[go: up one dir, main page]

CN107399977A - A kind of compound saggar and preparation method thereof - Google Patents

A kind of compound saggar and preparation method thereof Download PDF

Info

Publication number
CN107399977A
CN107399977A CN201710581074.2A CN201710581074A CN107399977A CN 107399977 A CN107399977 A CN 107399977A CN 201710581074 A CN201710581074 A CN 201710581074A CN 107399977 A CN107399977 A CN 107399977A
Authority
CN
China
Prior art keywords
parts
saggar
powder
mud
raw material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710581074.2A
Other languages
Chinese (zh)
Inventor
谭海燕
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hengdong Dong Kang Porcelain Industry Co Ltd
Original Assignee
Hengdong Dong Kang Porcelain Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hengdong Dong Kang Porcelain Industry Co Ltd filed Critical Hengdong Dong Kang Porcelain Industry Co Ltd
Priority to CN201710581074.2A priority Critical patent/CN107399977A/en
Publication of CN107399977A publication Critical patent/CN107399977A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/66Monolithic refractories or refractory mortars, including those whether or not containing clay
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/16Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
    • C04B35/18Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay rich in aluminium oxide
    • C04B35/185Mullite 3Al2O3-2SiO2
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/62204Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products using waste materials or refuse
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D5/00Supports, screens or the like for the charge within the furnace
    • F27D5/0006Composite supporting structures
    • F27D5/0012Modules of the sagger or setter type; Supports built up from them
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3206Magnesium oxides or oxide-forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3217Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3217Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
    • C04B2235/3218Aluminium (oxy)hydroxides, e.g. boehmite, gibbsite, alumina sol
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3418Silicon oxide, silicic acids or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
    • C04B2235/3436Alkaline earth metal silicates, e.g. barium silicate
    • C04B2235/3445Magnesium silicates, e.g. forsterite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
    • C04B2235/3463Alumino-silicates other than clay, e.g. mullite
    • C04B2235/3481Alkaline earth metal alumino-silicates other than clay, e.g. cordierite, beryl, micas such as margarite, plagioclase feldspars such as anorthite, zeolites such as chabazite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/349Clays, e.g. bentonites, smectites such as montmorillonite, vermiculites or kaolines, e.g. illite, talc or sepiolite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/40Metallic constituents or additives not added as binding phase
    • C04B2235/402Aluminium
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/52Constituents or additives characterised by their shapes
    • C04B2235/5208Fibers

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Compositions Of Oxide Ceramics (AREA)

Abstract

A kind of compound saggar disclosed by the invention and preparation method thereof, it is prepared by the raw material of following parts by weight:Magnesia 10~13 parts of mud, 10~12 parts of black talc, 33~35 parts of fire clay, old 10~12 parts of sand, 4~6 parts of ballstone, 4~6 parts of aluminium powder, 5~7 parts of bauxite, 17~19 parts of fine purifiation mud, 90 160 parts of mullite, 22 35 parts of cordierite powder, 8 12 parts of attapulgite, 8 12 parts of calcined kaolin, 8 12 parts of diopside, 18 parts of fused magnesite, 13 parts of red mud;13 parts of nano-aluminum hydroxide colloidal sol, 13 parts of silicon powder, 13 parts of reinforcing fiber.The present invention is formed by optimizing the raw material of saggar, to improve the heat endurance of saggar, anti-pressure ability, corrosion resistance and the performance such as not easy to crack so that saggar has the advantages of service life length, light weight.The raw material that the present invention uses is cheap, and preparation technology is simply green, can industrializing implementation.

