CN106922714A - Plant growth regulator composition with synergistic effect - Google Patents
Plant growth regulator composition with synergistic effect Download PDFInfo
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- CN106922714A CN106922714A CN201710114135.4A CN201710114135A CN106922714A CN 106922714 A CN106922714 A CN 106922714A CN 201710114135 A CN201710114135 A CN 201710114135A CN 106922714 A CN106922714 A CN 106922714A
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- thidiazuron
- diethyl aminoethyl
- aminoethyl hexanoate
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- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000012948 isocyanate Substances 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- 150000004702 methyl esters Chemical class 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 239000004530 micro-emulsion Substances 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000012764 mineral filler Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229910052901 montmorillonite Inorganic materials 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 239000003895 organic fertilizer Substances 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 229940044654 phenolsulfonic acid Drugs 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 230000029553 photosynthesis Effects 0.000 description 1
- 238000010672 photosynthesis Methods 0.000 description 1
- LGRFSURHDFAFJT-UHFFFAOYSA-N phthalic anhydride Chemical compound C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 229920000570 polyether Polymers 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920001451 polypropylene glycol Polymers 0.000 description 1
- 229920002689 polyvinyl acetate Polymers 0.000 description 1
- 239000011118 polyvinyl acetate Substances 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- HZRSNVGNWUDEFX-UHFFFAOYSA-N pyraclostrobin Chemical compound COC(=O)N(OC)C1=CC=CC=C1COC1=NN(C=2C=CC(Cl)=CC=2)C=C1 HZRSNVGNWUDEFX-UHFFFAOYSA-N 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 239000011265 semifinished product Substances 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 238000009331 sowing Methods 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 229930192474 thiophene Natural products 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 230000017260 vegetative to reproductive phase transition of meristem Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/36—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< directly attached to at least one heterocyclic ring; Thio analogues thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/12—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group, wherein Cn means a carbon skeleton not containing a ring; Thio analogues thereof
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of plant growth regulator composition with synergistic effect, its active ingredient includes A and B, and wherein active component A is Thidiazuron, and active component B is diethyl aminoethyl hexanoate, and the weight ratio of active component A and active component B is 1：0.7~140.Present invention also offers the Preparation method and use of said composition.Result of the test shows, composition of the invention can regulating crop growth well, improve disease-resistant resistance, promote crop health benefit, improve crop yield.
Description
Technical field
It is more particularly to a kind of with the plant growth regulator for improving performance the invention belongs to agriculture plant protection field
Composition, concretely relates to a kind of composition comprising Thidiazuron and diethyl aminoethyl hexanoate agricultural chemicals.
Background technology
Diethyl aminoethyl hexanoate (diethyl aminoethyl hexanoate) is a kind of high energy with wide spectrum and breakthrough effect
Plant growth regulator, it can improve the activity of plant peroxidases and nitrate reductase, and the content for improving chlorophyll is accelerated
Photosynthetic speed, promotes the division and elongation of plant cell, promotes the development of root system, adjusts the balance of internal nutrient.To various agricultures
Crop has a significant volume increase, degeneration-resistant, disease-resistant, improving quality, it is precocious the effects such as, the compound with very high bioactivity.It
Can be compounded with multiple element, can also be used with bactericide compounded, strengthen the resistance against diseases of plant, improve bactericidal effect；Can be single
Solely using can also use with fertilizer, bactericide, insecticide and mixture of herbicides.
Thidiazuron (pyraclostrobin) is new and effective plant growth regulator, after Thidiazuron is absorbed by plants, can
Promote the chorista between petiole and stem, form nature and come off, can be widely used in agricultural chemicals, fertilizer.It has extremely strong
Bioactivity, its induction plant cell division, more much higher than the general basic element of cell division times of ability of Callus formation.Improve
Crop absorbability, increases photosynthesis, so as to reach volume increase, increase excellent purpose.Can be used for all kinds of melons, fruits and vegetables, nursery stock, flower
The crops such as grass, grain, tobacco, it may also be used for tissue cultures, genetic engineering etc..Crop yield can be significantly improved in production, is changed
Kind quality and have consumption it is few, to ecological environmental nonpollution, the features such as to people, animal, bird, honeybee, nontoxic natural enemy.
The plant growth regulator of current commercial type is mainly based on single dose, and action effect is single.
