CN106974845B - Essence composition and preparation method and application thereof - Google Patents
Essence composition and preparation method and application thereof Download PDFInfo
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- CN106974845B CN106974845B CN201710170144.5A CN201710170144A CN106974845B CN 106974845 B CN106974845 B CN 106974845B CN 201710170144 A CN201710170144 A CN 201710170144A CN 106974845 B CN106974845 B CN 106974845B
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- 239000000203 mixture Substances 0.000 title claims abstract description 58
- 238000002360 preparation method Methods 0.000 title claims description 11
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 51
- OSWPMRLSEDHDFF-UHFFFAOYSA-N methyl salicylate Chemical compound COC(=O)C1=CC=CC=C1O OSWPMRLSEDHDFF-UHFFFAOYSA-N 0.000 claims abstract description 49
- 239000001525 mentha piperita l. herb oil Substances 0.000 claims abstract description 47
- 235000019477 peppermint oil Nutrition 0.000 claims abstract description 47
- MGSRCZKZVOBKFT-UHFFFAOYSA-N thymol Chemical compound CC(C)C1=CC=C(C)C=C1O MGSRCZKZVOBKFT-UHFFFAOYSA-N 0.000 claims abstract description 46
- NFLGAXVYCFJBMK-UHFFFAOYSA-N Menthone Chemical compound CC(C)C1CCC(C)CC1=O NFLGAXVYCFJBMK-UHFFFAOYSA-N 0.000 claims abstract description 44
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 claims abstract description 36
- 239000002826 coolant Substances 0.000 claims abstract description 34
- 239000000606 toothpaste Substances 0.000 claims abstract description 31
- 229940034610 toothpaste Drugs 0.000 claims abstract description 31
- NFLGAXVYCFJBMK-RKDXNWHRSA-N (+)-isomenthone Natural products CC(C)[C@H]1CC[C@@H](C)CC1=O NFLGAXVYCFJBMK-RKDXNWHRSA-N 0.000 claims abstract description 30
- 229930007503 menthone Natural products 0.000 claims abstract description 30
- 239000005844 Thymol Substances 0.000 claims abstract description 23
- 229960000790 thymol Drugs 0.000 claims abstract description 23
- 239000001683 mentha spicata herb oil Substances 0.000 claims abstract description 21
- 235000019721 spearmint oil Nutrition 0.000 claims abstract description 21
- RUVINXPYWBROJD-ONEGZZNKSA-N trans-anethole Chemical compound COC1=CC=C(\C=C\C)C=C1 RUVINXPYWBROJD-ONEGZZNKSA-N 0.000 claims abstract description 20
- RUVINXPYWBROJD-UHFFFAOYSA-N para-methoxyphenyl Natural products COC1=CC=C(C=CC)C=C1 RUVINXPYWBROJD-UHFFFAOYSA-N 0.000 claims abstract description 19
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000005770 Eugenol Substances 0.000 claims abstract description 18
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 claims abstract description 18
- 229960002217 eugenol Drugs 0.000 claims abstract description 18
- 229960001047 methyl salicylate Drugs 0.000 claims abstract description 18
- 235000006679 Mentha X verticillata Nutrition 0.000 claims abstract description 16
- 235000002899 Mentha suaveolens Nutrition 0.000 claims abstract description 16
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims abstract description 16
- 239000010648 geranium oil Substances 0.000 claims abstract description 11
- 235000019717 geranium oil Nutrition 0.000 claims abstract description 11
- WEEGYLXZBRQIMU-UHFFFAOYSA-N Eucalyptol Chemical compound C1CC2CCC1(C)OC2(C)C WEEGYLXZBRQIMU-UHFFFAOYSA-N 0.000 claims description 30
- ULDHMXUKGWMISQ-SECBINFHSA-N (-)-carvone Chemical compound CC(=C)[C@@H]1CC=C(C)C(=O)C1 ULDHMXUKGWMISQ-SECBINFHSA-N 0.000 claims description 26
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims description 17
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims description 17
- 229940041616 menthol Drugs 0.000 claims description 17
- 239000010651 grapefruit oil Substances 0.000 claims description 15
- NFLGAXVYCFJBMK-IUCAKERBSA-N (-)-isomenthone Chemical compound CC(C)[C@@H]1CC[C@H](C)CC1=O NFLGAXVYCFJBMK-IUCAKERBSA-N 0.000 claims description 14
- 235000019501 Lemon oil Nutrition 0.000 claims description 14
- 239000010501 lemon oil Substances 0.000 claims description 14
- 239000003921 oil Substances 0.000 claims description 10
- 235000019198 oils Nutrition 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 8
- 239000002304 perfume Substances 0.000 claims description 7
