CN106883676A - A kind of water-based flexographic ink and preparation method thereof - Google Patents
A kind of water-based flexographic ink and preparation method thereof Download PDFInfo
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 64
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 239000000839 emulsion Substances 0.000 claims abstract description 39
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 38
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 26
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 17
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000004132 cross linking Methods 0.000 claims abstract description 13
- 239000003431 cross linking reagent Substances 0.000 claims abstract description 13
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000004094 surface-active agent Substances 0.000 claims abstract description 12
- 239000000080 wetting agent Substances 0.000 claims abstract description 12
- -1 film-forming aid Substances 0.000 claims abstract description 10
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims abstract description 3
- 239000007788 liquid Substances 0.000 claims description 12
- 239000000049 pigment Substances 0.000 claims description 12
- 239000004925 Acrylic resin Substances 0.000 claims description 11
- 229920000178 Acrylic resin Polymers 0.000 claims description 11
- 239000013530 defoamer Substances 0.000 claims description 11
- 239000002480 mineral oil Substances 0.000 claims description 11
- 235000010446 mineral oil Nutrition 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 11
- 239000002994 raw material Substances 0.000 claims description 11
- 239000001967 plate count agar Substances 0.000 claims description 8
- 239000003085 diluting agent Substances 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 238000007639 printing Methods 0.000 claims description 5
- XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 2
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 claims 2
- 239000013543 active substance Substances 0.000 claims 1
- 239000000758 substrate Substances 0.000 abstract description 4
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 230000007547 defect Effects 0.000 abstract 1
- 230000009965 odorless effect Effects 0.000 abstract 1
- 239000000976 ink Substances 0.000 description 28
- 239000003995 emulsifying agent Substances 0.000 description 3
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 101100257127 Caenorhabditis elegans sma-2 gene Proteins 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000007645 offset printing Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000010023 transfer printing Methods 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
本发明提供了一种水性柔版油墨及其制备方法，以克服现有水性柔版油墨所存在的缺陷。为实现上述目的，本发明是以色浆、水性丙烯酸成膜乳液、丙烯酰胺高光泽乳液、丙烯酸自交联乳液、润湿剂、成膜助剂、乙醇、炔二醇表面活性剂、交联剂、手感助剂25、转印剂为组分混合而成。本发明适用基材广，包括PET，PE，PC，铜版纸等；制备方法简单，无毒，无味，转移性和附着牢度良好；性能稳定，墨层光泽度高，手感好，具有良好的耐水性和耐候性。The invention provides a water-based flexographic ink and a preparation method thereof to overcome the defects of the existing water-based flexographic ink. To achieve the above object, the present invention is based on color paste, water-based acrylic film-forming emulsion, acrylamide high-gloss emulsion, acrylic acid self-crosslinking emulsion, wetting agent, film-forming aid, ethanol, acetylenic glycol surfactant, crosslinking agent, hand feeling aid 25, and transfer agent are mixed components. The invention is suitable for a wide range of substrates, including PET, PE, PC, coated paper, etc.; the preparation method is simple, non-toxic, odorless, and the transferability and adhesion fastness are good; the performance is stable, the ink layer has high gloss, good hand feeling, and has good Water and weather resistance.
Description
技术领域technical field
本发明涉及一种水性油墨，尤其涉及一种水性柔版油墨及其制备方法。The invention relates to a water-based ink, in particular to a water-based flexographic ink and a preparation method thereof.
背景技术Background technique
随着全球经济的快速发展，生活质量的不断提高，人们对环保健康的要求在不断增强，水性柔版油墨具有环保优势所以在市场投入潜力巨大，因而它受到人们越来越多的关注，水性柔版油墨成为了油墨行业重要发展的方向和趋势。水性柔版油墨主要以水为溶剂，不含有易挥发性有毒有机溶剂，印刷适应性良好，具有良好的透过性，其透过性更好因而得到广泛应用。因此水性柔版印刷墨水有着比较广阔的前景和发展空间。With the rapid development of the global economy and the continuous improvement of the quality of life, people's requirements for environmental protection and health are constantly increasing. Water-based flexographic ink has environmental protection advantages, so it has great investment potential in the market, so it has attracted more and more attention. Flexographic ink has become an important development direction and trend of the ink industry. Water-based flexographic ink mainly uses water as a solvent, does not contain volatile toxic organic solvents, has good printing adaptability, and has good permeability. Its permeability is better and it is widely used. Therefore, water-based flexographic printing ink has relatively broad prospects and development space.