The content of the invention
It is an object of the invention to provide a kind of plant growth regulator composition, to promote plant growth, crop is improved
Disease-resistant, crop yield and the quality of improvement crop.Inventor has found that diethyl aminoethyl hexanoate is adjusting or promoting to plant between the two with Thidiazuron
Thing growth aspect has significant collaboration castering action.
It is a further object to provide the system comprising two kinds of effective constituents As and B plant growth regulator compositions
Preparation Method and agriculture field adjust and promote crop growth application.
The purpose of the present invention can be reached by following measures：
A kind of plant growth regulator composition with synergistic effect, said composition includes two kinds of active components of A and B,
Wherein active component A is Thidiazuron, and active component B is diethyl aminoethyl hexanoate, and the weight ratio between two components is active component A and activearm
The weight ratio for dividing B is 1：0.7~140.
In a kind of preferred scheme, the weight ratio of active component A and active component B is 1：0.75~130, it is further to carry
The weight ratio of the effect of high synergy, active component A and active component B is 1：0.8~120.
In a kind of preferred scheme, the weight ratio between A and the components of B two can arbitrarily in the range of following proportionings
It is adjusted：1：0.7、1：0.75、1：0.8、1：0.85、1：0.9、1：0.95、1：1、1：2、1：3、1：4、1：5、1：6、1：7、
1：8、1：9、1：10、1：15、1：20、1：25、1：30、1：35、1：40、1：45、1：50、1：55、1：60、1：65、1：70、1：
75、1：80、1：85、1：90、1：95、1：100、1：110、1：115、1：120、1：125、1：130、1：135 or 1：140, also may be used
With in the proportioning of any of the above two selected in the range of composition.
Inventor is found by experiment that composition of the invention is the growth for can preferably adjust crop, promotes
The health benefit of crop, improves the yield of crop, improves crop quality；Therefore composition pesticide of the invention can be applied to agriculture neck
Domain promotes or coordinate plant growth aspect.
The invention provides the composition comprising component A (Thidiazuron) and component B (diethyl aminoethyl hexanoate) agriculture is adjusted in agriculture field
The purposes of plant growth, particularly in paddy rice, corn or in terms of fruit tree, regulating crop growth improves the use of the aspects such as disease resisting effect
On the way.
To give full play to advantageous effect of the invention, composition of the invention can also with other agricultural chemicals (such as bactericide, kill
Worm agent, herbicide, plant growth regulator), fertilizer etc. be used in mixed way, these are mixed therewith to be disclosed in prior art often
Agricultural chemicals or fertilizer.
To improve using effect, composition of the invention can be processed into the preparation of various formulations, or and fertilizer with fertilizer
Common use is mixed.Suitable fertilizer includes：Inorganic fertilizer or organic fertilizer, specific fertilizer such as contain in nitrogen, phosphorus, potassium
Plant or several a great number of elements, or containing one or more trace elements in copper, iron, manganese, zinc, boron, calcium, magnesium, sulphur etc., or contain
At least one mixture of the fertilizer such as humic acid, amino acid, chitosan.
Composition of the invention can be made the formulation allowed on agricultural chemicals by active component and insecticides adjuvant.
In the present composition, active component mass content in the composition can for 0.5~85%, preferably 0.85~
50%.
Above-mentioned composition can specifically include insecticides adjuvant, such as carrier, solvent, dispersant, wetting agent, adhesive, thickening
One or more in agent, adhesive, surfactant etc., can mix conventional auxiliary agent during administration.
Suitable auxiliary agent can be solid or liquid, and they are typically the material commonly used during formulation, such as day
Right or regeneration mineral matter, solvent, dispersant, wetting agent, adhesive, thickener, adhesive or fertilizer.
The application process of the present composition includes being used for composition of the invention the aerial part of plant growth, especially
It is leaf portion or blade face.Can select to soak seed or be applied to controlling object surface.The frequency and amount of application of administration depend on crop
Growing state.
These compositions only can be administered comprising active component, it is also possible to be mixed together with additive (insecticides adjuvant)
Conjunction is used.
Composition of the invention can be prepared into acceptable formulation on agricultural chemicals, such as aqua, suspending agent, soluble liquid
Agent, oil-suspending agent, encapsulated form, microemulsion, wettable powder etc..Property and administration composition institute according to these compositions
The purpose and ambient conditions to be reached, can select composition to spray, atomizing, dust, broadcast sowing or sprinkle the side poured or the like
Method is applied.
