CN107050905A - A kind of intelligent distillation still - Google Patents
A kind of intelligent distillation still Download PDFInfo
- Publication number
- CN107050905A CN107050905A CN201710478741.4A CN201710478741A CN107050905A CN 107050905 A CN107050905 A CN 107050905A CN 201710478741 A CN201710478741 A CN 201710478741A CN 107050905 A CN107050905 A CN 107050905A
- Authority
- CN
- China
- Prior art keywords
- kettle
- submerged pump
- steam
- distillation still
- inwall
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004821 distillation Methods 0.000 title claims abstract description 25
- 238000007599 discharging Methods 0.000 claims abstract description 11
- 239000013536 elastomeric material Substances 0.000 claims abstract description 8
- 239000000945 filler Substances 0.000 claims abstract description 6
- 239000000463 material Substances 0.000 abstract description 17
- 238000010438 heat treatment Methods 0.000 abstract description 9
- 238000004939 coking Methods 0.000 abstract description 6
- 238000003756 stirring Methods 0.000 abstract description 6
- 238000009835 boiling Methods 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 239000012535 impurity Substances 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/02—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in boilers or stills
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a kind of intelligent distillation still, including kettle, kettle cover, agitating shaft, motor I and steam comb, kettle has kettle inwall and kettle outer wall, elastomeric material is provided between kettle inwall and kettle outer wall, the temperature sensor and pressure sensor electrically connected with control device are installed on kettle inwall, the electrically heated rod extended laterally is symmetrical arranged on agitating shaft, filler is provided with steam comb, one end of steam comb is connected with steam (vapor) outlet, the other end of steam comb is sequentially connected condenser and collecting tank, submerged pump is additionally provided with kettle, the outlet of submerged pump faces discharging opening, submerged pump is connected with motor II.The present invention is carried out simultaneously using electrically heated rod as stirring rod, stirring and heating, and material is heated evenly, and effectively prevent material coking；There is provided submerged pump, submerged pump quickly can transfer out the decorating film or high boiler material of distillation still bottom from discharging opening, the efficiency of distillation is improved.
Description
Technical field
The present invention relates to a kind of intelligent distillation still, belong to fine chemistry industry apparatus field.
Background technology
Distillation still is the difference according to cut boiling point, is vaporized desired cut by heating, then is collected by condensing, and
Decorating film or high boiling material will be deposited in the bottom of distillation still in material, finally be discharged from material outlet.
Existing distillation still is generally by the way of surrounding heating or bottom-heated, and heating is uneven, causes some things
The easy coking of matter, is collected at bottom or four walls of reactor after coking.In addition, can overstock a certain amount of in distillation still bottom
Decorating film or high boiler material, take the inner space of distillation still, cause the device space to waste, can influence heat transfer efficiency, waste
The energy, influences distillation speed.
The content of the invention
It is an object of the invention to provide a kind of intelligent distillation still, homogeneous heating can be prevented effectively from coking material and gather, and energy
Quick decorating film or high boiler material by distillation still bottom is discharged from material outlet.
To achieve the above object, a kind of intelligent distillation still of the invention, including kettle, be arranged at the top of kettle kettle cover,
The agitating shaft being arranged in kettle, the motor I and steam comb that are arranged on the outside of kettle, the kettle cover are provided with charging aperture and steaming
Vapor outlet, the autoclave body bottom is provided with discharging opening, and the upper end of the agitating shaft is extended on the outside of kettle, the output shaft with motor I
Drive connection,
The kettle has kettle inwall and kettle outer wall, and elastomeric material is provided between the kettle inwall and kettle outer wall, described
The temperature sensor and pressure sensor electrically connected with control device are installed on kettle inwall,
The electrically heated rod extended laterally is symmetrical arranged on the agitating shaft,
Filler is provided with the steam comb, one end of the steam comb is connected with steam (vapor) outlet, the steam comb
The other end be sequentially connected condenser and collecting tank,
Submerged pump is additionally provided with the kettle, the outlet of the submerged pump faces discharging opening, and submerged pump is with being arranged on kettle
The output shaft drive connection of the motor II of external side.
It is preferred that, the elastomeric material is rubber.
Further, it is additionally provided with observation window on the kettle cover.
Further, the autoclave body bottom is additionally provided with the support for supporting kettle.
The beneficial effects of the invention are as follows：
(1) present invention is carried out simultaneously using electrically heated rod as stirring rod, stirring and heating, and material is heated evenly, effectively
Avoid and heat the unfavorable factors such as uneven, material coking caused by same position heating；
(2) present invention be provided with submerged pump, submerged pump can quickly by the decorating film or high boiler material of distillation still bottom from
Discharging opening is transferred out, and improves the efficiency of distillation；
(3) filler is set in steam comb, the solvent being evaporated need to first pass through packing layer, extends gas and flow through road
Footpath, wherein high-boiling-point impurity will be condensed out, and the low boiling point solvent purity collected is then higher；
(4) observation window is provided with kettle cover of the invention, is easy to observe the reaction condition in kettle.
