CN106727058A - Emulsion preparation method and cosmetic composition containing lacquer tree seed extract - Google Patents
Emulsion preparation method and cosmetic composition containing lacquer tree seed extract Download PDFInfo
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- CN106727058A CN106727058A CN201710128430.5A CN201710128430A CN106727058A CN 106727058 A CN106727058 A CN 106727058A CN 201710128430 A CN201710128430 A CN 201710128430A CN 106727058 A CN106727058 A CN 106727058A
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- 244000044283 Toxicodendron succedaneum Species 0.000 title claims abstract description 49
- 239000000203 mixture Substances 0.000 title claims abstract description 28
- 239000002537 cosmetic Substances 0.000 title claims abstract description 23
- 239000000839 emulsion Substances 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- 239000003973 paint Substances 0.000 claims abstract description 8
- 108010082495 Dietary Plant Proteins Proteins 0.000 claims abstract 2
- 239000003963 antioxidant agent Substances 0.000 claims abstract 2
- 230000003078 antioxidant effect Effects 0.000 claims abstract 2
- 235000006708 antioxidants Nutrition 0.000 claims abstract 2
- 238000009472 formulation Methods 0.000 claims abstract 2
- 150000004676 glycans Chemical class 0.000 claims abstract 2
- 229920001282 polysaccharide Polymers 0.000 claims abstract 2
- 239000005017 polysaccharide Substances 0.000 claims abstract 2
- 230000037303 wrinkles Effects 0.000 claims abstract 2
- 239000007788 liquid Substances 0.000 claims description 10
- 238000000926 separation method Methods 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 8
- -1 sucrose ester Chemical class 0.000 claims description 7
- 239000003995 emulsifying agent Substances 0.000 claims description 6
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 5
- 229930195729 fatty acid Natural products 0.000 claims description 5
- 239000000194 fatty acid Substances 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000005119 centrifugation Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000012535 impurity Substances 0.000 claims description 4
- 239000008041 oiling agent Substances 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 238000004945 emulsification Methods 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims description 2
- CTKINSOISVBQLD-UHFFFAOYSA-N Glycidol Chemical compound OCC1CO1 CTKINSOISVBQLD-UHFFFAOYSA-N 0.000 claims description 2
- 229930006000 Sucrose Natural products 0.000 claims description 2
- 239000003921 oil Substances 0.000 claims description 2
- 239000005720 sucrose Substances 0.000 claims description 2
- 239000006071 cream Substances 0.000 claims 6
- 230000000844 anti-bacterial effect Effects 0.000 claims 1
- 230000003110 anti-inflammatory effect Effects 0.000 claims 1
- 230000001815 facial effect Effects 0.000 claims 1
- 125000005313 fatty acid group Chemical group 0.000 claims 1
- 239000000499 gel Substances 0.000 claims 1
- 150000003017 phosphorus Chemical class 0.000 claims 1
- 239000002453 shampoo Substances 0.000 claims 1
- 239000000344 soap Substances 0.000 claims 1
- 230000000475 sunscreen effect Effects 0.000 claims 1
- 239000000516 sunscreening agent Substances 0.000 claims 1
- 239000000606 toothpaste Substances 0.000 claims 1
- 229940034610 toothpaste Drugs 0.000 claims 1
- 239000002994 raw material Substances 0.000 abstract description 2
- 206010061218 Inflammation Diseases 0.000 abstract 1
- 230000003020 moisturizing effect Effects 0.000 abstract 1
- 239000004922 lacquer Substances 0.000 description 6
- 235000019197 fats Nutrition 0.000 description 5
- 239000003760 tallow Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- 235000019198 oils Nutrition 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 239000008157 edible vegetable oil Substances 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- CNNRPFQICPFDPO-UHFFFAOYSA-N octacosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCO CNNRPFQICPFDPO-UHFFFAOYSA-N 0.000 description 2
- 239000002023 wood Substances 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- RMTXUPIIESNLPW-UHFFFAOYSA-N 1,2-dihydroxy-3-(pentadeca-8,11-dienyl)benzene Natural products CCCC=CCC=CCCCCCCCC1=CC=CC(O)=C1O RMTXUPIIESNLPW-UHFFFAOYSA-N 0.000 description 1
- 229960002666 1-octacosanol Drugs 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QARRXYBJLBIVAK-UEMSJJPVSA-N 3-[(8e,11e)-pentadeca-8,11-dienyl]benzene-1,2-diol;3-[(8e,11e)-pentadeca-8,11,14-trienyl]benzene-1,2-diol;3-[(8e,11e,13e)-pentadeca-8,11,13-trienyl]benzene-1,2-diol;3-[(e)-pentadec-8-enyl]benzene-1,2-diol;3-pentadecylbenzene-1,2-diol Chemical compound CCCCCCCCCCCCCCCC1=CC=CC(O)=C1O.CCCCCC\C=C\CCCCCCCC1=CC=CC(O)=C1O.CCC\C=C\C\C=C\CCCCCCCC1=CC=CC(O)=C1O.C\C=C\C=C\C\C=C\CCCCCCCC1=CC=CC(O)=C1O.OC1=CC=CC(CCCCCCC\C=C\C\C=C\CC=C)=C1O QARRXYBJLBIVAK-UEMSJJPVSA-N 0.000 description 1
