CN106852468A

CN106852468A - A kind of composition containing moringa oleifera leaf extractive and preparation method thereof, preparation and application

Info

Publication number: CN106852468A
Application number: CN201611134627.1A
Authority: CN
Inventors: 赵益
Original assignee: Yunnan Beilian Biotechnology Development Co Ltd
Current assignee: Yunnan Lianhua Investment Co.,Ltd.
Priority date: 2016-12-11
Filing date: 2016-12-11
Publication date: 2017-06-16
Anticipated expiration: 2036-12-11
Also published as: CN106852468B

Abstract

The invention discloses a kind of composition containing moringa oleifera leaf extractive and preparation method thereof, preparation and application, the composition includes the raw material of following percentage by weight：30 ~ 80 parts of moringa oleifera leaf extractive, 5 ~ 25 parts of emblic leafflower powder, 5 ~ 25 parts of Noni fruit powder, 1 ~ 15 part of aloe extract.Composition toxin expelling of the invention defaecation, replenish the calcium, the effect is significant of facilitating alcohol metabolism and protecting liver, strengthen immunity, using heat-clearing, facilitating alcohol metabolism and protecting liver, oxidation resistant material optimization prescription, treat constipation while replenish the calcium, strengthen immunity, liver protection, accelerate metabolism.

Description

A kind of composition containing moringa oleifera leaf extractive and preparation method thereof, preparation and application

Technical field

The invention belongs to health-oriented products preparing technical field, and in particular to a kind of composition containing moringa oleifera leaf extractive and its Preparation method, preparation and application.

Background technology

Due to the quickening of rhythm of life, the increase of pressure, and bad habits and customs cause the toxin in body to be piled up Excessively, constipation is caused.Detoxicating intestine has become hot issue, and constipation is the natural enemy of modern, disturbs us normally to give birth to Living, the toxin that constipation causes excessively also contributes to the health of body, causes skin poor, and implication is not pure and fresh, strong influence I Daily life.Nowadays many people are perplexed by constipation, are particularly all women and the elderly.With interpersonal Communication it is increasingly extensive, wine as few medium that must get along well, because the accident and hepatopathy of initiation of drinking are increasing.City white collar female Property and the elderly simultaneously be also calcium loss group of people at high risk, how treat constipation while replenished the calcium, facilitating alcohol metabolism and protecting liver, be also Instantly the problem that should be studied.

Treatment in the market or improve constipation, the product replenishing the calcium, sober up it is various, but most of effects are not good enough, work( Can be single, the many-side that improve body is uncomfortable, need to take multiple product, cures the symptoms, not the disease, or even have very big side effect.Cause This research and development one kind is provided simultaneously with improving constipation, replenishes the calcium, the multi-functional unification such as facilitating alcohol metabolism and protecting liver protect liver, takes again easily product It is necessary.

The content of the invention

The first object of the present invention is to provide a kind of composition containing moringa oleifera leaf extractive, and the second purpose is offer one The preparation method of the composition containing moringa oleifera leaf extractive is planted, the 3rd purpose is to provide a kind of composition containing moringa oleifera leaf extractive Preparation, the 4th purpose is to provide a kind of application of the composition containing moringa oleifera leaf extractive.

The first object of the present invention is achieved in that the raw material including following weight portion：Moringa oleifera leaf extractive 30 ~ 80 Part, 5 ~ 25 parts of emblic leafflower powder, 5 ~ 25 parts of Noni fruit powder, 1 ~ 15 part of aloe extract.

The second object of the present invention is achieved in that described preparation method to weigh raw material input wet method by weight In mixer-granulator, after mixing 25 ~ 35 minutes, it is 1 to spray into material with the weight ratio of alcohol：0.025 95% edible alcohol, mixes Close granulation to discharge for 20 ~ 30 minutes, obtain composition.

The third object of the present invention is achieved in that described preparation is to add pharmaceutically to connect in described composition The auxiliary material received is prepared into capsule, tablet, powder, granule, liquid preparation, pill, medicinal tea.

What the fourth object of the present invention was realized in, described composition leads in preparation prevention/auxiliary treatment toxin expelling Just the application, replenished the calcium in similar drug, facilitating alcohol metabolism and protecting liver or health food.

Beneficial effects of the present invention：

1st, composition toxin expelling of the invention defaecation, replenish the calcium, the effect is significant of facilitating alcohol metabolism and protecting liver, employ heat-clearing, facilitating alcohol metabolism and protecting liver, antioxygen The material optimization prescription of change, replenished the calcium while constipation is treated, liver protection, strengthen immunity, accelerate metabolism, with three high drop, anti- Effect of cancer, effectively reduces hypertension, hyperglycaemia and high fat of blood, while antitumous effect is notable.

2nd, efficacy effect of the moringa oleifera leaf extractive in this composition in raw material of the present invention：With hypoglycemic, lipid-loweringing, wake up Wine, step-down, antitumor, anti-oxidant, liver protection, replenish the calcium, defaecation, diuresis, the effect such as improve the health care of sleep；Pu'er tea is combined herein Efficacy effect in thing：Lipid-loweringing, fat-reducing, beauty treatment, step-down, anti arteriosclerosis, antitumor, nourishing the stomach, sterilization, the anti-ageing effect of waiting for a long time； The effect of emblic leafflower powder effect in this composition：With anti-oxidant, liver protection, anti-inflammatory, clearing heat and cooling blood, food digesting stomach fortifying, promote the production of body fluid only The effect such as cough；The effect of Noni fruit powder effect in this composition：With antioxidation activity, protection cardiac muscle cell, anti-inflammatory, anti-tired Labor, sober up, toxin expelling, hypotensive, defaecation, the effect of strengthen immunity；The effect of aloe extract effect in this composition：Kill Let out under bacterium anti-inflammatory, stomach invigorating, cardiac stimulant promoting blood circulation, immunity anticancer, removing toxic substances, the effect such as analgesia so that leaf of Moringa of the present invention is instant Tea is in good taste, replenish the calcium, facilitating alcohol metabolism and protecting liver, promote the production of body fluid to quench thirst, toxin expelling defaecation and can strengthen immunity, while solve replenish the calcium, liver protection shield The problem that liver, toxin expelling defaecation are treated both principal and secondary aspect of disease.

3rd, formulation of the invention can be prepared into granulated quickly dissolving, thus melting to finished product, color and luster, it is limpid it is transparent, The requirement such as mouthfeel, effect, bioavilability is higher, and raw material of the invention uses different preprocess methods, Moringa leaf raw material row Malicious defaecation, strengthen immunity, fiber are more, thermal sensitivity is strong, unfavorable instant absorption and preparation processing, so using low temperature seepage pressure effects Concentration technique is conducive to improving bioavilability；The Pu'er tea raw material heat-clearing inverse, fiber of drop is more, thermal sensitivity is strong, unfavorable instant absorption And preparation processing, so extracting effective ingredient using low temperature ultrasonic technology；Emblic, Noni fruit dry difficulty, no matter are processed into The aspects such as sheet, preparation processing Feasible degree are all unfavorable, so extracting fine powder using spray drying technology of squeezing the juice, are conducive to preserving, have Beneficial to preparation processing, be conducive to improving bioavilability；The defaecation of aloe raw material toxin expelling, strengthen immunity, fiber are more, thermal sensitivity By force, unfavorable instant absorption and preparation processing, so extract effective ingredient using low temperature ultrasonic technology to be conducive to improving biological utilisation Degree.This process advan in attractive in appearance, the flavouring taste of product, enhancing is replenished the calcium, liver protection, promote the production of body fluid to quench thirst, toxin expelling aperient effects, make product Active ingredient concentration is greatly improved, mouthfeel more preferable, effect is more notable.Product is made granule, makes processing, takes, preserves, carrying Extremely convenient, to realize that large-scale production creates condition.

4th, on inventive formulation：Using the raw material let out under poison expelling and beautifying, clearing heat and detoxicating, defaecation of replenishing the calcium, liver protecting, stomach invigorating Prescription is arranged in pairs or groups, in process technology：Using seepage pressure effects technology, low temperature ultrasonic extractive technique, vacuum concentration technology, spray drying skill Art, microwave drying technology, vacuum drying technique, wet-mixing granulation technique, fluidized drying technology, particle packing technology etc. are favourable The technology of product efficacy advantage is combined.

5th, between each raw material of the invention, cooperate, complement each other, inventive formulation combinatorial principle：Raw material Moringa Leaf extract, is toxin expelling defaecation of the present invention, strengthen immunity, facilitating alcohol metabolism and protecting liver, the principal ingredients for playing a decisive role of replenishing the calcium, but Moringa oleifera leaf extractive protein is very high, easily induces gout；Pu'er tea tool enhancing diarrhea, the effect for neutralizing uric acid, but It is that cold in nature also easy stimulation enteron aisle induces enteritis, so increase matching somebody with somebody emblic leafflower powder and aloe, emblic leafflower powder is mild-natured, with enhancing uric acid Metabolism prevention pain wind action, the tartaric acid of emblic leafflower powder can with food digesting stomach fortifying and promote the production of body fluid, fructose can be with additional heat and vigour, day Right vitamin C and hepatocuprein [SOD] can be with strengthen immunities, and emblic leafflower powder not only counteracts the secondary work of leaf of Moringa With, but also with toxin expelling defaecation, anti-aging, anticancer, suppress hepatitis B effect；Plug Luoning in Noni fruit powder is human body The necessary material that protein plays a role, with enhance immunity, promotes digestion with toxin expelling, reparation damaged cell, anti-oxidant, drop Blood fat, regulation blood sugar, the effect of easing pain and diminishing inflammation, in Noni fruit powder organized enzyme element ache with removal, fatigue, sober up, anti-inflammatory, Antirheumatic, toxin expelling, cytothesis, improve nerve cell, treatment hemorrhoid, hair tonic, control impotence, control infertile effect：Aloe Prebiotics in raw material can effectively protect enteron aisle, but also can promote enterocinesia enhancing effect of ejecting poison, promote this product to absorb Beneficial to fast onset；Protein sugar favorably increases metabolism and mouthfeel；Cyclodextrin can be prevented in product caking, the moisture absorption, reduction dispensing Bitter taste and peculiar smell, enhanced products fragrance.Extract dispensing and the direct dispensing of raw material are combined, and constitute matching somebody with somebody for present invention optimization Side.

