CN107259562A - Tomato peel is the method that raw material produces health food soft capsule of lycopene - Google Patents
Tomato peel is the method that raw material produces health food soft capsule of lycopene Download PDFInfo
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- CN107259562A CN107259562A CN201710388419.2A CN201710388419A CN107259562A CN 107259562 A CN107259562 A CN 107259562A CN 201710388419 A CN201710388419 A CN 201710388419A CN 107259562 A CN107259562 A CN 107259562A
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- tomato
- lycopene
- oleoresin
- soft capsule
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- 235000007688 Lycopersicon esculentum Nutrition 0.000 title claims abstract description 148
- UPYKUZBSLRQECL-UKMVMLAPSA-N Lycopene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1C(=C)CCCC1(C)C)C=CC=C(/C)C=CC2C(=C)CCCC2(C)C UPYKUZBSLRQECL-UKMVMLAPSA-N 0.000 title claims abstract description 80
- JEVVKJMRZMXFBT-XWDZUXABSA-N Lycophyll Natural products OC/C(=C/CC/C(=C\C=C\C(=C/C=C/C(=C\C=C\C=C(/C=C/C=C(\C=C\C=C(/CC/C=C(/CO)\C)\C)/C)\C)/C)\C)/C)/C JEVVKJMRZMXFBT-XWDZUXABSA-N 0.000 title claims abstract description 80
- 235000012661 lycopene Nutrition 0.000 title claims abstract description 80
- OAIJSZIZWZSQBC-GYZMGTAESA-N lycopene Chemical compound CC(C)=CCC\C(C)=C\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C=C(/C)CCC=C(C)C OAIJSZIZWZSQBC-GYZMGTAESA-N 0.000 title claims abstract description 80
- 239000001751 lycopene Substances 0.000 title claims abstract description 80
- 229960004999 lycopene Drugs 0.000 title claims abstract description 80
- ZCIHMQAPACOQHT-ZGMPDRQDSA-N trans-isorenieratene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/c1c(C)ccc(C)c1C)C=CC=C(/C)C=Cc2c(C)ccc(C)c2C ZCIHMQAPACOQHT-ZGMPDRQDSA-N 0.000 title claims abstract description 80
- 239000007901 soft capsule Substances 0.000 title claims abstract description 41
- 239000002994 raw material Substances 0.000 title claims abstract description 30
- 238000000034 method Methods 0.000 title claims abstract description 29
- 235000013402 health food Nutrition 0.000 title claims abstract description 22
- 240000003768 Solanum lycopersicum Species 0.000 title claims description 141
- 239000008601 oleoresin Substances 0.000 claims abstract description 55
- 238000004821 distillation Methods 0.000 claims abstract description 41
- 235000015112 vegetable and seed oil Nutrition 0.000 claims abstract description 20
- 239000000843 powder Substances 0.000 claims abstract description 19
- 239000012043 crude product Substances 0.000 claims abstract description 18
- 239000008158 vegetable oil Substances 0.000 claims abstract description 17
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000002893 slag Substances 0.000 claims abstract description 11
- 238000004519 manufacturing process Methods 0.000 claims abstract description 10
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 8
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 8
- 238000000926 separation method Methods 0.000 claims description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 238000000199 molecular distillation Methods 0.000 claims description 11
- 238000000605 extraction Methods 0.000 claims description 8
- 238000001035 drying Methods 0.000 claims description 7
- 239000000284 extract Substances 0.000 claims description 7
- 235000019486 Sunflower oil Nutrition 0.000 claims description 3
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- 239000002600 sunflower oil Substances 0.000 claims description 3
- 239000003292 glue Substances 0.000 claims description 2
- 244000061458 Solanum melongena Species 0.000 claims 1
- 235000002597 Solanum melongena Nutrition 0.000 claims 1
- 239000002775 capsule Substances 0.000 claims 1
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- 238000005516 engineering process Methods 0.000 abstract description 3
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- 238000013329 compounding Methods 0.000 abstract 1
- 238000000194 supercritical-fluid extraction Methods 0.000 abstract 1
- 238000005457 optimization Methods 0.000 description 7
- 239000000047 product Substances 0.000 description 6
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 4
- 244000147058 Derris elliptica Species 0.000 description 3
- 235000021466 carotenoid Nutrition 0.000 description 3
- 150000001747 carotenoids Chemical class 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
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- 229930003427 Vitamin E Natural products 0.000 description 2
- OENHQHLEOONYIE-UKMVMLAPSA-N all-trans beta-carotene Natural products CC=1CCCC(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C OENHQHLEOONYIE-UKMVMLAPSA-N 0.000 description 2
