first surface activating agent of the 700g is by 500g
DBSA and 200g neopelex composition；The second surface activating agent of the 1150g is 1150g
Methyl sodiosul foaliphatate.
Formula 5 is formed by following raw material by weight ratio：1500g first surface activating agent, 2000g second surface
Activating agent, 3000g food-grade sodium carbonate, 3500g food grade sodium chloride；The first surface activating agent of the 1500g by
1000g DBSA and 500g neopelex composition；The second surface activating agent of the 2000g is
2000g methyl sodiosul foaliphatate.
Formula 6 is formed by following raw material by weight ratio：1500g first surface activating agent, 1800g second surface
Activating agent, 2700g food-grade sodium carbonate, 2000g food grade sodium chloride；The first surface activating agent of the 1500g by
1000g DBSA and 500g neopelex composition；The second surface activating agent of the 1800g is
1800g methyl sodiosul foaliphatate.
Formula 7 is formed by following raw material by weight ratio：1500g first surface activating agent, 1450g second surface
Activating agent, 3000g food-grade sodium carbonate, 4050g food grade sodium chloride；The first surface activating agent of the 1500g is
1500g DBSA；The second surface activating agent of the 1450g by 1200g a- sodium olefin sulfonates and 250g
APG compounding composition.
Embodiment 1
First by it is described formula 1 in described first surface activating agent, the second surface activating agent by it is described be formulated 1 ratio
8min is stirred with 180 r/min speed；Ratio in the formula 1 is added with 140 r/min speed while stirring again
The food-grade sodium carbonate, and be stirred 12min, temperature sensor shows that material mixt system temperature exists in the process
Between 40-50 DEG C；Add the food-grade chlorination of ratio in the formula 1 while stirring again and with 170 r/min speed
Sodium, 12min is stirred, a kind of final fruits and vegetables and tableware powder detergent that the present invention is made.
Embodiment 2
First by it is described formula 2 in described first surface activating agent, the second surface activating agent by it is described be formulated 2 ratio
10min is stirred with 160 r/min speed；Ratio in the formula 2 is added with 110 r/min speed while stirring again
The food-grade sodium carbonate, and be stirred 15min, temperature sensor shows that material mixt system temperature exists in the process
Between 40-50 DEG C；Add the food-grade chlorination of ratio in the formula 2 while stirring again and with 130 r/min speed
Sodium, 14min is stirred, a kind of final fruits and vegetables and tableware powder detergent that the present invention is made.
Embodiment 3
First by it is described formula 3 in described first surface activating agent, the second surface activating agent by it is described be formulated 3 ratio
12min is stirred with 100 r/min speed；Ratio in the formula 3 is added with 160 r/min speed while stirring again
The food-grade sodium carbonate, and be stirred 16min, temperature sensor shows that material mixt system temperature exists in the process
Between 40-50 DEG C；Add the food-grade chlorination of ratio in the formula 3 while stirring again and with 100 r/min speed
Sodium, 18min is stirred, a kind of final fruits and vegetables and tableware powder detergent that the present invention is made.
Embodiment 4
First by it is described formula 4 in described first surface activating agent, the second surface activating agent by it is described be formulated 4 ratio
9min is stirred with 200 r/min speed；Ratio in the formula 4 is added with 100 r/min speed while stirring again
The food-grade sodium carbonate, and be stirred 15min, temperature sensor shows that material mixt system temperature exists in the process
Between 40-50 DEG C；Add the food-grade chlorination of ratio in the formula 4 while stirring again and with 100 r/min speed
Sodium, 18min is stirred, a kind of final fruits and vegetables and tableware powder detergent that the present invention is made.
Embodiment 5
First by it is described formula 5 in described first surface activating agent, the second surface activating agent by it is described be formulated 5 ratio
11min is stirred with 150 r/min speed；Ratio in the formula 5 is added with 200 r/min speed while stirring again
The food-grade sodium carbonate, and be stirred 18min, temperature sensor shows that material mixt system temperature exists in the process
Between 40-50 DEG C；Add the food-grade chlorination of ratio in the formula 5 while stirring again and with 170 r/min speed
Sodium, 15min is stirred, a kind of final fruits and vegetables and tableware powder detergent that the present invention is made.
Embodiment 6
First by it is described formula 6 in described first surface activating agent, the second surface activating agent by it is described be formulated 6 ratio
9min is stirred with 170 r/min speed；Ratio in the formula 6 is added with 130 r/min speed while stirring again
The food-grade sodium carbonate, and be stirred 13min, temperature sensor shows that material mixt system temperature exists in the process
Between 40-50 DEG C；Add the food-grade chlorination of ratio in the formula 6 while stirring again and with 200 r/min speed
Sodium, 12min is stirred, a kind of final fruits and vegetables and tableware powder detergent that the present invention is made.
Embodiment 7
First by it is described formula 7 in described first surface activating agent, the second surface activating agent by it is described be formulated 7 ratio
11min is stirred with 140 r/min speed；Ratio in the formula 7 is added with 200 r/min speed while stirring again
The food-grade sodium carbonate, and be stirred 15min, being provided as stirring by constant temperature jacket pot in the process provides constant temperature ring
Border, make material mixt system temperature between 40-50 DEG C, prevent that material mixt system temperature is too high；Again and with 200 r/min's
Speed adds the food grade sodium chloride of ratio in the formula 7 while stirring, is stirred 12min, and this hair is finally made
A kind of bright fruits and vegetables and tableware powder detergent.
