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CN106621745A - Bamboo joint series-combined vacuum-pumping exhaust gas purification pipe - Google Patents

Bamboo joint series-combined vacuum-pumping exhaust gas purification pipe Download PDF

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Publication number
CN106621745A
CN106621745A CN201611215558.7A CN201611215558A CN106621745A CN 106621745 A CN106621745 A CN 106621745A CN 201611215558 A CN201611215558 A CN 201611215558A CN 106621745 A CN106621745 A CN 106621745A
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Prior art keywords
pipe
purification pipe
head
tail gas
separator tube
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张磊
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Jiangnan University
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Jiangnan University
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/26Drying gases or vapours
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/30Particle separators, e.g. dust precipitators, using loose filtering material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/38Removing components of undefined structure
    • B01D53/44Organic components
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/74General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/74General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/86Catalytic processes
    • B01D53/8678Removing components of undefined structure
    • B01D53/8687Organic components

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Separation Of Gases By Adsorption (AREA)

Abstract

本发明涉及一种竹节串联组合式抽真空尾气净化管,包括头段带进气口外螺纹缓冲管、尾段带出气口内螺纹缓冲管和至少一个两端分别有内外螺纹并一端有带孔隙封头的中段净化管,所述竹节串联组合式抽真空尾气净化管的中段净化管通过内外螺纹依次连接,然后与首尾段缓冲管通过对应的螺纹连接组合,所述竹节串联组合式抽真空尾气净化管的中段净化管可根据不同的化学反应系统填充干燥剂、吸附剂、氧化剂、还原剂、催化剂、滤棉等,所述中段净化管的带孔隙封头的孔隙直径小于填充的干燥剂、吸附剂、氧化剂、还原剂、催化剂等直径。有益效果为:有效净化真空尾气,保护真空泵;拆卸方便,减少制作成本。

The invention relates to a bamboo joint series combined vacuum exhaust gas purification pipe, which comprises an externally threaded buffer pipe with an air inlet at the head section, an internally threaded buffer pipe with an air outlet at the tail section, and at least one of the two ends respectively having internal and external threads and one end having a hole. The middle purification pipe of the head, the middle purification pipe of the bamboo joint series combined vacuum exhaust gas purification pipe is sequentially connected through internal and external threads, and then combined with the head and tail section buffer pipes through corresponding thread connections, the bamboo joint series combined vacuum exhaust gas purification pipe The middle purification pipe of the vacuum tail gas purification pipe can be filled with desiccant, adsorbent, oxidant, reducing agent, catalyst, filter cotton, etc. according to different chemical reaction systems, and the pore diameter of the porous head of the middle purification pipe is smaller than the filled dry Diameters of agents, adsorbents, oxidizing agents, reducing agents, catalysts, etc. The beneficial effects are: effectively purifying the vacuum tail gas, protecting the vacuum pump; being convenient to disassemble and reducing the production cost.

Description

一种竹节串联组合式抽真空尾气净化管A bamboo joint series combined vacuum exhaust gas purification pipe

技术领域technical field

本发明属于实验器材领域,尤其涉及使用真空泵的化学实验反应系统的保护真空泵的装置,The invention belongs to the field of experimental equipment, in particular to a device for protecting a vacuum pump of a chemical experiment reaction system using a vacuum pump,

背景技术Background technique

目前化学实验抽真空的反应系统,在真空状态下反应器内的少量有机溶媒汽化后会同气相一抽到真空泵中,有机溶媒进入真空泵是真空抽力下降,甚至导致机械故障,影响真空泵寿命。公知的方法为加装多组玻璃干燥塔或冷凝器,但玻璃干燥塔,稳定性差,易倒伏,易堵塞;冷凝器占用空间大,耗能高,操作时具有一定危险性,效果也一般。At present, in the vacuum reaction system of chemical experiments, a small amount of organic solvent in the reactor will be vaporized and pumped into the vacuum pump together with the gas phase in the vacuum state. When the organic solvent enters the vacuum pump, the vacuum pumping force will drop, and even cause mechanical failure, affecting the life of the vacuum pump. The known method is to add multiple groups of glass drying towers or condensers, but the glass drying towers have poor stability, are prone to lodging, and are easy to block; the condensers take up a lot of space, consume high energy, are dangerous to operate, and have mediocre effects.