6th, leaf of Moringa material effective component ratio is relatively low, direct dispensing not only effective ingredient and absorptivity is low can not manifest work( Effect, and preparation processing is difficult, so needing extracts active ingredients out dispensing again.It is guaranteed quality, using drink in technique Extracted with water, it can be ensured that active ingredient farthest selectivity dissolution, technically continuously extracted using low-temperature dynamic diacolation, it is molten Seen off at once after matter dissolution, increase solute dissolution gradient in extractor, extracted more complete, speed faster.Low-temperature dynamic is oozed Filtering active ingredient of at utmost protect is not destroyed, and in the case that equivalent feeds intake, relative boiling puies forward technique, and mouthfeel is more preferably, effectively Components and concentration is higher；The heat-clearing of Pu'er tea raw material drops that inverse but effective ingredient is low, fiber is more, thermal sensitivity is strong, unfavorable instant absorption and system Agent is processed, so extracting effective ingredient using low temperature ultrasonic technology；The unfavorable preservation of wild fresh fruit of fructus phyllanthi, Noni fruit, dries tired The aspects such as difficulty, processing cost, preparation processing Feasible degree are all unfavorable, so using the method for dry extraction fine powder of squeezing the juice, having Beneficial to preserve, be conducive to preparation processing, be conducive to improve bioavilability.Because the natural complex C heated times in fruit juice Long largely to reduce, to ensure effect of product, concrete technology route uses the dry technique of fruit juice Direct spraying, makes fruit juice In moisture flash evapn, particles of solute hot blast moment taken to whirlwind powder collector formed fine powder, granularity up to 200 ~ 300 mesh, Relative enhancement, drying, disintegrating process, fruit juice Direct spraying drying process take short, good product quality, product granularity and reach ultra micro Powder rank, is conducive to preparation processing and product efficacy；The effect of aloe raw material toxin elimination and clot absorbing is very strong but fiber is more, is unfavorable for directly Dispensing preparation processing, bioavilability, prominent product efficacy, so extracting skill using low temperature ultrasonic are improved in order to promote to absorb Art.

Specific embodiment

With reference to embodiment, the present invention is further illustrated, but the present invention is any limitation as never in any form, Based on present invention teach that any conversion or replacement made, belong to protection scope of the present invention.

Composition containing moringa oleifera leaf extractive of the invention, including following weight portion raw material：Moringa oleifera leaf extractive 30 ~ 80 Part, 5 ~ 25 parts of emblic leafflower powder, 5 ~ 25 parts of Noni fruit powder, 1 ~ 15 part of aloe extract.

The described composition containing moringa oleifera leaf extractive, including following weight portion raw material：Moringa oleifera leaf extractive 50 ~ 65 Part, 6 ~ 11 parts of emblic leafflower powder, 6 ~ 15 parts of Noni fruit powder, 2 ~ 8 parts of aloe extract.

The described composition containing moringa oleifera leaf extractive, including following weight portion raw material：Moringa oleifera leaf extractive 52 ~ 62 Part, 7 ~ 10 parts of emblic leafflower powder, 7 ~ 12 parts of Noni fruit powder, 3 ~ 6 parts of aloe extract.

The described composition also Pu'er tea including 2 ~ 10 weight portions.

The described composition also Pu'er tea including 4 ~ 8 weight portions.

Described composition also includes 1 ~ 8 part of protein sugar of weight portion.

Described composition also includes 2 ~ 6 parts of protein sugars of weight portion.

The extracting method of described moringa oleifera leaf extractive includes extracting and developing, concentration, dries and postprocessing working procedures, specifically For：

1）Extract：During leaf of Moringa raw material weighing put into extractor, 3 ~ 7 times of pure water of amount are added, soak 1 ~ 3h；Steam adds Hot extractor simultaneously extracts 25 ~ 35min at maintaining the temperature at 80 ~ 85 DEG C, then keeps the temperature at 75 ~ 80 DEG C and carries out diacolation and carries Take, keep extract solution sealing and circulating in extractor and circulating pump to extract 4 ~ 5h, stop circulation, will extract pot liquid derives To first time extract solution；Then the hot water by 4 ~ 5 times of Moringa leaf raw material inventorys, temperature for 75 DEG C ~ 80 DEG C adds extractor It is interior, keep extract solution to derive second extract solution after 4 ~ 5h of sealing and circulating in extractor and circulating pump again, carried with first time Liquid is taken to merge and be well mixed；Moringa leaf slag abandons it；

2）Separate：By step 1）Extract solution staticly settle 2 ~ 4h, take supernatant high speed centrifugation, obtain pure leaf of Moringa and carry Liquid is taken, precipitation abandons it；

3）Concentration：By step 2）Moringa leaf extract import in inspissator, vacuumize and be concentrated into relative proportion 1.15 ~ 1.2, receive Cream；

4）Dry：By step 3）The condensed cream for obtaining is dried under vacuum to rewinding during moisture 4.5% ~ 5%, obtains leaf of Moringa cream；

5）Post processing：By step 4）Leaf of Moringa cream with pulverizer crush, sieving, obtain moringa oleifera leaf extractive, it is standby.

Step 1）Described in pure water for add 6 ~ 7 times amount.

Step 1）Described in steam be heated to be extractor condenser cooling water pressure be maintained at 0.3 ~ 0.4MPa, extractor Steam heated pressure is maintained at 0.2 ~ 0.25MPa.

Step 2）Described in high speed centrifugation be using high speed tube centrifuge filter, rotating speed be 16000 ~ 20000r/min。

Step 3）Described in vacuum concentration for keep vacuum carried out in -0.07 ~ -0.075MPa, 60 ~ 65 DEG C of temperature it is dense Contracting.

Step 4）Described in vacuum drying be uniformly to be laid on the baking tray of vacuum drying chamber condensed cream, keep vacuum It is dried under the conditions of -0.07 ~ -0.075MPa of degree, 60 ~ 65 DEG C of temperature.

The extracting method of described Pu'er tea includes extracting and developing, concentration, dries and postprocessing working procedures, specifically For：

1）Extract：During Pu'er tea raw material weighing put into extractor, 3 ~ 8 times of drinking water of amount are added, keep 10 ~ 30 DEG C, leaching 2 ~ 3h of bubble；Steam heating extraction tank simultaneously controls ultrasonically treated 0.5 ~ 1.5h at 50 ~ 60 DEG C of temperature, then by leaching liquor closed cycle 0.5 ~ 1.5h, ultrasonically treated and closed cycle is repeated 2 ~ 4 times, and tea liquid is obtained after filtering, and tea grounds abandons it；

2）Separate：Centrifugal filtration is first carried out, by step 1）Tea liquid 3 ~ 5h of natural sedimentation, take supernatant high speed centrifugation, obtain To the tea liquid that translucency is poor, precipitate discarded；Membrane filtration is carried out again, by the tea liquid of centrifugal filtration by membrane filtration, institute Filter sizes are stated for 0.1 ~ 0.22 μm, the good tea liquid of translucency is obtained；

3）Concentration：Will be by step 2）It is 1.2 ~ 1.25 that the tea liquid of separation carries out being concentrated in vacuo to proportion, receives cream；

4）Dry：By step 3）Condensed cream carry out microwave drying, dry to rewinding during moisture 4% ~ 4.5%, obtain Pu'er tea paste；

5）Post processing：By step 4）Pu'er tea paste, with pulverizer crush, sieving, obtain Pu'er tea, it is standby.

Step 1）Described in drinking water addition for 6 ~ 8 times amount.

Step 1）Described in be filtered into through 100 mesh filter screens filter.

Step 2）Described in the pressure of membrane filtration be maintained at 0.4 ~ 0.5MPa.

Step 3）Described in vacuum concentration for keep vacuum carried out in -0.07 ~ -0.075MPa, 50 ~ 60 DEG C of temperature it is dense Contracting.

The preparation method of the described composition containing moringa oleifera leaf extractive puts into wet-mixing to weigh raw material by weight In granulator, after 25 ~ 35min of mixing, it is 1 to spray into material with the weight ratio of alcohol：0.025 95% edible alcohol, mixing system Grain 20 ~ 30min dischargings, obtain composition.

The preparation of the described composition containing moringa oleifera leaf extractive is to add pharmaceutically to receive in described composition Auxiliary material is prepared into granule, tablet, powder, capsule, liquid preparation, pill, medicinal tea.

Contain cyclodextrin in described auxiliary material.

The application of the described composition containing moringa oleifera leaf extractive is that described composition is preparing prevention/auxiliary treatment row Application in malicious defaecation, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food.

Described emblic leafflower powder is emblic fine powder, and described Noni fruit powder is Noni fruit fine powder.

The preparation method of described emblic leafflower powder includes：

1）Drum-type fruit washing machine, cylinder rotating speed is used to be maintained at 15 ~ 20 revs/min after wild fresh fruit of fructus phyllanthi is rejected into decayed fruit, impurity Clock, 5 ~ 10m of Water spray flow³/ h, charging rate is maintained at 8 ~ 10 kg/minutes, the fresh fruit for being cleaned up, described water It is drinking water；

2）Using fruit crusher, charging rate is maintained at 5 ~ 8 kg/minutes, the fresh fruit that will be cleaned up be broken for granularity 2 ~ The particle of 5mm；

3）Using fruit pressafiner, rotating speed is maintained at 60 ~ 70 revs/min, and particle is at the uniform velocity added, and charging rate is maintained at 3 ~ 5 kg/minutes, pomace is discharged, and underflow fruit juice flows out through filter screen from bottom；

4）Using centrifuge, drum speed is maintained at 1000 ~ 1500 revs/min, by step 3）The underflow fruit juice for obtaining at the uniform velocity adds Enter, charging rate is maintained at 0.2 ~ 0.5 m³/ minute, the slag discharge isolated obtains fruit juice clear liquid；

5）Natural sedimentation 3 hours in fruit juice feeding taper settling tank, it is 16000 ~ 20000r/min's to take supernatant by rotating speed High speed tube centrifuge is filtered, obtain it is limpid it is transparent, without insoluble and suspended particulate substance phyllanthus emblica L.juice is precipitated, precipitation is discarded；

6）By step（5）The fruit juice clear liquid of gained is spray-dried, and high speed centrifugal atomization device rotating speed is maintained at 6000 ~ 6500 Rev/min, the air flow rate proportioning of regulation air-supply and air inducing makes spraying system be maintained between 50 ~ 200Pa of negative pressure, tower top import temperature Degree is maintained at 230 ~ 240 DEG C, and bottom of towe outlet temperature is maintained at 110 ~ 120 DEG C, and 10 beats/min of pulse rapping, stabilization screw pump enters Stream amount was carried out continuously spray drying at 80 ~ 100L/ minutes, obtained the emblic leafflower powder that granularity is 200 ~ 300 mesh.

