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CN107102019A - Without magnetic imbibition device - Google Patents

Without magnetic imbibition device Download PDF

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Publication number
CN107102019A
CN107102019A CN201610099076.3A CN201610099076A CN107102019A CN 107102019 A CN107102019 A CN 107102019A CN 201610099076 A CN201610099076 A CN 201610099076A CN 107102019 A CN107102019 A CN 107102019A
Authority
CN
China
Prior art keywords
hole
rock core
lining
plug
cylinder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610099076.3A
Other languages
Chinese (zh)
Inventor
王海涛
伦增珉
吕成远
潘伟义
郎东江
骆铭
赵淑霞
王友启
赵春鹏
刘玄
龚凯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Petroleum and Chemical Corp
Sinopec Exploration and Production Research Institute
Original Assignee
China Petroleum and Chemical Corp
Sinopec Exploration and Production Research Institute
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Petroleum and Chemical Corp, Sinopec Exploration and Production Research Institute filed Critical China Petroleum and Chemical Corp
Priority to CN201610099076.3A priority Critical patent/CN107102019A/en
Publication of CN107102019A publication Critical patent/CN107102019A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N24/00Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects
    • G01N24/08Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects by using nuclear magnetic resonance
    • G01N24/081Making measurements of geologic samples, e.g. measurements of moisture, pH, porosity, permeability, tortuosity or viscosity

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  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Pressure Vessels And Lids Thereof (AREA)

Abstract

One kind without magnetic imbibition device, including:Cylinder (6);Lining (5), lining (5) is arranged in cylinder (6), the outer surface of lining (5) and the inner surface of cylinder (6) are cooperated by screw thread, and lining (5) is internally formed imbibition room (7);Rock core plug (4), rock core plug is arranged on the two ends of lining (5), rock core plug and is provided with the first hole;Plug (3), plug (3) is arranged on the outside of rock core plug (4), the second hole and conduction oil outlet (2) are provided with plug (3), second hole is coaxial and interconnected with the first hole, and conduction oil outlet (2) is communicated to rock core plug (4), lining (5) and the space of cylinder (6) formation;And lengthening joint (1), lengthening joint (1) is through the 3rd hole is provided with the second hole and the first hole, and lengthening joint (1), and the 3rd hole and first hole are coaxial and interconnected.