柔性版水墨属于液体体系油墨类。相比胶印油墨要粘度小得多。这种水墨可以在水和乙醇等与水互溶的溶剂以任意比稀释。柔性版水墨可以在自来水中直接清洗,而且在承印物上干燥之后，它不溶于水而且抗水性较好，水墨粘度低，凝固性高，墨色牢固，印迹清晰，清洗简便。Flexographic ink belongs to liquid system ink. Much less viscous than offset printing inks. This ink can be diluted in any ratio in water and ethanol and other water-miscible solvents. Flexographic ink can be washed directly in tap water, and after drying on the substrate, it is insoluble in water and has good water resistance, low ink viscosity, high coagulation, firm ink color, clear imprint, and easy cleaning.
但是目前市场上流通的大多数柔性版水墨存在适用基材单一，抗刮耐磨程度差等问题，给使用者带来了不便，降低了使用效率。However, most of the flexographic inks currently on the market have problems such as a single applicable substrate, poor scratch resistance and wear resistance, which brings inconvenience to users and reduces the use efficiency.
发明内容Contents of the invention
本发明的目的是提供一种水性柔版油墨及其制备方法，以克服现有水性柔版油墨所存在的缺陷。The purpose of the present invention is to provide a kind of water-based flexo printing ink and preparation method thereof, to overcome the defective that existing water-based flexo printing ink exists.
为实现上述目的，本发明是以色浆、水性丙烯酸成膜乳液、丙烯酰胺高光泽乳液、丙烯酸自交联乳液、润湿剂、成膜助剂、乙醇、炔二醇表面活性剂、交联剂、手感助剂25、转印剂为组分混合而成，各组分重量百分比为：To achieve the above object, the present invention is based on color paste, water-based acrylic film-forming emulsion, acrylamide high-gloss emulsion, acrylic acid self-crosslinking emulsion, wetting agent, film-forming aid, ethanol, acetylenic glycol surfactant, crosslinking agent, hand feeling aid 25, and transfer printing agent are mixed components, and the weight percentage of each component is:
色浆 30%-40%Color paste 30%-40%
水性丙烯酸成膜乳液 15%-20%Water-based acrylic film-forming emulsion 15%-20%
丙烯酰胺高光泽乳液 20%-32%Acrylamide High Gloss Emulsion 20%-32%
丙烯酸自交联乳液 10%-20%Acrylic self-crosslinking emulsion 10%-20%
润湿剂 0.1%-1%Wetting agent 0.1%-1%
成膜助剂 0.1%-1%Coalescing agent 0.1%-1%
乙醇 0.1%-1%Ethanol 0.1%-1%
炔二醇表面活性剂 0.1%-1%Alkyne diol surfactant 0.1%-1%
交联剂 0.1%-1%Cross-linking agent 0.1%-1%
手感助剂25 0.1%-1%Hand feeling additive 25 0.1%-1%
转印剂 0.5%-1.5%Transfer agent 0.5%-1.5%
其中色浆是由以下重量百分比的原料组成：Wherein color paste is made up of the raw material of following percentage by weight:
颜料 30%-50%Pigment 30%-50%
超分散剂SMA 2%-10%Hyperdispersant SMA 2%-10%
水 30%-50%Water 30%-50%
矿物油消泡剂 0.1%-1%Mineral oil defoamer 0.1%-1%
丙烯酸树脂液576 4%-22%Acrylic resin liquid 576 4%-22%
将颜料、超分散剂SMA、水、矿物油消泡剂、丙烯酸树脂液576混合物按比例混和均匀进行研磨分散，至颗粒粒度达300nm左右，制得色浆，然后按照上述重量百分比，将色浆、水性丙烯酸成膜乳液、丙烯酰胺高光泽乳液、丙烯酸自交联乳液、润湿剂、成膜助剂、乙醇、炔二醇表面活性剂、交联剂、手感助剂25、转印剂充分混合，搅拌均匀，即制得该水性柔版油墨，使用时利用水和乙醇作为稀释剂。Mix the mixture of pigment, hyperdispersant SMA, water, mineral oil defoamer, and acrylic resin liquid 576 in proportion, grind and disperse evenly, until the particle size reaches about 300nm, and prepare the color paste, and then mix the color paste according to the above weight percentage , water-based acrylic film-forming emulsion, acrylamide high-gloss emulsion, acrylic self-crosslinking emulsion, wetting agent, film-forming aid, ethanol, acetylenic glycol surfactant, cross-linking agent, hand additive 25, transfer agent fully Mixing and stirring evenly, the water-based flexographic ink is prepared, and water and ethanol are used as diluents during use.
本发明具有以下显著特点：The present invention has the following salient features:
(1) 发明所述水性柔版油墨，适用基材广，包括PET，PE，PC，铜版纸等；(1) The water-based flexographic ink described in the invention is applicable to a wide range of substrates, including PET, PE, PC, coated paper, etc.;
(2) 发明所述水性柔版油墨制备方法简单，无毒，无味，转移性和附着牢度良好；(2) The preparation method of the water-based flexographic ink described in the invention is simple, non-toxic, tasteless, good in transferability and adhesion fastness;
(3) 发明所述水性柔版油墨性能稳定，墨层光泽度高，手感好，具有良好的耐水性和耐候性。(3) The performance of the water-based flexographic ink described in the invention is stable, the gloss of the ink layer is high, the hand feeling is good, and it has good water resistance and weather resistance.