Description

A kind of compound saggar and preparation method thereof
Technical field
The invention belongs to refractory material saggar field, more particularly to a kind of compound saggar and preparation method thereof.
Background technology
Saggar is one of kiln furnitures.During firing ceramics device, to prevent gas and harmful substance from being broken to base substrate, glaze paint Badly and it is stained, ware and base substrate is placed in container made of refractory material and are calcined, this container claims saggar, also known as casket Son.
Using saggar firing ceramics device, dress burning amount can be not only improved, product will not bond, improve yield rate, and saggar Also there is certain thermal conductivity and heat endurance, it is ensured that ceramic mass.The shape of saggar, it is different according to implements shape.China dragon The eggshell black pottery that mountain culture period fires, using special saggar.Once gathered in Shandong Province Zhucheng poplar home ruins Two pieces fires the saggar of Longshan culture egg-shell pottery, and this is current known earliest saggar.The saggar that later age finds, to contain porcelain Based on, Sui Dynasty Hunan kiln it has been found that.
With the application of clean energy resource, saggar is fewer and fewer in the use of Domestic ceramic enterprise as supporting body.But casket Alms bowl is still very universal in the application of ceramic pigment enterprise as charge vessel, in recent years, due to raw material, fuel, artificial etc. Cost rises steadily, and the price of saggar also increases substantially, despite this, the service life of saggar is but reducing, saggar makes With breakage rate the serious wasting of resources and economic loss are caused per kiln up to 16~22%.Saggar access times how are improved, are dropped Low saggar uses breakage rate, reduces solid waste discharge, improves the performance of enterprises, be present urgent problem to be solved.
The content of the invention
The technical problems to be solved by the invention are the above-mentioned technical problem present in existing saggar and provide one Kind of service life is long, light compound saggar and preparation method thereof.
The technical problems to be solved by the invention can be achieved through the following technical solutions:
A kind of compound saggar, it is prepared by the raw material of following parts by weight:Magnesia 10~13 parts of mud, black talc 10~12 Part, 33~35 parts of fire clay, old 10~12 parts of sand, 4~6 parts of ballstone, 4~6 parts of aluminium powder, 5~7 parts of bauxite, fine purifiation mud 17~ 19 parts, mullite 90-160 parts, cordierite powder 22-35 parts, attapulgite 8-12 parts, calcined kaolin 8-12 parts, diopside 8- 12 parts, fused magnesite 1-8 parts, red mud 1-3 parts;Nano-aluminum hydroxide colloidal sol 1-3 parts, silicon powder 1-3 parts, reinforcing fiber 1-3 parts.
In a preferred embodiment of the invention, the saggar for being used to produce ceramics is by the raw material system of following parts by weight It is standby to form:Magnesia 11.22 parts of mud, 10.21 parts of black talc, 34.15 parts of fire clay, old 11.18 parts of sand, 4.65 parts of ballstone, aluminium powder 4.23 parts, 6.24 parts of bauxite, 18.12 parts of fine purifiation mud, 122 parts of mullite, 25 parts of cordierite powder, 9 parts of attapulgite, calcining height 9 parts of ridge soil, 9 parts of diopside, 2 parts of fused magnesite, 2 parts of red mud;2 parts of nano-aluminum hydroxide colloidal sol, 2 parts of silicon powder;Reinforcing fiber 2 Part.
The preparation method of above-mentioned compound saggar, comprises the following steps:
1) will each raw material mix after carry out wet ball grinding, powder is formed after ball milling, and to cross 60 mesh sieves standby;
2) pressed compact is molded, and powder after ball milling is molded through granulation, pressed compact, compressing under 60Mpa pressure, insulation 2.5 Hour, the demoulding, obtain saggar body;
3) by base substrate pre-burning at 500-600 DEG C, water quenching is then carried out, base substrate is quickly put into water, time 22- 35s;Then the base substrate after water quenching is put into 50-60 DEG C of oil, oil cooling 22-35s;
4) base substrate after processing is dried into 10-22h under field conditions (factors), is put into kiln and is burnt till, firing temperature is 1160-1350 DEG C, firing time is 10-16 hours;
5) the compound saggar after burning till is post-processed, some dilatation joints is cut in side, are filled at dilatation joint Ceramic wool, you can obtain compound saggar.
As a result of technical scheme as above, the present invention is formed by optimizing the raw material of saggar, to improve the heat of saggar Stability, anti-pressure ability, corrosion resistance and the performance such as not easy to crack so that saggar has service life length, light weight it is excellent Point.The raw material that the present invention uses is cheap, and preparation technology is simply green, can industrializing implementation.
Embodiment