- 235000013734 beta-carotene Nutrition 0.000 description 2
- 239000011648 beta-carotene Substances 0.000 description 2
- TUPZEYHYWIEDIH-WAIFQNFQSA-N beta-carotene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CCCC1(C)C)C=CC=C(/C)C=CC2=CCCCC2(C)C TUPZEYHYWIEDIH-WAIFQNFQSA-N 0.000 description 2
- 229960002747 betacarotene Drugs 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 2
- 231100001261 hazardous Toxicity 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
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- 235000019165 vitamin E Nutrition 0.000 description 2
- 229940046009 vitamin E Drugs 0.000 description 2
- 239000011709 vitamin E Substances 0.000 description 2
- OENHQHLEOONYIE-JLTXGRSLSA-N β-Carotene Chemical compound CC=1CCCC(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C OENHQHLEOONYIE-JLTXGRSLSA-N 0.000 description 2
- 201000001320 Atherosclerosis Diseases 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
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- 229930182558 Sterol Natural products 0.000 description 1
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- 238000003379 elimination reaction Methods 0.000 description 1
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- 235000019322 gelatine Nutrition 0.000 description 1
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- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
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- 150000003432 sterols Chemical class 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 235000015193 tomato juice Nutrition 0.000 description 1
- 235000015113 tomato pastes and purées Nutrition 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/30—Encapsulation of particles, e.g. foodstuff additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/005—Processes comprising at least two steps in series
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/04—Purification; Separation; Use of additives by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/10—Purification; Separation; Use of additives by extraction, i.e. purification or separation of liquid hydrocarbons with the aid of liquids
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Water Supply & Treatment (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Botany (AREA)
- Mycology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
It is a kind of method that tomato peel produces health food soft capsule of lycopene for raw material the present invention relates to food technology field；The first step, raw material tomato skin slag crust seed is separated；Second step, tomato skin powder carbon dioxide supercritical extraction；3rd step, lycopene oleoresin crude product distillation processing；Soft capsule of lycopene is made with vegetable oil compounding in 4th step, tomato oleoresin.The lycopene content for the tomato oleoresin that the more existing extracting method of the lycopene content of tomato oleoresin is obtained improves a lot in the present invention, and the production process environmental protection of the present invention, has prevented the pollution to air and soil；Meanwhile, there is no chemical solvent residual in tomato oleoresin and soft capsule of lycopene that the present invention is obtained, completely remain the bioactivity and trace element of lycopene, be a kind of health food of environmental protection safety.
Description
Technical field
It is that a kind of tomato peel produces health food soft capsule of lycopene for raw material the present invention relates to food technology field
Method.
Background technology
Lycopene is a kind of important carotenoid, is the intermediate of many carrotene synthesis, it has unique
Long-chain molecule structure, 13 double bonds more than other carotenoid.Just because of its special construction makes it have strong elimination
Free radical ability and higher oxidation resistance, its antioxidation are 2 times of beta carotene, are 100 times of vitamin E,
The healthcare function of lycopene cover anti-aging, pre- anti-cancer, enhancing immunity of organisms, improve atherosclerosis and
The many aspects such as beauty, ultra-violet radiation resisting, have the laudatory title of " gold ensconced in tomato ", are a kind of good Natural Foods
Product additive.Therefore, lycopene has been increasingly becoming the new heat of health food on international market, cosmetics and field of medicaments research
Point.Because mammal can not synthesize carotenoid in vivo（Including lycopene）, therefore lycopene is main in human body
It is to obtain from fruit and in vegetables, especially tomato and tomato products.
