CN106990010A - Liquid erosion test device in a kind of many reference amounts regulation and control pipeline - Google Patents
Liquid erosion test device in a kind of many reference amounts regulation and control pipeline Download PDFInfo
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Abstract
Description
技术领域technical field
本发明属于材料腐蚀研究技术领域,特别是涉及一种可控温、可控PH值、可调节流量的多参量调控管道内液体冲蚀试验装置。The invention belongs to the technical field of material corrosion research, and in particular relates to a temperature-controllable, pH-value-controllable and flow-adjustable multi-parameter regulating liquid erosion test device in a pipeline.
背景技术Background technique
管道输送流体具有安全性高、便捷、成本低等优点,是目前应用最为广泛的流体输送方式。现如今,世界各国对能源的需求日益增加,管道运输业的发展十分迅速,现已形成了许多规模庞大的大型输油管道网和供气系统。但是由于运输管道大多数埋于地下,会受到土壤、地下水等外部因素和内部的运输流体的共同腐蚀作用,因此管道会发生渗漏,其使用寿命会大大降低,这不仅会造成严重的经济损失,还会带来环境污染问题。据中国工程院调查表明,2014年我国腐蚀总成本为21278.2亿元人民币,约占当年GDP的3.34%,相当于每个中国人当年承担1555元的腐蚀成本。管道腐蚀是世界各国共同面临的问题,涉及安全、经济和生态文明,已成为影响国民经济和社会可持续发展的重要因素之一。Pipeline transportation of fluid has the advantages of high safety, convenience, and low cost, and is currently the most widely used method of fluid transportation. Nowadays, countries all over the world have an increasing demand for energy, and the pipeline transportation industry has developed very rapidly, and many large-scale large-scale oil pipeline networks and gas supply systems have been formed. However, since most of the transportation pipelines are buried underground, they will be corroded by external factors such as soil and groundwater and the internal transportation fluid, so the pipeline will leak and its service life will be greatly reduced, which will not only cause serious economic losses , will also cause environmental pollution problems. According to the survey of the Chinese Academy of Engineering, the total cost of corrosion in my country in 2014 was 2,127.82 billion yuan, accounting for about 3.34% of GDP in that year, which is equivalent to the corrosion cost of 1,555 yuan for each Chinese person in that year. Pipeline corrosion is a common problem faced by all countries in the world, involving safety, economy and ecological civilization, and has become one of the important factors affecting the sustainable development of national economy and society.
随着管件应用环境的复杂化和多样化,管件往往承受内部流体腐蚀和外部载荷的复合作用,比如,在飞机的内部结构中,液压系统的液压管路与发动机内部的回油滑油管道内壁由于长期受到流动液体的冲蚀作用,管路内壁的结构会遭到侵蚀。同时,管道构件在飞机的飞行过程中发生振动,会受到动载荷的作用,从而形成在外力作用下的腐蚀裂纹扩展,最终导致管道的渗漏,因此,急需一种试样形状适用于后续力学测试的管道内冲蚀装置。With the complexity and diversification of the application environment of pipe fittings, pipe fittings often bear the combined effect of internal fluid corrosion and external loads. The structure of the inner wall of the pipeline will be eroded by the erosion of the flowing liquid for a long time. At the same time, the pipeline components vibrate during the flight of the aircraft and will be subjected to dynamic loads, thereby forming corrosion cracks under the action of external forces and eventually causing leakage of the pipeline. Therefore, there is an urgent need for a sample shape suitable for subsequent mechanics. Inline erosion device for testing.
目前虽然有关于腐蚀装置方面的研究,但一方面所用的腐蚀处理方法普遍为盐雾和浸泡,这两种方法都不能研究流动的液体对物体的冲刷腐蚀作用,在输油管道中,其内壁上附着的腐蚀产物会减缓管道内壁的腐蚀速率,但是由于管道内液体的流动作用,会带走部分腐蚀产物,从而加剧了管道内壁的腐蚀,所以流体流速对管道内壁腐蚀情况的研究就显得尤为重要。另一方面现有冲蚀研究和模拟的试样多为试片级,后续不适于进行相关的力学测试。Although there are currently researches on corrosion devices, on the one hand, the corrosion treatment methods used are generally salt spray and immersion. These two methods cannot study the erosion and corrosion effect of flowing liquid on objects. The corrosion products will slow down the corrosion rate of the inner wall of the pipeline, but due to the flow of the liquid in the pipeline, some corrosion products will be taken away, thereby intensifying the corrosion of the inner wall of the pipeline, so the research on the corrosion of the inner wall of the pipeline by the fluid flow rate is particularly important. On the other hand, most of the existing erosion research and simulation samples are at the test piece level, which is not suitable for subsequent related mechanical tests.
