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CN106872309A - Method for measuring viscosity of micro sliding block surface contact lubricating oil - Google Patents

Method for measuring viscosity of micro sliding block surface contact lubricating oil Download PDF

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Publication number
CN106872309A
CN106872309A CN201710106604.8A CN201710106604A CN106872309A CN 106872309 A CN106872309 A CN 106872309A CN 201710106604 A CN201710106604 A CN 201710106604A CN 106872309 A CN106872309 A CN 106872309A
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viscosity
lubricating oil
slider
micro
film thickness
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郭峰
王茜
李超
栗心明
韩素立
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Qingdao University of Technology
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N11/00Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N11/00Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
    • G01N2011/006Determining flow properties indirectly by measuring other parameters of the system

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Abstract

本发明属于润滑油粘度测量技术领域,涉及一种微型滑块面接触润滑油粘度的测量方法,主要按照如下步骤进行:(1)试样的清洗;(2)安装微型滑块,安装与调平玻璃盘;(3)、固定接触副倾角α为恒定值;(4)、载荷的平衡和施加;(5)、绘制润滑油粘度η随出口处油膜厚度h的变化曲线图;本发明利用控制单一变量的方法,测量出已知粘度的几种润滑油的油膜厚度,找出膜厚与粘度之间的函数关系,该发明在测量油膜厚度的同时,能够间接得出润滑油的粘度,无需使用粘度计再测量粘度,节省工作时间,为指导润滑油的研究提供了方便,其原理简单可靠,操作方便,测量准确度高,能够适用于不同类型的润滑油粘度的测量,应用环境友好,市场前景广阔。

The invention belongs to the technical field of viscosity measurement of lubricating oil, and relates to a method for measuring the viscosity of lubricating oil in contact with the surface of a miniature slider, which is mainly carried out according to the following steps: (1) cleaning of the sample; Flat glass disc; (3), fixed contact sub-inclination angle α is a constant value; (4), balance and application of load; (5), draw lubricating oil viscosity η with the change curve figure of outlet oil film thickness h; The present invention utilizes The method of controlling a single variable measures the oil film thickness of several lubricating oils with known viscosities, and finds out the functional relationship between film thickness and viscosity. This invention can indirectly obtain the viscosity of lubricating oil while measuring the thickness of the oil film. There is no need to use a viscometer to measure the viscosity, which saves working time and provides convenience for guiding the research of lubricating oil. Its principle is simple and reliable, easy to operate, and has high measurement accuracy. It can be applied to the measurement of the viscosity of different types of lubricating oils and is environmentally friendly. ,Market prospects.

Description

一种微型滑块面接触润滑油粘度的测量方法A Method for Measuring the Viscosity of Lubricating Oil Contacted by Miniature Sliding Blocks

技术领域:Technical field:

本发明属于润滑油粘度测量技术领域,涉及一种润滑油粘度的测量方法,特别是一种微型滑块面接触润滑油粘度的测量方法,基于微型滑块面接触试验台,通过测量油膜厚度来间接测量润滑油粘度。The invention belongs to the technical field of lubricating oil viscosity measurement, and relates to a method for measuring the viscosity of lubricating oil, in particular to a method for measuring the viscosity of lubricating oil in contact with the surface of a miniature slider. Indirect measurement of lubricating oil viscosity.

背景技术:Background technique:

润滑油的粘度是流体动压润滑中最重要的物理特性之一,它既是评价油品的重要指标,也是研究润滑油各种特性时要涉及的重要因素之一。目前,实验中测量润滑油粘度的方法有很多,常用的方法有如下四种:The viscosity of lubricating oil is one of the most important physical properties in hydrodynamic lubrication. It is not only an important index for evaluating oil products, but also one of the important factors involved in studying various properties of lubricating oil. At present, there are many methods for measuring the viscosity of lubricating oil in experiments, and the commonly used methods are as follows:

1.毛细管方法1. Capillary method

测量原理:根据Hagen-Poiseuille定律,一定体积的液体在一定压力梯度下通过给定毛细管所需时间正比于层流液体的粘度,因此,通过测量液体流速和液体流经毛细管产生的压力差即可得出液体粘度;Measurement principle: According to the Hagen-Poiseuille law, the time required for a certain volume of liquid to pass through a given capillary under a certain pressure gradient is proportional to the viscosity of the laminar flow liquid. Therefore, by measuring the liquid flow rate and the pressure difference generated by the liquid flowing through the capillary. Find the viscosity of the liquid;

测量方法:实验采用的方法是通过测量一定体积的润滑油流过毛细血管的时间来计算η。流经细管的流量Q为从而得其中:V-t内流过毛细血管的体积;R-细管的半径;L-细管的长度;P-细管两端的压强差。这就是泊塞勒公式,但它是建立在理想情况下得出的公式,必须进行修正,最后:其中:m-动能修正系数;n-末端修正系数,其值在0~1.2之间;ρ-为流体密度。Measurement method: The method used in the experiment is to calculate η by measuring the time for a certain volume of lubricating oil to flow through the capillary. The flow Q through the thin tube is thus get Among them: the volume flowing through the capillary in Vt; R-the radius of the capillary; L-the length of the capillary; P-the pressure difference at both ends of the capillary. This is the Posseler formula, but it is based on the ideal formula and must be corrected. Finally: Among them: m-kinetic energy correction coefficient; n-terminal correction coefficient, its value is between 0 and 1.2; ρ-is the fluid density.

该方法的优点在于毛细管粘度计制造简单,价格较低,温度控制简单,实验操作方便,测量精度高,能够进行粘度的绝对测量,因此毛细管法是一种有吸引力的测量方法,但是该方法中的毛细管容易被小颗粒物堵塞,因此对样品纯度要求较高,还由于样品容易与毛细管发生反应,因此不适合高温下使用。The advantage of this method is that the capillary viscometer is easy to manufacture, low in price, simple in temperature control, convenient in experimental operation, high in measurement accuracy, and capable of absolute measurement of viscosity, so the capillary method is an attractive measurement method, but the method The capillary in the method is easily blocked by small particles, so the requirement for sample purity is high, and because the sample is easy to react with the capillary, it is not suitable for use at high temperature.