At present, tomato in China production is mainly distributed on Xinjiang, Gansu and Inner Mongol, and wherein Xinjiang region accounts for national total amount
90% or so, the tomato of present China plantation has quite a few to be production for tomato processing product, and catsup, kind
In the production processes such as tomato juice, concentrated tomato paste and tomato meal, there is the tomato peel for accounting for raw material tomato content 4% to 5% to produce,
In tomato peel the content of tomato skin is 42% to 45% or so, wherein, contain with lycopene in the pulp of pericarp connected component
High many of the lycopene at more other than the fruit positions of amount, so tomato skin is a kind of comparatively ideal source for obtaining lycopene.
But existing tomato peel is used generally as feed, also it has been documented from tomato peel and has extracted lycopene
Method, but existing extracting method has the following disadvantages：1. having used chemical solvent in extraction process, change in process of production
Learn solvent easily to pollute air and soil, to operating personnel, there is also potential safety hazard；2. easy chemical residue solvent in product,
It is hazardous to the human body；3. destroying the bioactivity of lycopene, some trace elements are easily lost or converted in process of production,
Effect can have a greatly reduced quality after human body is edible.
The content of the invention
It is the method that raw material produces health food soft capsule of lycopene the invention provides a kind of tomato peel, overcomes
The deficiency of above-mentioned prior art, its can effectively solve existing extracting method easily air and soil are polluted, exist safety it is hidden
Suffer from, be hazardous to the human body the problem of being had a greatly reduced quality with the edible rear effect of human body.
The technical scheme is that realized by following measures：A kind of tomato peel is that raw material produces health food
The method of soft capsule of lycopene, is carried out in the steps below：The first step, skin seed separation, skin seed point are carried out by raw material tomato skin slag
Tomato peel is obtained from after, tomato peel after drying, crushing, obtains tomato skin powder successively；Second step, tomato skin powder is in temperature
For 31 DEG C to 33 DEG C, pressure be 7.2Mpa to 7.4Mpa carbon dioxide supercritical extract 1h to 2h, obtain tomato red after extraction
Vegetable oil resin crude product；3rd step, lycopene oleoresin crude product obtains tomato oleoresin after distillation；4th step, tomato oil tree
Fat is re-dubbed after soft capsule content with vegetable oil, and soft capsule of lycopene is made.
Here is the further optimization and/or improvements to foregoing invention technical scheme：
In the above-mentioned first step, raw material tomato skin slag carries out skin seed separation in water, is passed through after the tomato peel separation floated on the surface
Vibratory sieve or squeezer processing, the water content that tomato peel is made after processing is 70% to 75%, obtains tomato peel.
In the above-mentioned first step, tomato peel dries 5s to 10s in the case where temperature is 80 DEG C to 100 DEG C, through crushing after drying, obtains
To tomato skin powder.
In above-mentioned 3rd step, lycopene oleoresin crude product after distillation still distillation and short-range molecular distillation, is obtained successively
Tomato oleoresin.
The vacuum of above-mentioned distillation still distillation is 0.07Mpa to 0.1Mpa, and distillation time is 3h to 5h；Short-range molecular distillation
Vacuum be 0 to 5pa, distillation time be 4min to 6min.
In above-mentioned 4th step, tomato oleoresin is 1 in mass ratio with vegetable oil:3.6 to 1:4.7 are re-dubbed soft capsule content
Thing.
Above-mentioned vegetable oil is sunflower oil or tomato seed oil or safflower seed oil or linseed oil.
The tomato for the tomato oleoresin that the more existing extracting method of the lycopene content of tomato oleoresin is obtained in the present invention
Lycopene content improves a lot, and the production process environmental protection of the present invention, has prevented the pollution to air and soil；Meanwhile,
There is no chemical solvent residual in tomato oleoresin and soft capsule of lycopene that the present invention is obtained, completely remain lycopene
Bioactivity and trace element, are a kind of health foods of environmental protection safety.
Embodiment
The present invention is not limited by following embodiments, can technique according to the invention scheme and actual conditions it is specific to determine
Embodiment.Percentage in the present invention is as being mass percent without specified otherwise.