Being adapted to encapsulated form of the invention includes：Microcapsule suspending agent, microcapsule suspension-suspendinagent agent, microcapsule suspension-aqueous emulsion
Deng, it is characterised in that (i.e. capsule-core) includes the mixture by active ingredient diethyl aminoethyl hexanoate and Thidiazuron according to a certain percentage in cyst wall,
Will both be mixed and made into microencapsulation.Microencapsulation is stably disperseed using certain concentration, is suspended in as continuous phase
Microcapsule suspending agent is formed in water.Or one of which active ingredient is prepared into microcapsule suspending agent, by another active ingredient
Be prepared into emulsion, the two kinds of compositions that will be prepared in mixing, stirring, shake up obtain final product microcapsule suspending agent-suspending agent or microcapsule suspending agent-
Aqueous emulsion.
Composition of the invention can be prepared into various formulations with known method, can by active ingredient with help
Agent, such as solvent, solid carrier, it is necessary to when can uniformly mix together with surfactant, grind, be prepared into required agent
Type.
Above-mentioned solvent may be selected from aromatic hydrocarbon, preferably containing 8-12 carbon atom, such as xylene mixture or substituted benzene, phthalein
The octanoic acid of esters of gallic acid, such as Dibutyl phthalate or phthalandione two, such as fat hydrocarbon, thiacyclohexane or paraffin, alcohol and ethylene glycol and their ether
And ester, such as ethanol, ethylene glycol, ethylene glycol monomethyl；Ketone, such as cyclohexanone, such as highly polar solvent, N- methyl -2- pyrrolidines
Ketone, dimethyl sulfoxide (DMSO) or dimethylformamide, and vegetable oil or vegetable oil, such as soybean oil.
Above-mentioned solid carrier, is such as used for wettable powder and dispersibles the typically natural mineral fillers of agent, for example, slide
Stone, kaolin, montmorillonite or atlapulgite.In order to manage the physical property of composition, it is also possible to add polymolecularity silicic acid or
Polymolecularity adsorpting polymerization thing carrier, such as granulated adsorptive carriers or non-adsorbed carrier, suitable granulated adsorptive carriers are porous
Type, such as float stone, bentonite or bentonite；Suitable non-adsorbed carrier such as calcite or sand.Further, it is possible to use substantial amounts of inorganic
The prefabricated material for granulating of property or organic nature is used as carrier, particularly dolomite.
The chemical property of the active ingredient in composition of the invention, suitable surfactant is sulfomethylated lignin
Acid, naphthalene sulfonic acids, phenolsulfonic acid, alkali salt or amine salt, alkylaryl sulfonates, alkyl sulfate, alkylsulfonate, fat
The condensation product of alcohol sulfate, aliphatic acid and sulphated fatty alcohol glycol ether, also sulfonated naphthalene and naphthalene derivatives and formaldehyde, naphthalene or
Naphthalene sulfonic acids and phenol and the condensation product of formaldehyde, NONIN HS 240, ethoxylated isooctyl-phenol, octyl phenol, nonyl phenol,
Alkylaryl polyglycol ether, tributyl benzene polyglycol ether, three stearyl phenyl polyglycol ethers, alkyl aryl polyether alcohol,
Ethoxylated castor oil, polyoxyethylene alkyl ether, ethylene oxide condensation product, ethoxylation polyoxypropylene, bay acid polyethylene glycol
Ether acetal, sorbitol ester, lignin sulfite waste liquor and methylcellulose.
Plant in the present invention includes but is not limited to apple or corn.
Two kinds of active ingredients show as synergistic effect in composition of the invention, and the activity of said composition is than using individualized
The expected summation of activity of compound, and the independent activity of single compound is more notable.Composition of the invention shows
Other features are mainly shown as：1st, composition mixture of the invention has obvious synergistic function；2nd, combination of the invention
Thing can regulating crop growth well, improve disease-resistant resistance, promote crop health benefit, improve crop yield.
Specific embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that specific embodiment described herein is only used to explain the present invention, limit is not used to
The fixed present invention, all any modification, equivalent and improvement made within the spirit and principles in the present invention etc., should be included in
Within protection scope of the present invention.
Percentage is weight percentage (folding hundred) in all formulas of following examples.The various preparations of the present composition
Processing technology is prior art, can be varied from according to different situations.