2.旋转法2. Rotation method

旋转式粘度计从结构上来划分主要分为两种:单圆桶旋转式粘度计和双圆桶旋转式粘度计,双圆筒旋转式粘度计有两个圆筒,它又可以分为内筒旋转式和外筒旋转式两种。Rotary viscometers are mainly divided into two types in terms of structure: single-cylinder rotary viscometers and double-cylinder rotary viscometers. Double-cylinder rotary viscometers have two cylinders, which can be divided into inner cylinders There are two types: rotary type and outer cylinder rotary type.

工作原理:单圆筒旋转式粘度计只有一个圆筒,由一台微型同步电动机带动上、下两个圆盘和圆筒一起旋转,由于受到流体的粘滞力作用,圆筒及与圆筒刚性连接的下盘的旋转将会滞后于上盘,从而使得弹性元件产生扭转,通过测量这个扭转来得到小圆筒所受到的粘性力矩M,再根据马克斯公式计算得到流体的粘度:式中:η—液体动力粘度,Pa·s;H—测量小圆筒浸于待测液体中的高度;Rf—小圆筒的半径;Ra待测液体容器的半径;M—粘性力矩;Ω—小圆筒旋转角速度。Working principle: The single-cylinder rotary viscometer has only one cylinder, and a miniature synchronous motor drives the upper and lower discs to rotate together with the cylinder. Due to the viscous force of the fluid, the cylinder and the cylinder The rotation of the rigidly connected lower plate will lag behind the upper plate, so that the elastic element will be twisted. By measuring this twist, the viscous moment M on the small cylinder can be obtained, and then the viscosity of the fluid can be calculated according to the Max formula: In the formula: η—liquid dynamic viscosity, Pa s; H—measuring the height of the small cylinder immersed in the liquid to be measured; R f —the radius of the small cylinder; R a the radius of the liquid container to be measured; M—viscous moment ; Ω—the rotational angular velocity of the small cylinder.

内筒旋转式粘度计测量时,外圆筒是用来盛被测液体的容器,固定不动,内圆筒为浸入被测流体中进行旋转的空心圆筒,与外圆筒同轴。驱动用的微型同步电动机的壳体采用悬挂式安装,通过转轴带动内圆筒以一定的速率旋转,内圆筒在被测流体中旋转时受到了粘滞阻力的作用,产生反作用迫使电机壳体偏转,电机壳体和两根一正一反安装的金属游丝相连,当壳体偏转时,使游丝产生扭转,当游丝的扭矩与粘滞阻力力矩达到平衡时,与电动机壳体相连接的指针便在刻度盘上指出某一数值。此数值与转筒所受的粘滞阻力成正比。因此,将刻度读数乘上特定系数F(即转筒因子),就表示成粘滞系数的量值。When measuring with an inner cylinder rotary viscometer, the outer cylinder is a container for the liquid to be measured, which is fixed, and the inner cylinder is a hollow cylinder immersed in the fluid to be measured and rotated, coaxial with the outer cylinder. The shell of the miniature synchronous motor used for driving is installed in a suspended type, and the inner cylinder is driven to rotate at a certain speed through the rotating shaft. body deflection, the motor casing is connected with two metal hairsprings installed one positive and the other reversely installed, when the casing deflects, the hairspring will be twisted, and when the torque of the hairspring and the viscous resistance torque reach a balance, it will be connected with the motor casing The pointer will indicate a certain value on the dial. This value is proportional to the viscous resistance experienced by the drum. Therefore, the scale reading is multiplied by a specific coefficient F (that is, the drum factor), which is expressed as the value of the viscosity coefficient.

外筒旋转式粘度计测量时将内、外圆筒都浸入被测流体中,由电动机带动外圆筒以一定的速率进行旋转,内圆筒由于受到两圆筒之间的被测流体的粘滞力作用而发生偏转,与内圆筒相连的张丝扭转所产生的恢复力矩与粘滞力矩的方向相反,当张丝的恢复力矩和粘滞力矩达到平衡时,内圆筒的偏转角θ大小与引起粘滞力矩的粘滞系数η成正比。由此推导出粘滞系数η和偏转角θ的函数关系[η=f(θ)],即可通过测量内圆筒的偏转角θ来计算出粘滞系数值η。When measuring the external cylinder rotary viscometer, both the inner and outer cylinders are immersed in the measured fluid, and the motor drives the outer cylinder to rotate at a certain speed. Due to the viscosity of the measured fluid between the two cylinders, the inner cylinder The deflection occurs due to the action of the hysteresis force, and the restoring moment generated by the torsion of the wire connected to the inner cylinder is opposite to the direction of the viscous moment. When the restoring moment and the viscous moment of the tensioning wire are balanced, the deflection angle θ The size is proportional to the viscosity coefficient η that causes the viscous moment. From this, the functional relationship [η=f(θ)] between the viscosity coefficient η and the deflection angle θ is derived, and the value of the viscosity coefficient η can be calculated by measuring the deflection angle θ of the inner cylinder.

该方法的优点在于单圆筒旋转式粘度计结构简单,便于安装,因此适用于流体粘度的在线测量,同时单圆筒旋转式粘度计具有较高的测量精度,较快的响应速度,较低的生产成本,是一种比较理想的在线粘度计,便于在生产过程中对产品粘度进行随时监测及控制。内筒旋转式粘度计是最普通的一种旋转式粘度计,从它的结构以及运转方式来看,它主要用于流体粘度的离线式测量,如在实验室中测量采样流体的粘度值,而外筒旋转式粘度计同单圆简旋转式粘度计一样,直接读数手动计算很麻烦。The advantage of this method is that the single-cylinder rotary viscometer has a simple structure and is easy to install, so it is suitable for on-line measurement of fluid viscosity. At the same time, the single-cylinder rotary viscometer has high measurement accuracy, fast response speed, and low It is an ideal online viscometer, which is convenient for monitoring and controlling the product viscosity at any time during the production process. The inner cylinder rotary viscometer is the most common rotary viscometer. From its structure and operation mode, it is mainly used for off-line measurement of fluid viscosity, such as measuring the viscosity value of sampled fluid in the laboratory. The external cylinder rotary viscometer is the same as the single-circle rotary viscometer, and it is very troublesome to read directly and calculate manually.