Embodiment 1, the tomato peel is the method that raw material produces health food soft capsule of lycopene, is entered in the steps below
OK：The first step, carries out skin seed separation by raw material tomato skin slag, tomato peel is obtained after the separation of skin seed, tomato peel is successively through dry
After dry, crushing, tomato skin powder is obtained；Second step, tomato skin powder temperature be 31 DEG C to 33 DEG C, pressure be 7.2Mpa to 7.4Mpa
Lycopene oleoresin crude product is obtained after carbon dioxide supercritical extract 1h to 2h, extraction；3rd step, lycopene oleoresin
Crude product obtains tomato oleoresin after distillation；4th step, tomato oleoresin is re-dubbed after soft capsule content with vegetable oil, is made
Soft capsule of lycopene.Lycopene is to be easy to dissolving after liposoluble substance, plus vegetable oil, beneficial to absorption of human body.Tomato peel
It is the mixture of tomato peel, Tomato Seed and a small amount of tomato pulp（Tomato peel accounts for 40%, and Tomato Seed accounts for 50%, tomato pulp
Account for 10%）.The water content of tomato skin powder can pass through 60 mesh sieves 5% to 15%.
Embodiment 2, the tomato peel is the method that raw material produces health food soft capsule of lycopene, is entered in the steps below
OK：The first step, carries out skin seed separation by raw material tomato skin slag, tomato peel is obtained after the separation of skin seed, tomato peel is successively through dry
After dry, crushing, tomato skin powder is obtained；Second step, tomato skin powder temperature be 31 DEG C or 33 DEG C, pressure be 7.2Mpa or 7.4Mpa
Carbon dioxide supercritical extract 1h or 2h, obtain lycopene oleoresin crude product after extraction；3rd step, lycopene oleoresin
Crude product obtains tomato oleoresin after distillation；4th step, tomato oleoresin is re-dubbed after soft capsule content with vegetable oil, is made
Soft capsule of lycopene.
Embodiment 3, as the optimization of above-described embodiment, in the first step, raw material tomato skin slag carries out skin seed separation in water,
Handled after the tomato peel separation floated on the surface through vibratory sieve or squeezer, the water content that tomato peel is made after processing is 70%
To 75%, tomato peel is obtained.
Embodiment 4, as the optimization of above-described embodiment, in the first step, tomato peel is to do at 80 DEG C to 100 DEG C in temperature
Dry 5s to 10s, through crushing after drying, obtains tomato skin powder.
Embodiment 5, as the optimization of above-described embodiment, in the 3rd step, lycopene oleoresin crude product is successively through distillation still
After distillation and short-range molecular distillation, tomato oleoresin is obtained.Lycopene oleoresin crude product is distilled off greatly with distillation still first
Part moisture, water content can be controlled in less than 3%, and about 30% some lightweight tomato oils things are then removed with short-range molecular distillation
Lycopene is rich in matter, tomato oleoresin now.
Embodiment 6, as the optimization of above-described embodiment, the vacuum of distillation still distillation is 0.07Mpa to 0.1Mpa, distillation
Time is 3h to 5h；The vacuum of short-range molecular distillation is 0 to 5pa, and distillation time is 4min to 6min.
Embodiment 7, as the optimization of above-described embodiment, in the 4th step, tomato oleoresin is 1 in mass ratio with vegetable oil:
3.6 to 1:4.7 are re-dubbed soft capsule content.
Embodiment 8, as the optimization of above-described embodiment, vegetable oil is sunflower oil or tomato seed oil or safflower seed oil or Asia
Flaxseed oil.
Embodiment 9, the tomato peel is the method that raw material produces health food soft capsule of lycopene, is entered in the steps below
OK：The first step, skin seed separation is carried out by raw material tomato skin slag in water, through vibratory sieve after the tomato peel separation floated on the surface
Or squeezer processing, the water content that tomato peel is made after processing is 75%, obtains tomato peel, and tomato peel is 80 DEG C in temperature
Lower dry 10s, through crushing after drying, obtains tomato skin powder；Second step, tomato skin powder temperature be 31 DEG C, pressure be 7.2Mpa
Carbon dioxide supercritical extract 2h, obtains lycopene oleoresin crude product after extraction；3rd step, lycopene oleoresin crude product
First distilled through distillation still, the vacuum of distillation still distillation is 0.1Mpa, and distillation time is 5h, then again through short-range molecular distillation,
The vacuum of short-range molecular distillation is 5pa, and distillation time is to obtain tomato oleoresin after 6min, distillation；4th step, tomato oil tree
Fat is 1 in mass ratio with vegetable oil:3.6 are re-dubbed after soft capsule content, and soft capsule of lycopene is made.In the present embodiment 9,
The lycopene content of tomato oleoresin can reach 6.5%.