具体实施方式：detailed description:
下面以具体实施例对本发明作进一步的说明，但本发明不受下述实施例的限定。The present invention will be further described below with specific examples, but the present invention is not limited by the following examples.
实施例1：Example 1:
一种水性柔版油墨，它由以下重量比的原料组成：色浆为30%、水性丙烯酸成膜乳液为20%、丙烯酰胺高光泽乳液为30%、丙烯酸自交联乳液为16%、润湿剂为0.4%、成膜助剂为0.6%、乙醇为0.6%、炔二醇表面活性剂为0.4%、交联剂为0.6%、手感助剂25为0.4%、转印剂为1%；其中色浆是由以下重量百分比的原料组成：颜料黄Y-12为40%、超分散剂SMA为8%、水为41.6%、矿物油消泡剂为0.4%、丙烯酸树脂液576为10%；将颜料黄Y-12、超分散剂SMA、水、矿物油消泡剂、丙烯酸树脂液576混合物按比例混和均匀后进行研磨分散，至颗粒粒度达300nm左右，制得色浆，然后按照上述重量百分比，将色浆、水性丙烯酸成膜乳液、丙烯酰胺高光泽乳液、丙烯酸自交联乳液、润湿剂、成膜助剂、乙醇、炔二醇表面活性剂、交联剂、手感助剂25、转印剂充分混合，搅拌均匀，即制得该水性柔版油墨，使用时利用水和乙醇作为稀释剂。A water-based flexographic ink, which is composed of the following raw materials by weight: 30% of color paste, 20% of water-based acrylic film-forming emulsion, 30% of acrylamide high-gloss emulsion, 16% of acrylic self-crosslinking emulsion, emulsifier Wetting agent is 0.4%, film-forming aid is 0.6%, ethanol is 0.6%, acetylenic glycol surfactant is 0.4%, cross-linking agent is 0.6%, hand feeling aid 25 is 0.4%, transfer agent is 1% Wherein the color base is made up of the following raw materials in weight percentage: pigment yellow Y-12 is 40%, hyperdispersant SMA is 8%, water is 41.6%, mineral oil defoamer is 0.4%, acrylic resin liquid 576 is 10% %; Mix the mixture of pigment yellow Y-12, hyperdispersant SMA, water, mineral oil defoamer, and acrylic resin liquid 576 evenly in proportion, then grind and disperse until the particle size reaches about 300nm to prepare the color paste, and then follow In the above weight percentage, color paste, water-based acrylic film-forming emulsion, acrylamide high-gloss emulsion, acrylic self-crosslinking emulsion, wetting agent, film-forming aid, ethanol, acetylenic glycol surfactant, cross-linking agent, hand feeling aid Agent 25 and the transfer agent are fully mixed and stirred evenly to obtain the water-based flexographic ink, and water and ethanol are used as diluents during use.
实施例2：Example 2:
一种水性柔版油墨，它由以下重量比的原料组成：色浆为40%、水性丙烯酸成膜乳液为20%、丙烯酰胺高光泽乳液为20%、丙烯酸自交联乳液为15.4%、润湿剂为0.4%、成膜助剂为0.6%、乙醇为0.6%、炔二醇表面活性剂为0.4%、交联剂为0.6%、手感助剂25为1%、转印剂为1%；其中色浆是由以下重量百分比的原料组成：颜料红R-57：1为37.6%、超分散剂SMA为6%、水为45%、矿物油消泡剂为0.4%、丙烯酸树脂液576为11%；将颜料红R-57：1、超分散剂SMA、水、矿物油消泡剂、丙烯酸树脂液576混合物按比例混和均匀后进行研磨分散，至颗粒粒度达300nm左右，制得色浆，然后按照上述重量百分比，将色浆、水性丙烯酸成膜乳液、丙烯酰胺高光泽乳液、丙烯酸自交联乳液、润湿剂、成膜助剂、乙醇、炔二醇表面活性剂、交联剂、手感助剂25、转印剂充分混合，搅拌均匀，即制得该水性柔版油墨，使用时利用水和乙醇作为稀释剂。A water-based flexographic ink, which is composed of the following raw materials in weight ratio: 40% of color paste, 20% of water-based acrylic film-forming emulsion, 20% of acrylamide high-gloss emulsion, 15.4% of acrylic self-crosslinking emulsion, emulsifier 0.4% wet agent, 0.6% film-forming aid, 0.6% ethanol, 0.4% acetylenic glycol surfactant, 0.6% cross-linking agent, 1% hand feeling aid 25, and 1% transfer agent ; wherein the color paste is made up of the following raw materials in weight percentage: pigment red R-57: 1 is 37.6%, hyperdispersant SMA is 6%, water is 45%, mineral oil defoamer is 0.4%, acrylic resin liquid 576 11%; mix the mixture of pigment red R-57:1, hyperdispersant SMA, water, mineral oil defoamer, and acrylic resin liquid 576 evenly in proportion, then grind and disperse until the particle size reaches about 300nm. pulp, and then according to the above weight percentage, color paste, water-based acrylic film-forming emulsion, acrylamide high-gloss emulsion, acrylic self-crosslinking emulsion, wetting agent, film-forming aid, ethanol, acetylenic glycol surfactant, cross-linking agent, hand feeling aid 25, and transfer agent are fully mixed and stirred evenly to obtain the water-based flexographic ink, and water and ethanol are used as diluents during use.