Description

Without magnetic imbibition device
Technical field
The present invention relates to oil-gas field development field, more particularly to it is a kind of be resistant to HTHP without magnetic imbibition Device.
Background technology
Imbibition is the process of spontaneous suction certain wetting fluid of porous media under static conditions, and its driving force is Capillary force.Evaluating imbibition effect needs specific experimental provision, and the device be able to will be carried to fluid and rock core For the space of static state interaction, and imbibition device must possess the survey for characterizing fluid content change in rock core Measure function.Existing imbibition experimental provision is atmospheric unit, and operating pressure is atmospheric pressure.Reservoir Development mistake Journey is HTHP process, and the fluid of injection is acted on reservoir fluid under high pressure.For researching high-temperature high pressure Under the conditions of imbibition act on, it is necessary to design HTHP imbibition experimental provision.Fluid and rock can be provided While static state interaction confined space, the device allows for proof pressure and temperature, and simulation high temperature is high Pressure ring border.Simultaneously the device also can in quantitatively characterizing rock core fluid content change.
Application of the nuclear magnetic resonance technique in petroleum exploration and development, which is concentrated mainly on reservoir structure, to be researched and analysed and comments In valency, Reservoir rocks in terms of fluid distrbution feature, seepage flow mechanism research.Utilize nuclear magnetic resonance technique energy Reach the change of fluid content in rock core under quantitatively characterizing different condition.
To carry out imbibition experiment under high temperature, condition of high voltage using nuclear magnetic resonance technique, it must just develop and set Count the nuclear-magnetism imbibition experimental provision studied dedicated for oil-gas field development.The device must be without nuclear magnetic signal, together When with the airtight cavity for being resistant to HTHP, the cavity can place outside rock core, and rock core according to So there is free space, the space can be filled with fluid, and with rock core imbibition work occurs in airtight cavity for fluid With.The influence to fluid content in rock core is acted on using the imbibition of nuclear magnetic resonance technique quantitatively characterizing, is evaluated with this Imbibition action rule.
Rock core nuclear magnetic resonance experiment is that the rock core containing oil, water and gas is put into magnetostatic field radio-frequency coil, There can not be metal material encirclement around rock core, otherwise metal material can shield transmitting and excite rock core nuclear magnetic resonance letter Number RF pulses.Other any material containing ferromagnetic material can not be put into magnetostatic field.
Patent CN102062742B discloses a kind of sand-filling type clamp fastener for nuclear magnetic resonance imaging, and it designs pressure Power is 0-15MPa, and design temperature is 0-70 DEG C, can carry out multi-phase multi-component fluid seepage flow in simulation core With the in-house laboratory investigation of transport property, its part uses polyamide-imides material.Two of the patent Cavity filling porous media between end socket and interior body, installs end cap seal.It must be filled with its cavity porous Medium is to support two end sockets, and otherwise two plugs will depart from initial position in injection flow liquid process, difficult To form seal cavity.Therefore the structure can not be provided while accommodating the sky of fluid and rock core at high temperature under high pressure Between.In addition, the material that the patent is used is polyamide-imides, it is difficult to withstand greater than 15MPa pressure.
Patent CN102507626A discloses a kind of compatible rock core of nuclear magnetic resonance and accommodates device, can be on simulation ground Rock core is carried out under the conditions of layer to carry out nuclear magnetic resonance on-line measurement while oil-water displacement.It uses the non-gold of no magnetic Belong to material polyimides, and radio-frequency coil is embedded into core holding unit.Its entirety is still clamper knot Structure:The outside cylinder with pressure-bearing, inside has the polytetrafluoroethylene (PTFE) gum cover of parcel rock core, and it is non-pressure Material is, it is necessary to press the stream pressure in the pressure balance gum cover of fluid by ring, and then carry out displacement test, this knot Structure is difficult to the airtight cavity to form tolerance HTHP.
Patent CN104020098A discloses imbibition under a kind of high-temperature and high-pressure conditions and dynamically determines device, and it is adopted HTHP kettle is stainless steel, and is continuously measured using weighing method and be immersed in high temperature and high pressure flow Internal rock core, obtains the imbibition rule of rock core, and the stainless steel kettle that the patent is provided is difficult to meet nuclear-magnetism and is total to The requirement of vibration analysis.
Existing literature, which has no, can carry out the device of high-temperature and high-pressure conditions nuclear magnetic resonance imbibition experiment.
The content of the invention