- 239000001920 pimenta acris kostel leaf oil terpeneless Substances 0.000 claims description 7
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 5
- 239000000047 product Substances 0.000 claims description 5
- 239000000706 filtrate Substances 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 4
- 239000003975 dentin desensitizing agent Substances 0.000 claims description 3
- 239000000796 flavoring agent Substances 0.000 claims description 3
- 235000019634 flavors Nutrition 0.000 claims description 3
- 235000010333 potassium nitrate Nutrition 0.000 claims description 3
- 239000004323 potassium nitrate Substances 0.000 claims description 3
- 229910001631 strontium chloride Inorganic materials 0.000 claims description 3
- AHBGXTDRMVNFER-UHFFFAOYSA-L strontium dichloride Chemical group [Cl-].[Cl-].[Sr+2] AHBGXTDRMVNFER-UHFFFAOYSA-L 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 2
- 229940011037 anethole Drugs 0.000 claims 1
- 235000009508 confectionery Nutrition 0.000 abstract description 12
- 235000019658 bitter taste Nutrition 0.000 abstract description 10
- 230000001680 brushing effect Effects 0.000 abstract description 9
- 239000003205 fragrance Substances 0.000 abstract description 7
- 239000006072 paste Substances 0.000 abstract description 4
- 239000000686 essence Substances 0.000 description 29
- 235000019640 taste Nutrition 0.000 description 8
- 230000003266 anti-allergic effect Effects 0.000 description 6
- 210000000214 mouth Anatomy 0.000 description 4
- 229940090898 Desensitizer Drugs 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 235000003332 Ilex aquifolium Nutrition 0.000 description 2
- 235000002296 Ilex sandwicensis Nutrition 0.000 description 2
- 235000002294 Ilex volkensiana Nutrition 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- ULDHMXUKGWMISQ-UHFFFAOYSA-N carvone Chemical compound CC(=C)C1CC=C(C)C(=O)C1 ULDHMXUKGWMISQ-UHFFFAOYSA-N 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 235000002566 Capsicum Nutrition 0.000 description 1
- 239000005973 Carvone Substances 0.000 description 1
- 241000207199 Citrus Species 0.000 description 1
- 206010018275 Gingival atrophy Diseases 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 244000024873 Mentha crispa Species 0.000 description 1
- 235000014749 Mentha crispa Nutrition 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- 208000002193 Pain Diseases 0.000 description 1
- 239000006002 Pepper Substances 0.000 description 1
- 235000016761 Piper aduncum Nutrition 0.000 description 1
- 235000017804 Piper guineense Nutrition 0.000 description 1
- 244000203593 Piper nigrum Species 0.000 description 1
- 235000008184 Piper nigrum Nutrition 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 208000002697 Tooth Abrasion Diseases 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000740 bleeding effect Effects 0.000 description 1
- 235000020971 citrus fruits Nutrition 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 201000002170 dentin sensitivity Diseases 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 208000007565 gingivitis Diseases 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- -1 levomenthone Chemical compound 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 208000028169 periodontal disease Diseases 0.000 description 1
- 201000001245 periodontitis Diseases 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 235000019654 spicy taste Nutrition 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000036347 tooth sensitivity Effects 0.000 description 1
- 208000004371 toothache Diseases 0.000 description 1
- 239000009637 wintergreen oil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Emergency Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses an essence composition, which comprises the following components: spearmint oil, geranium oil, peppermint oil, methyl salicylate, anise camphor, eugenol, thymol, cooling agent, menthone glycerol ketal; wherein the proportion of the spearmint oil, the peppermint oil and the anise camphor is 1-5: 1-10: 5-15. The essence composition can effectively relieve the bitter taste of the anti-sensitive toothpaste, and meanwhile, the mint fragrance and the sweet and warm tooth brushing experience are given to the paste.