Embodiment 10, the tomato peel is the method that raw material produces health food soft capsule of lycopene, in the steps below
Carry out：The first step, skin seed separation is carried out by raw material tomato skin slag in water, through vibration after the tomato peel separation floated on the surface
Sieve or squeezer processing, the water content that tomato peel is made after processing is 73%, obtains tomato peel, and tomato peel is 90 in temperature
8s is dried at DEG C, through crushing after drying, tomato skin powder is obtained；Second step, tomato skin powder temperature be 32 DEG C, pressure be 7.3Mpa
Carbon dioxide supercritical extract 1.5h, obtains lycopene oleoresin crude product after extraction；3rd step, lycopene oleoresin is thick
Product first distill through distillation still, and the vacuum of distillation still distillation is 0.09Mpa, and distillation time is 4h, is then steamed again through short distance molecule
Evaporate, the vacuum of short-range molecular distillation is 3pa, distillation time is to obtain tomato oleoresin after 5min, distillation；4th step, tomato
Oleoresin is 1 in mass ratio with vegetable oil:4.0 are re-dubbed after soft capsule content, and soft capsule of lycopene is made.The present embodiment
In 10, the lycopene content of tomato oleoresin can reach 7.2%.
Embodiment 11, the tomato peel is the method that raw material produces health food soft capsule of lycopene, in the steps below
Carry out：The first step, skin seed separation is carried out by raw material tomato skin slag in water, through vibration after the tomato peel separation floated on the surface
Sieve or squeezer processing, the water content that tomato peel is made after processing is 70%, obtains tomato peel, and tomato peel is 100 in temperature
5s is dried at DEG C, through crushing after drying, tomato skin powder is obtained；Second step, tomato skin powder temperature be 33 DEG C, pressure be 7.4Mpa
Carbon dioxide supercritical extract 1h, obtains lycopene oleoresin crude product after extraction；3rd step, lycopene oleoresin crude product
First distilled through distillation still, the vacuum of distillation still distillation is 0.07Mpa, and distillation time is 3.5h, is then steamed again through short distance molecule
Evaporate, the vacuum of short-range molecular distillation is 0, distillation time is to obtain tomato oleoresin after 5min, distillation；4th step, tomato oil
Resin is 1 in mass ratio with vegetable oil:4.2 are re-dubbed after soft capsule content, and soft capsule of lycopene is made.The present embodiment 11
In, the lycopene content of tomato oleoresin can reach 8.0%.
In 4th step of the invention, tomato oleoresin is re-dubbed after soft capsule content with vegetable oil, then can be with gelatin, sweet
The glue that oil, polyethylene glycol 400 and purified water are made is pressed into soft capsule through pellet press.
The lycopene content average out to 6.2% for the tomato oleoresin that tomato peel is obtained by existing extracting method, this hair
The lycopene content of bright middle tomato oleoresin can reach 6.5% to 8.0%, illustrate the lycopene of tomato oleoresin in the present invention
The lycopene content for the tomato oleoresin that the more existing extracting method of content is obtained improves a lot, and is obtained by tomato oleoresin
Soft capsule of lycopene of the present invention in lycopene content can reach 1.12% to 2.52%, and the production process green of the present invention
Environmental protection, has prevented the pollution to air and soil；Meanwhile, do not have in tomato oleoresin and soft capsule of lycopene that the present invention is obtained
There is chemical solvent residual, in addition to lycopene, also the one of the needed by human body such as beta carotene, vitamin E, sterol, phosphatide
Secondary element, completely remains the bioactivity and trace element of lycopene slightly, is a kind of health care food of environmental protection safety
Product.