The purpose of the disclosure is to provide one kind without magnetic imbibition experimental provision, with reference to nuclear magnetic resonance technique and the experiment Device can carry out nuclear magnetic resonance imbibition experiment, evaluate the imbibition effect of fluid and rock under high-temperature and high-pressure conditions.
The disclosure uses solution below:
One kind without magnetic imbibition device, including:
Cylinder;
Lining, the lining is arranged in the cylinder, the outer surface of the lining and the interior table of the cylinder Face is cooperated by screw thread, and the lining is internally formed imbibition room;
A pair of rock core plugs, the pair of rock core plug is arranged at the two ends of the lining, the rock core plug On be provided with the first hole;
A pair of plugs, the plug is arranged on the outside of the rock core plug, and the second hole is provided with the plug And conduction oil outlet, second hole and first hole be coaxial and interconnected, and the conduction oil outlet connects Pass to the rock core plug, the lining and the space of cylinder formation;And
A pair of lengthening joints, the lengthening joint passes through second hole and the first hole, and the lengthening joint On be provided with the 3rd hole, the 3rd hole and first hole are coaxial and interconnected.
Preferably, the diameter in second hole is more than the external diameter of the lengthening joint.
Preferably, it is provided with sealing ring between the lining and the rock core plug.
Preferably, the rock core plug is included under the step-like structure of enlarged-diameter, the step-like structure The outer face of lining described in the clamping of surface.
Preferably, the outer surface of the plug and the inner surface of the cylinder are cooperated by screw thread.
Preferably, it is provided with sealing ring between the plug and the cylinder.
Preferably, cooperated between the lengthening joint and first hole by screw thread.
Preferably, it is provided with sealing ring between the lengthening joint and first hole.
Preferably, the lining has smooth inner surface.
Preferably, the cylinder is made up of fiberglass, the lengthening joint, plug, rock core plug and lining It is made by polyether-ether-ketone.
Compared with prior art, the disclosure without magnetic imbibition device by rock core plug and lining constitutes imbibition room, Rock core is placed in it, rock core surrounding is full of fluid, imbibition experiment is carried out with this.Cylinder without magnetic imbibition device Using non-magnetic material fiberglass, remaining part uses non-magnetic material polyether-ether-ketone, can bear HTHP Working environment.
Brief description of the drawings
By the way that disclosure exemplary embodiment is described in more detail with reference to accompanying drawing, the disclosure it is above-mentioned with And other purposes, feature and advantage will be apparent, wherein, in disclosure exemplary embodiment mode In, identical reference number typically represents same parts.
Fig. 1 shows the sectional view without magnetic imbibition device according to exemplary embodiment;
Fig. 2 shows A-A ' cross-sectional views in Fig. 1.
Main Reference Numerals explanation:
1- lengthening joints;2- conduction oil outlets;3- plugs;4- rock core plugs;5- linings;6- cylinders;7- imbibitions Room;8- conduction oil passages.
Embodiment
Preferred embodiment of the present disclosure is more fully described below with reference to accompanying drawings.Although showing this in accompanying drawing Disclosed preferred embodiment, however, it is to be appreciated that may be realized in various forms the disclosure without should be by here The embodiment of elaboration is limited.On the contrary, these embodiments are provided so that the disclosure is more thorough and complete, And the scope of the present disclosure can intactly be conveyed to those skilled in the art.
Included according to exemplary embodiment without magnetic imbibition device:
Cylinder;
Lining, lining is arranged in cylinder, and the outer surface of lining passes through screw thread phase interworking with the inner surface of cylinder Close, lining is internally formed imbibition room;
A pair of rock core plugs, a pair of rock core plugs are arranged on the two ends of lining, rock core plug and are provided with first Hole;
A pair of plugs, plug is arranged on the outside of rock core plug, and the second hole and conduction oil outlet are provided with plug, Second hole is coaxial and interconnected with the first hole, and conduction oil outlet is communicated to rock core plug, lining and cylinder-shaped Into space;And
A pair of lengthening joints, lengthening joint passes through the second hole and the first hole, and the 3rd is provided with lengthening joint Hole, the 3rd hole and the first hole are coaxial and interconnected.
In use, rock core is placed in imbibition room.The first hole on rock core plug and the 3rd hole on lengthening joint It is interconnected, so that high-pressure fluid can be entered by the 3rd hole on lengthening joint, the first hole on rock core plug Infiltrate in suction-chamber.Conduction oil outlet is communicated to the space of rock core plug, lining and cylinder formation, so that heat conduction Oil can enter screw thread between lining and cylinder by conduction oil outlet, screw thread as conduction oil passage so that Imbibition room in the recyclable heating lining of conduction oil, and then heat the rock core in imbibition room.