发明内容Contents of the invention

为了解决上述问题,提供一种保护真空泵的装置,发明了一种竹节串联组合式抽真空尾气净化管,本发明不但能有效净化抽真空尾气,改善有机溶媒夹带使真空泵真空抽力下降甚至发生机械故障的现象,还具有结构简单、体积小、稳定性好、易维护、安全耐用的优点。In order to solve the above problems, a device for protecting the vacuum pump is provided, and a bamboo joint series combined vacuum exhaust gas purification tube is invented. The invention can not only effectively purify the vacuum exhaust gas, but also improve the entrainment of organic solvents, so that the vacuum pumping force of the vacuum pump decreases or even occurs. It also has the advantages of simple structure, small size, good stability, easy maintenance, safety and durability.

本发明解决其技术问题所采用的技术方案是:The technical solution adopted by the present invention to solve its technical problems is:

所述竹节串联组合式抽真空尾气净化管,包括头段带进气口外螺纹缓冲管、尾段带出气口内螺纹缓冲管和至少一个两端分别有内外螺纹并一端有带孔隙封头的中段净化管,所述竹节串联组合式抽真空尾气净化管的中段净化管通过内外螺纹依次连接,然后与首尾两段缓冲管通过对应的螺纹连接组合,所述竹节串联组合式抽真空尾气净化管的中段净化管可根据不同的化学反应系统填充干燥剂、吸附剂、氧化剂、还原剂、催化剂、滤棉等,所述中段净化管的带孔隙封头的孔隙直径小于填充的干燥剂、吸附剂、氧化剂、还原剂、催化剂等直径。The bamboo joint series combined vacuum exhaust gas purification pipe includes an externally threaded buffer pipe with an air inlet at the head section, an internally threaded buffer pipe with an air outlet at the tail section, and at least one with internal and external threads at both ends and a cap with a hole at one end. The middle section of the purification pipe, the middle section of the bamboo joint series combined vacuum exhaust gas purification pipe is sequentially connected through internal and external threads, and then combined with the first and last two buffer pipes through corresponding thread connections, the bamboo joint series combined vacuum exhaust gas The middle purification pipe of the purification pipe can be filled with desiccant, adsorbent, oxidizing agent, reducing agent, catalyst, filter cotton, etc. according to different chemical reaction systems. Diameter of adsorbent, oxidizing agent, reducing agent, catalyst, etc.

所述竹节串联组合式抽真空尾气净化管的进一步设计在于,所述净化管采用透明玻璃、树脂材料及不锈钢材料的一种或多种。A further design of the bamboo joint series combined vacuum exhaust gas purification pipe is that the purification pipe is made of one or more of transparent glass, resin material and stainless steel material.

所述竹节串联组合式抽真空尾气净化管的进一步设计在于,所述中间段净化管的外径为4-10cm,长度为12-25cm,首尾两段缓冲管的外径为4-15cm,长度为3-10cm。The further design of the bamboo joint series combined vacuum exhaust gas purification pipe is that the outer diameter of the middle section of the purification pipe is 4-10cm, the length is 12-25cm, and the outer diameter of the first and last two buffer pipes is 4-15cm. The length is 3-10cm.

所述竹节串联组合式抽真空尾气净化管的进一步设计在于,所述首段缓冲管的进气口的管径为5-10mm,长度为3-6cm,尾段缓冲管的出气口的管径为5-10mm,长度为3-6cm。The further design of the bamboo joint series combined vacuum exhaust gas purification pipe is that the pipe diameter of the air inlet of the first section buffer pipe is 5-10mm, and the length is 3-6cm, and the pipe of the air outlet of the tail section buffer pipe The diameter is 5-10mm, and the length is 3-6cm.

所述竹节串联组合式抽真空尾气净化管的进一步设计在于,所述中段净化管的带孔隙封头可以位于外螺纹一端,也可以位于内螺纹一端。The further design of the bamboo joint series combined vacuum exhaust gas purification pipe is that the end of the middle purification pipe with holes can be located at the end of the external thread or at the end of the internal thread.

所述竹节串联组合式抽真空尾气净化管的进一步设计在于,所述中段净化管的带孔隙封头的孔径为2-15mm,并均部于封头处。The further design of the bamboo joint series combined vacuum exhaust gas purification pipe is that the hole diameter of the head with holes in the middle section of the purification pipe is 2-15 mm, and all of them are located at the head.

所述竹节串联组合式抽真空尾气净化管的进一步设计在于,所述首段缓冲管的进气口可以是直型或90°弯曲,尾段缓冲管的出气口可以是直型或90°弯曲。The further design of the bamboo joint series combined vacuum exhaust gas purification pipe is that the air inlet of the first section buffer pipe can be straight or bent at 90°, and the air outlet of the tail section buffer pipe can be straight or 90° bending.