3.振动法测量3. Vibration measurement

振动法测量方式较多,有扭转振动式,振动片式等,常用的为扭转振动式测量,包括衰减振动式和强制振动式。There are many measurement methods of vibration method, such as torsional vibration type, vibrating plate type, etc. The commonly used one is torsional vibration type measurement, including damping vibration type and forced vibration type.

测量原理:衰减振动式基于浸于润滑油中作扭转振动的物体由于受到润滑油施加的粘性力,其扭转振幅会衰减,测量出振幅衰减情况和衰减周期,即可通过相应公式计算出液体粘度;强制振动式的测量原理是由外界补充振动物体由于粘性所损耗的能量,使振动物体维持恒定振动频率和振幅,由所补充的能量和润滑油粘度之间的关系计算粘度值。Measuring principle: The attenuation vibration method is based on the torsional vibration of the object immersed in lubricating oil. Due to the viscous force exerted by the lubricating oil, the torsional amplitude will attenuate. After measuring the amplitude attenuation and attenuation period, the liquid viscosity can be calculated through the corresponding formula. The measurement principle of the forced vibration type is to supplement the energy lost by the vibrating object due to the viscosity from the outside, so that the vibrating object maintains a constant vibration frequency and amplitude, and the viscosity value is calculated from the relationship between the added energy and the viscosity of the lubricating oil.

该方法的优点在于振动法常用于低粘度液体的粘度测量,因此该方法主要适用于多数熔体粘度测量,振动法的优点在于振动周期和衰减测量方便、样品用量少、控温方便,但是没有公认的理想粘度计算公式。The advantage of this method is that the vibration method is often used in the viscosity measurement of low-viscosity liquids, so this method is mainly suitable for the viscosity measurement of most melts. The advantages of the vibration method are that the vibration period and attenuation measurement are convenient, the sample consumption is small, and the temperature control is convenient, but There is no generally accepted formula for calculating ideal viscosity.

4.落球法4. Drop ball method

测量原理:球体或柱体在被测液体中下落,通过测量落体通过两定点所用的时间来测定粘度,也可以让球体滚动通过倾斜的平面。Measuring principle: The sphere or cylinder falls in the measured liquid, and the viscosity is measured by measuring the time it takes for the falling body to pass through two fixed points, or the sphere can be rolled through an inclined plane.

该方法的优点在于落球法原则上可以测定绝对粘度,由于不同的液体的粘性系数相差很大,同一种液体随着温度的不同粘性系数的变化有的也很大,所以还要考虑小球的直径与容积的尺度之比要满足实验的要求,因此,符合实验条件的小球直径范围也将变化。由于采用手控停表计时和由于人的视觉暂留效应的影响,小球下落的速度要尽可能的慢。采用相同原理的粘度计有滚动落球粘度计,圆柱落下粘度计和落体式连续粘度计等。The advantage of this method is that the falling ball method can measure the absolute viscosity in principle. Since the viscosity coefficients of different liquids vary greatly, and the viscosity coefficient of the same liquid varies greatly with different temperatures, the small ball should also be considered. The scale ratio of diameter to volume must meet the requirements of the experiment, therefore, the diameter range of the small balls that meet the experimental conditions will also vary. Due to the adoption of manual stop watch timing and due to the impact of people's visual persistence effect, the speed of the ball falling will be as slow as possible. Viscometers using the same principle include rolling falling ball viscometer, cylindrical falling viscometer and falling continuous viscometer.

因此,设计制备一种微型滑块面接触润滑油粘度的测量方法,该方法以青岛理工大学设计研发的微型滑块轴承润滑油膜测量仪及其滑块调节方法(专利号为ZL200810249672.0)中的实验设备为基础,能够设定并且调节微滑块工作平面与透明光学圆盘之间倾角α,这为面接触润滑油粘度测量方法提供了实验硬件基础。Therefore, a method for measuring the viscosity of lubricating oil in contact with the surface of a miniature slider is designed and prepared. This method is based on the miniature slider bearing lubricating oil film measuring instrument and its slider adjustment method (patent number ZL200810249672.0) designed and developed by Qingdao University of Technology. Based on the experimental equipment, it can set and adjust the inclination α between the working plane of the micro-slider and the transparent optical disc, which provides the experimental hardware basis for the surface contact lubricant viscosity measurement method.

发明内容:Invention content:

本发明的目的在于克服现有技术存在的缺点,寻求设计提供一种微型滑块面接触润滑油粘度的测量新方法,在一定载荷下以静止的微型滑块平面和旋转的光学透明圆盘平面形成低压流体动压润滑油膜,利用光干涉技术对润滑油膜的厚度进行测量,根据流体动压润滑理论,润滑油粘度越高,油膜厚度越大,通过测量部分润滑油的油膜厚度,找出膜厚与粘度之间的函数关系,进而间接得出任意膜厚下润滑油的粘度。The purpose of the present invention is to overcome the shortcomings of the prior art, and seek to design a new method for measuring the viscosity of lubricating oil in contact with the surface of a miniature slider. Form a low-pressure fluid dynamic pressure lubricating oil film, and use optical interference technology to measure the thickness of the lubricating oil film. According to the theory of hydrodynamic pressure lubrication, the higher the viscosity of the lubricating oil, the greater the thickness of the oil film. By measuring the thickness of the oil film of part of the lubricating oil, find the film The functional relationship between thickness and viscosity, and then indirectly obtain the viscosity of lubricating oil at any film thickness.