Claims (10)
1. a kind of fruits and vegetables and tableware powder detergent, it is characterised in that the fruits and vegetables and tableware are with powder detergent by following
The formula that raw material forms by weight ratio is made：The first surface activating agent of 7-15 parts, the second surface activity of 11.5-20 parts
Agent, the food-grade sodium carbonate of 20-30 parts, the food grade sodium chloride of 20-60 parts；The first surface activating agent is detergent alkylate
Sulfonic acid, or be made up of DBSA and neopelex；The second surface activating agent is fatty acid methyl ester
Sodium sulfonate, or be made up of a- sodium olefin sulfonates and APG compounding.
2. a kind of fruits and vegetables according to claim 1 and tableware powder detergent, it is characterised in that the of described 7-15 parts
One surfactant is made up of the DBSA of 5-10 parts and the neopelex of 2-5 parts.
3. a kind of fruits and vegetables according to claim 1 and tableware powder detergent, it is characterised in that described 11.5-20 parts
Second surface activating agent by 10-15 parts a- sodium olefin sulfonates and 1.5-5 parts APG compounding form.
4. a kind of fruits and vegetables according to claim 1 and tableware powder detergent, it is characterised in that described 11.5-20 parts
Second surface activating agent be 11.5-20 parts methyl sodiosul foaliphatate.
5. the preparation method of a kind of fruits and vegetables according to claim 1 and tableware powder detergent, it is characterised in that including
Following steps：
A. the first mixing：Described first surface activating agent in the formula, the second surface activating agent are matched somebody with somebody as described
The ratio of side is well mixed, and the first mixture is made；
B. the second mixing：By ratio of the food-grade sodium carbonate in the formula in the formula and institute made from step A
State the first mixture to be well mixed, the second mixture is made；
C. the 3rd mixing：By ratio of the food grade sodium chloride in the formula in the formula and institute made from step B
State the second mixture to be well mixed, fruits and vegetables and tableware powder detergent is made.
6. the preparation method of a kind of fruits and vegetables according to claim 5 and tableware powder detergent, it is characterised in that step
In the second mixed processes described in B, material mixt system temperature control is 40-50 DEG C.
7. the preparation method of a kind of fruits and vegetables according to claim 5 and tableware powder detergent, it is characterised in that step
The speed that is stirred of the first mixing is 100-200r/min described in A, and it is 8-12min to be stirred the time.
8. the preparation method of a kind of fruits and vegetables according to claim 5 and tableware powder detergent, it is characterised in that step
The speed that is stirred of the second mixing is 100-200r/min described in B, and it is 12-18min to be stirred the time；Institute in step C
The speed that is stirred for stating the 3rd mixing is 100-200r/min, and it is 12-18min to be stirred the time.
9. the preparation method of a kind of fruits and vegetables according to claim 5 and tableware powder detergent, it is characterised in that described
Step A, step B, step C are continuous.
A kind of 10. preparation method of fruits and vegetables and tableware powder detergent according to claim 2 or 5, it is characterised in that
The speed that is stirred of the first mixing is 160-180r/min described in step A, and it is 8-10min to be stirred the time；In step B
The speed that is stirred of second mixing is 110-140r/min, and it is 12-15min to be stirred the time；Described in step C
The speed that is stirred of three mixing is 130-170r/min, and it is 12-14min to be stirred the time.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710825713.5A CN107446721A (en) | 2017-09-14 | 2017-09-14 | A kind of fruits and vegetables and tableware powder detergent and preparation method thereof |
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| CN201710825713.5A CN107446721A (en) | 2017-09-14 | 2017-09-14 | A kind of fruits and vegetables and tableware powder detergent and preparation method thereof |
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| CN107446721A true CN107446721A (en) | 2017-12-08 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108300590A (en) * | 2018-01-17 | 2018-07-20 | 江西艾丽斯日化有限公司 | A kind of fruits and vegetables detergent and preparation method thereof |
| CN110408474A (en) * | 2019-09-04 | 2019-11-05 | 中欧生态合作(香港)控股有限公司 | A kind of tableware cleaning powder of alkyl polyglucoside and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1345365A (en) * | 1999-03-30 | 2002-04-17 | 荷兰联合利华有限公司 | Detergent powder composition |
| CN103525595A (en) * | 2013-10-23 | 2014-01-22 | 杨解定 | Fatty acid-containing soap powder |
| CN103602528A (en) * | 2013-10-15 | 2014-02-26 | 青岛叁鼎卫生制品有限公司 | Washing agent for fruits and vegetables |
-
2017
- 2017-09-14 CN CN201710825713.5A patent/CN107446721A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1345365A (en) * | 1999-03-30 | 2002-04-17 | 荷兰联合利华有限公司 | Detergent powder composition |
| CN103602528A (en) * | 2013-10-15 | 2014-02-26 | 青岛叁鼎卫生制品有限公司 | Washing agent for fruits and vegetables |
| CN103525595A (en) * | 2013-10-23 | 2014-01-22 | 杨解定 | Fatty acid-containing soap powder |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108300590A (en) * | 2018-01-17 | 2018-07-20 | 江西艾丽斯日化有限公司 | A kind of fruits and vegetables detergent and preparation method thereof |
| CN110408474A (en) * | 2019-09-04 | 2019-11-05 | 中欧生态合作(香港)控股有限公司 | A kind of tableware cleaning powder of alkyl polyglucoside and preparation method thereof |
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Application publication date: 20171208 |