Description
Technical Field
The invention relates to the technical field of oral care products, in particular to an essence composition and a preparation method and application thereof.
Background
The toothpaste is an indispensable oral cavity cleaning sanitary article in daily life, and has the basic functions of cleaning teeth, refreshing breath and keeping the oral cavity clean. At present, the traditional Chinese medicine toothpaste commonly used in the market has a plurality of types, and can inhibit harmful bacteria in the oral cavity, diminish inflammation, relieve pain, prevent acid, desensitize, prevent decayed teeth, and prevent and treat periodontal diseases such as gingivitis, periodontitis, tooth bleeding and the like. The essence is the most expensive component in the toothpaste, and the efficacy of the toothpaste basically depends on the essence used, which not only gives the toothpaste a certain type of aroma, but also provides the toothpaste with corresponding mouthfeel.
The anti-allergy toothpaste is specially developed for sensitive teeth, and can effectively relieve the sensitivity of the teeth and enhance the tolerance of the teeth to cold, hot, acid and sweet. The desensitizing toothpaste usually has bitter taste due to the fact that desensitizers such as strontium chloride and potassium nitrate are contained, and when mint raw materials are used as toothpaste essence, the bitter taste and spicy stimulation taste brought by the mint raw materials can further aggravate the bitter taste of the desensitizers, so that the toothpaste is uncomfortable in tooth brushing taste. At present, most of anti-allergic toothpaste on the market has bitter taste, and the anti-allergic effect and the comfortable tooth brushing taste are difficult to be considered simultaneously, so that the sale market of the anti-allergic toothpaste is greatly influenced.
Disclosure of Invention
Based on the essence, the invention overcomes the defects of the prior art and provides the essence composition suitable for the anti-sensitive toothpaste, and the essence composition can effectively solve the bitter taste of the anti-sensitive toothpaste and endow the paste with mint fragrance and sweet, delicious and mild tooth brushing experience.
The specific technical scheme is as follows:
a perfume composition comprising the following components: spearmint oil, geranium oil, peppermint oil, methyl salicylate, anise camphor, eugenol, thymol, cooling agent, menthone glycerol ketal; wherein the weight ratio of the spearmint oil to the peppermint oil to the anise camphor is 1-5: 1-10: 5-15.
The inventor finds through experiments that the essence composition prepared from the raw materials can effectively solve the bitter taste of the anti-sensitive toothpaste, the spearmint oil, the peppermint oil and the anise camphor are matched for use, so that the bitter taste of the spearmint oil and the green and slightly spicy taste brought by the spearmint oil are combined with the full and sweet hay-like taste of the anise camphor, and the proper amount ratio combination can generate cool, fresh, full and sweet taste experience. Thymol has a green-like herbal smell and a grapefruit-like fruity flavor, has a green herbal sensation in a hot mouthfeel, is pleasant in mouthfeel, and can enhance oral salivary secretion. Eugenol has a similar mouthfeel to thymol, is strong and intense, and even has a numb feeling similar to that of pepper. The bay leaf oil has a special sweet and moderate floral sweet note, resembling a rose. The methyl salicylate has the complete and clean perfect green and fragrant note of the holly, and the mouthfeel is sweet, mild and powerful. The menthone glycerol ketal and the cooling agent have long and gradually enhanced cooling mouthfeel, can show strong and smooth cooling taste impact with eugenol and thymol under the appropriate amount ratio, and can thoroughly shield the bitter and unpleasant mouthfeel after an overlong duration. The green combination of the spearmint oil, the carvone and the methyl salicylate can form fresh and powerful special green and fresh fragrance under a proper amount ratio, and the sweet and moist flower fragrance of the bay leaf oil can show a pleasant dynamic experience.
In one embodiment, the perfume composition further comprises: 1, 8-cineole, lemon oil, grapefruit oil, levocarvone, levomenthone, isomenthone, wintergreen oil, peppermint oil, and menthol. The 1, 8-cineole has a transparent and fresh cool feeling, the lemon oil is fresh and slightly sour, the grapefruit oil can be matched with the lemon oil to enhance the complex feeling of citrus, and the grapefruit oil and the levocarvone have the characteristic of special linear aroma. The levorotatory menthone and the isomenthone are combined with a proper equivalent ratio to enrich and refine the characteristic fragrance of the peppermint. Menthol can enhance the strong cool impact force in peppermint oil and can make the mouth cool in a short time reach a peak value.