The present invention is described in further detail with reference to specific embodiment, and with reference to data.It should be understood that these embodiments It is of the invention solely for the purpose of illustration, rather than the scope limiting the invention in any way.
Embodiment 1
A kind of preparation method of compound saggar, including following preparation process:
1) compound saggar raw material is prepared, the raw material composition of the compound saggar is:Magnesia 10 parts of mud, 10 parts of black talc, fire resisting 33 parts of mud, old 10 parts of sand, 4 parts of ballstone, 4 parts of aluminium powder, 5 parts of bauxite, 17 parts of fine purifiation mud, 90 parts of mullite, 22 parts of cordierite powder, 8 parts of attapulgite, 8 parts of calcined kaolin, 8 parts of diopside, 1 part of fused magnesite, 1 part of red mud;1 part of nano-aluminum hydroxide colloidal sol, 1 part of silicon powder, 1 part of reinforcing fiber.
2) will each raw material mix after carry out wet ball grinding, powder is formed after ball milling, and to cross 65 mesh sieves standby;
3) pressed compact is molded, and powder after ball milling is molded through granulation, pressed compact, compressing under 60Mpa pressure, insulation 2.5 Hour, the demoulding, obtain saggar body;
4) by base substrate pre-burning at 600 DEG C, water quenching is then carried out, base substrate is quickly put into water, time 25s;Then Base substrate after water quenching is put into 55 DEG C of oil, oil cooling 25s;
5) base substrate after processing is dried into 16h under field conditions (factors), is put into kiln and is burnt till, firing temperature 1220 DEG C, firing time is 12 hours.
6) the compound saggar after burning till is post-processed, some dilatation joints is cut in side, are filled at dilatation joint Ceramic wool, you can obtain compound saggar.
Embodiment 2:
A kind of preparation method of compound saggar, including following preparation process:
1) compound saggar raw material is prepared, the raw material composition of the compound saggar is:Magnesia 11.22 parts of mud, black talc 10.21 Part, 34.15 parts of fire clay, old 11.18 parts of sand, 4.65 parts of ballstone, 4.23 parts of aluminium powder, 6.24 parts of bauxite, fine purifiation mud 18.12 Part, 122 parts of mullite;25 parts of cordierite powder, 9 parts of attapulgite, 9 parts of calcined kaolin, 9 parts of diopside, 2 parts of fused magnesite, 2 parts of red mud;2 parts of nano-aluminum hydroxide colloidal sol, 2 parts of silicon powder;2 parts of reinforcing fiber.
2) will each raw material mix after carry out wet ball grinding, powder is formed after ball milling, and to cross 65 mesh sieves standby;
3) pressed compact is molded, and powder after ball milling is molded through granulation, pressed compact, compressing under 60Mpa pressure, insulation 2.5 Hour, the demoulding, obtain saggar body;
4) by base substrate pre-burning at 600 DEG C, water quenching is then carried out, base substrate is quickly put into water, time 25s;Then Base substrate after water quenching is put into 55 DEG C of oil, oil cooling 25s;
5) base substrate after processing is dried into 16h under field conditions (factors), is put into kiln and is burnt till, firing temperature 1220 DEG C, firing time is 12 hours;
6) the compound saggar after burning till is post-processed, some dilatation joints is cut in side, are filled at dilatation joint Ceramic wool, you can obtain compound saggar.
Embodiment 3:
A kind of preparation method of compound saggar, including following preparation process:
1) compound saggar raw material is prepared, the raw material composition for being used to produce the saggar of ceramics is:Magnesia 13 parts of mud, black talc 12 parts, 35 parts of fire clay, old 12 parts of sand, 6 parts of ballstone, 6 parts of aluminium powder, 7 parts of bauxite, 19 parts of fine purifiation mud, 160 parts of mullite, violet 35 parts of bluestone powder, 12 parts of attapulgite, 12 parts of calcined kaolin, 12 parts of diopside, 8 parts of fused magnesite, 3 parts of red mud;Nanometer hydrogen 3 parts of alumina sol, 3 parts of silicon powder, 3 parts of reinforcing fiber.
2) will each raw material mix after carry out wet ball grinding, powder is formed after ball milling, and to cross 65 mesh sieves standby;
3) pressed compact is molded, and powder after ball milling is molded through granulation, pressed compact, compressing under 60Mpa pressure, insulation 2.5 Hour, the demoulding, obtain saggar body;
4) by base substrate pre-burning at 600 DEG C, water quenching is then carried out, base substrate is quickly put into water, time 25s;Then Base substrate after water quenching is put into 55 DEG C of oil, oil cooling 25s;
5) base substrate after processing is dried into 16h under field conditions (factors), is put into kiln and is burnt till, firing temperature 1220 DEG C, firing time is 12 hours;
6) the compound saggar after burning till is post-processed, some dilatation joints is cut in side, are filled at dilatation joint Ceramic wool, you can obtain compound saggar.