为了实现上述目的,本发明所述的微型滑块面接触润滑油粘度的测量方法是在微型滑块轴承润滑油膜测量仪中完成,其主体结构包括:滑块固定单元、玻璃盘回转单元、光干涉系统、加载装置和机架底盘;滑块固定单元的主要部件包括微型滑块,玻璃盘回转单元的主要部件包括玻璃盘,光干涉系统的主要部件为同轴照明设备和位于玻璃盘下部的显微镜,加载装置的主要部件为加载杠杆和调节螺钉;面接触润滑副由光学透明玻璃圆盘和微型滑块组成,将滑块固定在玻璃盘的上方,滑块作为润滑副的上表面,工作面高精度反光处理,玻璃盘为下表面,其中玻璃盘旋转,滑块静止,能够通过倾角调节装置改变滑块与玻璃盘表面间的倾斜角度,光干涉条纹的数量和条纹的倾斜角度可以反映出微型滑块和玻璃盘之间的倾斜角度,通过调节不同位置的调节螺杆,改变干涉条纹的数量和倾斜角度,进而达到改变倾角大小和方向的目的,并在玻璃盘的转动过程中保持该倾角的大小和方向不发生变化,从而保证实验的稳定性;由加载装置对两平面施加载荷,当玻璃盘以一定的角速度旋转时,将润滑油卷吸入两平面间形成润滑油膜,油膜厚度由玻璃盘下方的光干涉测量系统测得,该系统利用多光束干涉法进行油膜厚度的计算,实验过程中红光平行入射到微型滑块、润滑油和透明玻璃盘组成的多层界面系统,经过多次投射和反射,相干光束形成接触区对应的明暗相间的干涉条纹,通过干涉条纹强度和极次推断接触区油膜厚度情况。具体测量方法按如下步骤进行:In order to achieve the above object, the method for measuring the viscosity of lubricating oil in contact with the surface of the miniature slider of the present invention is completed in a miniature slider bearing lubricating oil film measuring instrument, and its main structure includes: a slider fixing unit, a glass disk rotating unit, Interference system, loading device and rack chassis; the main components of the slider fixing unit include micro-sliders, the main components of the glass disc rotation unit include glass discs, the main components of the light interference system are coaxial lighting equipment and the Microscope, the main components of the loading device are the loading lever and the adjusting screw; the surface contact lubrication pair is composed of an optically transparent glass disc and a miniature slider, the slider is fixed above the glass disc, and the slider is used as the upper surface of the lubrication pair. Surface high-precision reflective treatment, the glass disc is the lower surface, the glass disc rotates, the slider is stationary, the inclination angle between the slider and the surface of the glass disc can be changed by the tilt angle adjustment device, the number of light interference fringes and the inclination angle of the fringes can reflect The inclination angle between the micro-slider and the glass plate can be adjusted by adjusting the adjusting screw at different positions to change the number and inclination angle of interference fringes, thereby achieving the purpose of changing the size and direction of the inclination angle, and maintaining the inclination angle during the rotation of the glass plate. The size and direction of the inclination angle do not change, so as to ensure the stability of the experiment; the load is applied to the two planes by the loading device, and when the glass disk rotates at a certain angular speed, the lubricating oil is sucked into the two planes to form a lubricating oil film, and the thickness of the oil film is determined by Measured by the optical interferometry system under the glass disk, the system uses multi-beam interferometry to calculate the thickness of the oil film. After multiple projections and reflections, the coherent light beam forms light and dark interference fringes corresponding to the contact area, and the thickness of the oil film in the contact area is inferred from the intensity and polarity of the interference fringes. The specific measurement method is carried out as follows:

(1)、试样的清洗:(1) Cleaning of the sample:

在试验开始之前对微型滑块(L-长,B-宽)和玻璃圆盘进行清洗,用以防止细微颗粒的吸附导致润滑油油膜厚度测量的不准确,具体工艺步骤为先将微型滑块和玻璃盘用洗手液去除表面的油污等杂质,在油污不易去除的特殊情况下,则采用丙酮、石油醚或其他强有机溶剂进行清洗;然后将清洗后的微型滑块和玻璃盘放入无水乙醇中超声清洗3-5分钟,最后用高压氮气或压缩空气将清洗后的微型滑块和玻璃盘吹干;Before the start of the test, the micro-slider (L-length, B-width) and the glass disc are cleaned to prevent the adsorption of fine particles from causing inaccurate measurement of the lubricating oil film thickness. The specific process steps are to first clean the micro-slider Use hand sanitizer to remove oil stains and other impurities on the surface, and in special cases where the oil stains are not easy to remove, use acetone, petroleum ether or other strong organic solvents to clean; Ultrasonic cleaning in water and ethanol for 3-5 minutes, and finally dry the cleaned micro-slides and glass discs with high-pressure nitrogen or compressed air;

(2)、安装微型滑块,安装与调平玻璃盘:(2), install the micro-slider, install and level the glass plate:

先将微型滑块安装在微型滑块轴承润滑油膜测量仪上,再安装玻璃盘,安装玻璃盘时依次旋转其表面8颗定位螺钉至轻微旋紧,在安装时应防止玻璃盘的磕伤并避免玻璃盘表面被污染,由微型滑块和玻璃盘组成面接触副,在玻璃盘上添加待测润滑油,确定待测润滑油的动力粘度η及折射率n,其中润滑油的动力粘度η由粘度计测量获得,待测润滑油的折射率n由阿贝折射仪确定;然后,使用千分表对玻璃盘进行调平,使其端面跳动在3μm以内;First install the miniature slider on the miniature slider bearing lubricating oil film measuring instrument, and then install the glass plate. When installing the glass plate, turn the 8 positioning screws on its surface in turn until they are slightly tightened. During installation, the glass plate should be prevented from being damaged and damaged. To avoid contamination of the surface of the glass disc, the surface contact pair is composed of a micro-slider and a glass disc. Add the lubricating oil to be tested on the glass disc to determine the dynamic viscosity η and refractive index n of the lubricating oil to be tested, where the dynamic viscosity η of the lubricating oil is Measured by a viscometer, the refractive index n of the lubricating oil to be tested is determined by an Abbe refractometer; then, use a dial gauge to level the glass disc so that the runout of the end face is within 3 μm;

(3)、固定接触副倾角α为恒定值:(3) The inclination angle α of the fixed contact pair is a constant value:

波长为λ的红光经同轴照明设备输入显微镜照射在微型滑块和玻璃盘形成的楔形间隙上形成干涉图像,通过调节8颗调节螺钉确定干涉图像条纹的数目N,由倾角计算公式确定此时微型滑块和玻璃盘之间的倾斜角度α;对压环上的8颗定位螺钉进行微调,来控制倾角的动态平衡,使得回转过程中倾角不发生变化,其中α为微型滑块倾角,rad;λ为光源的波长,m;N为条纹数;n为润滑介质的折射率;B为微型滑块宽度,m;The red light with a wavelength of λ enters the microscope through the coaxial lighting device and irradiates on the wedge-shaped gap formed by the micro-slider and the glass disc to form an interference image. The number N of interference image fringes is determined by adjusting 8 adjustment screws, and the inclination angle is calculated by the formula Determine the inclination angle α between the micro-slider and the glass plate at this time; fine-tune the 8 positioning screws on the pressure ring to control the dynamic balance of the inclination angle so that the inclination angle does not change during the rotation process, where α is the micro-slider Inclination angle, rad; λ is the wavelength of the light source, m; N is the number of stripes; n is the refractive index of the lubricating medium; B is the width of the micro-slider, m;