The preparation method of described Noni fruit powder includes：

1）Drum-type fruit washing machine, cylinder rotating speed is used to be maintained at 10 ~ 15 revs/min, water after Noni fruit fresh fruit is rejected into decayed fruit, impurity 3 ~ 7m of spray flow³/ h, charging rate is maintained at 3 ~ 5 kg/minutes, the fresh fruit for being cleaned up, and described water is to drink Water；

2）Using fruit spiral juice extractor, rotating speed is maintained at 50 ~ 60 revs/min, and particle is at the uniform velocity added, and charging rate is maintained at 1 ~ 3 kg/minute, pomace is discharged, and underflow fruit juice flows out through filter screen from bottom；

3）Using centrifuge, drum speed is maintained at 1000 ~ 1500 revs/min, by step 2）The underflow fruit juice for obtaining at the uniform velocity adds Enter, charging rate is maintained at 0.2 ~ 0.5 m³/ minute, the slag discharge isolated obtains fruit juice clear liquid；

4）Natural sedimentation 3 hours in fruit juice feeding taper settling tank, it is 16000 ~ 20000r/min's to take supernatant by rotating speed High speed tube centrifuge is filtered, obtain it is limpid it is transparent, without insoluble and suspended particulate substance Morinda Citrifolia juice is precipitated, precipitation is discarded；

5）By step 4）The fruit juice clear liquid of gained is spray-dried, high speed centrifugal atomization device rotating speed be maintained at 6000 ~ 6500 turns/ Minute, the air flow rate proportioning of regulation air-supply and air inducing makes spraying system be maintained between 50 ~ 200Pa of negative pressure, and tower top inlet temperature is protected Hold at 220 ~ 230 DEG C, bottom of towe outlet temperature is maintained at 100 ~ 110 DEG C, and 10 beats/min of pulse rapping, stabilization screw pump enters stream Amount was carried out continuously spray drying at 80 ~ 100L/ minutes, obtained the Noni fruit powder that granularity is 200 ~ 300 mesh.

The preparation method of described aloe extract includes：

1）Aloe raw material is weighed in putting into extractor, add 6 ~ 8 times of drinking water of amount, kept for 10 ~ 30 DEG C, immersion 2 ~ 3 is small When；

2）Extractor condenser and steam heating are opened, when temperature reaches 50 ~ 60 DEG C in tank to be extracted, and temperature 50 ~ 60 is controlled Ultrasonically treated 0.5 ~ 1.5h at DEG C, then leaching liquor is extracted out in 0.5 ~ 1.5h of top addition closed cycle from tank bottom, it is ultrasonically treated Repeated 2 ~ 4 times with closed cycle, extract solution, slag discharge are obtained after filtering；

3）Extract solution feeding settling tank natural sedimentation 3 hours, takes high-velocity tube of the supernatant by 16000 ~ 20000r/min of rotating speed Formula centrifuge is filtered, and is obtained without precipitation insoluble and suspended particulate substance but the poor extract solution of translucency, and precipitation is discarded；

4）The extract solution filtered by high speed tube centrifuge is filtered by the Membrane filtering machine that filter sizes are 0.1 ~ 0.22 μm, mistake Filtering pressure power is maintained at 0.4 ~ 0.5MPa, obtains the good extract solution from aloe of limpid transparent, translucency；

5）Extract solution starts vacuum concentration, keeps vacuum in 60 ~ 65 DEG C of -0.07 ~ -0.075MPa, temperature, and being concentrated into proportion is 1.2 ~ 1.25, cream is received, condensed cream is uniformly laid on baking tray, baking tray is placed on the grill of rotation, keep vacuum -0.07 Microwave drying is carried out under the conditions of ~ -0.075MPa, 60 ~ 65 DEG C of temperature, is dried to rewinding during moisture 5% ~ 5.5%；Then by drying Aloe ointment, with 5.5KW Universalpulverizers crush, sieving, obtain granularity be 80 ~ 120 mesh aloe extract.

Embodiment 1

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：30 parts of moringa oleifera leaf extractive, emblic leafflower powder 5 parts, 5 parts of Noni fruit powder, 1 part of aloe extract.

The auxiliary material for pharmaceutically receiving is added to be prepared into liquid preparation in the composition of embodiment 1.Described composition exists Prepare the application in the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food.

Embodiment 2

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：80 parts of moringa oleifera leaf extractive, emblic leafflower powder 25 parts, 25 parts of Noni fruit powder, 15 parts of aloe extract.

The auxiliary material for pharmaceutically receiving is added to be prepared into pill in the composition of embodiment 2.It is prepared by described composition Application in the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food.

Embodiment 3

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：50 parts of moringa oleifera leaf extractive, emblic leafflower powder 6 parts, 6 parts of Noni fruit powder, 2 parts of aloe extract.

The auxiliary material for pharmaceutically receiving is added to be prepared into granule in the composition of embodiment 3.Contain in described auxiliary material Cyclodextrin.Described composition is preparing the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food In can apply.

Embodiment 4

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：65 parts of moringa oleifera leaf extractive, emblic leafflower powder 11 parts, 15 parts of Noni fruit powder, 8 parts of aloe extract.

The auxiliary material for pharmaceutically receiving is added to prepare piece agent in the composition of embodiment 4.Contain ring in described auxiliary material Dextrin.Described composition is in the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food is prepared Application.

Embodiment 5

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：50 parts of moringa oleifera leaf extractive, emblic leafflower powder 6 parts, 6 parts of Noni fruit powder, 2 parts of aloe extract, 2 parts of Pu'er tea.

The auxiliary material for pharmaceutically receiving is added to be prepared into powder in the composition of embodiment 5.Contain ring in described auxiliary material Dextrin.Described composition is in the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food is prepared Application.

Embodiment 6

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：60 parts of moringa oleifera leaf extractive, emblic leafflower powder 10 parts, 12 parts of Noni fruit powder, 6 parts of aloe extract, 10 parts of Pu'er tea.

The auxiliary material for pharmaceutically receiving is added to be prepared into capsule in the composition of embodiment 6.Contain in described auxiliary material Cyclodextrin.Described composition is preparing the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food In application.

Embodiment 7

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：40 parts of moringa oleifera leaf extractive, emblic leafflower powder 8 parts, 8 parts of Noni fruit powder, 4 parts of aloe extract, 4 parts of Pu'er tea, 1 part of protein sugar.

The auxiliary material for pharmaceutically receiving is added to be prepared into liquid preparation in the composition of embodiment 7.Described composition exists Prepare the application in the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food.

Embodiment 8

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：Raw material including following weight portion：Moringa 70 parts of leaf extract, 14 parts of emblic leafflower powder, 14 parts of Noni fruit powder, 7 parts of aloe extract, 8 parts of Pu'er tea, protein sugar 8 Part.

The auxiliary material for pharmaceutically receiving is added to be prepared into pill in the composition of embodiment 8.It is prepared by described composition Application in the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food.

Embodiment 9

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：55 parts of moringa oleifera leaf extractive, emblic leafflower powder 7 parts, 7 parts of Noni fruit powder, 3 parts of aloe extract, 3 parts of Pu'er tea, 3 parts of protein sugar.

The auxiliary material for pharmaceutically receiving is added to be prepared into medicinal tea in the composition of embodiment 9.It is prepared by described composition Application in the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food.

Embodiment 10

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：52 parts of moringa oleifera leaf extractive, emblic leafflower powder 8 parts, 8 parts of Noni fruit powder, 6 parts of aloe extract, 4 parts of Pu'er tea, 4 parts of protein sugar.

The auxiliary material for pharmaceutically receiving is added to be prepared into granule in the composition of embodiment 10.Contain in described auxiliary material Cyclodextrin.Described composition is preparing the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food In application.

Embodiment 11

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：45 parts of moringa oleifera leaf extractive, emblic leafflower powder 9 parts, 9 parts of Noni fruit powder, 9 parts of aloe extract, 9 parts of Pu'er tea, 7 parts of protein sugar.

The auxiliary material for pharmaceutically receiving is added to prepare piece agent in the composition of embodiment 11.It is prepared by described composition Application in the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food.

Embodiment 12

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：58 parts of moringa oleifera leaf extractive, emblic leafflower powder 20 parts, 20 parts of Noni fruit powder, 13 parts of aloe extract, 5 parts of Pu'er tea, 5 parts of protein sugar.

The auxiliary material for pharmaceutically receiving is added to be prepared into powder in the composition of embodiment 12.Contain ring in described auxiliary material Dextrin.Described composition is in the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food is prepared Application.

Embodiment 13

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：68 parts of moringa oleifera leaf extractive, emblic leafflower powder 12 parts, 13 parts of Noni fruit powder, 10 parts of aloe extract.

The auxiliary material for pharmaceutically receiving is added to be prepared into medicinal tea in the composition of embodiment 13.It is prepared by described composition Application in the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food.

Embodiment 14

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：57 parts of moringa oleifera leaf extractive, emblic leafflower powder 9 parts, 11 parts of Noni fruit powder, 5 parts of aloe extract, 6 parts of Pu'er tea, 5 parts of protein sugar.

The auxiliary material for pharmaceutically receiving is added to be prepared into granule in the composition of embodiment 14.Contain in described auxiliary material Cyclodextrin.Described composition is preparing the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food In application.

Embodiment 15

A kind of composition containing moringa oleifera leaf extractive, including following weight portion raw material：62 parts of moringa oleifera leaf extractive, emblic leafflower powder 10 parts, 12 parts of Noni fruit powder, 6 parts of aloe extract, 7 parts of Pu'er tea.

The auxiliary material for pharmaceutically receiving is added to prepare piece agent in the composition of embodiment 15.It is prepared by described composition Application in the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food.

