CN106609333A - Industrial titanium alloy and preparation method - Google Patents
Industrial titanium alloy and preparation method Download PDFInfo
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- CN106609333A CN106609333A CN201611157725.7A CN201611157725A CN106609333A CN 106609333 A CN106609333 A CN 106609333A CN 201611157725 A CN201611157725 A CN 201611157725A CN 106609333 A CN106609333 A CN 106609333A
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- titanium
- titanium alloy
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- 229910001069 Ti alloy Inorganic materials 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 46
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 17
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000010936 titanium Substances 0.000 claims abstract description 17
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 17
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims abstract description 16
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims abstract description 16
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 16
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052804 chromium Inorganic materials 0.000 claims abstract description 16
- 239000011651 chromium Substances 0.000 claims abstract description 16
- 229910052735 hafnium Inorganic materials 0.000 claims abstract description 16
- VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052750 molybdenum Inorganic materials 0.000 claims abstract description 16
- 239000011733 molybdenum Substances 0.000 claims abstract description 16
- 229910052758 niobium Inorganic materials 0.000 claims abstract description 16
- 239000010955 niobium Substances 0.000 claims abstract description 16
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052702 rhenium Inorganic materials 0.000 claims abstract description 16
- WUAPFZMCVAUBPE-UHFFFAOYSA-N rhenium atom Chemical compound [Re] WUAPFZMCVAUBPE-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052715 tantalum Inorganic materials 0.000 claims abstract description 16
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052720 vanadium Inorganic materials 0.000 claims abstract description 16
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052726 zirconium Inorganic materials 0.000 claims abstract description 16
- 239000000956 alloy Substances 0.000 claims description 21
- 229910045601 alloy Inorganic materials 0.000 claims description 20
- 239000011230 binding agent Substances 0.000 claims description 15
- 238000010438 heat treatment Methods 0.000 claims description 6
- 238000005266 casting Methods 0.000 claims description 3
- 239000012153 distilled water Substances 0.000 claims description 3
- 238000005242 forging Methods 0.000 claims description 3
- 238000002844 melting Methods 0.000 claims description 3
- 230000008018 melting Effects 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000000853 adhesive Substances 0.000 abstract 1
- 230000001070 adhesive effect Effects 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- 230000007797 corrosion Effects 0.000 description 3
- 238000005260 corrosion Methods 0.000 description 3
- 229910000883 Ti6Al4V Inorganic materials 0.000 description 2
- 229910021330 Ti3Al Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000007634 remodeling Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C30/00—Alloys containing less than 50% by weight of each constituent
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/02—Making non-ferrous alloys by melting
- C22C1/03—Making non-ferrous alloys by melting using master alloys
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/06—Making non-ferrous alloys with the use of special agents for refining or deoxidising
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C14/00—Alloys based on titanium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/16—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
- C22F1/18—High-melting or refractory metals or alloys based thereon
- C22F1/183—High-melting or refractory metals or alloys based thereon of titanium or alloys based thereon
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Forging (AREA)
Abstract
The invention discloses industrial titanium alloy and a preparation method. The industrial titanium alloy is composed of the following components in parts by mass:40-45 parts of titanium, 10-15 parts of aluminum, 5-10 parts of iron, 5-8 parts of molybdenum, 5-6 parts of niobium, 3-5 parts of tantalum, 3-4 parts of vanadium, 1-2 parts of chromium, 1-2 parts of zirconium, 1-2 parts of rhenium, 1-2 parts of hafnium, 5-6 parts of glycerinum and 1-2 parts of an adhesive. The titanium alloy disclosed by the invention is relatively good in mechanical property and suitable for industrial application.
Description
Technical field
The present invention relates to metal alloy compositions field, in particular to a kind of industrial titanium alloy and preparation method thereof.
Background technology
At present, many countries all recognize the importance of titanium alloy material in the world, and in succession which is researched and developed, and
It is applied.First practical titanium alloy is the Ti-6Al-4V alloys that the U.S. in 1954 succeeds in developing, due to it
Thermostability, intensity, plasticity, toughness, formability, solderability, corrosion resistance and biocompatibility are preferable, and become titanium alloy industry
In trump alloy, the alloy usage amount accounted for the 75%～85% of whole titanium alloys.Other many titanium alloys can be seen as
It is the remodeling of Ti-6Al-4V alloys.50～sixties of 20th century, mainly develop the high-temperature titanium alloy and machine of aero-engine
The structural titanium alloy of body, develops a collection of corrosion resistant Ti alloy the seventies, since the eighties, corrosion resistant Ti alloy and high-strength titanium alloy
It is further developed.The use temperature of heat-resistant titanium alloy has brought up to 600～650 DEG C of the nineties from the 400 of the fifties DEG C.
