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CN107238560A - Constant speed balance soot dust granule thing concentration readout portable measurement system and method - Google Patents

Constant speed balance soot dust granule thing concentration readout portable measurement system and method Download PDF

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Publication number
CN107238560A
CN107238560A CN201710627439.0A CN201710627439A CN107238560A CN 107238560 A CN107238560 A CN 107238560A CN 201710627439 A CN201710627439 A CN 201710627439A CN 107238560 A CN107238560 A CN 107238560A
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China
Prior art keywords
shakes
bar
chamber
sensor cluster
processing unit
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Granted
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CN201710627439.0A
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Chinese (zh)
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CN107238560B (en
Inventor
孙作福
吕卫涛
徐立佳
刘凯
王桐
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Qingdao Junray Intelligent Instrument Co Ltd
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Qingdao Junray Intelligent Instrument Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/06Investigating concentration of particle suspensions
    • G01N15/0606Investigating concentration of particle suspensions by collecting particles on a support
    • G01N15/0618Investigating concentration of particle suspensions by collecting particles on a support of the filter type
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/06Investigating concentration of particle suspensions
    • G01N15/0656Investigating concentration of particle suspensions using electric, e.g. electrostatic methods or magnetic methods
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/20Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters

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  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The present invention relates to constant speed balance soot dust granule thing concentration readout portable measurement system and method, including quality collecting unit, sensor cluster, sampling head, center processing unit, quality collecting unit includes:Shake chamber, and in intracavitary of shaking provided with vibrating diaphragm and the bar that shakes, the entrance hole diameter on the bar top that shakes is 7 9mm, and the wall thickness for the bar that shakes is 0.45 0.55mm, and the end aperture for the bar that shakes is 19 21mm;Length is 100 120mm, and bar side of shaking face is curve, and vibrating diaphragm is arranged at the top of the bar that shakes;Chamber top shake provided with air inlet, gas outlet is provided with below the chamber that shakes, intracavitary of shaking is provided with sensor cluster;Sampling head is arranged in exhaust emission pipe, is connected with air inlet;Sensor cluster is again provided with exhaust piping;Center processing unit includes center processor, flue dust flow detection and control unit, sampling pump, and center processing unit is mutually communicated with quality collecting unit, sensor cluster, and sampling pump is connected by pipeline with the chamber gas outlet that shakes.The present invention is suitable for high-altitude, the direct-reading of narrow, bad environments portable rapid field tests.