Preferably, the diameter in the second hole less times greater than lengthening joint external diameter so that lengthening joint with It is interference fit between hole, prevents high pressure fluid leak.
Preferably, sealing ring is provided between lining and rock core plug, such as it is corrosion resistant O-shaped close Seal, to seal the high-pressure fluid in lining, prevents high-pressure fluid from revealing.
Preferably, rock core plug includes the step-like structure of enlarged-diameter, the following table of step-like structure It is capable of the outer face of clamping lining in face.
Preferably, the outer surface of plug and the inner surface of cylinder are cooperated by screw thread, and plug Sealing ring, such as O-ring seal are provided between cylinder, to prevent conduction oil from leaking.
Preferably, cooperated between lengthening joint and the first hole by screw thread, and lengthening joint with Sealing ring, such as O-ring seal are provided between first hole, to seal between lengthening joint and rock core plug Space, prevent high pressure fluid leak.
Preferably, lining has smooth inner surface.
Preferably, cylinder is made up of fiberglass, and lengthening joint, plug, rock core plug and lining are equal It is made up of polyether-ether-ketone.The maximum working pressure that can be born is 30MPa, and maximum operating temperature is 80 DEG C.
Specific step that imbibition experiment is carried out without magnetic imbibition device described further below using exemplary embodiment Suddenly:
(1) the rock core plug of side is loaded in lining, rock core plug clamping lining outer face;
(2) the side lengthening joint is threadedly coupled with rock core plug;
(3) circular hole of the side plug is passed through into lengthening joint, and by being threaded into before cylinder, plug The tight rock core plug outer face of side pressure;
(4) rock core is loaded into imbibition room from the opposite side of lining;
(5) the rock core plug of the opposite side is loaded in lining, rock core plug clamping lining outer face;
(6) lengthening joint of the opposite side is threadedly coupled with rock core plug;
(7) circular hole of the opposite side plug is passed through into lengthening joint, by being threaded into cylinder, and plug Front end compress rock core plug outer face;
(8) using circulating pump conduction oil is cyclically injected from the conduction oil outlet of side, from opposite side Conduction oil outlet flows out, heating a period of time (such as 48 hours), it is ensured that the core temperature in imbibition room reaches To design temperature.
(9) high-pressure fluid is injected from the circular hole of the lengthening joint of the side, high-pressure fluid is by rock core plug Circular hole enters imbibition room, imbibition room is pressurizeed using high-pressure fluid, until reaching setting pressure.
(10) NMR relaxation spectrum and imaging analysis are carried out.
Below with reference to the accompanying drawings it is described in detail according to exemplary embodiment without magnetic imbibition device.Such as Fig. 1 and 2 institutes Show, included according to exemplary embodiment without magnetic imbibition device:Cylinder 6, lining 5, a pair of rock core plugs 4, A pair of plugs 3 and a pair of lengthening joints 1.
Lining 5 is arranged in cylinder 6, and the outer surface of lining 5 and the inner surface of cylinder 6 are mutual by screw thread Coordinate, screw thread formation conduction oil passage 8.Lining 5 has smooth inner surface, and it is internally formed imbibition room 7. A pair of rock core plugs are respectively arranged on the two ends of lining 5, rock core plug and are provided with the first hole.Plug 3 is set It is placed on the outside of rock core plug 4, plug 3 and is provided with the second hole and conduction oil outlet 2, the second hole and the first hole Coaxial and interconnected, conduction oil outlet 2 is communicated to rock core plug 4, lining 5 and the space of the formation of cylinder 6. Lengthening joint 1 is through being provided with the 3rd hole on the second hole and the first hole, and lengthening joint 1, the 3rd hole and the One hole is coaxial and interconnected.
The diameter in the second hole of plug 3 is slightly larger than the external diameter of lengthening joint 1, is therebetween interference fit. Between plug 3 and cylinder 6, it is mutual by screw thread between the first hole of lengthening joint 1 and rock core plug 4 Coordinate.And between lining 5 and rock core plug 4, between plug 3 and cylinder 6 and lengthening joint 1 O-ring seal is provided between the first hole, with prevent leakage.
Rock core plug 4 includes the step-like structure of enlarged-diameter, after installing, the following table of step-like structure The outer face of face clamping lining 5.In addition, after plug 3 is completely screwed into cylinder, the end face of plug 3 It is in close contact with the end face of rock core plug 4, it is ensured that rock core plug 4 is by the pressure transmission of fluid to plug 3.
Cylinder 6 is made up of fiberglass, and lengthening joint 1, plug 3, rock core plug 4 and lining 5 are by polyethers Ether ketone is made.
Above-mentioned technical proposal is a kind of embodiment of the present invention, for those skilled in the art, On the basis of the invention discloses application process and principle, it is easy to make various types of improvement or deformation, The method described by above-mentioned specific embodiment of the invention is not limited solely to, therefore previously described mode is excellent Choosing, and not restrictive meaning.