First, formulation prepares embodiment
(1) processing of suspending agent and embodiment
By active component diethyl aminoethyl hexanoate and Thidiazuron, with each component such as dispersant, wetting agent, thickener and water by formula ratio
Example is well mixed, through sand milling and/or high speed shear after, obtain semi-finished product, the filtering that is mixed with water is mended after analysis and is got product.
Embodiment 1：25.25% Thidiazuron diethyl aminoethyl hexanoate suspending agent
Thidiazuron 0.25%, diethyl aminoethyl hexanoate 25%, xanthans 4%, glycerine 2%, kaolin 5%, Magnesiumaluminumsilicate 5%, wood
Quality sodium sulfonate 5%, water complements to 100%.
Embodiment 2：25.5% Thidiazuron diethyl aminoethyl hexanoate suspending agent
Thidiazuron 0.5%, diethyl aminoethyl hexanoate 25%, bentonite 7%, ethylene glycol 3%, methyl naphthalene sulfonate formaldehyde condensate 5%,
Water complements to 100%.
Embodiment 3：0.875% Thidiazuron diethyl aminoethyl hexanoate suspending agent
Thidiazuron 0.5%, diethyl aminoethyl hexanoate 0.375%, white carbon 5%, glycerine 6%, Sodium Benzoate 3%, fatty alcohol polyoxy
Ethene ether phosphate 5%, water complements to 100%.
(2) processing of microcapsules and embodiment
By active ingredient Thidiazuron and diethyl aminoethyl hexanoate mixture according to a certain percentage, will both be mixed and made into miniature glue
Capsule.Microencapsulation is stably disperseed using certain concentration, is suspended in and is formed microcapsule suspending agent as in the water of continuous phase.Or
One of which active ingredient is prepared into microcapsule suspending agent, another active ingredient is prepared into emulsion, two kinds for preparing
Composition shakes up and obtains final product microcapsule suspending agent-suspending agent or microcapsule suspending agent-aqueous emulsion in mixing, stirring.
Embodiment 4：16.2% Thidiazuron diethyl aminoethyl hexanoate microcapsule suspending agent
Thidiazuron 0.2%, diethyl aminoethyl hexanoate 16%, rosinweed oil 12%, glyceride lactate 4%, emulsifier polyoxyethylene castor
Sesame oil 3%, stabilizer triphenyl phosphite 3.5%, toluene di-isocyanate(TDI) 15%, acrylic acid and acrylic ester copolymers 5%,
DPG 3%, preservative sodium benzoate 1%, thickener xanthans 2.1%, water complements to 100%.
Embodiment 5:6.2% Thidiazuron diethyl aminoethyl hexanoate microcapsule suspension-suspendinagent agent
Thidiazuron 0.2%, diethyl aminoethyl hexanoate 6%, methyl esters coconut oil 15%, polyoxyethylene monopalmitate 5%, draws BHT5%
Lure amino acid 2%, Sodium Benzoate 5%, ethylene glycol 5%, poly (vinyl acetate) emulsions 4%, xanthans 2%, water complements to 100%.
Embodiment 6:1.8% Thidiazuron diethyl aminoethyl hexanoate microcapsule suspension-aqueous emulsion
Thidiazuron 1%, diethyl aminoethyl hexanoate 0.8%, gelatin 15%, ethanol 4%, ethylenediamine 5%, the contracting of methyl naphthalene sulfonic acid sodium formaldehyde
Compound 5%, water complements to 100%.
(3) processing of soluble powder and embodiment
By active ingredient Thidiazuron and diethyl aminoethyl hexanoate mixture, surfactant, auxiliary agent, filler according to a certain percentage, put
In kettle, it is sufficiently stirred for, obtains final product soluble powder.
Embodiment 7:19.65% Thidiazuron diethyl aminoethyl hexanoate soluble powder
Thidiazuron 0.15%, diethyl aminoethyl hexanoate 19.5%, sodium alkyl benzene sulfonate 5%, kaolin complements to 100%.
Embodiment 8:30.5% Thidiazuron diethyl aminoethyl hexanoate soluble powder
Thidiazuron 0.5%, diethyl aminoethyl hexanoate 30%, APES polyethenoxy ether 2%, bentonite is complemented to
100%
Embodiment 9:2% Thidiazuron diethyl aminoethyl hexanoate soluble powder
Thidiazuron 1%, diethyl aminoethyl hexanoate 1%, benzyl dimethyl phenol polyethenoxy ether 4%, ammonium sulfate complements to 100%.