Description

Constant speed balance soot dust granule thing concentration readout portable measurement system and method
Technical field
The present invention relates in a organized way or uncontrollable discharge measuring concentration of granules in certain, such as flue dust direct-reading particularly relates to And the portable measurement system and method for a kind of particle concentration direct-reading such as flue dust based on constant speed balance.
Background technology
Of the measuring concentration of granules in certain of current discharge or uncontrollable discharge in a organized way, flue dust or uncontrollable discharge Grain thing concentration determination belongs to routine monitoring in China, and daily monitoring task is very heavy.
In the method for airborne particulate analyte detection, oscillating balance method for principle live flue dust direct reading test instrument at home and abroad It has been used widely.But use the flue dust flow of oscillating balance method measurement general in 1L/min or so, apply " empty In gas " particulate matter (such as TSP of PM2.5 10), the measurement of the concentration of " microgram rank ".
And be in the particle concentration detection of discharge or uncontrollable discharge in a organized way, the characteristics of its pollutant:Discharge Soot dust granule logistics capacity it is big, (general milligram rank) much higher in the concentration relative atmospheric of particulate matter, high humidity, particle is close The features such as spending changeable, according to GB16157 (particulate matter and the gaseous contaminant method of sampling in Concentration in Fixed Pollutants Source) requirement not The measurement of " constant speed " or constant flow (general 20~30L/min or so) can be used for by the way of " full stream ", especially in flue dust High-precision direct-reading in terms of;Therefore it is difficult to oscillating balance method being applied in the detection of flue dust or uncontrollable discharge.
In the detection of current flue dust or uncontrollable discharge, typically from filter membrane weight method, with oscillating balance method Compare, it weighs quality again after needing collecting sample, time laboratory heat treatment at the scene, and then obtains mass concentration, discharges dense The data such as degree, the cycle is long, expends a large amount of manpowers, financial resources, material resources, does not meet low-carbon environment-friendly, efficient policy that country advocates;And And filter membrane weight method needs the equipment carried a lot, takes larger space;Applied existing at present in the detection of stationary source flue dust Patent have " a kind of oscillating balance dust concentration direct reading measurement instrument with flow dividing structure of CN201520460472.5 ", but its side Method core content is to use " shunting " scheme, and artificial is divided into emission two strands, but two strands of emissions of shunting is real-time " constant speed " property is difficult manual control, and " constant speed " of flue dust will influence oscillating balance measurement result accuracy, directly affect detection As a result accuracy;And the separate system is extremely complex, high-altitude is not suitable for, narrow, bad environments portable quick On-the-spot test.
The content of the invention
In view of the above-mentioned problems, this patent provides a kind of soot dust granule thing concentration portable type measuring based on oscillating balance method System and method, can realize that " live direct-reading " is (existing using the present apparatus in the detection of current flue dust or uncontrollable discharge Field can obtain the finally detection data such as particle concentration, concentration of emission) and be easy to carry;Testing result closely conforms to national inspection Mark is accurate.
The technical solution used in the present invention is as follows:
Constant speed balance soot dust granule thing concentration readout portable measurement system and method, including quality collecting unit, sensing Device assembly, sampling head, center processing unit, the quality collecting unit include:Shake chamber, in intracavitary of shaking provided with vibrating diaphragm and the bar that shakes, The entrance hole diameter on the bar top that shakes is 7-9mm, and the wall thickness for the bar that shakes is 0.45-0.55mm, and the end aperture for the bar that shakes is 19- 21mm;Length is 100-120mm, and bar side of shaking face is curve, and the vibrating diaphragm is arranged at the top of the bar that shakes;Chamber top shake provided with air inlet Mouthful, gas outlet is provided with below the chamber that shakes, intracavitary of shaking is provided with sensor cluster;The sensor cluster includes temperature sensor, flow velocity Sensor, pressure sensor;The sampling head is arranged in exhaust emission pipe, is connected with air inlet;It is same in exhaust piping Sample is provided with sensor cluster;The center processing unit includes center processor, flue dust flow detection and control unit, sampling Pump;The center processing unit is mutually communicated with quality collecting unit, sensor cluster, and sampling pump passes through pipeline and the chamber outlet that shakes Mouth connection.
Further:The chamber that shakes includes cavity of resorption and is hinged on the upper chamber cover of cavity of resorption side, between cavity of resorption and upper chamber cover Provided with sealing strip, shock absorber, heat-insulation layer and vibration insulation, the wall of chamber four that shakes is provided with heater element.
Further:The air inlet is arranged on upper chamber cover, with intake interface and guide channel;Described be oriented to is led to Road upper end is connected with intake interface, and extension covers vibrating diaphragm downwards for lower end.