Brief description of the drawings
Fig. 1 is structural representation of the invention；
Fig. 2 is the structural representation of kettle in Fig. 1；
In figure, 1, kettle, 1-1, kettle inwall, 1-2, kettle outer wall, 1-3, elastomeric material, 2, kettle cover, 3, agitating shaft, 4, motor
I, 5, charging aperture, 6, discharging opening, 7, steam (vapor) outlet, 8, steam comb, 9, electrically heated rod, 10, filler, 11, condenser, 12, receive
Collect tank, 13, submerged pump, 14, motor II, 15, control device, 16, temperature sensor, 17, pressure sensor, 18, support.
Embodiment
The present invention is described in further detail with specific embodiment below in conjunction with the accompanying drawings.
As depicted in figs. 1 and 2, a kind of intelligent distillation still of the invention, including kettle 1, the kettle cover for being arranged on the top of kettle 1
2nd, the agitating shaft 3 that is arranged in kettle 1, the motor I 4 and steam comb 8 for being arranged on the outside of kettle 1, the kettle cover 2 be provided with into
Material mouth 5 and steam (vapor) outlet 7, the bottom of kettle 1 are provided with discharging opening 6, and the upper end of the agitating shaft 3 extends to the outside of kettle 1, with
The output shaft drive connection of motor I 4,
The kettle 1 has kettle inwall 1-1 and kettle outer wall 1-2, is provided between the kettle inwall 1-1 and kettle outer wall 1-2
Elastomeric material 1-3；It is preferred that, the elastomeric material 1-3 is rubber, can prevent that distillation temperature in the kettle, pressure are excessive to kettle 1
Cause damage, extend the service life of kettle 1；
The temperature sensor 16 and pressure sensor 17 electrically connected with control device 15 is installed on the kettle inwall 1-1,
Temperature sensor 16 and pressure sensor 17 are controlled using control device 15, can be cleverer to temperature in the kettle and pressure operation
It is quick；
The electrically heated rod 9 extended laterally is symmetrical arranged on the agitating shaft 3, stirring rod, stirring are used as using electrically heated rod 9
Carried out simultaneously with heating, so that material is heated evenly, effectively prevent and heat uneven, material caused by same position heating
The unfavorable factors such as coking；
Filler 10 is provided with the steam comb 8, one end of the steam comb 8 is connected with steam (vapor) outlet 7, the steam
The other end of comb 8 is sequentially connected condenser 11 and collecting tank 12, and the solvent being evaporated need to first pass through packing layer, extend gas
Body flows through path, and wherein high-boiling-point impurity will be condensed out, and the low boiling point solvent purity collected is then higher；
Be additionally provided with submerged pump 13 in the kettle 1, the outlet of the submerged pump 13 faces discharging opening 6, submerged pump 13 with
The output shaft drive connection of the motor II 14 in the outside of kettle 1 is arranged on, submerged pump 13 can be quickly by the decorating film of distillation still bottom
Or high boiler material is transferred out from discharging opening, the efficiency of distillation is improved.
Preferably, observation window (not shown) is additionally provided with the kettle cover 2, is easy to staff to observe kettle
Interior reaction condition.
Preferably, the bottom of kettle 1 is additionally provided with the support 18 for supporting kettle 1, is easy to consolidating for kettle 1
It is fixed.
Claims (4)
1. a kind of intelligent distillation still, including kettle (1), be arranged at the top of kettle (1) kettle cover (2), be arranged in kettle (1)
Agitating shaft (3), the motor I (4) being arranged on the outside of kettle (1) and steam comb (8), the kettle cover (2) are provided with charging aperture (5)
With steam (vapor) outlet (7), kettle (1) bottom is provided with discharging opening (6), and the upper end of the agitating shaft (3) extends to kettle (1) outside
Side, is connected with the output shaft of motor I (4), it is characterised in that
The kettle (1) has kettle inwall (1-1) and kettle outer wall (1-2), the kettle inwall (1-1) and kettle outer wall (1-2) it
Between be provided with elastomeric material (1-3), the temperature sensor electrically connected with control device (15) is installed on the kettle inwall (1-1)
(16) and pressure sensor (17),
The electrically heated rod (9) extended laterally is symmetrical arranged on the agitating shaft (3),
Filler (10) is provided with the steam comb (8), one end of the steam comb (8) is connected with steam (vapor) outlet (7), described
The other end of steam comb (8) is sequentially connected condenser (11) and collecting tank (12),
Submerged pump (13) is additionally provided with the kettle (1), the outlet of the submerged pump (13) faces discharging opening (6), submerged pump
(13) output shaft of the motor II (14) with being arranged on the outside of kettle (1) is connected.
2. intelligent distillation still according to claim 1, it is characterised in that the elastomeric material (1-3) is rubber.
3. intelligent distillation still according to claim 1 or 2, it is characterised in that be additionally provided with observation window on the kettle cover (2).