发明内容Contents of the invention
为了解决上述问题,本发明的目的在于提供一种多参量调控管道内液体冲蚀试验装置。In order to solve the above problems, the purpose of the present invention is to provide a multi-parameter control pipeline liquid erosion test device.
为了达到上述目的,本发明提供的多参量调控管道内液体冲蚀试验装置包括依次相连的PH值可控的腐蚀液供给模块a、腐蚀液流量可调节模块b、腐蚀温度可控模块c以及腐蚀液回流过滤模块d;所述的PH值可控的腐蚀液供给模块a包括盛有PH调节液的烧杯、蠕动泵、第一稳流阀、PH调控仪、恒温锅、盛有腐蚀液的烧杯、PH调控仪探针和第一管路,其中,盛有腐蚀液的烧杯放置在恒温锅中;第一管路的一端设置在盛有腐蚀液的烧杯中,另一端浸没在盛有PH调节液的烧杯内的PH调节液中;蠕动泵设置在第一管路上靠近盛有PH调节液的烧杯处;第一稳流阀设置在第一管路上靠近盛有腐蚀液的烧杯处;PH调控仪探针放置在盛有腐蚀液的烧杯内的腐蚀液中,且通过导线依次与PH调控仪以及蠕动泵电连接;In order to achieve the above object, the multi-parameter control pipeline liquid erosion test device provided by the present invention includes a corrosive solution supply module a with controllable pH value, a corrosive solution flow adjustable module b, a corrosive temperature controllable module c and a corrosive solution connected in sequence. Liquid backflow filter module d; the corrosive liquid supply module a with controllable pH value includes a beaker filled with pH regulating liquid, a peristaltic pump, a first steady flow valve, a pH regulator, a constant temperature pot, and a beaker filled with corrosive liquid , PH controller probe and the first pipeline, wherein, the beaker filled with corrosive liquid is placed in the constant temperature pot; in the PH regulating liquid in the beaker of the liquid; the peristaltic pump is set on the first pipeline close to the beaker containing the PH regulating liquid; the first steady flow valve is set on the first pipeline close to the beaker containing the corrosive liquid; the pH control The instrument probe is placed in the corrosive liquid in the beaker containing the corrosive liquid, and is electrically connected to the pH regulator and the peristaltic pump through wires in turn;
所述的腐蚀液流量可调节模块b包括若干组相互并联的腐蚀液流量调节系统,每组腐蚀液流量调节系统包括第二管路和依次设置在第二管路上的无级调节蠕动泵、第二稳流阀和流量计,并且第二管路上靠近无级调节蠕动泵的一端放置于盛有腐蚀液的烧杯内的腐蚀液中;The corrosive liquid flow adjustable module b includes several groups of corrosive liquid flow regulating systems connected in parallel, each group of corrosive liquid flow regulating systems includes a second pipeline and steplessly adjustable peristaltic pumps arranged sequentially on the second pipeline, the first Two steady flow valves and a flow meter, and one end of the second pipeline close to the stepless adjustment peristaltic pump is placed in the corrosive liquid in the beaker containing the corrosive liquid;
所述的腐蚀温度可控模块c包括若干个待腐蚀的管道试样、若干个温度控制仪探针、若干条第三管路和一个温度控制仪;每个管道试样的进液口连接在一组腐蚀液流量调节系统中第二管路的另一端,出液口与一条第三管路的一端相连;每个管道试样内设有一个温度控制仪探针;温度控制仪同时与若干个温度控制仪探针以及恒温锅电连接;The corrosion temperature controllable module c includes several pipeline samples to be corroded, several temperature controller probes, several third pipelines and a temperature controller; the liquid inlet of each pipeline sample is connected to The other end of the second pipeline in a group of corrosive liquid flow regulation systems, the liquid outlet is connected to one end of a third pipeline; each pipeline sample is equipped with a temperature controller probe; the temperature controller is connected to several A temperature controller probe and a constant temperature pot are electrically connected;
所述的腐蚀液回流过滤模块d包括第四管路和设置在第四管路上的至少一个过滤器;第四管路的一端设置在盛有腐蚀液的烧杯内,另一端连接若干条第三管路,并且管道试样的设置位置高于盛有腐蚀液的烧杯。The corrosive liquid return filter module d includes a fourth pipeline and at least one filter arranged on the fourth pipeline; one end of the fourth pipeline is set in a beaker filled with corrosive liquid, and the other end is connected to several third pipeline, and the location of the pipeline sample is higher than the beaker containing the corrosive solution.