In one embodiment, the essence composition comprises the following components in parts by weight:
1-5 parts of 1, 8-cineole;
1-3 parts of lemon oil;
1-3 parts of grapefruit oil;
2-5 parts of spearmint oil;
2-5 parts of levo carvone;
1-5 parts of levorotatory menthone;
1-5 parts of isomenthone;
0.1-3 parts of bay leaf oil;
1-10 parts of peppermint oil;
1-5 parts of natural wintergreen oil;
10-30 parts of methyl salicylate;
5-15 parts of anise camphor;
1-5 parts of eugenol;
0.1-3 parts of thymol;
1-5 parts of peppermint oil;
10-40 parts of menthol;
1-5 parts of cooling agent;
1-5 parts of menthone glycerol ketal.
The inventor finds out through experiments that the essence composition prepared according to the proportion has better effect.
In one embodiment, the essence composition comprises the following components in parts by weight:
3 parts of 1, 8-cineole;
2 parts of lemon oil;
1 part of grapefruit oil;
2 parts of spearmint oil;
5 parts of levocarvone;
3 parts of levorotatory menthone;
1 part of isomenthone;
0.5 part of Chinese geranium oil;
2 parts of Chinese peppermint oil;
3 parts of peppermint oil;
5 parts of American peppermint oil;
5 parts of natural wintergreen oil;
15 parts of methyl salicylate;
10 parts of anise camphor;
2.5 parts of eugenol;
1 part of thymol;
3 parts of Asian mint oil;
25 parts of natural menthol;
WS-35 parts of cooling agent;
WS-53 parts of cooling agent;
menthone glycerol ketal 3 parts.
The invention also aims to provide a preparation method of the essence composition.
The specific technical scheme is as follows:
the preparation method of the essence composition comprises the following steps:
s1, uniformly mixing the cooling agent, thymol and menthol, adding other components, and uniformly stirring and mixing to obtain a mixture;
s2, filtering the mixture, and taking the filtrate to obtain the product.
In one embodiment, the preparation method of the essence composition comprises the following steps:
s1, uniformly mixing the cooling agent, thymol and menthol, adding other components, and uniformly mixing for 30-60 minutes by using an electric stirrer to obtain a mixture;
and S2, sealing and standing the mixture in a container for 60-90 minutes, filtering, and taking the filtrate to obtain the product.
The invention also aims to provide application of the essence composition.
Use of the above perfume composition in an oral care composition.
In one embodiment, the oral care composition is an anti-sensitivity toothpaste.
Another object of the present invention is to provide an anti-sensitivity toothpaste.
An anti-allergy toothpaste comprises the essence composition.
In some of these embodiments, the anti-sensitivity toothpaste further comprises a desensitizing agent which is strontium chloride and/or potassium nitrate.
The anti-allergy toothpaste disclosed by the invention contains a desensitizer, has a good relieving effect on tooth pain caused by tooth abrasion, gum atrophy, tooth root exposure and tooth allergy such as cold, hot, sour and sweet, and the like, can effectively relieve tooth sensitivity, enhances the tolerance of teeth to cold, hot, sour and sweet, has no bitter taste during tooth brushing, enables the paste to have mint fragrance, and can provide a user with sweet, delicious and warm tooth brushing experience.
The invention has the beneficial effects that:
the essence composition can effectively relieve the bitter taste of the anti-sensitive toothpaste, and endows the paste with the fragrance of mint, fresh spearmint, green holly and the like and the sweet and mild tooth brushing experience; the anti-sensitivity toothpaste prepared by the essence composition can greatly improve the tooth brushing taste of a user, and has considerable market prospect.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the detailed description and specific examples, while indicating the scope of the invention, are intended for purposes of illustration only and are not intended to limit the scope of the invention.
The starting materials used in the following examples are all common commercial products.