Further:Also include probe tube, the probe tube is arranged between sampling head and quality collecting unit, described to take Sample inside pipe wall is enclosed with heater element.
Further:Also include probe tube, the probe tube is arranged between quality collecting unit and center processing unit.
Constant speed balance soot dust granule thing concentration readout portable measurement system and method, comprise the following steps:
(1) sensor cluster is set in flue, by sensor cluster by cigarette temperature, flow velocity, the flue gas pressures in flue Relevant information pass to center processing unit;
(2) mass measurement of particulate matter in flue dust in flue is completed by quality collecting unit, passes through quality collecting unit Interior sensor cluster passes information to center processing unit;
(3) center processing unit completes flue dust volume acquisition, the quality gathered data of bond quality collecting unit, Yi Jiyan The data of flue gas, which are calculated, in road obtains mass concentration, concentration of emission final data.
Beneficial effect
The present invention is suitable for high-altitude, narrow, bad environments portable rapid field tests.It is real by center processor It is existing " live direct-reading ", " full stream " that flue dust can be realized by the bar that shakes of special construction, single by flue dust flow detection and control Member can realize " constant speed " of flue dust flow velocity and realize measuring system and method portable, that meet national standard, greatly shorten Detection cycle.
Brief description of the drawings
Fig. 1 the structural representation of present invention one;
The structural representation two of Fig. 2 present invention;
Fig. 3 is a chamber internal structure schematic diagram of shaking of the invention;
Fig. 4 is to be weighed correction data using the sampling of the present invention and the soot dust granule amount of substance of filter membrane weight method;
In figure:1- temperature sensors, 2- flow sensors, 3- flue gas pressures sensor, 4- samplings elbow, 5- heating members Part, 51 heat-insulation layers;
Shake bar, 63- of 6- mass collecting unit, 61- vibrating diaphragms, 62- shakes chamber, 631 upper chamber covers, 632 cavity of resorptions, air inlet 66, goes out Gas port 65, damper 67;
7- exhaust emission pipes;Sample gas flows of the 8- containing particle, 9- center processing units, 10- probe tubes.
Embodiment
The present invention is described in further details with reference to specific embodiment and accompanying drawing.
As shown in Figure 1, Figure 2, Figure 3 shows, constant speed balance soot dust granule thing concentration readout portable measurement system and method, including Quality collecting unit, sensor cluster, sampling head, center processing unit, the quality collecting unit include:Shake chamber, in the chamber that shakes Interior to be provided with vibrating diaphragm and the bar that shakes, the entrance hole diameter on the bar top that shakes is 7-9mm, and the wall thickness for the bar that shakes is 0.45-0.55mm, and shake bar End aperture is 19-21mm;Length is 100-120mm, and bar side of shaking face is curve, and the vibrating diaphragm is arranged at the top of the bar that shakes;Shake chamber Top is provided with air inlet, and gas outlet is provided with below the chamber that shakes, and intracavitary of shaking is provided with sensor cluster;The sensor cluster includes temperature Sensor, flow sensor, pressure sensor;The sampling head is arranged in exhaust emission pipe, is connected with air inlet;Useless Sensor cluster is again provided with feed channel;The center processing unit includes center processor, flue dust flow detection and control Unit, sampling pump;The center processing unit is mutually communicated with quality collecting unit, sensor cluster, and sampling pump passes through pipeline Chamber gas outlet is connected with shaking.
The present invention is in the detection of flue dust or uncontrollable discharge, by the way that upper end open is small, lower ending opening is big, be sideways song The bar that shakes of line, the bar top that shakes is tapered rod, middle indent, bottom evagination, per part between all rounding ofves, from top to end The free form surface of the indent of smoothness is formed for free forming, compared with bar is shaken in conventional taper, the bar that shakes of this shape is in flue dust stream When measuring unstable, especially in the case where soot dust granule density is changeable, vibrational feedback result is reliable and stable, close in soot dust granule Spend playing a major role for the bar top that shaken in the case of stablizing, when soot dust granule density is unstable, the arch of underlying protrusion Shape space, the feedback for vibration is more sensitive, it is ensured that the precision of quality collection, without vibrating diaphragm is removed into measurement, is more suitable for Used in the detection of flue dust or uncontrollable discharge.
The shake entrance hole diameter of bar is controlled in 8mm or so, it is possible to achieve the collection of the flue dust of big flow, such as 20~30L/min Detection, the collection of the flue dust flow of left and right.Center processing unit is communication with each sensor cluster, quality collecting unit, can With steady temperature 30 to 110 degrees Celsius according to stationary source in a organized way or the sampling operating mode of uncontrollable discharge can be set; Resolution capability can reach 0.1 milligram, reach high accuracy, realize live direct-reading.The setting of the sensor cluster for intracavitary of shaking, passes through Center processor can realize automatic compensation, to adapt to diversified working environment.