Claims (3)

1. a kind of compound saggar, it is characterised in that be prepared by the raw material of following parts by weight:Magnesia 10~13 parts of mud, black cunning 10~12 parts of stone, 33~35 parts of fire clay, old 10~12 parts of sand, 4~6 parts of ballstone, 4~6 parts of aluminium powder, 5~7 parts of bauxite, essence Wash 17~19 parts of mud, mullite 90-160 parts, cordierite powder 22-35 parts, attapulgite 8-12 parts, calcined kaolin 8-12 parts, Diopside 8-12 parts, fused magnesite 1-8 parts, red mud 1-3 parts;Nano-aluminum hydroxide colloidal sol 1-3 parts, silicon powder 1-3 parts, enhancing are fine Tie up 1-3 parts.
A kind of 2. compound saggar as claimed in claim 1, it is characterised in that the compound saggar by following parts by weight raw material It is prepared:Magnesia 11.22 parts of mud, 10.21 parts of black talc, 34.15 parts of fire clay, old 11.18 parts of sand, 4.65 parts of ballstone, aluminium 4.23 parts of powder, 6.24 parts of bauxite, 18.12 parts of fine purifiation mud, 122 parts of mullite, 25 parts of cordierite powder, 9 parts of attapulgite, calcining 9 parts of kaolin, 9 parts of diopside, 2 parts of fused magnesite, 2 parts of red mud;2 parts of nano-aluminum hydroxide colloidal sol, 2 parts of silicon powder;Enhancing is fine 2 parts of dimension.
3. the preparation method of a kind of compound saggar described in claim 1 or 2, it is characterised in that comprise the following steps:
1) will each raw material mix after carry out wet ball grinding, powder is formed after ball milling, and to cross 60 mesh sieves standby;
2) pressed compact is molded, and powder after ball milling is molded through granulation, pressed compact, compressing under 60Mpa pressure, is incubated 2.5 hours, The demoulding, obtains saggar body;
3) by base substrate pre-burning at 500-600 DEG C, water quenching is then carried out, base substrate is quickly put into water, time 22-35s;With The base substrate after water quenching is put into 50-60 DEG C of oil afterwards, oil cooling 22-35s;
4) base substrate after processing is dried into 10-22h under field conditions (factors), is put into kiln and is burnt till, firing temperature 1160- 1350 DEG C, firing time is 10-16 hours;
5) the compound saggar after burning till is post-processed, some dilatation joints is cut in side, ceramics are filled at dilatation joint Cotton, you can obtain compound saggar.
CN201710581074.2A 2017-07-17 2017-07-17 A kind of compound saggar and preparation method thereof Pending CN107399977A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710581074.2A CN107399977A (en) 2017-07-17 2017-07-17 A kind of compound saggar and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710581074.2A CN107399977A (en) 2017-07-17 2017-07-17 A kind of compound saggar and preparation method thereof

Publications (1)

Publication Number Publication Date
CN107399977A true CN107399977A (en) 2017-11-28

Family

ID=60400725

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710581074.2A Pending CN107399977A (en) 2017-07-17 2017-07-17 A kind of compound saggar and preparation method thereof

Country Status (1)

Country Link
CN (1) CN107399977A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108083824A (en) * 2017-12-25 2018-05-29 浙江大学 Corrosion-resistant saggar, preparation method and applications
CN108395206A (en) * 2018-04-18 2018-08-14 福建省东丰阁文化发展有限公司 A kind of pseudo-classic formula of saggar embryo soil and preparation method
CN108649148A (en) * 2018-06-20 2018-10-12 上海定向材料科技有限公司 A kind of preparation method of lean property aluminium titanate composite material saggar
CN109305808A (en) * 2018-10-16 2019-02-05 武汉科技大学 A kind of sagger for firing cathode material of lithium battery and preparation method thereof
CN112378349A (en) * 2020-09-28 2021-02-19 湖南海森格诺信息技术有限公司 Sagger flatness detection device based on binocular structured light and detection method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1803705A (en) * 2006-01-20 2006-07-19 刘兴良 Sagger for calcination of talc and method for manufacturing the same
CN101955364A (en) * 2010-10-21 2011-01-26 淄博鲁铭高温材料科技有限公司 Method for producing corundum-mullite sagger
CN106083083A (en) * 2016-06-12 2016-11-09 姚焕根 The preparation method of compound saggar
CN106083082A (en) * 2016-06-12 2016-11-09 尹天锋 A kind of mullite corundum is combined the preparation method of saggar