(4) processing of aqua and embodiment
Active ingredient and auxiliary agent are added in a kettle., and surplus is supplied with water, and is stirred, you can obtain Thidiazuron
Diethyl aminoethyl hexanoate aqua.
Embodiment 10:28.2% Thidiazuron diethyl aminoethyl hexanoate aqua
Thidiazuron 0.2%, dimethyl sulfoxide (DMSO) 5%, ethanol 5% are mixed, are stirred 20 minutes, add diethyl aminoethyl hexanoate 28%,
Stirring is completely dissolved to diethyl aminoethyl hexanoate for 30 minutes；8% alkylol sodium sulphate is added, surplus is supplied with water.
Embodiment 11:10.5% Thidiazuron diethyl aminoethyl hexanoate aqua
Thidiazuron active compound 0.5% and ethanol 8% are added in a kettle., are stirred 20 minutes；Diethyl aminoethyl hexanoate 10% is added, is stirred
Mix 30 minutes and be completely dissolved to diethyl aminoethyl hexanoate；10% AEO is added, surplus is supplied with water.
Embodiment 12:0.8% Thidiazuron diethyl aminoethyl hexanoate aqua
Thidiazuron 0.5% and ethanol 5% are added in a kettle., are stirred 20 minutes；Diethyl aminoethyl hexanoate 0.3% is added, is stirred
It is completely dissolved to diethyl aminoethyl hexanoate within 30 minutes；5% AEO is added, surplus is supplied with water.
(5) processing of aqueous emulsion and embodiment
By active component diethyl aminoethyl hexanoate and Thidiazuron, with each component such as solvent, emulsifying agent, dispersant, antifreeze and water by matching somebody with somebody
The ratio mixing of side is placed in reactor, is sufficiently stirred for, you can obtain aqueous emulsion.
Embodiment 13:15.125% Thidiazuron diethyl aminoethyl hexanoate aqueous emulsion
Thidiazuron 0.125%, diethyl aminoethyl hexanoate 15%, neopelex 10%, toluene 10%, polyvinyl alcohol 5%,
Glycerine 5%, organic silicon defoamer 1%, water complements to 100%.
Embodiment 14:8.2% Thidiazuron diethyl aminoethyl hexanoate aqueous emulsion
Thidiazuron 0.2%, diethyl aminoethyl hexanoate 8%, dimethylbenzene 10%, polyvinyl alcohol 5%, glycerine 5%, organic silicon defoamer
1%, water complements to 100%.
Embodiment 15:11% Thidiazuron diethyl aminoethyl hexanoate aqueous emulsion
Thidiazuron 1%, diethyl aminoethyl hexanoate 10%, neopelex 10%, methyl alcohol 10%, polyvinyl alcohol 5%, the third three
Alcohol 5%, organic silicon defoamer 1%, water complements to 100%.
Embodiment 16:0.85% Thidiazuron diethyl aminoethyl hexanoate aqueous emulsion
Thidiazuron 0.5%, diethyl aminoethyl hexanoate 0.35%, APES 10%, toluene 10%, glycerine 5% is organic
Silicon defoaming agent 1%, water complements to 100%.
2nd, drug effect checking test
(1) Assays Example
1st, Thidiazuron and DA-6 compoundings are to apple development regulation synthesis measuring experiment
Thidiazuron and DA-6 acetone are diluted according to finite concentration, cauline leaf spraying is carried out to crop, determine each between garden
The influence that individual concentration grows to Apple, including transverse diameter, vertical footpath, single fruit weight, disease-resistant situation, fruit quality to apple, with
And output condition etc. carries out overall merit.
Transverse diameter control rate=(transverse diameter after clear water control transverse diameter-treatment)/clear water control transverse diameter * 100%
Vertical footpath increase rate=(the vertical footpath after the vertical footpath-treatment of clear water control) vertical footpath * 100% of/clear water control
The disease index * of preventive effect=(disease index after the disease index-treatment of clear water control)/clear water control
100%
The single fruit weight * of single fruit weight increase rate=(single fruit weight after the single fruit weight-treatment of clear water control)/clear water control
100%
The per mu yield * 100% of per mu yield increase rate=(per mu yield after the per mu yield-treatment of clear water control)/clear water control
The Thidiazuron of table 1. is compounded with diethyl aminoethyl hexanoate and adjusts synthesis measuring summary sheet to apple development
Note：" amine " is " diethyl aminoethyl hexanoate " abbreviation in form, and " thiophene " is the abbreviation of " Thidiazuron ".Dispenser period：Initial stage early flowering season,
The stage apple tree takes place apple anthracnose.Spraying times：3 times, 7-10 days dispenser interval；Insecticide-applying way：
Cauline leaf is sprayed；Investigation period：Apple expands the initial stage；In this experiment, the index such as transverse diameter, vertical footpath, disease index, single fruit weight is respectively
The average value for the treatment of.