所述的腐蚀液回流过滤模块d中过滤器的数量为若干个时,若干个过滤器采用串联方式设置在第四管路上。When the number of filters in the corrosive liquid return filter module d is several, the several filters are arranged in series on the fourth pipeline.
所述的管道试样采用透明材质,以便于试验人员观察管道试样内壁的腐蚀情况。The pipeline sample is made of transparent material so that the test personnel can observe the corrosion condition of the inner wall of the pipeline sample.
本发明提供的多参量调控管道内液体冲蚀试验装置结构简单,其腐蚀试样便于加工和更换,可实用性强,可以实现流动冲蚀这一功能,为研究管道内液体冲蚀提供更优的试验装置,便于后续对该试样的管内腐蚀情况及力学性能进行研究,适用于环保、材料腐蚀研究等技术领域。The multi-parameter control pipeline liquid erosion test device provided by the present invention has a simple structure, and its corrosion samples are easy to process and replace, and have strong practicability. The test device is convenient for subsequent research on the corrosion situation and mechanical properties of the sample in the pipe, and is suitable for environmental protection, material corrosion research and other technical fields.
附图说明Description of drawings
图1是本发明提供的多参量调控管道内液体冲蚀试验装置结构示意图。Fig. 1 is a schematic structural diagram of a multi-parameter control pipeline liquid erosion test device provided by the present invention.
具体实施方式detailed description
以下结合附图和具体实施例对本发明提供的多参量调控管道内液体冲蚀试验装置进行详细说明:The multi-parameter control pipeline liquid erosion test device provided by the present invention will be described in detail below in conjunction with the accompanying drawings and specific examples:
如图1所示,本发明提供的多参量调控管道内液体冲蚀试验装置包括依次相连的PH值可控的腐蚀液供给模块a、腐蚀液流量可调节模块b、腐蚀温度可控模块c以及腐蚀液回流过滤模块d;所述的PH值可控的腐蚀液供给模块a包括盛有PH调节液的烧杯1、蠕动泵2、第一稳流阀3、PH调控仪4、恒温锅5、盛有腐蚀液的烧杯6、PH调控仪探针7和第一管路15,其中,盛有腐蚀液的烧杯6放置在恒温锅5中;第一管路15的一端设置在盛有腐蚀液的烧杯6中,另一端浸没在盛有PH调节液的烧杯1内的PH调节液中;蠕动泵2设置在第一管路15上靠近盛有PH调节液的烧杯1处;第一稳流阀3设置在第一管路15上靠近盛有腐蚀液的烧杯6处;PH调控仪探针7放置在盛有腐蚀液的烧杯6内的腐蚀液中,且通过导线依次与PH调控仪4以及蠕动泵2电连接;As shown in Figure 1, the multi-parameter control pipeline liquid erosion test device provided by the present invention includes a corrosive solution supply module a with controllable pH value, a corrosive solution flow adjustable module b, a corrosive temperature controllable module c and a corrosive solution supply module connected in sequence. The corrosive liquid backflow filter module d; the corrosive liquid supply module a with controllable pH value includes a beaker 1 filled with a pH regulating liquid, a peristaltic pump 2, a first steady flow valve 3, a pH regulator 4, a constant temperature pot 5, The beaker 6 containing the corrosive liquid, the pH controller probe 7 and the first pipeline 15, wherein the beaker 6 containing the corrosive liquid is placed in the constant temperature pot 5; one end of the first pipeline 15 is set on the In the beaker 6, the other end is submerged in the pH adjusting liquid in the beaker 1 filled with the pH adjusting liquid; the peristaltic pump 2 is arranged on the first pipeline 15 near the beaker 1 filled with the pH adjusting liquid; the first steady flow The valve 3 is set on the first pipeline 15 close to the beaker 6 containing the corrosive liquid; the probe 7 of the pH controller is placed in the corrosive liquid in the beaker 6 containing the corrosive liquid, and is sequentially connected with the pH controller 4 through wires. And the peristaltic pump 2 is electrically connected;