- IYROWZYPEIMDDN-UHFFFAOYSA-N 3-n-pentadec-8,11,13-trienyl catechol Natural products CC=CC=CCC=CCCCCCCCC1=CC=CC(O)=C1O IYROWZYPEIMDDN-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- 235000019750 Crude protein Nutrition 0.000 description 1
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- UELITFHSCLAHKR-UHFFFAOYSA-N acibenzolar-S-methyl Chemical compound CSC(=O)C1=CC=CC2=C1SN=N2 UELITFHSCLAHKR-UHFFFAOYSA-N 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 125000005233 alkylalcohol group Chemical group 0.000 description 1
- 230000002929 anti-fatigue Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 125000005456 glyceride group Chemical group 0.000 description 1
- 239000003630 growth substance Substances 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 1
- 235000020778 linoleic acid Nutrition 0.000 description 1
- 239000004530 micro-emulsion Substances 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 150000004671 saturated fatty acids Chemical class 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- DQTMTQZSOJMZSF-UHFFFAOYSA-N urushiol Natural products CCCCCCCCCCCCCCCC1=CC=CC(O)=C1O DQTMTQZSOJMZSF-UHFFFAOYSA-N 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 230000036642 wellbeing Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/068—Microemulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Dermatology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dispersion Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses emulsion preparation method and cosmetic composition containing lacquer tree seed extract.The present invention is, with lacquer tree seed extract as primary raw material, to mainly contain lacquer tree fat, lacquer tree seed nucleolus oil, paint seed polysaccharide, paint seed peel vegetable protein.Said composition can be used in cosmetic formulations, have functions that skin care, moisturizing, anti-oxidant, anti-inflammation, wrinkle of skin improve and skin holding elasticity.
Description
Technical field
Field is utilized the present invention relates to natural products, and in particular to emulsion preparation method and change containing lacquer tree seed extract
Cosmetic compositions.
Background technology
Lacquer tree is that a kind of whole body is precious commodity trees.It is well known that paint wood is corrosion resistant moisture-proof high-quality timber;Originate from lacquer tree
Raw lacquer be production Super-ageing resistance anticorrosive paint, environmental top grade Urushiol furniture lacquer, exquisite raw lacquer, lacquerware furniture, raw lacquer wood ground
The important source material of lath etc., is currently the only natural, reproducible, excellent performance bion coating, have " coating it
The good reputation of king ";The leaf of lacquer tree, flower, fruit and dried lacquer are traditional traditional Chinese medical science medicinal materials.Lacquer tree seed has Development volue very high.Paint
Containing more than 35% wax and fatty acid material in the seeds of trees, the mixture of extraction is referred to as lacquer tree fat.Lacquer tree fat is the various fat of production
The important industrial chemicals of acid, fatty alkyl alcohol etc., application field is broad.50~55 DEG C of lacquer tree fat fusing point, normal temperature is solid-state, purified essence
It is made " Chinese haze tallow ".Haze tallow is the natural biological wax of excellent performance, is widely used, and global haze tallow market is main to be supplied by Japan
Should, claiming Japanese haze tallow, resource is very rare.Also containing high triacontanols such as n-octacosanol, triacontanols in lacquer tree fat, the former is generation
The generally acknowledged anti-fatigue effect material in boundary, the latter is a kind of natural plants growth regulator, person poultry harmless is had no side effect, to ring
Border is pollution-free, and Development volue is high.Paint seed nuclei is practically free of wax, fat content 12%~15%, and extract normal temperature is liquid, no
Saturated fatty acid(Oleic acid, linoleic acid)Content is up to 80%, is good edible vegetable oil.The crude protein content for painting seed reaches
20%, crude fiber content reaches 19%, and its cake protein matter and coarse-fibred content are above 31%, is the nutrient source of high-quality.But it is long
Since phase, China's extracting and based on utilizing with raw lacquer main to the utilization of lacquer tree resource, except a small number of regional utilization parts among the people
Lacquer tree seed produce haze tallow as edible oil outside, substantial amounts of lacquer tree seed be nobody shows any interest in, lacquer tree seed value do not obtain due exploitation
Utilize, cause the huge waste of resource.