所述竹节串联组合式抽真空尾气净化管的进一步设计在于,所述首段缓冲管的进气口可以位于缓冲管的尾端或者侧端,尾段缓冲管的出气口可以位于缓冲管的尾端或者侧端。The further design of the bamboo joint series combined vacuum exhaust gas purification pipe is that the air inlet of the first section buffer pipe can be located at the tail end or side end of the buffer pipe, and the air outlet of the tail section buffer pipe can be located at the end of the buffer pipe. end or side.

所述竹节串联组合式抽真空尾气净化管的进一步设计在于,所述首段缓冲管的封头可以圆形封头、椭圆封头或者直型封头,尾段缓冲管的封头可以圆形封头、椭圆封头或者直型封头。The further design of the bamboo joint series combined vacuum exhaust gas purification pipe is that the head of the first buffer pipe can be a circular head, an elliptical head or a straight head, and the head of the tail buffer pipe can be round. Shaped head, oval head or straight head.

本发明的优点如下:The advantages of the present invention are as follows:

本发明的竹节串联组合式抽真空尾气净化管不但能有效净化抽真空尾气,改善有机溶媒夹带使真空泵真空抽力下降甚至发生机械故障的现象,还具有结构简单、体积小、稳定性好、拆卸方便,便于更换耗材,易维护、安全耐用的优点。The bamboo joint series combined vacuum exhaust gas purification tube of the present invention can not only effectively purify the vacuum exhaust gas, but also improve the phenomenon that the organic solvent is entrained to cause the vacuum pumping force of the vacuum pump to drop or even cause mechanical failure. It also has the advantages of simple structure, small volume, good stability, Easy to disassemble, easy to replace consumables, easy to maintain, safe and durable.

附图说明Description of drawings

图1为竹节串联组合式抽真空尾气净化管的内部结构图Figure 1 is the internal structure diagram of the bamboo joint series combined vacuum exhaust gas purification pipe

图2为尾段内螺纹缓冲管结构图Figure 2 is the structural diagram of the internally threaded buffer tube at the tail section

图3为中段净化管结构图Figure 3 is the structural diagram of the middle purification pipe

图4为头段外螺纹缓冲管结构图Figure 4 is the structural diagram of the externally threaded buffer tube at the head section

1-为进气口,2为头段缓冲管,3-中段净化管,4-中段净化管,5-尾段缓冲管1- is the air inlet, 2 is the head buffer pipe, 3- the middle purification pipe, 4- the middle purification pipe, 5- the tail buffer pipe

具体实施方式detailed description

下面结合附图对本发明方案进行详细说明。The solution of the present invention will be described in detail below in conjunction with the accompanying drawings.

如图1,本实施例提供的竹节串联组合式抽真空尾气净化管,包括头段带进气口外螺纹缓冲管、尾段带出气口内螺纹缓冲管和两个两端分别有内外螺纹并一端有带孔隙封头的中段净化管,竹节串联组合式抽真空尾气净化管的中段净化管通过内外螺纹依次连接,然后与首尾两段缓冲管通过对应的螺纹连接组合;如图3,中段净化管填充干燥剂、氧化剂,中段净化管的带孔隙封头的孔隙直径为2mm。如图2,尾段缓冲管出气口的管径为8mm,长度为4cm。如图4,头段缓冲管进气口的管径为8mm,长度为4cm。另一方面,中段净化管可以为1个或多个,原理同上,不再赘述。As shown in Figure 1, the bamboo joint series combined vacuum exhaust gas purification pipe provided in this embodiment includes a head section with an externally threaded buffer pipe with an air inlet, a tail section with an internally threaded buffer pipe with an air outlet, and two internally and externally threaded buffer pipes at both ends. One end has a middle-section purification pipe with a porous head, and the middle-section purification pipe of the bamboo joint series combined vacuum exhaust gas purification pipe is sequentially connected through internal and external threads, and then combined with the first and last two buffer pipes through corresponding thread connections; as shown in Figure 3, the middle section The purification pipe is filled with desiccant and oxidant, and the pore diameter of the head with pores in the middle purification pipe is 2mm. As shown in Figure 2, the diameter of the gas outlet of the tail section buffer tube is 8mm and the length is 4cm. As shown in Figure 4, the diameter of the air inlet of the buffer tube at the head section is 8mm and the length is 4cm. On the other hand, there can be one or more purification pipes in the middle section, and the principle is the same as above, which will not be repeated here.