所述的腐蚀液流量可调节模块b包括若干组相互并联的腐蚀液流量调节系统,每组腐蚀液流量调节系统包括第二管路16和依次设置在第二管路16上的无级调节蠕动泵8、第二稳流阀9和流量计10,并且第二管路16上靠近无级调节蠕动泵8的一端放置于盛有腐蚀液的烧杯6内的腐蚀液中;The corrosive liquid flow adjustable module b includes several groups of corrosive liquid flow regulation systems connected in parallel, and each group of corrosive liquid flow regulation systems includes a second pipeline 16 and a stepless adjustment peristaltic system sequentially arranged on the second pipeline 16 The pump 8, the second steady flow valve 9 and the flow meter 10, and the end of the second pipeline 16 close to the stepless adjustment peristaltic pump 8 is placed in the corrosive solution in the beaker 6 containing the corrosive solution;
所述的腐蚀温度可控模块c包括若干个待腐蚀的管道试样11、若干个温度控制仪探针12、若干条第三管路17和一个温度控制仪13;每个管道试样11的进液口连接在一组腐蚀液流量调节系统中第二管路16的另一端,出液口与一条第三管路17的一端相连;每个管道试样11内设有一个温度控制仪探针12;温度控制仪13同时与若干个温度控制仪探针12以及恒温锅5电连接;The corrosion temperature controllable module c includes several pipeline samples 11 to be corroded, several temperature controller probes 12, several third pipelines 17 and a temperature controller 13; The liquid inlet is connected to the other end of the second pipeline 16 in a group of corrosive liquid flow regulation systems, and the liquid outlet is connected to one end of a third pipeline 17; each pipeline sample 11 is provided with a temperature control instrument probe Needle 12; temperature controller 13 is electrically connected with several temperature controller probes 12 and thermostatic pot 5 at the same time;
所述的腐蚀液回流过滤模块d包括第四管路18和设置在第四管路18上的至少一个过滤器14;第四管路18的一端设置在盛有腐蚀液的烧杯6内,另一端连接若干条第三管路17,并且管道试样11的设置位置高于盛有腐蚀液的烧杯6。The corrosive liquid return filter module d includes a fourth pipeline 18 and at least one filter 14 arranged on the fourth pipeline 18; one end of the fourth pipeline 18 is arranged in the beaker 6 containing the corrosive liquid, and the other One end is connected to several third pipelines 17, and the pipeline sample 11 is set higher than the beaker 6 containing the corrosive liquid.
所述的腐蚀液回流过滤模块d中过滤器14的数量为若干个时,若干个过滤器14采用串联方式设置在第四管路18上。When the number of filters 14 in the corrosive liquid return filter module d is several, the several filters 14 are arranged in series on the fourth pipeline 18 .
所述的管道试样11采用透明材质,以便于试验人员观察管道试样11内壁的腐蚀情况。The pipeline sample 11 is made of transparent material so that the test personnel can observe the corrosion condition of the inner wall of the pipeline sample 11 .