Embodiment 16

1）Weigh：62 parts of moringa oleifera leaf extractive, 7 parts of emblic leafflower powder, 8 parts of Noni fruit powder, 6 parts of aloe extract, Pu'er tea is extracted 5 parts of thing, 2 parts of protein sugar is standby；

2）Mixing：By step 1）In the material input wet mixing pelletizer of middle weighing, after mixing 30 minutes, material and wine are sprayed into The weight ratio of essence is 1：0.025 95% edible alcohol, mixer-granulator continues to run with discharging in 24 minutes, obtains composition.

The extracting method of described moringa oleifera leaf extractive includes：

1）Extract：During leaf of Moringa raw material weighing put into extractor, 6 times of drinking water of amount are added, soaked 2 hours；To extract Tank condenser cooling water pressure is maintained at 0.3MPa, and extractor steam heated pressure is maintained at 0.2MPa, tank Nei Wenduda to be extracted It is back to when in tank to 85 DEG C, water vapor condensate, keeps the temperature at 80 DEG C and boil and carry 25 minutes, is then shut off extractor steaming Vapour, temperature is maintained at 75 DEG C in tank；Seepage pressure effects are carried out, extract solution sealing and circulating 4 in extractor and circulating pump is kept Hour, stop circulation, the liquid in extractor is all drained, obtain first time extract solution；Then by 4 times of Moringa leaf raw materials Inventory, the hot water addition extractor that temperature is 75 DEG C DEG C, after hot water is added, keep extract solution in extractor and circulation again Sealing and circulating 4 hours in pump, then all drain the liquid in extractor, obtain second extract solution, by Moringa leaf slag row Put；

2）Centrifugal filtration：ON cycle pump circulation mixes 25 minutes, and first time extract solution and second extract solution are well mixed； Extract solution natural sedimentation by evenly mixing 2 hours, it is the high speed tube centrifuge of 16000r/min to take supernatant by rotating speed Filtering, obtain it is limpid it is transparent, without insoluble and suspended particulate substance Moringa leaf extract is precipitated, precipitation is discarded；

3）Concentrate drying：Moringa leaf extract is pumped into inspissator, with the hot water heating that temperature is 90 DEG C, starts vacuum dense Contracting, keeps vacuum in -0.07MPa, temperature 60 C, and it is 1.15 to be concentrated into proportion, receives cream, and condensed cream is uniformly laid on into vacuum On the baking tray of drying box, baking tray is placed on grill, carrying out vacuum under the conditions of holding vacuum -0.07MPa, temperature 60 C does It is dry, dry to rewinding during moisture 4.5%；Then by dry leaf of Moringa cream, crushed with pulverizer, sieving, it is 80 to obtain granularity Purpose moringa oleifera leaf extractive.

The extracting method of described Pu'er tea includes：

1）Extract：During Pu'er tea raw material weighing put into extractor, 6 times of drinking water of amount are added, kept for 10 DEG C, immersion 2 is small When；Extractor condenser cooling water and the heating of extractor jacket steam are opened, when temperature reaches 50 DEG C in tank to be extracted, and is controlled Ultrasonically treated 0.5h under temperature 50 C, then by leaching liquor closed cycle 0.5h, ultrasonically treated and closed cycle is repeated 2 times, Tea liquid, tea grounds discharge are obtained after being filtered through 100 mesh filter screens；

2）Filtering：Centrifugal filtration is first carried out, by step（1）The tea liquid natural sedimentation for obtaining 3 hours, take supernatant is by rotating speed The high speed tube centrifuge filtering of 16000r/min, obtains the tea liquid poor without insoluble and suspended particulate substance, translucency is precipitated, and sinks The protein and impurity for forming sediment are discarded；Membrane filtration is carried out again, is 0.1 μm by filter sizes by the tea liquid of centrifugal filtration Membrane filtering machine filtering, filter pressure is maintained at 0.4MPa, obtains the good tea liquid of limpid transparent, translucency；

3）Concentrate drying：By step（2）The tea liquid for obtaining is concentrated in vacuo, and keeps vacuum in -0.07MPa, temperature 50 C, It is 1.2 to be concentrated into proportion, receives cream, and condensed cream is uniformly laid on baking tray, and baking tray is placed on the grill of rotation, keeps vacuum Microwave drying is carried out under the conditions of degree -0.075MPa, temperature 50 C, is dried to rewinding during moisture 4%；Then by dry tea cream, Crushed with pulverizer, sieving obtains the Pu'er tea that granularity is 80 mesh.

The preparation method of composition is put into wet mixing pelletizer to weigh raw material by weight, after mixing 25 minutes, It is 1 that material is sprayed into the weight ratio of alcohol：0.025 95% edible alcohol, mixing granulation discharges for 20 minutes, obtains composition.

The auxiliary material for pharmaceutically receiving is added to prepare piece agent in the composition that embodiment 16 is obtained.Contain in described auxiliary material There is 10 parts of cyclodextrin（It is identical with the parts by weight of raw materials for weighing）.

The composition that embodiment 16 is obtained preparing prevention/auxiliary treatment toxin expelling defaecation, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or Application in health food.

Embodiment 17

1）Weigh：63 parts of moringa oleifera leaf extractive, 7 parts of emblic leafflower powder, 9 parts of Noni fruit powder, 3 parts of aloe extract, Pu'er tea is extracted 4 parts of thing, 3 parts of protein sugar is standby；

2）Mixing：By step 1）In the material input wet mixing pelletizer of middle weighing, after mixing 33 minutes, material and wine are sprayed into The weight ratio of essence is 1：0.025 95% edible alcohol, mixer-granulator continues to run with discharging in 25 minutes, obtains composition.

The extracting method of described moringa oleifera leaf extractive includes：

1）Extract：During leaf of Moringa raw material weighing put into extractor, 6.5 times of drinking water of amount are added, soaked 2.5 hours；Will Extractor condenser cooling water pressure is maintained at 0.35MPa, and extractor steam heated pressure is maintained at 0.225MPa, in tank to be extracted Temperature reach 85 DEG C, water vapor condensate be back to when in tank, keep the temperature at 82 DEG C and boil and carry 30 minutes, be then shut off extracting Tank steam, temperature is maintained at 77 DEG C in tank；Carry out seepage pressure effects, keep that extract solution is closed in extractor and circulating pump to follow Ring 4.5 hours, stops circulation, and the liquid in extractor is all drained, and obtains first time extract solution；Then it is peppery by 4.5 times Wooden leaf raw material inventory, the hot water addition extractor that temperature is 78 DEG C, after hot water is added, keep extract solution in extractor again With sealing and circulating in circulating pump 4.5 hours, then the liquid in extractor is all drained, obtain second extract solution, will be peppery Wooden leaf slag discharge；

2）Centrifugal filtration：ON cycle pump circulation mixes 30 minutes, and first time extract solution and second extract solution are well mixed； Extract solution natural sedimentation by evenly mixing 3 hours, it is the high speed tube centrifuge of 18000r/min to take supernatant by rotating speed Filtering, obtain it is limpid it is transparent, without insoluble and suspended particulate substance Moringa leaf extract is precipitated, precipitation is discarded；

3）Concentrate drying：Moringa leaf extract is pumped into inspissator, with the hot water heating that temperature is 92 DEG C, starts vacuum dense Contracting, keeps vacuum in 62 DEG C of -0.0725MPa, temperature, and it is 1.17 to be concentrated into proportion, receives cream, condensed cream is uniformly laid on true On the baking tray of empty drying box, baking tray is placed on grill, keeps carrying out vacuum under the conditions of vacuum -0.0725MPa, 62 DEG C of temperature Dry, dry to rewinding during moisture 4.25%；Then by dry leaf of Moringa cream, crushed with pulverizer, sieving, obtaining granularity is The moringa oleifera leaf extractive of 100 mesh.

The extracting method of described Pu'er tea includes：

1）Extract：During Pu'er tea raw material weighing put into extractor, 7 times of drinking water of amount are added, keep 20 DEG C, immersion 2.5 Hour；Extractor condenser cooling water and the heating of extractor jacket steam are opened, when temperature reaches 55 DEG C in tank to be extracted, and is controlled Ultrasonically treated 1h at 55 DEG C of temperature processed, then by leaching liquor closed cycle 1h, ultrasonically treated and closed cycle is repeated 3 times, is passed through Tea liquid, tea grounds discharge are obtained after the filtering of 100 mesh filter screens；

2）Filtering：Centrifugal filtration is first carried out, by step（1）The tea liquid natural sedimentation for obtaining 4 hours, take supernatant is by rotating speed The high speed tube centrifuge filtering of 18000r/min, obtains the tea liquid poor without insoluble and suspended particulate substance, translucency is precipitated, and sinks The protein and impurity for forming sediment are discarded；Membrane filtration is carried out again, is 0.2 μm by filter sizes by the tea liquid of centrifugal filtration Membrane filtering machine filtering, filter pressure is maintained at 0.45MPa, obtains the good tea liquid of limpid transparent, translucency；

3）Concentrate drying：By step（2）The tea liquid for obtaining is concentrated in vacuo, and keeps vacuum in -0.0725MPa, temperature 55 DEG C, it is 1.225 to be concentrated into proportion, receives cream, and condensed cream is uniformly laid on baking tray, and baking tray is placed on the grill of rotation, is protected Hold and carry out under the conditions of vacuum -0.0775MPa, 55 DEG C of temperature microwave drying, dry to rewinding during moisture 4.25%；Then will be dry Dry tea cream, is crushed with pulverizer, and sieving obtains the Pu'er tea that granularity is 100 mesh.

The preparation method of composition is put into wet mixing pelletizer to weigh raw material by weight, after mixing 30 minutes, It is 1 that material is sprayed into the weight ratio of alcohol：0.025 95% edible alcohol, mixing granulation discharges for 25 minutes, obtains composition.

The auxiliary material for pharmaceutically receiving is added to be prepared into powder in composition obtained in embodiment 17.

Composition obtained in embodiment 17 preparing prevention/auxiliary treatment toxin expelling defaecation, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or Application in health food.

Embodiment 18

1）Weigh：65 parts of moringa oleifera leaf extractive, 6 parts of emblic leafflower powder, 7 parts of Noni fruit powder, 3 parts of aloe extract, Pu'er tea is extracted 8 parts of thing, 2 parts of protein sugar is standby；

2）Mixing：By step 1）In the material input wet mixing pelletizer of middle weighing, after mixing 35 minutes, material and wine are sprayed into The weight ratio of essence is 1：0.025 95% edible alcohol, mixer-granulator continues to run with discharging in 27 minutes, obtains composition.