Therefore, strengthening exploitation to lacquer tree resource, on the one hand can bring economic well-being of workers and staff higher, on the other hand can also with move back
Plough the technologies such as also woods, rural area plant structural adjustment to match, preserved the ecological environment in ecological aspect.
The present invention substantially increases the attached of raw material by lacquer tree seed being prepared into microemulsion and being applied in cosmetics
It is value added, it is that lacquer tree industry is applied to do beneficial practice in new high-tech product.
The content of the invention
It is an object of the invention to provide a kind of emulsion containing lacquer tree seed extract, and it is applied in cosmetics, product
Exploitation is conducive to accelerating lacquer tree industrialization pace, lacquer tree resource is obtained effective comprehensive development and utilization of more high added value.
It is an object of the invention to provide the emulsion containing lacquer tree seed extract, its concrete technology step is as follows:
Step(1), lacquer tree seed is first carried out into skin core separation;
Step(2), make lacquer tree seed peel by g:G solid-to-liquid ratios 1:25~45 ratio adds water and heating stirring is stand-by to being completely dissolved;
Step(3), after the mixed liquor filtering separation of solid and liquid in step 2, solution for later use;
Step(4), the solution in above-mentioned steps 3 is carried out into centrifugation removal of impurities;
Step(5), the solution in above-mentioned steps 4 is added into lacquer tree seed nucleolus oil and emulsifying agent, heating stirring emulsification;
Step(6), the emulsion mixture in above-mentioned steps 5 is used into high pressure Microfluidizer, emulsion forms size after homogeneous
It is the Submicron Emulsion of 90-130nm.
Wherein described emulsifying agent be fatty acid mono glycidol, sucrose ester, sorbose alcohol ester, phosphatide, lauric monoglyceride,
Any of one or more in methyl glycol fatty acid ester and unsaturated phosphatide group compares mixture.
The lacquer tree seed peel core separation method is the separation method described in patent of invention CN201410114946.0.
The lacquer tree seed nucleolus oil is that lacquer tree seed nuclei benevolence is obtained using conventional press method or lixiviation process.
Specific embodiment:
The present invention is described in further detail below by embodiment, but protection scope of the present invention is not limited in described
Hold.
Embodiment 1
Step(1), lacquer tree seed is first carried out into skin core separation;
Step(2), make lacquer tree seed peel by g:G solid-to-liquid ratios 1:25 ratio adds water, and is heated to 80 DEG C of stirring 30min stand-by;
Step(3), the mixed liquor in step 2 is first passed through into the filtering of 100 mesh filter screens again by after butterfly seperator separation of solid and liquid, it is molten
Liquid is stand-by;
Step(4), by the solution in above-mentioned steps 3 in centrifuge speed 6000r/min, time 20min carries out centrifugation removal of impurities;
Step(5), the solution in above-mentioned steps 4 is added into g:G mass ratioes 1:0.2 lacquer tree seed nucleolus oil and emulsifying agent aliphatic acid
Single glyceride(Both gross masses are step(2)The 20% of middle lacquer tree seed peel mass percent), it is heated to 60 DEG C of stirring 30min breasts
Change;
Step(6), the emulsion mixture in above-mentioned steps 5 is used into high pressure Microfluidizer, microjet is in 1000bar conditions
Under carry out three times and pass through, it is the Submicron Emulsion of 100nm that emulsion forms size after homogeneous.
Embodiment 2
Step(1), lacquer tree seed is first carried out into skin core separation;
Step(2), make lacquer tree seed peel by g:G solid-to-liquid ratios 1:45 ratio adds water, and it is stand-by to be heated to 95 DEG C of stirring 15min;
Step(3), 100 mesh filter screens that first pass through in step 2 are filtered again by the way that after butterfly seperator separation of solid and liquid, solution is treated
With;
Step(4), by the solution in above-mentioned steps 3 in centrifuge speed 10000r/min, time 10min carries out centrifugation removal of impurities;
Step(5), the solution in above-mentioned steps 4 is added into g:G mass ratioes 1:0.15 lacquer tree seed nucleolus oil and emulsifying agent phosphatide
(Both gross masses are step(2)The 15% of middle lacquer tree seed peel mass percent), it is heated to 70 DEG C of stirring 20min emulsifications;
Step(6), the emulsion mixture in above-mentioned steps 5 is used into high pressure Microfluidizer, microjet is in 1000bar conditions
Under carry out three times and pass through, it is the Submicron Emulsion of 105nm that emulsion forms size after homogeneous.