(4)、载荷的平衡和施加:(4), load balance and application:

通过调节弹簧可平衡整个加载的自重,一般地,认为当干涉图像若有若无时即完成了自重的平衡,然后施加实验要求的载荷w,实验过程中施加的载荷固定不变;The self-weight of the entire load can be balanced by adjusting the spring. Generally, it is considered that the balance of the self-weight is completed when the interference image is present or absent, and then the load w required by the experiment is applied, and the load applied during the experiment is fixed;

(5)、绘制出口处润滑油粘度η随油膜厚度h变化的曲线图:(5), draw the curve graph that the lubricating oil viscosity η at the outlet changes with the oil film thickness h:

上述步骤(3)中形成的干涉图像通过显微镜放大投射到CCD(图像控制器)上,经CCD和图像采集卡的处理在电脑屏幕上显示出放大干涉图像;将放大干涉图像处理转换成光强曲线,由光强曲线得出干涉级次,利用干涉级次与润滑油膜厚度之间的关系计算出口处润滑油油膜厚度h;在接触副的夹角α=α1,速度ud=u1,载荷w=w1的条件下,测量已知粘度的几种润滑油的油膜厚度,然后将所测润滑油的粘度和油膜厚度的数据点用origin或其他函数绘图软件绘制出粘度η随油膜厚度h的变化曲线图,然后得出拟合曲线,最后根据上述已知数据关系推算得到粘度的计算公式:The interference image formed in the above step (3) is enlarged and projected onto the CCD (image controller) through the microscope, and the enlarged interference image is displayed on the computer screen through the processing of the CCD and the image acquisition card; the enlarged interference image is processed and converted into light intensity Curve, the interference order is obtained from the light intensity curve, and the lubricating oil film thickness h at the outlet is calculated by using the relationship between the interference order and the lubricating oil film thickness; the included angle α=α 1 of the contact pair, the speed u d =u 1 , under the condition of load w=w 1 , measure the oil film thickness of several lubricating oils with known viscosities, and then use origin or other function drawing software to draw the viscosity η with oil film The change curve of the thickness h, and then draw the fitting curve, and finally calculate the viscosity calculation formula according to the above-mentioned known data relationship:

η0=10χ η 0 =10 χ

χ=2.15062·logh+1.71367。χ=2.15062·logh+1.71367.

进一步的,所述玻璃盘为K9玻璃盘,玻璃盘在工作表面一侧镀有铬膜和二氧化硅膜(Cr+SiO2),用以获得清晰的干涉条纹,同时将反射率控制在18-22%左右,以保证干涉条纹对比度,表面粗糙度Ra为4nm。Further, the glass disc is a K9 glass disc, and the glass disc is plated with chrome film and silicon dioxide film (Cr+SiO 2 ) on one side of the working surface to obtain clear interference fringes while controlling the reflectivity at 18 -22% or so to ensure the contrast of interference fringes, the surface roughness R a is 4nm.

进一步的,所用微型滑块的尺寸为4×4mm,微型滑块的工作表面为高反射率的精密研抛表面,表面粗糙度为Ra=8~10nm,试验在受控的环境中进行,温度控制在20±0.5℃,湿度控制在30±5%。Further, the size of the micro-slider used is 4×4mm, the working surface of the micro-slider is a high-reflectivity precision polishing surface, the surface roughness is Ra = 8-10nm, and the test is carried out in a controlled environment. The temperature is controlled at 20±0.5°C, and the humidity is controlled at 30±5%.

本发明与现有技术相比,利用控制单一变量的方法,固定玻璃盘旋转速度ud,滑块倾角α,施加的载荷w,测量出已知粘度的几种润滑油的油膜厚度,根据流体动压润滑理论,粘度越高,油膜厚度越大,找出膜厚与粘度之间的函数关系,如此实现了只要在能够测量的范围内,就可以根据所得公式得知任意膜厚下的润滑油粘度。该方法在测量油膜厚度的同时,能够间接得出润滑油的粘度,无需使用粘度计再测量润滑油粘度,节省了工作量和时间,为指导润滑油的研究提供了方便,其原理简单可靠,操作方便,测量准确度高,能够适用于不同类型的润滑油粘度的测量,应用环境友好,市场前景广阔。Compared with the prior art, the present invention uses the method of controlling a single variable, fixes the rotation speed u d of the glass disc, the inclination angle α of the slider, and the applied load w, and measures the oil film thickness of several lubricating oils with known viscosities. The theory of dynamic pressure lubrication, the higher the viscosity, the greater the thickness of the oil film, find out the functional relationship between film thickness and viscosity, so that as long as it is within the range that can be measured, the lubrication under any film thickness can be known according to the obtained formula oil viscosity. This method can indirectly obtain the viscosity of the lubricating oil while measuring the thickness of the oil film. It does not need to use a viscometer to measure the viscosity of the lubricating oil, which saves workload and time, and provides convenience for guiding the research of lubricating oil. The principle is simple and reliable. The operation is convenient, the measurement accuracy is high, it can be applied to the measurement of the viscosity of different types of lubricating oils, the application environment is friendly, and the market prospect is broad.

附图说明:Description of drawings:

图1为本发明涉及的所用实验装置的主体原理示意图。Fig. 1 is a schematic diagram of the main body principle of the experimental device used in the present invention.

图2为本发明涉及的固定玻璃盘旋转速度ud,滑块倾角α,施加的载荷w条件下,润滑油粘度随出口处油膜厚度h的变化曲线图。Fig. 2 is a curve diagram of the variation of lubricating oil viscosity with the oil film thickness h at the outlet under the conditions of rotation speed ud of the fixed glass disk, slider inclination α, and applied load w in the present invention.

具体实施方式:detailed description:

下面通过实施例并结合附图对本发明做进一步说明。The present invention will be further described below through the embodiments and in conjunction with the accompanying drawings.