Example 1
A essence composition comprises the following formula: 3 parts of 1, 8-cineole; 2 parts of lemon oil; 1 part of grapefruit oil; 2 parts of spearmint oil; 5 parts of levo carvone; 3 parts of levorotatory menthone; 1 part of isomenthone; 0.5 part of Chinese geranium oil; 2 parts of Chinese peppermint oil; 3 parts of peppermint oil; 5 parts of American peppermint oil; 5 parts of natural wintergreen oil; 15 parts of methyl salicylate; 10 parts of anise camphor; 2.5 parts of eugenol; 1 part of thymol; 3 parts of Asian mint oil; 25 parts of natural menthol; WS-35 parts of cooling agent; WS-53 parts of cooling agent; menthone glycerol ketal 3 parts.
The preparation process of the essence composition comprises the following steps:
s1, uniformly mixing the cooling agent WS-3, the cooling agent WS-5, thymol and natural menthol, adding other components, and uniformly mixing for 30-60 minutes by using an electric stirrer to obtain a mixture;
and S2, sealing and standing the mixture in a container for 60-90 minutes, filtering, taking filtrate, and filling to obtain the tea drink.
Example 2
A essence composition comprises the following formula: 2 parts of 1, 8-cineole; 4 parts of lemon oil; 4 parts of grapefruit oil; 3 parts of spearmint oil; 4 parts of levo carvone; 2 parts of levorotatory menthone; 5 parts of isomenthone; 2 parts of Chinese bay leaf oil; 2 parts of Chinese peppermint oil; 3 parts of peppermint oil; 4 parts of American peppermint oil; 2 parts of natural wintergreen oil; 35 parts of methyl salicylate; 12 parts of anise camphor; 4 parts of eugenol; 2 parts of thymol; 4 parts of Asian mint oil; 20 parts of natural menthol; WS-32 parts of cooling agent; WS-54 parts of cooling agent; 4 parts of menthone glycerol ketal.
The procedure for the preparation of the perfume composition was the same as in example 1.
Example 3
A essence composition comprises the following formula: 4 parts of 1, 8-cineole; 2 parts of lemon oil; 2 parts of grapefruit oil; 4 parts of spearmint oil; 2 parts of levo carvone; 4 parts of levorotatory menthone; 3 parts of isomenthone; 0.5 part of Chinese geranium oil; 4 parts of Chinese peppermint oil; 2 parts of peppermint oil; 3 parts of American peppermint oil; 2 parts of natural wintergreen oil; 15 parts of methyl salicylate; 8 parts of anise camphor; 3 parts of eugenol; 1 part of thymol; 2 parts of Asian mint oil; 15 parts of natural menthol; WS-36 parts of cooling agent; WS-52 parts of cooling agent; menthone glycerol ketal 3 parts.
The procedure for the preparation of the perfume composition was the same as in example 1.
Example 4
A essence composition comprises the following formula: 5 parts of 1, 8-cineole; 1 part of grapefruit oil; 4 parts of spearmint oil; 2 parts of levorotatory menthone; 5 parts of isomenthone; 3 parts of Chinese bay leaf oil; 3 parts of Chinese peppermint oil; 5 parts of peppermint oil; 1 part of American peppermint oil; 2 parts of natural wintergreen oil; 27 parts of methyl salicylate; 6 parts of anise camphor; 1 part of eugenol; 2 parts of thymol; 5 parts of Asian mint oil; WS-34 parts of cooling agent; WS-53 parts of cooling agent; menthone glycerol ketal 1 part.
The procedure for the preparation of the perfume composition was the same as in example 1.
Example 5
A essence composition comprises the following formula: 3 parts of 1, 8-cineole; 2 parts of spearmint oil, 0.5 part of Chinese geranium oil and 2 parts of Chinese peppermint oil; 3 parts of peppermint oil; 5 parts of peppermint oil, 15 parts of methyl salicylate, 10 parts of anise camphor, 2.5 parts of eugenol, 1 part of thymol and 35 parts of cooling agent WS; WS-53 parts of cooling agent and 3 parts of menthone glycerol ketal.
Example 6
A essence composition comprises the following formula: 2 parts of spearmint oil, 0.5 part of Chinese geranium oil and 2 parts of Chinese peppermint oil; 3 parts of peppermint oil; 5 parts of peppermint oil, 15 parts of methyl salicylate, 10 parts of anise camphor, 2.5 parts of eugenol, 1 part of thymol and 35 parts of cooling agent WS; WS-53 parts of cooling agent and 3 parts of menthone glycerol ketal.