Claims (10)
1. emulsion preparation method and cosmetic composition containing lacquer tree seed extract, it is characterised in that contain lacquer tree fat, lacquer tree seed
Nucleolus oil, paint seed polysaccharide, paint seed peel vegetable protein.
2. the emulsion preparation method of lacquer tree seed extract is contained according to claim 1, it is characterised in that including:
Step(1), lacquer tree seed is first carried out into skin core separation;
Step(2), make lacquer tree seed peel by g:G solid-to-liquid ratios 1:25~45 ratio adds water and heating stirring is stand-by to being completely dissolved;
Step(3), by step(2)In mixed liquor filtering separation of solid and liquid after, solution for later use;
Step(4), by above-mentioned steps(3)In solution carry out centrifugation removal of impurities;
Step(5), by above-mentioned steps(4)In solution add lacquer tree seed nucleolus oil and emulsifying agent, heating stirring emulsification;
Step(6), by above-mentioned steps(5)In emulsion mixture use high pressure Microfluidizer, emulsion is formed greatly after homogeneous
Small is the Submicron Emulsion of 90-130nm.
3. the emulsion preparation method of lacquer tree seed extract is contained according to claim 2, it is characterised in that:Mentioned emulsifier is
Fatty acid mono glycidol, sucrose ester, sorbose alcohol ester, phosphatide, lauric monoglyceride, methyl glycol fatty acid ester and unsaturated phosphorus
At least one in fat group.
4. a kind of cosmetic composition, it is characterised in that:Relative to the gross weight of cosmetic composition, comprising 1~50 weight hundred
Divide the emulsion containing lacquer tree seed extract of ratio.
5. cosmetic composition according to claim 4, it is characterised in that:The formulation of above-mentioned cosmetic composition is cosmetic
Water, massage cream, nourishing cream, facial mask, sun screen, vanishing cream, eye cream, shampoo, hair conditioner, shower cream, soap, toothpaste, emulsion,
Creams, gel.
6. cosmetic composition according to claim 4, it is characterised in that:Above-mentioned cosmetic composition is skin moisture-keeping
With.
7. cosmetic composition according to claim 4, it is characterised in that:Above-mentioned cosmetic composition is skin-whitening
With.
8. cosmetic composition according to claim 4, it is characterised in that:Above-mentioned cosmetic composition changes for wrinkle of skin
Kind and skin keeps elasticity to use.
9. cosmetic composition according to claim 4, it is characterised in that:Above-mentioned cosmetic composition is that skin is anti-oxidant
With.
10. cosmetic composition according to claim 4, it is characterised in that:Above-mentioned cosmetic composition is antibacterial skin
Anti-inflammatory is used.
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CN201710128430.5A CN106727058A (en) | 2017-03-06 | 2017-03-06 | Emulsion preparation method and cosmetic composition containing lacquer tree seed extract |
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Cited By (5)
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CN108478494A (en) * | 2018-06-08 | 2018-09-04 | 中华全国供销合作总社南京野生植物综合利用研究所 | A kind of all natural shampoo |
CN108587319A (en) * | 2018-08-05 | 2018-09-28 | 王忠良 | A kind of wood wax based ink and preparation method thereof |
CN108619061A (en) * | 2018-07-11 | 2018-10-09 | 广东泓睿科技有限公司 | A kind of chest enlarge lotion and preparation method thereof |
CN108653096A (en) * | 2018-07-11 | 2018-10-16 | 中山市智联企业孵化器发展有限公司 | A kind of skin daily nursing liquid and preparation method thereof |
CN109953906A (en) * | 2017-12-24 | 2019-07-02 | 王忠良 | A kind of natural wood wax-based lipstick and preparation method thereof |
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CN109953906A (en) * | 2017-12-24 | 2019-07-02 | 王忠良 | A kind of natural wood wax-based lipstick and preparation method thereof |
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CN108653096A (en) * | 2018-07-11 | 2018-10-16 | 中山市智联企业孵化器发展有限公司 | A kind of skin daily nursing liquid and preparation method thereof |
CN108587319A (en) * | 2018-08-05 | 2018-09-28 | 王忠良 | A kind of wood wax based ink and preparation method thereof |
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Application publication date: 20170531 |