Shake bar design parameter everywhere during actual use, according to different flow and resolving accuracy according to material Mechanics principle, adjusts the mass resolution needed for each gain of parameter of bar that shakes.
In center processing unit, the center processor of setting can be PLC, or other can realize the work( The intelligent processor of energy, is not limited herein.
In the present embodiment, use the magnetic field that electromagnet is produced and provide driving force for the bar that shakes;Flue dust flow detection and control Unit is adjusted in real time by the feedback of flow sensor to the flow velocity of flue dust (reaches adjustment mesh by controlling the rotating speed of sampling pump ), it is ensured that the flow velocity of flue dust is in a steady state value;Quality collecting unit is by measuring certain intervals time ventilation front and rear two Two intrinsic frequencies of the individual bar that shakes, can calculate the particulate matter quality on filter membrane, then divided by this time in the flue dust that flows through Cumulative volume can be obtained by the mean concentration of particulate matter, and all of above data processing is all completed by center processor.
Further:The chamber that shakes includes cavity of resorption and is hinged on the upper chamber cover of cavity of resorption side, between cavity of resorption and upper chamber cover Provided with sealing strip, shock absorber, heat-insulation layer and vibration insulation, the wall of chamber four that shakes is provided with heater element.
The concrete structure and form of shock absorber are not limited herein, can be elastomeric material parcel shake chamber or other Corresponding structure.
In the present embodiment, by the vibration insulation and shock absorber in the chamber that shakes, by setting damper so that vibration is not outer Pass, it is to avoid cause secondary vibration;By setting damping layer in the instantaneous position of the vibration of bar that shakes, it is to avoid vibrational energy, which is coupled into, to be come, Make to shake vibration of bar only have flue dust by when can just occur, can be with when flue dust is in big flow, particle concentration change Well adapt to, it is to avoid oscillatory instability;Further improve the accuracy of result.
Further:Air inlet is arranged on upper chamber cover, with intake interface and guide channel;Guide channel upper end with Intake interface is connected, and extension covers vibrating diaphragm downwards for lower end.
Guide channel ensures that flue dust circulation stability is more preferable, it is ensured that the flue dust of collection completely extends across vibrating diaphragm, as a result accurate steady It is fixed.
In the present embodiment, probe tube before quality collecting unit with air inlet if placed at connecting, then in sampling pipe Need to be enclosed with heater element on wall, it is ensured that flue dust is when entering quality collecting unit, in high temperature, if probe tube is arranged on It is connected after quality collecting unit with gas outlet, that need not set heater element.
Constant speed balance soot dust granule thing concentration readout portable measurement system and method, comprise the following steps:
(1) sensor cluster is set in flue, by sensor cluster by cigarette temperature, flow velocity, the flue gas pressures in flue Relevant information pass to center processing unit;
(2) mass measurement of particulate matter in flue dust in flue is completed by quality collecting unit, passes through quality collecting unit Interior sensor cluster passes information to center processing unit;
(3) center processing unit completes sampling volume collection, the quality gathered data of bond quality collecting unit, Yi Jiyan The data of flue gas, which are calculated, in road obtains mass concentration, concentration of emission final data.
When sampling air flow is by filter membrane, particulate matter therein is deposited on filter membrane, and the mass change of filter membrane causes oscillation frequency The change of rate, is changed by frequency of oscillation and calculates the quality for being deposited on particulate matter on filter membrane, further according to flow, site environment temperature Degree and air pressure calculate the mass concentration of the period particulate matter, will not be described here.
Shown in Fig. 4, in the present embodiment there is provided a kind of specific size for the bar that shakes, the entrance hole diameter 8mm on bar top shakes The wall thickness 0.5mm of bar, the end aperture 20mm for the bar that shakes;Length 110mm, in flue dust flow 25L/min, using this method with The particulate matter quality contrast number that filter membrane weight method is measured, the quality error of particulate matter is adopted within 5% using apparatus of the present invention The data measurement of collection is accurate, with a high credibility, it is possible to achieve " full stream ", " constant speed ", portable.Be particularly suitable for use in high-altitude, it is narrow, The portable rapid field test of bad environments.
The above described is only a preferred embodiment of the present invention, being not the limitation for making other forms to the present invention, appoint What those skilled in the art changed or be modified as possibly also with the technology contents of the disclosure above equivalent variations etc. Imitate embodiment and be applied to other fields, but every without departing from technical solution of the present invention content, the technical spirit according to the present invention Any simple modification, equivalent variations and the remodeling made to above example, still fall within the protection domain of technical solution of the present invention.