The extracting method of described moringa oleifera leaf extractive includes：

1）Extract：During leaf of Moringa raw material weighing put into extractor, 7 times of drinking water of amount are added, soaked 3 hours；To extract Tank condenser cooling water pressure is maintained at 0.4MPa, and extractor steam heated pressure is maintained at 0.25MPa, tank Nei Wenduda to be extracted It is back to when in tank to 85 DEG C, water vapor condensate, keeps the temperature at 85 DEG C and boil and carry 35 minutes, is then shut off extractor steaming Vapour, temperature is maintained at 80 DEG C in tank；Seepage pressure effects are carried out, extract solution sealing and circulating 5 in extractor and circulating pump is kept Hour, stop circulation, the liquid in extractor is all drained, obtain first time extract solution；Then by 5 times of Moringa leaf raw materials Inventory, the hot water addition extractor that temperature is 80 DEG C, after hot water is added, keep extract solution in extractor and circulating pump again Middle sealing and circulating 5 hours, then all drains the liquid in extractor, obtains second extract solution, by the discharge of Moringa leaf slag；

2）Centrifugal filtration：ON cycle pump circulation mixes 35 minutes, and first time extract solution and second extract solution are well mixed； Extract solution natural sedimentation by evenly mixing 4 hours, it is the high speed tube centrifuge of 20000r/min to take supernatant by rotating speed Filtering, obtain it is limpid it is transparent, without insoluble and suspended particulate substance Moringa leaf extract is precipitated, precipitation is discarded；

3）Concentrate drying：Moringa leaf extract is pumped into inspissator, with the hot water heating that temperature is 95 DEG C, starts vacuum dense Contracting, keeps vacuum in 65 DEG C of -0.075MPa, temperature, and it is 1.2 to be concentrated into proportion, receives cream, and condensed cream is uniformly laid on into vacuum On the baking tray of drying box, baking tray is placed on grill, carrying out vacuum under the conditions of holding vacuum -0.075MPa, 65 DEG C of temperature does It is dry, dry to rewinding during moisture 5%；Then by dry leaf of Moringa cream, crushed with pulverizer, sieving, obtain granularity for 120 mesh Moringa oleifera leaf extractive.

The extracting method of described Pu'er tea includes：

1）Extract：During Pu'er tea raw material weighing put into extractor, 8 times of drinking water of amount are added, kept for 30 DEG C, immersion 3 is small When；Extractor condenser cooling water and the heating of extractor jacket steam are opened, when temperature reaches 60 DEG C in tank to be extracted, and is controlled Ultrasonically treated 1.5h under temperature 60 C, then by leaching liquor closed cycle 1.5h, ultrasonically treated and closed cycle is repeated 4 times, Tea liquid, tea grounds discharge are obtained after being filtered through 100 mesh filter screens；

2）Filtering：Centrifugal filtration is first carried out, by step（1）The tea liquid natural sedimentation for obtaining 5 hours, take supernatant is by rotating speed The high speed tube centrifuge filtering of 20000r/min, obtains the tea liquid poor without insoluble and suspended particulate substance, translucency is precipitated, and sinks The protein and impurity for forming sediment are discarded；Membrane filtration is carried out again, is 0.22 μ by filter sizes by the tea liquid of centrifugal filtration The Membrane filtering machine filtering of m, filter pressure is maintained at 0.5MPa, obtains the good tea liquid of limpid transparent, translucency；

3）Concentrate drying：By step（2）The tea liquid for obtaining is concentrated in vacuo, and keeps vacuum in -0.075MPa, temperature 60 DEG C, it is 1.25 to be concentrated into proportion, receives cream, and condensed cream is uniformly laid on baking tray, and baking tray is placed on the grill of rotation, is kept Microwave drying is carried out under the conditions of vacuum -0.08MPa, temperature 60 C, is dried to rewinding during moisture 4.5%；Then will be dry Tea cream, is crushed with pulverizer, and sieving obtains the Pu'er tea that granularity is 120 mesh.

The preparation method of composition is put into wet mixing pelletizer to weigh raw material by weight, after mixing 35 minutes, It is 1 that material is sprayed into the weight ratio of alcohol：0.025 95% edible alcohol, mixing granulation discharges for 30 minutes, obtains composition.

The auxiliary material for pharmaceutically receiving is added to be prepared into capsule in composition obtained in embodiment 18.In described auxiliary material Containing 9 parts of cyclodextrin（It is herein weight portion, and it is identical with weight portion in raw material）.

Described composition is preparing the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food In application.

Embodiment 19

The extraction of moringa oleifera leaf extractive：

1）During leaf of Moringa raw material weighing put into extractor, 6 times of drinking water of amount are added, soaked 2 hours；

2）Extractor condenser cooling water and the heating of extractor jacket steam are opened, condenser cooling water pressure is maintained at 0.3MPa, Extractor steam heated pressure is maintained at 0.2MPa, and temperature reaches 85 DEG C in tank to be extracted, water vapor condensate is back in tank When, keep the temperature at 80 DEG C and boil and carry 30 minutes, extractor steam is then shut off, temperature is maintained at 75 DEG C in tank；

3）First time diacolation is circulated：Transfusion valve between standard-sized sheet extractor and outer circulation inspissator, makes the extraction in extractor Liquid is entered in stainless steel circulating pump by outlet valve, and be pumped into extractor the liquid of extract solution not again by open the circulation pump Disconnected circulation, extract solution enters to circulate pump valve and keeps standard-sized sheet, circulating-pump outlet to lead to extractor inner valve standard-sized sheet, towards extract solution storage The pipe valve of tank is closed, and cracked ends circulating pump is not pumped into extractor to liquid, and whole process is in dynamic, increased Moringa effectively into Divide the speed of dissolution, in this case sealing and circulating 4 hours；Stop circulation, close circulating-pump outlet and lead to extractor inner valve, The fully open pipe valve towards extraction liquid storage tank, the liquid in extractor is all drained；

4）Second diacolation circulation：The pipe valve and extractor bleeder valve for leading to and extracting liquid storage tank are closed, circulating-pump outlet leads to Toward extractor inner valve standard-sized sheet, standard-sized sheet hot-water cylinder enters circulation pump valve, by 4 times of Moringa leaf raw material inventorys, temperature be 75 DEG C of hot water is added and extracts storage tank, after hot water is added, repeat step（3）First time diacolation circulate operation after, by extractor Interior liquid is all drained, by the discharge of Moringa leaf slag；

5）No. first, second extract solution extracted in liquid storage tank is well mixed, standard-sized sheet extracts liquid storage tank and enters circulation pump valve, Standard-sized sheet circulating-pump outlet leads to extract solution storage tank valve, and ON cycle pump circulation mixes 30 minutes, termination of pumping；

6）Natural sedimentation 3 hours in extract solution feeding settling tank, it is the high speed tubular type of 16000r/min to take supernatant by rotating speed Centrifuge is filtered, obtain it is limpid it is transparent, without insoluble and suspended particulate substance Moringa leaf extract is precipitated, precipitation is discarded；

7）The extract solution that will be extracted in liquid storage tank is pumped into chuck vacuum concentrator, is added with the hot water that temperature in hot-water cylinder is 90 DEG C Heat, starts vacuum concentration, keeps vacuum in -0.07MPa, temperature 60 C, and it is 1.15 to be concentrated into proportion, cream is received, by condensed cream Uniformly it is laid on the baking tray of vacuum drying chamber, baking tray is placed on grill, keeps vacuum -0.07MPa, temperature 60 C condition Under be vacuum dried, dry to rewinding during moisture 4.5%；Then by dry leaf of Moringa cream, crushed with pulverizer, sieving, Obtain the moringa oleifera leaf extractive that granularity is 80 mesh.

The extraction of Pu'er tea：

1）During Pu'er tea raw material weighing put into extractor, 6 times of drinking water of amount are added, kept for 10 DEG C, soaked 2 hours；

2）Extractor condenser cooling water and the heating of extractor jacket steam are opened, when temperature reaches 50 DEG C in tank to be extracted, and Ultrasonically treated 0.5h under control temperature 50 C, then leaching liquor is extracted out in top addition closed cycle 0.5h, at ultrasound from tank bottom Reason and closed cycle are repeated 2 times, and tea liquid, tea grounds discharge are obtained after being filtered through 100 mesh filter screens；

3）Tea liquid feeding settling tank natural sedimentation 4 hours, takes supernatant by rotating speed for the high speed tubular type of 16000r/min is centrifuged Machine is filtered, and is obtained without precipitation insoluble and suspended particulate substance but the poor tea liquid of translucency, and the protein for precipitating and impurity are useless Abandon；

4）The tea liquid filtered by high speed tube centrifuge is filtered by the Membrane filtering machine that filter sizes are 0.1 μm, filter pressure 0.4MPa is maintained at, the good tea liquid of limpid transparent, translucency is obtained；

5）The tea liquid of extraction starts vacuum concentration, keeps vacuum in -0.07MPa, temperature 50 C, and it is 1.2 to be concentrated into proportion, is received Cream, condensed cream is uniformly laid on baking tray, and baking tray is placed on the grill of rotation, keeps vacuum -0.075MPa, temperature 50 Microwave drying is carried out under the conditions of DEG C, is dried to rewinding during moisture 4%；Then by dry tea cream, with 5.5KW Universalpulverizer powder Broken, sieving obtains the Pu'er tea that granularity is 80 mesh.

The preparation of emblic leafflower powder：

1）Drum-type fruit washing machine, cylinder rotating speed is used to be maintained at 15 revs/min after wild fresh fruit of fructus phyllanthi is rejected into decayed fruit, impurity, Water spray flow 5m³/ h, charging rate is maintained at 8 kg/minutes, the fresh fruit for being cleaned up, and described water is drinking water；

2）Using fruit crusher, charging rate is maintained at 5 kg/minutes, and the fresh fruit that will be cleaned up is broken for granularity 2mm's Particle；

3）Using fruit pressafiner, rotating speed is maintained at 60 revs/min, and particle is at the uniform velocity added, and it is public that charging rate is maintained at 3 Jin/minute, pomace is discharged, underflow fruit juice flows out through filter screen from bottom；

4）Using centrifuge, drum speed is maintained at 1000 revs/min, by step 3）The underflow fruit juice for obtaining at the uniform velocity is added, and is entered Material speed is maintained at 0.2 m³/ minute, the slag discharge isolated obtains fruit juice clear liquid；

5）Natural sedimentation 3 hours in fruit juice feeding taper settling tank, it is the high-velocity tube of 16000r/min to take supernatant by rotating speed Formula centrifuge is filtered, obtain it is limpid it is transparent, without insoluble and suspended particulate substance phyllanthus emblica L.juice is precipitated, precipitation is discarded；

6）By step（5）The fruit juice clear liquid of gained is spray-dried, and high speed centrifugal atomization device rotating speed is maintained at 6000 revs/min Clock, regulation air-supply and the air flow rate proportioning of air inducing, make spraying system be maintained between negative pressure 50Pa, and tower top inlet temperature is maintained at 230 DEG C, bottom of towe outlet temperature is maintained at 110 DEG C, and 10 beats/min of pulse rapping stablized screw pump feed rate at 80L/ minutes, Spray drying is carried out continuously, the emblic leafflower powder that granularity is 200 mesh is obtained.