Comparative example 1
A essence composition comprises the following formula: 3 parts of 1, 8-cineole; 2 parts of lemon oil; 1 part of grapefruit oil; 5 parts of levo carvone; 3 parts of levorotatory menthone; 1 part of isomenthone; 0.5 part of Chinese geranium oil; 2 parts of Chinese peppermint oil; 3 parts of peppermint oil; 5 parts of American peppermint oil; 5 parts of natural wintergreen oil; 15 parts of methyl salicylate; 2.5 parts of eugenol; 1 part of thymol; 3 parts of Asian mint oil; 25 parts of natural menthol; WS-35 parts of cooling agent; WS-53 parts of cooling agent; menthone glycerol ketal 3 parts.
Comparative example 2
A essence composition comprises the following formula: 3 parts of 1, 8-cineole; 2 parts of lemon oil; 1 part of grapefruit oil; 2 parts of spearmint oil; 5 parts of levo carvone; 3 parts of levorotatory menthone; 1 part of isomenthone; 0.5 part of Chinese geranium oil; 5 parts of Chinese peppermint oil; 5 parts of peppermint oil; 5 parts of American peppermint oil; 5 parts of natural wintergreen oil; 15 parts of methyl salicylate; 20 parts of anise camphor; 2.5 parts of eugenol; 1 part of thymol; 3 parts of Asian mint oil; 25 parts of natural menthol; WS-35 parts of cooling agent; WS-53 parts of cooling agent; menthone glycerol ketal 3 parts.
The procedure was the same as in example 1.
The essences prepared in examples 1 to 6 and comparative examples 1 and 2 were added to a toothpaste composition having the following formulation (parts by weight):
the toothpaste composition is subjected to performance test, 40 testers are used, 5 testers are used for each group, the prepared toothpaste composition is subjected to tooth brushing, the prepared toothpaste composition is subjected to grading on the taste and aroma of the toothpaste composition, each grading is fully 10 parts, the lowest grading is 0 part, the average value of the grading of each group is recorded, and the test result is as follows.
TABLE 1 taste scoring results
The technical features of the embodiments described above may be arbitrarily combined, and for the sake of brevity, all possible combinations of the technical features in the embodiments described above are not described, but should be considered as being within the scope of the present specification as long as there is no contradiction between the combinations of the technical features.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.
Claims (9)
1. The essence composition is characterized by comprising the following components in parts by weight:
1, 8-cineole 1-5 parts;
1-5 parts of lemon oil;
1-5 parts of grapefruit oil;
1-5 parts of spearmint oil;
1-5 parts of levo carvone;
1-5 parts of levorotatory menthone;
1-5 parts of isomenthone;
0.1-3 parts of bay leaf oil;
1-10 parts of peppermint oil;
1-5 parts of natural wintergreen oil;
10-30 parts of methyl salicylate;
5-15 parts of anethole;
1-5 parts of eugenol;
0.1-3 parts of thymol;
1-5 parts of peppermint oil;
10-30 parts of menthol;
1-10 parts of cooling agent;
1-5 parts of menthone glycerol ketal.
2. The essence composition according to claim 1, which is characterized by comprising the following components in parts by weight:
3 parts of 1, 8-cineole;
2 parts of lemon oil;
1 part of grapefruit oil;
2 parts of spearmint oil;
5 parts of levo carvone;
3 parts of levorotatory menthone;
1 part of isomenthone;
0.5 part of Chinese geranium oil;
2 parts of Chinese peppermint oil;
3 parts of peppermint oil;
5 parts of American peppermint oil;
5 parts of natural wintergreen oil;
15 parts of methyl salicylate;
10 parts of anise camphor;
2.5 parts of eugenol;
1 part of thymol;
3 parts of Asian mint oil;
25 parts of natural menthol;
WS-35 parts of cooling agent;
WS-53 parts of cooling agent;
menthone glycerol ketal 3 parts.
3. The essence composition according to claim 1, which is characterized by comprising the following components in parts by weight:
2 parts of 1, 8-cineole; 4 parts of lemon oil; 4 parts of grapefruit oil; 3 parts of spearmint oil; 4 parts of levo carvone; 2 parts of levorotatory menthone; 5 parts of isomenthone; 2 parts of Chinese bay leaf oil; 2 parts of Chinese peppermint oil; 3 parts of peppermint oil; 4 parts of American peppermint oil; 2 parts of natural wintergreen oil; 35 parts of methyl salicylate; 12 parts of anise camphor; 4 parts of eugenol; 2 parts of thymol; 4 parts of Asian mint oil; 20 parts of natural menthol; WS-32 parts of cooling agent; WS-54 parts of cooling agent; 4 parts of menthone glycerol ketal.