进一步的,本实施例的净化管采用透明树脂或玻璃材料。Further, the purification pipe of this embodiment is made of transparent resin or glass.

更为优选地,中段净化管的外径为6cm,长度为15cm,头段缓冲管的外径为6cm,长度为5cm,尾段缓冲管的外径为6cm,长度为5cm。More preferably, the outer diameter of the middle purification tube is 6 cm and the length is 15 cm, the outer diameter of the head buffer tube is 6 cm and the length is 5 cm, and the outer diameter of the tail buffer tube is 6 cm and the length is 5 cm.

本实施例的竹节串联组合式抽真空尾气净化管不但能有效的去除真空系统的尾气杂质,降低真空损失。另一方面净化管拆卸方便,便于更换耗材并大大地减少制作成本。The bamboo joint series combined vacuum exhaust gas purification pipe of this embodiment can not only effectively remove impurities in the exhaust gas of the vacuum system, but also reduce vacuum loss. On the other hand, the purification pipe is easy to disassemble, which is convenient for replacing consumables and greatly reduces the production cost.

Claims (9)

1. a kind of ring serial combination type vacuumizes tail gas clean-up pipe, including head section inlet external screw thread separator tube, rear band Gas outlet internal thread separator tube and at least one two ends have internal and external threads respectively and there is the purification of the stage casing with hole end socket pipe one end, The ring serial combination type is vacuumized the stage casing purification pipe of tail gas clean-up pipe and is sequentially connected by internal and external threads, then with head and the tail By corresponding threaded connection combination, the ring serial combination type vacuumizes the stage casing purification of tail gas clean-up pipe to two sections of separator tubes Pipe can, adsorbent desiccant-filled according to different chemical reaction systems, oxidant, reducing agent, catalyst, filter pulp etc., it is described Drier, adsorbent, oxidant, reducing agent, catalyst of the pore diameter with hole end socket of stage casing purification pipe less than filling Equal diameter.
2. according to claim 1 ring serial combination type vacuumizes tail gas clean-up pipe, it is characterised in that the purification pipe is adopted With one or more of clear glass, resin material and stainless steel material.
3. according to claim 2 ring serial combination type vacuumizes tail gas clean-up pipe, it is characterised in that interlude purification pipe External diameter be 4-10cm, length is 12-25cm, head and the tail two sections of separator tubes external diameter be 4-15cm, length is 3-10cm.
4. according to claim 3 ring serial combination type vacuumizes tail gas clean-up pipe, it is characterised in that stage casing purification pipe Band hole end socket may be located at external screw thread one end, it is also possible to positioned at internal thread one end.
5. ring serial combination type vacuumizes tail gas clean-up pipe according to right wants 4, it is characterised in that stage casing purifies the band of pipe The aperture of hole end socket is 2-15mm, and portion is at end socket.
6. according to claim 1 ring serial combination type vacuumizes tail gas clean-up pipe, it is characterised in that first section separator tube The caliber of air inlet is 5-10mm, and length is 3-6cm, and the caliber of the gas outlet of rear separator tube is 5-10mm, and length is 3- 6cm。
7. according to claim 6 ring serial combination type vacuumizes tail gas clean-up pipe, it is characterised in that first section separator tube Air inlet can be straight type or 90 ° of bendings, and the gas outlet of rear separator tube can be straight type or 90 ° of bendings.
8. according to claim 7 ring serial combination type vacuumizes tail gas clean-up pipe, it is characterised in that first section separator tube Air inlet may be located at the tail end or side of separator tube, the gas outlet of rear separator tube may be located at the tail end of separator tube or Side.
9. according to claim 8 ring serial combination type vacuumizes tail gas clean-up pipe, it is characterised in that first section separator tube End socket can with circular head, ellipse head or straight type end socket, the end socket of rear separator tube can with circular head, ellipse head or The straight type end socket of person.
CN201611215558.7A 2016-12-26 2016-12-26 Bamboo joint series-combined vacuum-pumping exhaust gas purification pipe Withdrawn CN106621745A (en)

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Cited By (3)

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CN108392946A (en) * 2018-04-13 2018-08-14 河南科技大学第附属医院 A kind of flue-gas purification equipment of double-pole electric coagulation forceps
CN111013268A (en) * 2019-12-09 2020-04-17 安徽科杰粮保仓储设备有限公司 Method and equipment for vacuum pumping of closed environment in granary
CN112843976A (en) * 2020-12-28 2021-05-28 江苏菲沃泰纳米科技股份有限公司 Tail gas filter equipment and coating equipment

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