4. intelligent distillation still according to claim 1 or 2, it is characterised in that kettle (1) bottom is additionally provided with for branch
Support the support (18) of kettle (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710478741.4A CN107050905A (en) | 2017-06-22 | 2017-06-22 | A kind of intelligent distillation still |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710478741.4A CN107050905A (en) | 2017-06-22 | 2017-06-22 | A kind of intelligent distillation still |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107050905A true CN107050905A (en) | 2017-08-18 |
Family
ID=59595720
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710478741.4A Pending CN107050905A (en) | 2017-06-22 | 2017-06-22 | A kind of intelligent distillation still |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107050905A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107308673A (en) * | 2017-08-21 | 2017-11-03 | 荆门市帅邦化学科技有限公司 | A kind of distillation type reactor |
| CN112933632A (en) * | 2019-12-11 | 2021-06-11 | 江苏民生特种设备集团有限公司 | High efficiency distillation column cauldron |
| CN115253576A (en) * | 2022-08-05 | 2022-11-01 | 章福涛 | An oil mist filter for waste gas treatment |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110073460A1 (en) * | 2009-09-25 | 2011-03-31 | Institute Of Nuclear Energy Research Atomic Energy Council, Executive Yuan | Wastewater treatment apparatus and method with stair-like heat treatment tanks |
| CN204522340U (en) * | 2015-03-19 | 2015-08-05 | 江西盛伟实业有限公司 | A kind of novel distillation still |
| CN204767503U (en) * | 2015-07-03 | 2015-11-18 | 宁波大学 | Stills for chemical industry |
| CN206103387U (en) * | 2016-08-30 | 2017-04-19 | 南京巴诗克化工有限公司 | Distilling device |
-
2017
- 2017-06-22 CN CN201710478741.4A patent/CN107050905A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110073460A1 (en) * | 2009-09-25 | 2011-03-31 | Institute Of Nuclear Energy Research Atomic Energy Council, Executive Yuan | Wastewater treatment apparatus and method with stair-like heat treatment tanks |
| CN204522340U (en) * | 2015-03-19 | 2015-08-05 | 江西盛伟实业有限公司 | A kind of novel distillation still |
| CN204767503U (en) * | 2015-07-03 | 2015-11-18 | 宁波大学 | Stills for chemical industry |
| CN206103387U (en) * | 2016-08-30 | 2017-04-19 | 南京巴诗克化工有限公司 | Distilling device |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107308673A (en) * | 2017-08-21 | 2017-11-03 | 荆门市帅邦化学科技有限公司 | A kind of distillation type reactor |
| CN112933632A (en) * | 2019-12-11 | 2021-06-11 | 江苏民生特种设备集团有限公司 | High efficiency distillation column cauldron |
| CN115253576A (en) * | 2022-08-05 | 2022-11-01 | 章福涛 | An oil mist filter for waste gas treatment |
| CN115253576B (en) * | 2022-08-05 | 2025-01-10 | 营口永力环保设备有限公司 | Oil mist filter for exhaust gas treatment |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104606909B (en) | One kind of plant Oleum sesami boiler | |
| CN107050905A (en) | A kind of intelligent distillation still | |
| CN205035347U (en) | Cinnamon essential oil boiling bulb | |
| CN202359093U (en) | Plant essential oil extraction device | |
| CN110038321A (en) | A kind of traditional Chinese medicine extraction device | |
| CN110478929A (en) | A kind of biomolecule distilling apparatus | |
| CN211097589U (en) | Convenient 3000L's of collecting stills | |
| CN116692984A (en) | Rare earth wastewater treatment system | |
| CN209848342U (en) | Rosin continuous distillation system | |
| CN210506261U (en) | High-efficient fish oil distillation plant | |
| CN221889200U (en) | Distillation device based on extraction and preparation of fucoxanthin from seaweed | |
| CN220597094U (en) | Silane treatment fluid waste liquid recovery unit | |
| CN208829602U (en) | Petroleum distillation device | |
| CN206853155U (en) | A kind of ethyl acetate reclaimer | |
| CN207405145U (en) | One kind continuously evaporates wine machine | |
| CN212308897U (en) | Integrated molecular distillation structure | |
| CN107320989B (en) | Cosmetics production facility | |
| CN210384863U (en) | Liquid phase organic matter dewatering device | |
| CN207446249U (en) | It is a kind of to pass through the production of resins of automatic water distributor and condenser control water reaction kettle device | |
| CN108434772A (en) | A kind of novel retort device | |
| CN205204846U (en) | Aluminium trichloride trap | |
| CN210905085U (en) | Waste oil refining and separating system | |
| CN206720777U (en) | Sewage-treatment plant with centrifugation Pistonless compressor | |
| CN206809815U (en) | A kind of efficient distillation still | |
| CN220276330U (en) | Fragrance material extraction equipment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170818 |
|
| RJ01 | Rejection of invention patent application after publication |