Find have between Thidiazuron and diethyl aminoethyl hexanoate and cooperate with castering action, Thidiazuron and amine very well by testing inventor
Under different ratio, with respect to Thidiazuron, diethyl aminoethyl hexanoate single dose, and clear water control, the growth regulating to apple is acted on fresh ester mixture
Substantially, it is mainly manifested in：1st, the present invention can be effectively increased the transverse diameter of Apple, vertical footpath, and it can improve plant peroxidases
With the activity of nitrate reductase, the content quickening photosynthetic speed of chlorophyll is improved, promote the division and elongation of plant cell, so that
Improve the quality of apple；2nd, Thidiazuron has certain disease-resistant degeneration-resistant effect when being used as single dose to plant growth, and amine
Fresh ester is a kind of high bioactivity compound, has certain immunity to crop disease, is applied jointly between diethyl aminoethyl hexanoate and Thidiazuron
With with good synergy, be can be seen that from upper table analysis and acted synergistically between Thidiazuron and diethyl aminoethyl hexanoate to apple anthrax
The preventive effect of disease is compareed relative to single dose and clear water, with good preventive effect；3rd, due to apple expanding stage Thidiazuron with
The synergy of diethyl aminoethyl hexanoate, promotes the nutrition conduction of apple, disease-resistant degeneration-resistant, in the ripe apples phase, to the single fruit weight of apple with
And unit per mu yield is obviously improved effect；4th, diethyl aminoethyl hexanoate and Thidiazuron are in proportioning (0.7~140)：When between 1, showed
Both synergistic function effects substantially, when the ratio of diethyl aminoethyl hexanoate and Thidiazuron is less than 0.7, imitate by both synergistic functions
Fruit is not obvious.
(2) field efficacy checking test
1st, Thidiazuron and diethyl aminoethyl hexanoate mixture are to corn crop growth regulation and the field compbined test of disease-resistant yield-increasing
Dispenser period：Corn takes out the easily disease such as generation helminthosporium maydis of male initial stage.
Spraying times：2 times.Sprayed using example of formulations of the invention, three repetitions, results averaged.
The Thidiazuron of table 2 and field Comprehensive Experiment of the diethyl aminoethyl hexanoate mixture to corn growth regulation
Shown from the experimental data of table 2, product of the invention is applied in corn tasseling stage, can effective adjusting corn health
Growth.In diethyl aminoethyl hexanoate and Thidiazuron in proportioning (0.7~140)：When between 1, it is mainly shown as：1st, corn kernel can significantly be carried
Weight；2nd, can be with Dwarf corn plant, the effectively control prosperous excessive growth of corn control prevents corn lodging；3rd, life of the Thidiazuron to corn
It is long that there is certain facilitation, and diethyl aminoethyl hexanoate has certain disease-resistant anti-adversity ability to corn growth, has after both mixtures
Certain synergistic function；4th, composition of the invention has to the specific yield of corn and is obviously improved effect；5th, implement
Example 12 (0.8% Thidiazuron diethyl aminoethyl hexanoate aqua), i.e. diethyl aminoethyl hexanoate：Thidiazuron proportioning 0.3:When 0.5, compareed relative to single dose and it
Its embodiment, synergistic action effect is not obvious.
Claims (10)
1. a kind of plant growth regulator composition with synergistic effect, it is characterised in that said composition includes two kinds of work of A and B
Property component, wherein active component A is Thidiazuron, and active component B is diethyl aminoethyl hexanoate, and the weight ratio of active component A and active component B is
1: 0.7~140.
2. composition according to claim 1, it is characterised in that the weight ratio of active component A and active component B is 1:
0.75~130.
3. composition according to claim 1, it is characterised in that the weight ratio of active component A and active component B is 1: 0.8
~120.