The preparation of Noni fruit powder：

1）Drum-type fruit washing machine, cylinder rotating speed is used to be maintained at 10 revs/min, water spray after Noni fruit fresh fruit is rejected into decayed fruit, impurity Drench flow 3m³/ h, charging rate is maintained at 3 kg/minutes, the fresh fruit for being cleaned up, and described water is drinking water；

2）Using fruit spiral juice extractor, rotating speed is maintained at 50 revs/min, and particle is at the uniform velocity added, and it is public that charging rate is maintained at 1 Jin/minute, pomace is discharged, underflow fruit juice flows out through filter screen from bottom；

3）Using centrifuge, drum speed is maintained at 1000 revs/min, by step 2）The underflow fruit juice for obtaining at the uniform velocity is added, and is entered Material speed is maintained at 0.2 m³/ minute, the slag discharge isolated obtains fruit juice clear liquid；

4）Natural sedimentation 3 hours in fruit juice feeding taper settling tank, it is the high-velocity tube of 16000r/min to take supernatant by rotating speed Formula centrifuge is filtered, obtain it is limpid it is transparent, without insoluble and suspended particulate substance Morinda Citrifolia juice is precipitated, precipitation is discarded；

5）By step（4）The fruit juice clear liquid of gained is spray-dried, and high speed centrifugal atomization device rotating speed is maintained at 6000 revs/min Clock, regulation air-supply and the air flow rate proportioning of air inducing, make spraying system be maintained between negative pressure 50Pa, and tower top inlet temperature is maintained at 220 DEG C, bottom of towe outlet temperature is maintained at 100 DEG C, and 10 beats/min of pulse rapping stablized screw pump feed rate at 80L/ minutes, Spray drying is carried out continuously, the Noni fruit powder that granularity is 200 mesh is obtained.

The preparation of aloe extract：

1）Aloe raw material is weighed in putting into extractor, add 6 times of drinking water of amount, 10 DEG C, soaked 2 hours；

2）Extractor condenser and steam heating are opened, when temperature reaches 50 DEG C in tank to be extracted, and controls to surpass under temperature 50 C Sonication 0.5h, then leaching liquor is extracted out in top addition closed cycle 0.5h from tank bottom, ultrasonically treated and closed cycle is repeated Operation 2 times, obtains extract solution, slag discharge after filtering；

3）Extract solution feeding settling tank natural sedimentation 3 hours, takes supernatant and is centrifuged by the high speed tubular type of rotating speed 16000r/min Machine is filtered, and is obtained without precipitation insoluble and suspended particulate substance but the poor extract solution of translucency, and precipitation is discarded；

4）The extract solution filtered by high speed tube centrifuge is filtered by the Membrane filtering machine that filter sizes are 0.1 μm, filtration pressure Power is maintained at 0.4MPa, obtains the good extract solution from aloe of limpid transparent, translucency；

5）Extract solution starts vacuum concentration, keeps vacuum in -0.07MPa, temperature 60 C, and it is 1.2 to be concentrated into proportion, receives cream, Condensed cream is uniformly laid on baking tray, baking tray is placed on the grill of rotation, keep vacuum -0.07MPa, temperature 60 C bar Microwave drying is carried out under part, is dried to rewinding during moisture 5%；Then by dry aloe ointment, with 5.5KW Universalpulverizer powder Broken, sieving obtains the aloe extract that granularity is 80 mesh.

The preparation of the granule of composition：

1）Weigh：50 parts of moringa oleifera leaf extractive, 6 parts of emblic leafflower powder, 6 parts of Noni fruit powder, 6 parts of aloe extract are weighed by weight It is standby；

2）Mixing granulation：By step 1）In the material input wet mixing pelletizer of middle weighing, after mixing 25 minutes, material is sprayed into It is 1 with the weight ratio of alcohol：0.025 95% edible alcohol, mixer-granulator continues to run with discharging in 20 minutes, obtains wet Grain；

3）Wet granular fluidized drying：By have to wet granular be placed on the hothouse dispersion plate of fluidized dryer, regulation is dry Dry room aspiration pressure is 0.5 MPa, temperature is 100 DEG C, fluidized drying is carried out, when hothouse leaving air temp rises to 60 DEG C, water Point 5% is no more than, closes air heater, when drying indoor temperature and being reduced to less than 40 DEG C, discharged, obtain dry particl；

4）Dried material particles are added in pelletizing machine, filter out the particle of even particle size, standby；5）Whole grain it is good Grain is dispensed with back of the body envelope formula particles packing machine, every bag of 0.5g of loading amount；

6）After the granule for having dispensed carries out irradiation sterilization, packed with tub outer box, 30 bags every barrel.

Case 1：Open XX, female, 48 years old, frequent constipation, difficult defecation.But also be fond of drinking, often dizzy, an XX is daily Adhere to that drinking the embodiment of the present invention 19 prepares 3 bags of leaf of Moringa granule, constipation and the dizziness for causing of drinking after taking two weeks Symptom mitigation, constipation and dizziness disappear after 3 months.

Embodiment 20

The extraction of moringa oleifera leaf extractive：

1）During leaf of Moringa raw material weighing put into extractor, 6.5 times of drinking water of amount are added, soaked 2.5 hours；

2）Extractor condenser cooling water and the heating of extractor jacket steam are opened, condenser cooling water pressure is maintained at 0.35MPa, Extractor steam heated pressure is maintained at 0.225MPa, in tank to be extracted temperature reach 85 DEG C, water vapor condensate be back to tank When interior, keep the temperature at 82 DEG C and boil and carry 30 minutes, be then shut off extractor steam, temperature is maintained at 78 DEG C in tank；

3）First time diacolation is circulated：Transfusion valve between standard-sized sheet extractor and outer circulation inspissator, makes the extraction in extractor Liquid is entered in stainless steel circulating pump by outlet valve, and be pumped into extractor the liquid of extract solution not again by open the circulation pump Disconnected circulation, extract solution enters to circulate pump valve and keeps standard-sized sheet, circulating-pump outlet to lead to extractor inner valve standard-sized sheet, towards extract solution storage The pipe valve of tank is closed, and cracked ends circulating pump is not pumped into extractor to liquid, and whole process is in dynamic, increased Moringa effectively into Divide the speed of dissolution, in this case sealing and circulating 4.5 hours；Stop circulation, close circulating-pump outlet and lead to extractor internal valve Door, it is fully open towards the pipe valve for extracting liquid storage tank, the liquid in extractor is all drained；

4）Second diacolation circulation：The pipe valve and extractor bleeder valve for leading to and extracting liquid storage tank are closed, circulating-pump outlet leads to Toward extractor inner valve standard-sized sheet, standard-sized sheet hot-water cylinder enters circulation pump valve, by 4.8 times of Moringa leaf raw material inventorys, temperature Storage tank, after hot water is added, repeat step are extracted for 78 DEG C of hot water are added（3）First time diacolation circulate operation after, will extract Liquid in tank is all drained, by the discharge of Moringa leaf slag；

6）Natural sedimentation 3 hours in extract solution feeding settling tank, it is the high speed tubular type of 18000r/min to take supernatant by rotating speed Centrifuge is filtered, obtain it is limpid it is transparent, without insoluble and suspended particulate substance Moringa leaf extract is precipitated, precipitation is discarded；

7）The extract solution that will be extracted in liquid storage tank is pumped into chuck vacuum concentrator, is added with the hot water that temperature in hot-water cylinder is 92 DEG C Heat, starts vacuum concentration, keeps vacuum in 62 DEG C of -0.0725MPa, temperature, and it is 1.175 to be concentrated into proportion, receives cream, will be concentrated Cream is uniformly laid on the baking tray of vacuum drying chamber, and baking tray is placed on grill, keeps vacuum -0.0725MPa, 62 DEG C of temperature Under the conditions of be vacuum dried, dry to rewinding during moisture 4.75%；Then by dry leaf of Moringa cream, crushed with pulverizer, Sieving, obtains the moringa oleifera leaf extractive that granularity is 100 mesh.

The extraction of Pu'er tea：

1）During Pu'er tea raw material weighing put into extractor, 7 times of drinking water of amount are added, kept for 20 DEG C, soaked 2.5 hours；

2）Extractor condenser cooling water and the heating of extractor jacket steam are opened, when temperature reaches 55 DEG C in tank to be extracted, and Ultrasonically treated 1h at 55 DEG C of temperature of control, then leaching liquor is extracted out from tank bottom add closed cycle 1h in top, it is ultrasonically treated and Closed cycle is repeated 3 times, and tea liquid, tea grounds discharge are obtained after being filtered through 100 mesh filter screens；

3）Tea liquid feeding settling tank natural sedimentation 4 hours, takes supernatant by rotating speed for the high speed tubular type of 18000r/min is centrifuged Machine is filtered, and is obtained without precipitation insoluble and suspended particulate substance but the poor tea liquid of translucency, and the protein for precipitating and impurity are useless Abandon；

4）The tea liquid filtered by high speed tube centrifuge is filtered by the Membrane filtering machine that filter sizes are 0.2 μm, filter pressure 0.45MPa is maintained at, the good tea liquid of limpid transparent, translucency is obtained；

5）The tea liquid of extraction starts vacuum concentration, keeps vacuum in 55 DEG C of -0.0725MPa, temperature, and being concentrated into proportion is 1.225, cream is received, condensed cream is uniformly laid on baking tray, baking tray is placed on the grill of rotation, holding vacuum- Microwave drying is carried out under the conditions of 0.0775MPa, 55 DEG C of temperature, is dried to rewinding during moisture 4.25；Then by dry tea cream, use 5.5KW Universalpulverizers are crushed, sieving, obtain the Pu'er tea that granularity is 100 mesh.