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1803705A (en) * 2006-01-20 2006-07-19 刘兴良 Sagger for calcination of talc and method for manufacturing the same
CN101955364A (en) * 2010-10-21 2011-01-26 淄博鲁铭高温材料科技有限公司 Method for producing corundum-mullite sagger
CN106083083A (en) * 2016-06-12 2016-11-09 姚焕根 The preparation method of compound saggar
CN106083082A (en) * 2016-06-12 2016-11-09 尹天锋 A kind of mullite corundum is combined the preparation method of saggar

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108083824A (en) * 2017-12-25 2018-05-29 浙江大学 Corrosion-resistant saggar, preparation method and applications
CN108083824B (en) * 2017-12-25 2021-02-19 浙江大学 Corrosion-resistant sagger, preparation method and application thereof
CN108395206A (en) * 2018-04-18 2018-08-14 福建省东丰阁文化发展有限公司 A kind of pseudo-classic formula of saggar embryo soil and preparation method
CN108649148A (en) * 2018-06-20 2018-10-12 上海定向材料科技有限公司 A kind of preparation method of lean property aluminium titanate composite material saggar
CN108649148B (en) * 2018-06-20 2021-05-14 上海定向材料科技有限公司 Preparation method of barren aluminum titanate composite material sagger
CN109305808A (en) * 2018-10-16 2019-02-05 武汉科技大学 A kind of sagger for firing cathode material of lithium battery and preparation method thereof
CN112378349A (en) * 2020-09-28 2021-02-19 湖南海森格诺信息技术有限公司 Sagger flatness detection device based on binocular structured light and detection method thereof

Similar Documents

Publication Publication Date Title
CN107399977A (en) A kind of compound saggar and preparation method thereof
CN106083083A (en) The preparation method of compound saggar
CN107344857B (en) A kind of high-strength low heat conductivity fire resisting energy conservation castable and preparation method thereof
CN106083082A (en) A kind of mullite corundum is combined the preparation method of saggar
CN106083081A (en) A kind of preparation method of compound saggar
CN102701763A (en) Low-aluminum sintered alumina-silica refractory material and preparation method thereof
CN106083084A (en) A kind of forsterite corundum is combined the preparation method of saggar
CN106007810B (en) A kind of ceramic insulator self-cleaning glaze
CN103664205A (en) Thermal shock-resistant low-expansion andalusite castable
CN101768006A (en) Lightweight refractory for glass smelting kiln
CN105000864A (en) Anti-crack ceramic tile
CN102503142A (en) Dry particles for crystal polishing tiles sintered at one step and application thereof
CN107892579A (en) Calcareous glass furnace molten tin bath suspended roof brick of aluminic acid and preparation method thereof
CN107805077A (en) Compound low aluminium checker brick and its production method
CN102303971B (en) Fused quartziferous cast glazed tile for coke oven and preparation method thereof
CN104030658B (en) Sand device kettle handle thermal insulation material and there is the preparation method of sand device kettle of adiabatic handle
CN106083085A (en) A kind of preparation method of alumina silicon carbide compound saggar
CN109437934A (en) A kind of mullite composite refractory brick
CN110204322A (en) A kind of mullite insulating fire brick and preparation method thereof
CN103130521B (en) Coating material on fireproof material for continuous casting device and use method thereof
CN105330159A (en) Glaze of coke oven door lining brick and processing method thereof
CN107266058A (en) It is a kind of to be used to produce modified saggar of ceramics and preparation method thereof
CN107382297A (en) It is a kind of to be used to produce saggar of ceramics and preparation method thereof
CN102850082A (en) Hole-closing and heat-preserving vitrified ceramic and preparation method thereof
CN102303972A (en) Cordierite-poured glazed tile for coke oven and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20171128

RJ01 Rejection of invention patent application after publication