现将本发明提供的多参量调控管道内液体冲蚀试验装置的使用方法阐述如下:Now the method for using the liquid erosion test device in the multi-parameter control pipeline provided by the present invention is set forth as follows:
首先由工作人员根据待腐蚀的管道试样11的个数开启与其相连的相应数量的无级调节蠕动泵8,由此将盛有腐蚀液的烧杯6中的腐蚀液通过第二管路16并经第二稳流阀9稳流后及流量计10计量后提供给待腐蚀的管道试样11内部,可利用控制无级调节蠕动泵8的方式使腐蚀液的流量保持在某个设定值,并由流量计10进行显示;在管道试样11内部,腐蚀液将与管道试样11的内壁发生腐蚀反应,然后经过反应的腐蚀液依靠位能经第三管路17流入第四管路18,设置在第四管路18上的过滤器14将经过反应的腐蚀液中的杂质进行过滤,最后流回盛有腐蚀液的烧杯6中。由于腐蚀液与管道试样11发生了腐蚀反应,因此盛有腐蚀液的烧杯6中的腐蚀液PH值会发生变化,从而偏离预定范围。在此过程中,PH调控仪探针7将实时检测盛有腐蚀液的烧杯6中的腐蚀液PH值并将检测数据传送给PH调控仪4,随后PH调控仪4根据上述检测结果控制蠕动泵2的启动或停止;当盛有腐蚀液的烧杯6内腐蚀液的PH值超出预定范围时,启动蠕动泵2,这时蠕动泵2将会吸入盛有PH调节液的烧杯1内的PH调节液,并通过第一管路15经第一稳流阀3稳流后注入盛有腐蚀液的烧杯6中,直到盛有腐蚀液的烧杯6中的腐蚀液PH值恢复到设定范围内,蠕动泵2才停止工作,从而可保证腐蚀液的PH值恒定。当盛有腐蚀液的烧杯6内腐蚀液的PH处于预定范围之内时,不启动蠕动泵2。Firstly, according to the number of pipeline samples 11 to be corroded, the staff opens the corresponding number of stepless adjustment peristaltic pumps 8 connected thereto, thereby passing the corrosive liquid in the beaker 6 containing the corrosive liquid through the second pipeline 16 and After the flow is stabilized by the second flow stabilization valve 9 and measured by the flow meter 10, it is provided to the inside of the pipeline sample 11 to be corroded, and the flow rate of the corrosion solution can be kept at a certain set value by controlling the stepless adjustment of the peristaltic pump 8 , and displayed by the flow meter 10; inside the pipeline sample 11, the corrosive liquid will react with the inner wall of the pipeline sample 11, and then the reacted corrosive liquid will flow into the fourth pipeline through the third pipeline 17 depending on the potential energy 18. The filter 14 arranged on the fourth pipeline 18 filters the impurities in the reacted corrosion solution, and finally flows back into the beaker 6 containing the corrosion solution. Since the corrosive reaction between the corrosive liquid and the pipeline sample 11 occurs, the pH value of the corrosive liquid in the beaker 6 containing the corrosive liquid will change, thereby deviating from the predetermined range. During this process, the pH controller probe 7 will detect the pH value of the corrosion solution in the beaker 6 containing the corrosion solution in real time and transmit the detection data to the pH controller 4, and then the pH controller 4 will control the peristaltic pump according to the above detection results 2 start or stop; when the pH value of the corrosion solution in the beaker 6 containing the corrosion solution exceeds the predetermined range, start the peristaltic pump 2, and at this time the peristaltic pump 2 will suck the pH adjustment in the beaker 1 containing the pH adjustment solution liquid, and inject it into the beaker 6 containing the corrosive liquid through the first steady flow valve 3 through the first pipeline 15 until the pH value of the corrosive liquid in the beaker 6 containing the corrosive liquid returns to the set range. The peristaltic pump 2 stops working, so that the pH value of the corrosion solution can be kept constant. When the pH of the corrosion solution in the beaker 6 containing the corrosion solution is within a predetermined range, the peristaltic pump 2 is not started.
随着腐蚀反应的进行,设置在管道试样11内的温度控制仪探针12将实时检测腐蚀液的温度,并将相应的检测数据传送给温度控制仪13。若温度偏离预定的范围,温度控制仪13在发出报警信号的同时会自动调节恒温锅5的温度,从而改变盛有腐蚀液的烧杯6中腐蚀液的温度,腐蚀液经腐蚀液流量可调节模块b再流入管道试样11内部,因而间接调控了管道试样11中腐蚀液的温度。As the corrosion reaction progresses, the probe 12 of the temperature controller installed in the pipeline sample 11 will detect the temperature of the corrosion solution in real time, and transmit the corresponding detection data to the temperature controller 13 . If the temperature deviates from the predetermined range, the temperature controller 13 will automatically adjust the temperature of the constant temperature pot 5 while sending an alarm signal, thereby changing the temperature of the corrosive liquid in the beaker 6 containing the corrosive liquid, and the corrosive liquid passes through the corrosive liquid flow adjustable module b then flows into the pipeline sample 11, thus indirectly regulating the temperature of the corrosive liquid in the pipeline sample 11.
以上所述实施例仅根据附图表达了本发明的具体实施方式,其描述相对具体和详细,但不能理解为本发明专利范围的限制。The above-mentioned embodiments only express the specific implementation manner of the present invention according to the accompanying drawings, and the description thereof is relatively specific and detailed, but should not be construed as a limitation of the patent scope of the present invention.
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