The preparation of emblic leafflower powder：

1）Drum-type fruit washing machine, cylinder rotating speed is used to be maintained at 18 revs/min after wild fresh fruit of fructus phyllanthi is rejected into decayed fruit, impurity, Water spray flow 8m³/ h, charging rate is maintained at 9 kg/minutes, the fresh fruit for being cleaned up, and described water is drinking water；

2）Using fruit crusher, charging rate is maintained at 6 kg/minutes, and the fresh fruit that will be cleaned up is broken for granularity 4mm's Particle；

3）Using fruit pressafiner, rotating speed is maintained at 65 revs/min, and particle is at the uniform velocity added, and it is public that charging rate is maintained at 4 Jin/minute, pomace is discharged, underflow fruit juice flows out through filter screen from bottom；

4）Using centrifuge, drum speed is maintained at 1250 revs/min, by step 3）The underflow fruit juice for obtaining at the uniform velocity is added, and is entered Material speed is maintained at 0.4 m³/ minute, the slag discharge isolated obtains fruit juice clear liquid；

5）Natural sedimentation 3 hours in fruit juice feeding taper settling tank, it is the high-velocity tube of 18000r/min to take supernatant by rotating speed Formula centrifuge is filtered, obtain it is limpid it is transparent, without insoluble and suspended particulate substance phyllanthus emblica L.juice is precipitated, precipitation is discarded；

6）By step（5）The fruit juice clear liquid of gained is spray-dried, and high speed centrifugal atomization device rotating speed is maintained at 6250 revs/min Clock, regulation air-supply and the air flow rate proportioning of air inducing, make spraying system be maintained between negative pressure 100Pa, and tower top inlet temperature is maintained at 230 ~ 240 DEG C, bottom of towe outlet temperature is maintained at 105 DEG C, and 10 beats/min of pulse rapping stablizes screw pump feed rate in 90L/ Minute, spray drying is carried out continuously, obtain the emblic leafflower powder that granularity is 250 mesh.

The preparation of Noni fruit powder：

1）Drum-type fruit washing machine, cylinder rotating speed is used to be maintained at 12 revs/min, water spray after Noni fruit fresh fruit is rejected into decayed fruit, impurity Drench flow 5m³/ h, charging rate is maintained at 4 kg/minutes, the fresh fruit for being cleaned up, and described water is drinking water；

2）Using fruit spiral juice extractor, rotating speed is maintained at 55 revs/min, and particle is at the uniform velocity added, and it is public that charging rate is maintained at 2 Jin/minute, pomace is discharged, underflow fruit juice flows out through filter screen from bottom；

3）Using centrifuge, drum speed is maintained at 1250 revs/min, by step 2）The underflow fruit juice for obtaining at the uniform velocity is added, and is entered Material speed is maintained at 0.4m³/ minute, the slag discharge isolated obtains fruit juice clear liquid；

4）Natural sedimentation 3 hours in fruit juice feeding taper settling tank, it is the high-velocity tube of 18000r/min to take supernatant by rotating speed Formula centrifuge is filtered, obtain it is limpid it is transparent, without insoluble and suspended particulate substance Morinda Citrifolia juice is precipitated, precipitation is discarded；

5）By step（4）The fruit juice clear liquid of gained is spray-dried, and high speed centrifugal atomization device rotating speed is maintained at 6250 revs/min Clock, regulation air-supply and the air flow rate proportioning of air inducing, make spraying system be maintained between negative pressure 100Pa, and tower top inlet temperature is maintained at 225 DEG C, bottom of towe outlet temperature is maintained at 105 DEG C, and 10 beats/min of pulse rapping stablized screw pump feed rate at 90L/ minutes, Spray drying is carried out continuously, the Noni fruit powder that granularity is 250 mesh is obtained.

The preparation of aloe extract：

1）Aloe raw material is weighed in putting into extractor, add 7 times of drinking water of amount, 20 DEG C, soaked 2.5 hours；

2）Extractor condenser and steam heating are opened, when temperature reaches 55 DEG C in tank to be extracted, and controls to surpass at 55 DEG C of temperature Sonication 1h, then leaching liquor is extracted out in top addition closed cycle 1h from tank bottom, ultrasonically treated and closed cycle repeats 3 It is secondary, extract solution, slag discharge are obtained after filtering；

3）Extract solution feeding settling tank natural sedimentation 3 hours, takes supernatant and is centrifuged by the high speed tubular type of rotating speed 18000r/min Machine is filtered, and is obtained without precipitation insoluble and suspended particulate substance but the poor extract solution of translucency, and precipitation is discarded；

4）The extract solution filtered by high speed tube centrifuge is filtered by the Membrane filtering machine that filter sizes are 0.2 μm, filtration pressure Power is maintained at 0.45MPa, obtains the good extract solution from aloe of limpid transparent, translucency；

5）Extract solution starts vacuum concentration, keeps vacuum in 62 DEG C of -0.0725MPa, temperature, and it is 1.225 to be concentrated into proportion, is received Cream, condensed cream is uniformly laid on baking tray, and baking tray is placed on the grill of rotation, keeps vacuum -0.0725MPa, temperature Microwave drying is carried out under the conditions of 62 DEG C, is dried to rewinding during moisture 5.25%；Then it is omnipotent with 5.5KW by dry aloe ointment Pulverizer is crushed, sieving, obtains the aloe extract that granularity is 100 mesh.

The preparation of the granule of composition：

1）Weigh：Weigh 55 parts of moringa oleifera leaf extractive, 10 parts of emblic leafflower powder, 10 parts of Noni fruit powder, 6 parts of aloe extract, Pu'er 4 parts of tea extraction, it is standby；

2）Mixing granulation：By step 1）In the material input wet mixing pelletizer of middle weighing, after mixing 26 minutes, material is sprayed into It is 1 with the weight ratio of alcohol：0.025 95% edible alcohol, mixer-granulator continues to run with discharging in 22 minutes, obtains wet Grain；

3）Wet granular fluidized drying：By have to wet granular be placed on the hothouse dispersion plate of fluidized dryer, regulation is dry Dry room aspiration pressure is 0.5 MPa, temperature is 100 DEG C, fluidized drying is carried out, when hothouse leaving air temp rises to 63 DEG C, water Point 5% is no more than, closes air heater, when drying indoor temperature and being reduced to less than 38 DEG C, discharged, obtain dry particl；

Case 2：Lee XX, man, 72 years old, retired professor was perplexed by the problem of constipation and osteoporosis always.Lee XX is hard daily Hold and take the embodiment of the present invention 20 and prepare 5 bags of the composition granule containing moringa oleifera leaf extractive, constipation and osteoporosis Problem is substantially improved, healthy.

Embodiment 21

The extraction of moringa oleifera leaf extractive：

1）During leaf of Moringa raw material weighing put into extractor, 7 times of drinking water of amount are added, soaked 3 hours；

2）Extractor condenser cooling water and the heating of extractor jacket steam are opened, condenser cooling water pressure is maintained at 0.4MPa, Extractor steam heated pressure is maintained at 0.25MPa, and temperature reaches 85 DEG C in tank to be extracted, water vapor condensate is back in tank When, keep the temperature at 85 DEG C and boil and carry 30 minutes, extractor steam is then shut off, temperature is maintained at 80 DEG C in tank；

3）First time diacolation is circulated：Transfusion valve between standard-sized sheet extractor and outer circulation inspissator, makes the extraction in extractor Liquid is entered in stainless steel circulating pump by outlet valve, and be pumped into extractor the liquid of extract solution not again by open the circulation pump Disconnected circulation, extract solution enters to circulate pump valve and keeps standard-sized sheet, circulating-pump outlet to lead to extractor inner valve standard-sized sheet, towards extract solution storage The pipe valve of tank is closed, and cracked ends circulating pump is not pumped into extractor to liquid, and whole process is in dynamic, increased Moringa effectively into Divide the speed of dissolution, in this case sealing and circulating 5 hours；Stop circulation, close circulating-pump outlet and lead to extractor inner valve, The fully open pipe valve towards extraction liquid storage tank, the liquid in extractor is all drained；

4）Second diacolation circulation：The pipe valve and extractor bleeder valve for leading to and extracting liquid storage tank are closed, circulating-pump outlet leads to Toward extractor inner valve standard-sized sheet, standard-sized sheet hot-water cylinder enters circulation pump valve, by 5 times of Moringa leaf raw material inventorys, temperature be 80 DEG C of hot water is added and extracts storage tank, after hot water is added, repeat step（3）First time diacolation circulate operation after, by extractor Interior liquid is all drained, by the discharge of Moringa leaf slag；

6）Natural sedimentation 3 hours in extract solution feeding settling tank, it is the high speed tubular type of 20000r/min to take supernatant by rotating speed Centrifuge is filtered, obtain it is limpid it is transparent, without insoluble and suspended particulate substance Moringa leaf extract is precipitated, precipitation is discarded；

7）The extract solution that will be extracted in liquid storage tank is pumped into chuck vacuum concentrator, is added with the hot water that temperature in hot-water cylinder is 95 DEG C Heat, starts vacuum concentration, keeps vacuum in 65 DEG C of -0.075MPa, temperature, and it is 1.2 to be concentrated into proportion, cream is received, by condensed cream Uniformly it is laid on the baking tray of vacuum drying chamber, baking tray is placed on grill, keeps vacuum -0.075MPa, 65 DEG C of bars of temperature It is vacuum dried under part, is dried to rewinding during moisture 5%；Then by dry leaf of Moringa cream, crushed with pulverizer, sieving, Obtain the moringa oleifera leaf extractive that granularity is 120 mesh.