实施例:Example:

本实施例在微型滑块轴承润滑油膜测量仪中完成,其主体结构包括微型滑块1、玻璃盘2、加载杠杆3、调节螺钉4、分束器5、载荷6、入口和7、出口8;玻璃盘2用于与微型滑块1接触形成面接触副,调节8颗调节螺钉4与压环上的8颗定位螺钉来控制倾角的动态平衡,使得回转过程中倾角不发生变化,加载杠杆3为微型滑块轴承润滑油膜测量试验台中加载单元的一部分,用于润滑工作表面载荷的施加,通过调节弹簧平衡整个加载的自重。本实施例中微型滑块的尺寸为4×4mm、所施加的载荷w=4N,条纹数控制在10个条纹,速度取ud=15.39mm/s,待测润滑油的动力粘度η及折射率n实验前已提前确定。测量所用润滑油特性见表1,通过实验确定不同油膜厚度下的润滑油粘度;具体测量方法按如下步骤进行:This embodiment is completed in a miniature slider bearing lubricating oil film measuring instrument, and its main structure includes a miniature slider 1, a glass disc 2, a loading lever 3, an adjustment screw 4, a beam splitter 5, a load 6, an inlet and 7, and an outlet 8 ; The glass disc 2 is used to contact the miniature slider 1 to form a surface contact pair, adjust the 8 adjusting screws 4 and the 8 positioning screws on the pressure ring to control the dynamic balance of the inclination angle, so that the inclination angle does not change during the rotation, and the load lever 3 is a part of the loading unit in the miniature slider bearing lubricating oil film measurement test bench, which is used to apply the load on the lubricated working surface, and balance the self-weight of the entire load by adjusting the spring. In this embodiment, the size of the miniature slider is 4×4mm, the applied load w=4N, the number of stripes is controlled at 10 stripes, the speed is taken as u d =15.39mm/s, the dynamic viscosity η and refraction of the lubricating oil to be measured The rate n has been determined in advance before the experiment. The characteristics of the lubricating oil used in the measurement are shown in Table 1, and the viscosity of the lubricating oil under different oil film thicknesses is determined through experiments; the specific measurement method is carried out as follows:

(1)、试样的清洗:(1) Cleaning of the sample:

在试验开始之前对微型滑块1和玻璃盘2进行清洗,用以防止细微颗粒的吸附导致润滑油油膜厚度测量的不准确,具体工艺步骤为先将滑块1和玻璃盘2用洗手液去除表面的油污等杂质,在油污不易去除的特殊情况下,则采用丙酮、石油醚或其他强有机溶剂进行清洗;然后将清洗后的微型滑块1和玻璃盘2放入无水乙醇中超声清洗3-5分钟,最后用高压氮气或压缩空气将清洗后的微型滑块1和玻璃盘2吹干;Clean the micro-slider 1 and the glass disc 2 before the start of the test to prevent the inaccurate measurement of the lubricating oil film thickness caused by the adsorption of fine particles. The specific process steps are to first remove the slider 1 and the glass disc 2 with hand sanitizer In special cases where oil stains and other impurities on the surface are difficult to remove, use acetone, petroleum ether or other strong organic solvents to clean; then put the cleaned micro slide 1 and glass disc 2 into absolute ethanol for ultrasonic cleaning 3-5 minutes, finally use high-pressure nitrogen or compressed air to dry the cleaned micro-slide 1 and glass disc 2;

(2)安装微型滑块,安装与调平玻璃盘:(2) Install the micro-slider, install and level the glass plate:

先将微型滑块1安装在微型滑块1轴承润滑油膜测量仪上,再安装玻璃盘2,安装玻璃盘2时依次旋转其表面8颗定位螺钉至轻微旋紧,在安装时应防止玻璃盘2的磕伤并避免玻璃盘2表面被污染。由微型滑块1和玻璃盘2组成面接触副,在玻璃盘2上添加待测润滑油,待测润滑油的动力粘度及折射率n如下表1,动力粘度η由粘度计测量获得,折射率n由阿贝折射仪测得;然后,使用千分表对玻璃盘2进行调平,使其端面跳动在3μm以内;First install the miniature slider 1 on the lubricating oil film measuring instrument of the miniature slider 1 bearing, and then install the glass plate 2. When installing the glass plate 2, turn the 8 positioning screws on its surface in turn until slightly tightened. During installation, the glass plate should be prevented from 2 and prevent the surface of the glass plate 2 from being polluted. The surface contact pair is composed of a micro-slider 1 and a glass disc 2, and the lubricating oil to be tested is added to the glass disc 2. The dynamic viscosity and refractive index n of the lubricating oil to be tested are shown in Table 1. The dynamic viscosity η is measured by a viscometer, and the refractive index The ratio n is measured by an Abbe refractometer; then, use a dial gauge to level the glass disc 2 so that the runout of the end face is within 3 μm;

(3)、固定接触副倾角α为恒定值:(3) The inclination angle α of the fixed contact pair is a constant value:

波长为λ=650nm的红光经玻璃盘2下部的同轴照明设备输入显微镜照射在微型滑块1和玻璃盘2形成的楔形间隙上形成干涉图像;通过调节8颗调节螺钉将干涉条纹的数目N保持在10条,由倾角计算公式确定此时接触副的夹角α=1:1781,其中折射率n取1.447;对压环上的8颗定位螺钉进行微调,来控制倾角的动态平衡,使得回转过程中倾角不发生变化;The red light with a wavelength of λ=650nm enters the microscope through the coaxial lighting device at the bottom of the glass disc 2 and irradiates on the wedge-shaped gap formed by the micro-slider 1 and the glass disc 2 to form an interference image; the number of interference fringes is adjusted by adjusting 8 adjustment screws. N is kept at 10, calculated by the inclination formula Determine the angle α=1:1781 of the contact pair at this time, where the refractive index n is 1.447; fine-tune the 8 positioning screws on the pressure ring to control the dynamic balance of the inclination angle, so that the inclination angle does not change during the rotation;

(4)、载荷的平衡和施加:(4), load balance and application:

通过加载单元中的加载杠杆3和调节弹簧平衡掉整个加载的自重,当干涉条纹若有若无时即完成了自重的平衡,然后施加载荷w=4N,实验过程中施加的载荷6固定不变;The self-weight of the entire loading is balanced by the loading lever 3 and the adjustment spring in the loading unit. When the interference fringes are present or absent, the self-weight balance is completed, and then the load w=4N is applied, and the load 6 applied during the experiment is fixed. ;