实施例3：Example 3:
一种水性柔版油墨，它由以下重量比的原料组成：色浆为36%、水性丙烯酸成膜乳液为16.3%、丙烯酰胺高光泽乳液为29.7%、丙烯酸自交联乳液为14%、润湿剂为0.4%、成膜助剂为0.6%、乙醇为0.6%、炔二醇表面活性剂为0.4%、交联剂为0.6%、手感助剂25为0.4%、转印剂为1%；其中色浆是由以下重量百分比的原料组成：颜料蓝15：3为40%、超分散剂SMA为4%、水为33.6%、矿物油消泡剂为0.4%、丙烯酸树脂液576为22%；将颜料蓝15：3、超分散剂SMA、水、矿物油消泡剂、丙烯酸树脂液576混合物按比例混和均匀后进行研磨分散，至颗粒粒度达300nm左右，制得色浆，然后按照上述重量百分比，将色浆、水性丙烯酸成膜乳液、丙烯酰胺高光泽乳液、丙烯酸自交联乳液、润湿剂、成膜助剂、乙醇、炔二醇表面活性剂、交联剂、手感助剂25、转印剂充分混合，搅拌均匀，即制得该水性柔版油墨，使用时利用水和乙醇作为稀释剂。A water-based flexographic ink, which is composed of the following raw materials by weight: 36% of color paste, 16.3% of water-based acrylic film-forming emulsion, 29.7% of acrylamide high-gloss emulsion, 14% of acrylic self-crosslinking emulsion, emulsifier Wetting agent is 0.4%, film-forming aid is 0.6%, ethanol is 0.6%, acetylenic glycol surfactant is 0.4%, cross-linking agent is 0.6%, hand feeling aid 25 is 0.4%, transfer agent is 1% Wherein the color paste is made up of the following raw materials in weight percentage: pigment blue 15:3 is 40%, hyperdispersant SMA is 4%, water is 33.6%, mineral oil defoamer is 0.4%, acrylic resin liquid 576 is 22% %; Mix the mixture of pigment blue 15:3, hyperdispersant SMA, water, mineral oil defoamer, and acrylic resin liquid 576 evenly in proportion, then grind and disperse until the particle size reaches about 300nm, and prepare the color paste, and then follow In the above weight percentage, color paste, water-based acrylic film-forming emulsion, acrylamide high-gloss emulsion, acrylic self-crosslinking emulsion, wetting agent, film-forming aid, ethanol, acetylenic glycol surfactant, cross-linking agent, hand feeling aid Agent 25 and the transfer agent are fully mixed and stirred evenly to obtain the water-based flexographic ink, and water and ethanol are used as diluents during use.
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| CN (1) | CN106883676A (en) |
Cited By (3)
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| CN107974132A (en) * | 2017-12-07 | 2018-05-01 | 珠海华彩打印耗材有限公司 | One kind weaving digit printing ink mill base |
| CN109897318A (en) * | 2019-02-26 | 2019-06-18 | 盐城远东化工有限公司 | A kind of plastics liquid coloring agent and its preparation process |
| CN112796125A (en) * | 2020-12-26 | 2021-05-14 | 山东德创精化科技有限公司 | Aqueous flexographic printing material for Tyvek and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107974132A (en) * | 2017-12-07 | 2018-05-01 | 珠海华彩打印耗材有限公司 | One kind weaving digit printing ink mill base |
| CN109897318A (en) * | 2019-02-26 | 2019-06-18 | 盐城远东化工有限公司 | A kind of plastics liquid coloring agent and its preparation process |
| CN112796125A (en) * | 2020-12-26 | 2021-05-14 | 山东德创精化科技有限公司 | Aqueous flexographic printing material for Tyvek and preparation method thereof |
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Application publication date: 20170623 |