Claims (6)

1. constant speed balance soot dust granule thing concentration readout portable measurement system and method, it is characterised in that including quality collection Unit, sensor cluster, sampling head, center processing unit,
The quality collecting unit includes:Shake chamber, intracavitary of shaking is provided with vibrating diaphragm and shakes bar, it is described shake bar top entrance hole diameter be 7-9mm, the wall thickness for the bar that shakes is 0.45-0.55mm, and the end aperture for the bar that shakes is 19-21mm;Length is 100-120mm;Shake bar side Face is curve, and the vibrating diaphragm is arranged at the top of the bar that shakes;Chamber top shake provided with air inlet, gas outlet, intracavitary of shaking are provided with below the chamber that shakes Provided with sensor cluster;
The sensor cluster includes temperature sensor, flow sensor, pressure sensor;
The sampling head is arranged in exhaust emission pipe, is connected with air inlet;Sensor group is again provided with exhaust piping Part;The center processing unit includes center processor, flue dust flow detection and control unit, sampling pump;The center processing Unit is mutually communicated with quality collecting unit, sensor cluster, and sampling pump is connected by pipeline with the chamber gas outlet that shakes.
2. constant speed balance soot dust granule thing concentration readout portable measurement system according to claim 1 and method, it is special Levy and be:The chamber that shakes is including cavity of resorption and is hinged on the upper chamber cover of cavity of resorption side, between cavity of resorption and upper chamber cover provided with sealing strip, Shock absorber, heat-insulation layer and vibration insulation, the wall of chamber four that shakes are provided with heater element.
3. constant speed balance soot dust granule thing concentration readout portable measurement system according to claim 2 and method, it is special Levy and be:The air inlet is arranged on upper chamber cover, with intake interface and guide channel;The guide channel upper end is with entering Gas interface is connected, and extension covers vibrating diaphragm downwards for lower end.
4. constant speed balance soot dust granule thing concentration readout portable measurement system according to claim 3 and method, it is special Levy and be:Also include probe tube, the probe tube is arranged between sampling head and quality collecting unit, the sampling inside pipe wall bag It is wrapped with heater element.
5. constant speed balance soot dust granule thing concentration readout portable measurement system according to claim 4 and method, it is special Levy and be:Also include probe tube, the probe tube is arranged between quality collecting unit and center processing unit.
6. constant speed balance soot dust granule thing concentration readout portable measurement system and method, it is characterised in that:Comprise the following steps:
(1) sensor cluster is set in flue, by sensor cluster by the cigarette temperature in flue, flow velocity, flue gas pressures phase Information transmission is closed to center processing unit;
(2) mass measurement of particulate matter in flue dust in flue is completed by quality collecting unit, by quality collecting unit Sensor cluster passes information to center processing unit;
(3) center processing unit is completed in flue dust volume acquisition, the quality gathered data and flue of bond quality collecting unit The data of flue gas, which are calculated, obtains mass concentration, concentration of emission final data.
CN201710627439.0A 2017-07-28 2017-07-28 Constant-speed balance smoke dust particle concentration direct-reading portable measuring system and method Active CN107238560B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114486404A (en) * 2022-01-29 2022-05-13 江苏省环境监测中心 Constant-speed sampling method for directly measuring waste gas particulate matters of fixed pollution source
CN115165694A (en) * 2022-08-03 2022-10-11 中国计量大学 An electric device for air intake control of an oscillating balance method dust concentration measuring instrument
CN117871314A (en) * 2024-01-30 2024-04-12 中汽研汽车检验中心(武汉)有限公司 Method for weighing particulate matter sampling filter paper in automobile emission test

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GB927271A (en) * 1958-09-16 1963-05-29 Coal Industry Patents Ltd Improvements in or relating to sampling apparatus
US5571945A (en) * 1995-03-13 1996-11-05 Koutrakis; Petros Method and apparatus to measure particulate matter in gas
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114486404A (en) * 2022-01-29 2022-05-13 江苏省环境监测中心 Constant-speed sampling method for directly measuring waste gas particulate matters of fixed pollution source
CN114486404B (en) * 2022-01-29 2023-11-24 江苏省环境监测中心 Constant-speed sampling method for directly measuring fixed pollution source exhaust gas particulate matters
CN115165694A (en) * 2022-08-03 2022-10-11 中国计量大学 An electric device for air intake control of an oscillating balance method dust concentration measuring instrument
CN117871314A (en) * 2024-01-30 2024-04-12 中汽研汽车检验中心(武汉)有限公司 Method for weighing particulate matter sampling filter paper in automobile emission test

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