(5)、绘制润滑油粘度η随出口处油膜厚度h的变化曲线图:(5), drawing the change curve of lubricating oil viscosity η with the oil film thickness h at the outlet:

上述步骤(3)中形成的干涉图像通过显微镜放大投射到CCD(图像控制器)上,经CCD和图像采集卡的处理在电脑屏幕上显示出放大干涉图像;将放大干涉图像处理转换成光强曲线,由光强曲线得出干涉级次,利用干涉级次与润滑油膜厚度之间的关系计算出口处润滑油膜厚度h;The interference image formed in the above step (3) is enlarged and projected onto the CCD (image controller) through the microscope, and the enlarged interference image is displayed on the computer screen through the processing of the CCD and the image acquisition card; the enlarged interference image is processed and converted into light intensity Curve, the interference order is obtained from the light intensity curve, and the lubricating oil film thickness h at the outlet is calculated using the relationship between the interference order and the lubricating oil film thickness;

在接触副的夹角α=1:1781,速度ud=15.39mm/s,载荷w=4N的条件下,测得已知粘度的几种润滑油的油膜厚度,其具体数值如下1所示:Under the conditions of contact angle α=1:1781, speed u d =15.39mm/s, and load w=4N, the oil film thickness of several lubricating oils with known viscosity is measured, and the specific values are shown in the following 1 :

表1M系列润滑油特性(22℃)Table 1M series lubricating oil characteristics (22°C)

将上述表1的实验数据M1、M2、M3、M4、M6润滑油的5对数据点用origin或其他函数绘图软件绘制出粘度η随油膜厚度h的变化曲线图,然后得出拟合曲线,如图2所示,由此得到粘度的计算公式(1):5 pairs of data points of the experimental data M1, M2, M3, M4, M6 lubricating oil in the above table 1 are drawn with origin or other function drawing software to draw the change curve of the viscosity η with the thickness of the oil film h, and then draw the fitting curve, As shown in Figure 2, thus obtain the calculation formula (1) of viscosity:

η0=10χ η 0 =10 χ

χ=2.15062·logh+1.71367 (1)χ=2.15062·logh+1.71367 (1)

将M5润滑油的膜厚带入拟合函数,η=151.645mPa·s,与实际测量值误差为3%,误差在允许范围内。Bringing the film thickness of M5 lubricating oil into the fitting function, η=151.645mPa·s, the error with the actual measured value is 3%, and the error is within the allowable range.

为了验证拟合函数的可靠性,测得了P系列润滑油的特性,如表2所示,利用所得公式(1)计算出了理论粘度η0,经验证实测粘度与理论粘度之间误差很小,在允许的范围内,证明了利用拟合函数计算任意膜厚下对应的粘度的可靠性。In order to verify the reliability of the fitting function, the characteristics of the P series lubricating oil were measured, as shown in Table 2, the theoretical viscosity η 0 was calculated using the obtained formula (1), and the error between the measured viscosity and the theoretical viscosity was proved to be very small , within the allowable range, it proves the reliability of using the fitting function to calculate the corresponding viscosity under any film thickness.

表2 P系列润滑油的特性(22℃)Table 2 Characteristics of P series lubricating oil (22°C)

针对测得的曲线可以利用插值法获得任意值,如图2所示,理论膜厚-粘度曲线与实验膜厚-粘度曲线在趋势上有很好的一致性,误差在4%以内,由此我们可以得出,通过测量润滑油的膜厚间接得出润滑油粘度的这种方法具有可行性。For the measured curve, any value can be obtained by interpolation method, as shown in Figure 2, the theoretical film thickness-viscosity curve and the experimental film thickness-viscosity curve have a good consistency in trend, and the error is within 4%. We can conclude that it is feasible to obtain the viscosity of lubricating oil indirectly by measuring the film thickness of lubricating oil.

以上所述,仅是对本发明的实施例而已,并非是对本发明做其他形式的限制,任何熟悉本专业的技术人员可能利用上述揭示的技术内容加以变更或改型为等同变化的等效实施例。但是,凡是未脱离本发明方案内容,依据本发明的技术实质对以上实施例所做的任何简单修改、等同变化与改型,仍属于本发明的保护范围。The above is only an embodiment of the present invention, and is not intended to limit the present invention in other forms. Any skilled person who is familiar with this field may use the technical content disclosed above to change or modify it into an equivalent embodiment with equivalent changes. . However, any simple modifications, equivalent changes and modifications made to the above embodiments according to the technical essence of the present invention still belong to the protection scope of the present invention, as long as they do not depart from the content of the solution of the present invention.

Claims (3)