In summary, the tomato oil tree that the more existing extracting method of lycopene content of tomato oleoresin is obtained in the present invention
The lycopene content of fat improves a lot, and the production process environmental protection of the present invention, has prevented the dirt to air and soil
Dye；Meanwhile, there is no chemical solvent residual in the obtained tomato oleoresin of the present invention and soft capsule of lycopene, completely remain kind
The bioactivity and trace element of Lycopene, are a kind of health foods of environmental protection safety.
Above technical characteristic constitutes embodiments of the invention, and it has stronger adaptability and implementation result, can basis
The non-essential technical characteristic of increase and decrease is actually needed, to meet the demand of different situations.
Claims (7)
1. a kind of tomato peel is the method that raw material produces health food soft capsule of lycopene, it is characterised in that in the steps below
Carry out：The first step, carries out skin seed separation by raw material tomato skin slag, obtains tomato peel after the separation of skin seed, tomato peel is passed through successively
After dry, crushing, tomato skin powder is obtained；Second step, tomato skin powder temperature be 31 DEG C to 33 DEG C, pressure be 7.2Mpa extremely
7.4Mpa carbon dioxide supercritical extract 1h to 2h, obtain lycopene oleoresin crude product after extraction；3rd step, lycopene
Oleoresin crude product obtains tomato oleoresin after distillation；4th step, tomato oleoresin is re-dubbed soft capsule content with vegetable oil
Afterwards, soft capsule of lycopene is made.
2. tomato peel according to claim 1 is the method that raw material produces health food soft capsule of lycopene, it is special
Levy and be in the first step, raw material tomato skin slag carries out skin seed separation in water, through shaking after the tomato peel separation floated on the surface
Dynamic sieve or squeezer processing, the water content that tomato peel is made after processing is 70% to 75%, obtains tomato peel.
3. tomato peel according to claim 1 or 2 is the method that raw material produces health food soft capsule of lycopene, its
It is characterised by the first step, tomato peel is to dry 5s to 10s at 80 DEG C to 100 DEG C in temperature, through crushing after drying, is obtained kind
Eggplant skin powder.
4. the tomato peel according to claim 1 or 2 or 3 produces the side of health food soft capsule of lycopene for raw material
Method, it is characterised in that in the 3rd step, lycopene oleoresin crude product after distillation still distillation and short-range molecular distillation, is obtained successively
Tomato oleoresin.
5. tomato peel according to claim 4 is the method that raw material produces health food soft capsule of lycopene, it is special
Levy and be that the vacuum that distillation still is distilled is 0.07Mpa to 0.1Mpa, distillation time is 3h to 5h；The vacuum of short-range molecular distillation
Spend for 0 to 5pa, distillation time is 4min to 6min.
6. the tomato peel according to claim 1 or 2 or 3 or 4 or 5 produces health food soft capsule of lycopene for raw material
Method, it is characterised in that in the 4th step, tomato oleoresin and vegetable oil are 1 in mass ratio:3.6 to 1:4.7 are re-dubbed flexible glue
It is intracapsular tolerant.
7. the tomato peel according to claim 1 or 2 or 3 or 4 or 5 or 6 is soft for raw material production health food lycopene
The method of capsule, it is characterised in that vegetable oil is sunflower oil or tomato seed oil or safflower seed oil or linseed oil.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108669557A (en) * | 2018-05-20 | 2018-10-19 | 苏州工业园区联创生物科技有限公司 | Soft capsule dosage form and preparation method thereof containing natural tomato extract liquor pumpkin seed oil |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101810225A (en) * | 2010-04-09 | 2010-08-25 | 新疆大学 | Method for producing lycopene oil resin and plant oil rich in lycopene |
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- 2017-05-27 CN CN201710388419.2A patent/CN107259562A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101810225A (en) * | 2010-04-09 | 2010-08-25 | 新疆大学 | Method for producing lycopene oil resin and plant oil rich in lycopene |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108669557A (en) * | 2018-05-20 | 2018-10-19 | 苏州工业园区联创生物科技有限公司 | Soft capsule dosage form and preparation method thereof containing natural tomato extract liquor pumpkin seed oil |
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