4. composition according to claim 1, it is characterised in that said composition is made up on agricultural chemicals of active component and auxiliary agent
The formulation of permission.
5. composition according to claim 4, it is characterised in that active component mass content in the composition is
0.5~85%.
6. composition according to claim 5, it is characterised in that active component mass content in the composition is
0.85~50%.
7. composition according to claim 4, it is characterised in that the formulation is aqua, suspending agent, soluble concentrate or micro-
Cap dosage.
8. composition according to claim 4, it is characterised in that the auxiliary agent is selected from carrier, solvent, dispersant, wetting
One or more in agent, adhesive, thickener, adhesive, surfactant or fertilizer.
9. the composition pesticide in claim 1~8 described in any one is in agriculture field promotion or the use of coordinate plant growth
On the way.
10. purposes according to claim 9, it is characterised in that the plant is selected from apple, paddy rice or corn.
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| CN2016102048381 | 2016-04-02 | ||
| CN201610204838 | 2016-04-02 |
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| CN106342853B (en) * | 2016-04-02 | 2018-12-14 | 江苏辉丰农化股份有限公司 | Plant growth regulator composition with synergistic effect |
| CN111374177A (en) * | 2018-12-29 | 2020-07-07 | 山东营养源食品科技有限公司 | Plant growth regulator composition |
| CN110663703A (en) * | 2019-10-21 | 2020-01-10 | 江西鑫邦生化有限公司 | Compound growth regulator and preparation method and application thereof |
| CN111406739A (en) * | 2020-04-01 | 2020-07-14 | 中化化工科学技术研究总院有限公司 | Agricultural diffusant, pesticide composition containing agricultural diffusant and preparation method of pesticide composition |
| CN115868488B (en) * | 2022-10-21 | 2024-03-12 | 郑州郑氏化工产品有限公司 | Preparation method of microcapsule suspending agent containing fatty acid diethylaminoethanol ester |
| CN115956571A (en) * | 2022-11-25 | 2023-04-14 | 长江大学 | A kind of plant growth regulator composition and application of regulating seed size |
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|---|---|---|---|---|
| CN101103727A (en) * | 2007-08-17 | 2008-01-16 | 咸阳德丰有限责任公司 | Method for preparing thidiazuron as active substance used for plant quality-promoting and yield-increasing product and its application |
| CN101836629A (en) * | 2010-06-17 | 2010-09-22 | 陕西韦尔奇作物保护有限公司 | Plant growth regulator containing diethyl aminoethyl hexanoate |
| CN106342853B (en) * | 2016-04-02 | 2018-12-14 | 江苏辉丰农化股份有限公司 | Plant growth regulator composition with synergistic effect |
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| CN1899021A (en) * | 2005-07-20 | 2007-01-24 | 陈清虎 | Quick breeding method for root of kudzu vine |
| CN101023729A (en) * | 2006-02-21 | 2007-08-29 | 陈清虎 | Raspberry quick-breeding method |
| CN102037830B (en) * | 2009-10-20 | 2012-09-12 | 四川国光农化股份有限公司 | Plant growth regulator composition |
| CN102303990B (en) * | 2010-10-13 | 2014-06-18 | 四川国光农化股份有限公司 | Medicinal fertilizer composition |
| CN102613246A (en) * | 2011-12-13 | 2012-08-01 | 四川龙蟒福生科技有限责任公司 | Plant growth regulating composition and its application |
| CN105284616B (en) * | 2015-10-30 | 2017-02-01 | 海南森祺制药有限公司 | Induction medium for nauclea officinalis aseptic seedlings and nauclea officinalis detoxification rapid propagation method |
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- 2016-08-08 WO PCT/CN2016/094032 patent/WO2017166567A1/en active Application Filing
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101103727A (en) * | 2007-08-17 | 2008-01-16 | 咸阳德丰有限责任公司 | Method for preparing thidiazuron as active substance used for plant quality-promoting and yield-increasing product and its application |
| CN101836629A (en) * | 2010-06-17 | 2010-09-22 | 陕西韦尔奇作物保护有限公司 | Plant growth regulator containing diethyl aminoethyl hexanoate |
| CN106342853B (en) * | 2016-04-02 | 2018-12-14 | 江苏辉丰农化股份有限公司 | Plant growth regulator composition with synergistic effect |
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| WO2017166567A1 (en) | 2017-10-05 |
| CN106342853A (en) | 2017-01-25 |
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