1.一种微型滑块面接触润滑油粘度的测量方法,该方法是在微型滑块轴承润滑油膜测量仪中完成,其特征在于具体测量方法按如下步骤进行:1. A method for measuring the viscosity of a miniature slider surface contact lubricating oil, the method is completed in a miniature slider bearing lubricating oil film measuring instrument, and it is characterized in that the specific measurement method is carried out as follows: (1)、试样的清洗:(1) Cleaning of the sample: 在试验开始之前对微型滑块和玻璃圆盘进行清洗,用以防止细微颗粒的吸附导致润滑油油膜厚度测量的不准确,具体工艺步骤为先将微型滑块和玻璃盘用洗手液去除表面的油污等杂质,在油污不易去除的特殊情况下,则采用丙酮、石油醚或其他强有机溶剂进行清洗;然后将清洗后的微型滑块和玻璃盘放入无水乙醇中超声清洗3-5分钟,最后用高压氮气或压缩空气将清洗后的微型滑块和玻璃盘吹干;Clean the micro-slider and glass disc before the start of the test to prevent the inaccurate measurement of lubricating oil film thickness caused by the adsorption of fine particles. For impurities such as oil stains, in special cases where oil stains are not easy to remove, use acetone, petroleum ether or other strong organic solvents to clean; then put the cleaned micro-slides and glass discs into absolute ethanol for ultrasonic cleaning for 3-5 minutes , and finally dry the cleaned micro-slides and glass discs with high-pressure nitrogen or compressed air; (2)、安装微型滑块,安装与调平玻璃盘:(2), install the micro-slider, install and level the glass plate: 先将微型滑块安装在微型滑块轴承润滑油膜测量仪上,再安装玻璃盘,安装玻璃盘时依次旋转其表面8颗定位螺钉至轻微旋紧,在安装时应防止玻璃盘的磕伤并避免玻璃盘表面被污染,由微型滑块和玻璃盘组成面接触副,在玻璃盘上添加待测润滑油,确定待测润滑油的动力粘度η及折射率n,其中润滑油的动力粘度η由粘度计测量获得,待测润滑油的折射率n由阿贝折射仪确定;然后,使用千分表对玻璃盘进行调平,使其端面跳动在3μm以内;First install the miniature slider on the miniature slider bearing lubricating oil film measuring instrument, and then install the glass plate. When installing the glass plate, turn the 8 positioning screws on its surface in turn until they are slightly tightened. During installation, the glass plate should be prevented from being damaged and damaged. To avoid contamination of the surface of the glass disc, the surface contact pair is composed of a micro-slider and a glass disc. Add the lubricating oil to be tested on the glass disc to determine the dynamic viscosity η and refractive index n of the lubricating oil to be tested, where the dynamic viscosity η of the lubricating oil is Measured by a viscometer, the refractive index n of the lubricating oil to be tested is determined by an Abbe refractometer; then, use a dial gauge to level the glass disc so that the runout of the end face is within 3 μm; (3)、固定接触副倾角α为恒定值:(3) The inclination angle α of the fixed contact pair is a constant value: 波长为λ的红光经同轴照明设备输入显微镜照射在微型滑块和玻璃盘形成的楔形间隙上形成干涉图像,通过调节8颗调节螺钉确定干涉图像条纹的数目N,由倾角计算公式确定此时微型滑块和玻璃盘之间的倾斜角度α;对压环上的8颗定位螺钉进行微调,来控制倾角的动态平衡,使得回转过程中倾角不发生变化,其中α为微型滑块倾角,rad;λ为光源的波长,m;N为条纹数;n为润滑介质的折射率;B为微型滑块宽度,m;The red light with a wavelength of λ enters the microscope through the coaxial lighting device and irradiates on the wedge-shaped gap formed by the micro-slider and the glass disc to form an interference image. The number N of interference image fringes is determined by adjusting 8 adjustment screws, and the inclination angle is calculated by the formula Determine the inclination angle α between the micro-slider and the glass plate at this time; fine-tune the 8 positioning screws on the pressure ring to control the dynamic balance of the inclination angle so that the inclination angle does not change during the rotation process, where α is the micro-slider Inclination angle, rad; λ is the wavelength of the light source, m; N is the number of fringes; n is the refractive index of the lubricating medium; B is the width of the micro-slider, m; (4)、载荷的平衡和施加:(4), load balance and application: 通过调节弹簧可平衡整个加载的自重,当干涉图像若有若无时即完成了自重的平衡,然后施加实验要求的载荷w,实验过程中施加的载荷固定不变;By adjusting the spring, the self-weight of the entire load can be balanced. When the interference image is absent or not, the self-weight balance is completed, and then the load w required by the experiment is applied, and the load applied during the experiment is fixed; (5)、绘制出口处润滑油粘度η随油膜厚度h变化的曲线图:(5), draw the curve graph that the lubricating oil viscosity η at the outlet changes with the oil film thickness h: 上述步骤(3)中形成的干涉图像通过显微镜放大投射到图像控制器上,经图像控制器和图像采集卡的处理在电脑屏幕上显示出放大干涉图像;将放大干涉图像处理转换成光强曲线,由光强曲线得出干涉级次,利用干涉级次与润滑油膜厚度之间的关系计算出口处润滑油油膜厚度h;在接触副的夹角α=α1,速度ud=u1,载荷w=w1的条件下,测量已知粘度的5种润滑油的油膜厚度;将所测润滑油的粘度和油膜厚度的数据点用软件绘制出粘度η随油膜厚度h的变化曲线图,然后得出拟合曲线,最后根据上述已知数据关系推算得到粘度的计算公式:The interference image formed in the above step (3) is enlarged and projected onto the image controller through the microscope, and the enlarged interference image is displayed on the computer screen through the processing of the image controller and the image acquisition card; the enlarged interference image is processed and converted into a light intensity curve , the interference order is obtained from the light intensity curve, and the lubricating oil film thickness h at the outlet is calculated by using the relationship between the interference order and the lubricating oil film thickness; at the contact angle α=α 1 , the speed u d =u 1 , Under the condition of load w=w 1 , measure the oil film thickness of five kinds of lubricating oils with known viscosity; use the data points of the viscosity and oil film thickness of the measured lubricating oil to draw the change curve of viscosity η with oil film thickness h, Then draw the fitting curve, and finally calculate the viscosity calculation formula according to the above-mentioned known data relationship: η0=10χ η 0 =10 χ χ=2.15062·log h+1.71367。χ=2.15062·log h+1.71367. 2.根据权利要求1所述的微型滑块面接触润滑油粘度的测量方法,其特征在于所述玻璃盘为K9玻璃盘,玻璃盘在工作表面一侧镀有铬膜和二氧化硅膜(Cr+SiO2),用以获得清晰的干涉条纹,同时玻璃盘工作表面的反射率为18-22%,用以保证干涉条纹对比度,玻璃盘表面粗糙度Ra为4nm。2. the measuring method of miniature slide block surface contact lubricating oil viscosity according to claim 1, it is characterized in that described glass disc is K9 glass disc, and glass disc is plated with chromium film and silica film ( Cr+SiO 2 ), to obtain clear interference fringes, and the reflectivity of the working surface of the glass disk is 18-22%, to ensure the contrast of the interference fringes, and the surface roughness Ra of the glass disk is 4nm. 3.根据权利要求1所述的微型滑块面接触润滑油粘度的测量方法,其特征在于微型滑块的尺寸为4×4mm,微型滑块的工作表面为粗糙度为Ra=8~10nm,试验温度控制在20±0.5℃,湿度控制在30±5%。3. the method for measuring the viscosity of the contact lubricating oil on the surface of the miniature slider according to claim 1, characterized in that the size of the miniature slider is 4 × 4mm, and the working surface of the miniature slider has a roughness of Ra =8~10nm , The test temperature is controlled at 20±0.5°C, and the humidity is controlled at 30±5%.
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