4. The essence composition according to claim 1, which is characterized by comprising the following components in parts by weight:
4 parts of 1, 8-cineole; 2 parts of lemon oil; 2 parts of grapefruit oil; 4 parts of spearmint oil; 2 parts of levo carvone; 4 parts of levorotatory menthone; 3 parts of isomenthone; 0.5 part of Chinese geranium oil; 4 parts of Chinese peppermint oil; 2 parts of peppermint oil; 3 parts of American peppermint oil; 2 parts of natural wintergreen oil; 15 parts of methyl salicylate; 8 parts of anise camphor; 3 parts of eugenol; 1 part of thymol; 2 parts of Asian mint oil; 15 parts of natural menthol; WS-36 parts of cooling agent; WS-52 parts of cooling agent; menthone glycerol ketal 3 parts.
5. A process for the preparation of a perfume composition according to any of claims 1 to 4, comprising the steps of:
s1, uniformly mixing the cooling agent, thymol and menthol, adding other components, and uniformly stirring and mixing to obtain a mixture;
s2, filtering the mixture, and taking the filtrate to obtain the product.
6. Use of a flavour composition according to any one of claims 1-4 in an oral care composition.
7. The use according to claim 6, wherein the oral care composition is an anti-sensitivity toothpaste.
8. An anti-sensitivity toothpaste comprising the flavor composition according to any one of claims 1 to 4.
9. The anti-sensitivity toothpaste according to claim 8, further comprising a desensitizing agent, wherein the desensitizing agent is strontium chloride and/or potassium nitrate.
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| CN110024783A (en) * | 2019-05-28 | 2019-07-19 | 贵州省茶叶研究所 | A kind of botanical sterilization preparation and its application method for preventing and treating tea tree anthracnose |
| CN110150280A (en) * | 2019-05-28 | 2019-08-23 | 贵州省生物技术研究所 | A kind of safe and environment-friendly preparation and application method for preventing and treating tea leaf spot |
| CN111100756A (en) * | 2019-12-31 | 2020-05-05 | 广州华芳烟用香精有限公司 | Micro-emulsified mint essence for cigarette paper, and preparation method and application thereof |
| CN112353700A (en) * | 2020-08-25 | 2021-02-12 | 广州途富香料科技有限公司 | Compound sweetener and preparation method thereof |
| CN112057390A (en) * | 2020-10-21 | 2020-12-11 | 广东南方洁灵科技实业有限公司 | Toothpaste for preventing and treating dental ulcer and preparation method and application thereof |
| CN112315833A (en) * | 2020-11-24 | 2021-02-05 | 广州途富香料科技有限公司 | Composite strong cooling agent applied to toothpaste essence |
| CN114931518B (en) * | 2022-06-08 | 2023-05-09 | 四川大学 | A kind of astringent taste masking agent of Chinese gallnut and its application |
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| CN85106825A (en) * | 1985-09-07 | 1987-03-25 | 昆明香料厂 | The concocting method of pseudo-ginseng toothpaste essence and application thereof |
| CN103468402A (en) * | 2013-08-16 | 2013-12-25 | 德利宝(广州)香料有限公司 | Essence containing natural snow pear extract and preparation method of toothpaste |
| CN105767837A (en) * | 2016-03-02 | 2016-07-20 | 广州满庭芳香料有限公司 | Cooling agent composition, essence containing the cooling agent composition and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN85106825A (en) * | 1985-09-07 | 1987-03-25 | 昆明香料厂 | The concocting method of pseudo-ginseng toothpaste essence and application thereof |
| CN103468402A (en) * | 2013-08-16 | 2013-12-25 | 德利宝(广州)香料有限公司 | Essence containing natural snow pear extract and preparation method of toothpaste |
| CN105767837A (en) * | 2016-03-02 | 2016-07-20 | 广州满庭芳香料有限公司 | Cooling agent composition, essence containing the cooling agent composition and application thereof |
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