Claims (10)

1. one kind is without magnetic imbibition device, including:
Cylinder (6);
Lining (5), the lining (5) is arranged in the cylinder (6), the appearance of the lining (5) The inner surface in face and the cylinder (6) is cooperated by screw thread, and the lining (5) is internally formed imbibition Room (7);
A pair of rock core plugs (4), the pair of rock core plug is arranged at the two ends of the lining (5), described The first hole is provided with rock core plug;
A pair of plugs (3), the plug (3) is arranged on the outside of the rock core plug (4), the plug (3) the second hole and conduction oil outlet (2) are provided with, second hole is coaxial and mutual with first hole Connection, the conduction oil outlet (2) be communicated to the rock core plug (4), the lining (5) with it is described The space of cylinder (6) formation;And
A pair of lengthening joints (1), the lengthening joint (1) passes through second hole and the first hole, and described The 3rd hole is provided with lengthening joint (1), the 3rd hole and first hole are coaxial and interconnected.
2. it is according to claim 1 without magnetic imbibition device, wherein the diameter in second hole is more than described The external diameter of lengthening joint (1).
3. it is according to claim 1 without magnetic imbibition device, wherein the lining (5) and the rock core Plug is provided with sealing ring between (4).
4. it is according to claim 1 without magnetic imbibition device, wherein the rock core plug (4) is included directly The step-like structure that footpath expands, the outer face of lining (5) described in the lower surface clamping of the step-like structure.
5. according to claim 1 without magnetic imbibition device, wherein the outer surface of the plug (3) with The inner surface of the cylinder (6) is cooperated by screw thread.
6. it is according to claim 5 without magnetic imbibition device, wherein the plug (3) and the cylinder (6) sealing ring is provided between.
7. according to claim 1 without magnetic imbibition device, wherein the lengthening joint (1) with it is described Cooperated between first hole by screw thread.
8. according to claim 7 without magnetic imbibition device, wherein the lengthening joint (1) with it is described Sealing ring is provided between first hole.
9. it is according to claim 1 without magnetic imbibition device, wherein the lining (5) is with smooth Inner surface.
10. it is according to claim 1 without magnetic imbibition device, wherein the cylinder (6) is by glass steel Into the lengthening joint (1), plug (3), rock core plug (4) and lining (5) are by polyether-ether-ketone It is made.
CN201610099076.3A 2016-02-23 2016-02-23 Without magnetic imbibition device Pending CN107102019A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610099076.3A CN107102019A (en) 2016-02-23 2016-02-23 Without magnetic imbibition device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610099076.3A CN107102019A (en) 2016-02-23 2016-02-23 Without magnetic imbibition device

Publications (1)

Publication Number Publication Date
CN107102019A true CN107102019A (en) 2017-08-29

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610099076.3A Pending CN107102019A (en) 2016-02-23 2016-02-23 Without magnetic imbibition device

Country Status (1)

Country Link
CN (1) CN107102019A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108801870A (en) * 2018-03-26 2018-11-13 中国石油大学(北京) It is a kind of can under simulation stratum condition reservoir rock imbibition experimental provision and method
CN114252378A (en) * 2020-09-24 2022-03-29 青岛石大华通科技有限公司 High-temperature and high-pressure clamp holder and using method thereof

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US20110050223A1 (en) * 2009-08-31 2011-03-03 University Of New Brunswick Magnetic resonance apparatus and method
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WO2013171544A1 (en) * 2012-05-15 2013-11-21 Schlumberger Canada Limited Nmr analysis of a core sample employing an open permanent magnet removable from a core holder
WO2014186154A1 (en) * 2013-05-14 2014-11-20 Chevron U.S.A. Inc. Formation core sample holder assembly and testing method for nuclear magnetic resonance measurements
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CN105277582A (en) * 2015-10-22 2016-01-27 成都岩心科技有限公司 Special core holder for nuclear magnetic resonance

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Publication number Priority date Publication date Assignee Title
US20110050223A1 (en) * 2009-08-31 2011-03-03 University Of New Brunswick Magnetic resonance apparatus and method
CN102288629A (en) * 2011-07-01 2011-12-21 中联煤层气国家工程研究中心有限责任公司 Core holder
WO2013171544A1 (en) * 2012-05-15 2013-11-21 Schlumberger Canada Limited Nmr analysis of a core sample employing an open permanent magnet removable from a core holder
WO2014186154A1 (en) * 2013-05-14 2014-11-20 Chevron U.S.A. Inc. Formation core sample holder assembly and testing method for nuclear magnetic resonance measurements
CN104897711A (en) * 2014-03-03 2015-09-09 中国石油化工股份有限公司 Core holder
WO2015142531A1 (en) * 2014-03-21 2015-09-24 Daedalus Innovations Llc Core sample holder
CN105277582A (en) * 2015-10-22 2016-01-27 成都岩心科技有限公司 Special core holder for nuclear magnetic resonance

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Title
蒙冕模 等: "基于核磁共振技术研究页岩自发渗吸过程", 《特种油气藏》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108801870A (en) * 2018-03-26 2018-11-13 中国石油大学(北京) It is a kind of can under simulation stratum condition reservoir rock imbibition experimental provision and method
CN114252378A (en) * 2020-09-24 2022-03-29 青岛石大华通科技有限公司 High-temperature and high-pressure clamp holder and using method thereof

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Application publication date: 20170829