The extraction of Pu'er tea：

1）During Pu'er tea raw material weighing put into extractor, 8 times of drinking water of amount are added, kept for 30 DEG C, soaked 3 hours；

2）Extractor condenser cooling water and the heating of extractor jacket steam are opened, when temperature reaches 60 DEG C in tank to be extracted, and Ultrasonically treated 1.5h under control temperature 60 C, then leaching liquor is extracted out in top addition closed cycle 1.5h, at ultrasound from tank bottom Reason and closed cycle are repeated 4 times, and tea liquid, tea grounds discharge are obtained after being filtered through 100 mesh filter screens；

3）Tea liquid feeding settling tank natural sedimentation 4 hours, takes supernatant by rotating speed for the high speed tubular type of 20000r/min is centrifuged Machine is filtered, and is obtained without precipitation insoluble and suspended particulate substance but the poor tea liquid of translucency, and the protein for precipitating and impurity are useless Abandon；

4）The tea liquid filtered by high speed tube centrifuge is filtered by the Membrane filtering machine that filter sizes are 0.22 μm, filter pressure 0.5MPa is maintained at, the good tea liquid of limpid transparent, translucency is obtained；

5）The tea liquid of extraction starts vacuum concentration, keeps vacuum in -0.075MPa, temperature 60 C, and it is 1.25 to be concentrated into proportion, Cream is received, condensed cream is uniformly laid on baking tray, baking tray is placed on the grill of rotation, keep vacuum -0.08MPa, temperature Microwave drying is carried out under the conditions of 60 DEG C, is dried to rewinding during moisture 4.5%；Then by dry tea cream, with the omnipotent crushing of 5.5KW Machine is crushed, sieving, obtains the Pu'er tea that granularity is 120 mesh.

The preparation of emblic leafflower powder：

1）Drum-type fruit washing machine, cylinder rotating speed is used to be maintained at 20 revs/min after wild fresh fruit of fructus phyllanthi is rejected into decayed fruit, impurity, Water spray flow 10m³/ h, charging rate is maintained at 10 kg/minutes, the fresh fruit for being cleaned up, and described water is to drink Water；

2）Using fruit crusher, charging rate is maintained at 8 kg/minutes, and the fresh fruit that will be cleaned up is broken for granularity 5mm's Particle；

3）Using fruit pressafiner, rotating speed is maintained at 70 revs/min, and particle is at the uniform velocity added, and it is public that charging rate is maintained at 5 Jin/minute, pomace is discharged, underflow fruit juice flows out through filter screen from bottom；

4）Using centrifuge, drum speed is maintained at 1500 revs/min, by step 3）The underflow fruit juice for obtaining at the uniform velocity is added, and is entered Material speed is maintained at 0.5 m³/ minute, the slag discharge isolated obtains fruit juice clear liquid；

5）Natural sedimentation 3 hours in fruit juice feeding taper settling tank, it is the high-velocity tube of 20000r/min to take supernatant by rotating speed Formula centrifuge is filtered, obtain it is limpid it is transparent, without insoluble and suspended particulate substance phyllanthus emblica L.juice is precipitated, precipitation is discarded；

6）By step（5）The fruit juice clear liquid of gained is spray-dried, and high speed centrifugal atomization device rotating speed is maintained at 6500 revs/min Clock, regulation air-supply and the air flow rate proportioning of air inducing, make spraying system be maintained between negative pressure 200Pa, and tower top inlet temperature is maintained at 240 DEG C, bottom of towe outlet temperature is maintained at 120 DEG C, and 10 beats/min of pulse rapping, stabilization screw pump feed rate divides in 100L/ Clock, is carried out continuously spray drying, obtains the emblic leafflower powder that granularity is 300 mesh.

The preparation of Noni fruit powder：

1）Drum-type fruit washing machine, cylinder rotating speed is used to be maintained at 15 revs/min, water spray after Noni fruit fresh fruit is rejected into decayed fruit, impurity Drench flow 7m³/ h, charging rate is maintained at 5 kg/minutes, the fresh fruit for being cleaned up, and described water is drinking water；

2）Using fruit spiral juice extractor, rotating speed is maintained at 60 revs/min, and particle is at the uniform velocity added, and it is public that charging rate is maintained at 3 Jin/minute, pomace is discharged, underflow fruit juice flows out through filter screen from bottom；

3）Using centrifuge, drum speed is maintained at 1500 revs/min, by step（2）The underflow fruit juice for obtaining at the uniform velocity is added, and is entered Material speed is maintained at 0.5 m³/ minute, the slag discharge isolated obtains fruit juice clear liquid；

4）Natural sedimentation 3 hours in fruit juice feeding taper settling tank, it is the high-velocity tube of 20000r/min to take supernatant by rotating speed Formula centrifuge is filtered, obtain it is limpid it is transparent, without insoluble and suspended particulate substance Morinda Citrifolia juice is precipitated, precipitation is discarded；

5）By step（4）The fruit juice clear liquid of gained is spray-dried, and high speed centrifugal atomization device rotating speed is maintained at 6500 revs/min Clock, regulation air-supply and the air flow rate proportioning of air inducing, make spraying system be maintained between negative pressure 200Pa, and tower top inlet temperature is maintained at 230 DEG C, bottom of towe outlet temperature is maintained at 110 DEG C, and 10 beats/min of pulse rapping, stabilization screw pump feed rate divides in 100L/ Clock, is carried out continuously spray drying, obtains the Noni fruit powder that granularity is 300 mesh.

The preparation of aloe extract：

1）Aloe raw material is weighed in putting into extractor, add 8 times of drinking water of amount, kept for 30 DEG C, soaked 3 hours；

2）Extractor condenser and steam heating are opened, when temperature reaches 60 DEG C in tank to be extracted, and controls to surpass under temperature 60 C Sonication 1.5h, then leaching liquor is extracted out in top addition closed cycle 1.5h from tank bottom, ultrasonically treated and closed cycle is repeated Operation 4 times, obtains extract solution, slag discharge after filtering；

3）Extract solution feeding settling tank natural sedimentation 3 hours, takes supernatant and is centrifuged by the high speed tubular type of rotating speed 20000r/min Machine is filtered, and is obtained without precipitation insoluble and suspended particulate substance but the poor extract solution of translucency, and precipitation is discarded；

4）The extract solution filtered by high speed tube centrifuge is filtered by the Membrane filtering machine that filter sizes are 0.22 μm, filtration pressure Power is maintained at 0.5MPa, obtains the good extract solution from aloe of limpid transparent, translucency；

5）Extract solution starts vacuum concentration, keeps vacuum in 65 DEG C of -0.075MPa, temperature, and it is 1.25 to be concentrated into proportion, is received Cream, condensed cream is uniformly laid on baking tray, and baking tray is placed on the grill of rotation, keeps vacuum -0.075MPa, temperature 65 Microwave drying is carried out under the conditions of DEG C, is dried to rewinding during moisture 5.5%；Then by dry aloe ointment, with the omnipotent crushing of 5.5KW Machine is crushed, sieving, obtains the aloe extract that granularity is 120 mesh.

The preparation of the granule of composition：

1）Weigh：Weigh 60 parts of moringa oleifera leaf extractive, 8 parts of emblic leafflower powder, 7 parts of Noni fruit powder, 4 parts of aloe extract, Pu'er tea 7 parts of extract, 3 parts of protein sugar, 11 parts of cyclodextrin is standby；

2）Mixing granulation：By step 1）In the material input wet mixing pelletizer of middle weighing, after mixing 28 minutes, material is sprayed into It is 1 with the weight ratio of alcohol：0.025 95% edible alcohol, mixer-granulator continues to run with discharging in 23 minutes, obtains wet Grain；

3）Wet granular fluidized drying：By have to wet granular be placed on the hothouse dispersion plate of fluidized dryer, regulation is dry Dry room aspiration pressure is 0.5 MPa, temperature is 100 DEG C, fluidized drying is carried out, when hothouse leaving air temp rises to 65 DEG C, water Point 5% is no more than, closes air heater, when drying indoor temperature and being reduced to less than 35 DEG C, discharged, obtain dry particl；

Case 3：Zhao XX, female, 23 years old, body immunity was low, liable to illness.Zhao XX adheres to taking the embodiment of the present invention daily 21 prepare 5 bags of the granule containing moringa oleifera leaf extractive, continuously take 3 months, and immunity is significantly improved, and sick number of times is big It is big to reduce and healthy, feel energetic.

Claims

1. a kind of composition containing moringa oleifera leaf extractive, it is characterised in that the raw material including following weight portion：Moringa oleifera leaf extractive 30 ~ 80 parts, 5 ~ 25 parts of emblic leafflower powder, 5 ~ 25 parts of Noni fruit powder, 1 ~ 15 part of aloe extract.

2. the composition containing moringa oleifera leaf extractive according to claim 1, it is characterised in that the original including following weight portion Material：50 ~ 65 parts of moringa oleifera leaf extractive, 6 ~ 11 parts of emblic leafflower powder, 6 ~ 15 parts of Noni fruit powder, 2 ~ 8 parts of aloe extract.

3. the composition containing moringa oleifera leaf extractive according to claim 1 and 2, it is characterised in that also including 2 ~ 10 weight portions Pu'er tea.

4. the composition containing moringa oleifera leaf extractive according to claim 1 and 2, it is characterised in that also including 1 ~ 8 part of weight The protein sugar of part.

5. the composition containing moringa oleifera leaf extractive according to claim 1, it is characterised in that described moringa oleifera leaf extractive Extracting method include extracting and developing, concentration, drying and postprocessing working procedures, specially：

6. the composition containing moringa oleifera leaf extractive according to claim 3, it is characterised in that described Pu'er tea Extracting method include extracting and developing, concentration, drying and postprocessing working procedures, specially：

7. according to the preparation method of any described composition containing moringa oleifera leaf extractive of claim 1 ~ 6, its feature exists one kind In described preparation method to weigh by weight in raw material input wet mixing pelletizer, after 25 ~ 35min of mixing, injectant Material is 1 with the weight ratio of alcohol：0.025 95% edible alcohol, 20 ~ 30min of mixing granulation dischargings, obtains composition.

8. preparation of the one kind according to any described composition containing moringa oleifera leaf extractive of claim 1 ~ 6, it is characterised in that institute The preparation stated be added in described composition the auxiliary material for pharmaceutically receiving be prepared into granule, tablet, powder, capsule, Liquid preparation, pill, medicinal tea.

9. the preparation of the composition containing moringa oleifera leaf extractive according to claim 8, it is characterised in that in described auxiliary material Contain cyclodextrin.

10. application of the one kind according to any described composition containing moringa oleifera leaf extractive of claim 1 ~ 6, it is characterised in that institute Application of the composition stated in the defaecation of prevention/auxiliary treatment toxin expelling, facilitating alcohol metabolism and protecting liver, replenish the calcium similar drug or health food is prepared.