The appearance of A2 (Ti3Al) and r (TiAl) based alloy, make titanium the use position of electromotor just by electromotor cold end (fan and
Compressor) advance to hot junction (turbine) direction of electromotor.Structural titanium alloy is to high-strength, high-plastic, high-strength and high ductility, high-moduluss and height
Damage tolerance direction is developed.Titanium alloy also has certain shortcoming in mechanical performance and tensile property at present.
The content of the invention
For the problems referred to above, the invention provides a kind of industrial titanium alloy and preparation method.
For achieving the above object, the present invention provides following technical scheme：
40～45 parts of titanium, 10～15 parts of aluminum, 5～10 parts of ferrum, 5～8 parts of molybdenum, 5～6 parts of niobium, 3～5 parts of tantalum, 3～4 parts of vanadium,
1～2 part of chromium, 1～2 part of zirconium, 1～2 part of rhenium, 1～2 part of hafnium, 5～6 parts of glycerol, 1～2 part of binding agent.
Further, it is made up of following mass fraction formula components：40 parts of titanium, 10 parts of aluminum, 5 parts of ferrum, 5 parts of molybdenum, 5 parts of niobium, tantalum 3
Part, 3 parts of vanadium, 1 part of chromium, 1 part of zirconium, 1 part of rhenium, 1 part of hafnium, 5 parts of glycerol, 1 part of binding agent.
Further, it is made up of following mass fraction formula components：45 parts of titanium, 15 parts of aluminum, 10 parts of ferrum, 8 parts of molybdenum, 6 parts of niobium, tantalum
5 parts, 4 parts of vanadium, 2 parts of chromium, 2 parts of zirconium, 2 parts of rhenium, 2 parts of hafnium, 6 parts of glycerol, 2 parts of binding agent.
Further, it is made up of following mass fraction formula components：42 parts of titanium, 12 parts of aluminum, 7 parts of ferrum, 7 parts of molybdenum, 5 parts of niobium, tantalum 4
Part, 3 parts of vanadium, 1 part of chromium, 2 parts of zirconium, 1 part of rhenium, 2 parts of hafnium, 5 parts of glycerol, 2 parts of binding agent.
Further：Preparation method of the present invention has following steps：
Titanium, ferrum are melted and are made intermediate alloy 1 by step one, and aluminum, molybdenum are melted and intermediate alloy 2 is made, then refine
Intermediate alloy 1 and 2 makes intermediate alloy 3；
Step 2, niobium, tantalum, vanadium, chromium, zirconium, rhenium, hafnium is melted and adds that intermediate alloy 3 mixes and melting is made from power consumption
Pole；
The consutrodes are carried out cogging casting by step 3, and temperature is 1000～1200 DEG C, makes middle base 1；
Step 4, middle base 1 is forged, and forging temperature is 700～750 DEG C, makes middle base 2；
Middle base 2 is carried out cured, makes middle base 3 by step 5.
Step 6, middle base 3 is added in container 1, adds glycerol and binding agent, is subsequently adding distilled water and was not had powder
Till, stirred 2 hours using motor stirrer, after stirring, add heating in baking oven, 1 hour heat time heating time of 100 DEG C of heating-up temperature,
Obtain middle base 4；
Step 7, by middle base 4 dry-mixed 5～6 hours, makes middle base 5；
Step 8, middle base 5 is poured into a mould, and pouring temperature is 1250 DEG C, makes finished product.
The invention has the beneficial effects as follows：
1st, titanium alloy mechanical strength of the invention is big；
2nd, titanium alloy of the invention has certain draftability；
3rd, titanium alloy preparation method of the invention is simple.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the invention, rather than the embodiment of whole.Based in the present invention
Embodiment, the every other embodiment obtained under the premise of creative work is not made by those of ordinary skill in the art, all
Belong to the scope of protection of the invention.
Embodiment one：
A kind of industrial titanium alloy, is made up of following mass fraction formula components：40～45 parts of titanium, 10～15 parts of aluminum, ferrum 5
～10 parts, 5～8 parts of molybdenum, 5～6 parts of niobium, 3～5 parts of tantalum, 3～4 parts of vanadium, 1～2 part of chromium, 1～2 part of zirconium, 1～2 part of rhenium, hafnium 1～2
Part, 5～6 parts of glycerol, 1～2 part of binding agent.
Embodiment two：
A kind of industrial titanium alloy, is made up of following mass fraction formula components：40 parts of titanium, 10 parts of aluminum, 5 parts of ferrum, molybdenum 5
Part, 5 parts of niobium, 3 parts of tantalum, 3 parts of vanadium, 1 part of chromium, 1 part of zirconium, 1 part of rhenium, 1 part of hafnium, 5 parts of glycerol, 1 part of binding agent.
Embodiment three：
A kind of industrial titanium alloy, is made up of following mass fraction formula components：45 parts of titanium, 15 parts of aluminum, 10 parts of ferrum, molybdenum 8
Part, 6 parts of niobium, 5 parts of tantalum, 4 parts of vanadium, 2 parts of chromium, 2 parts of zirconium, 2 parts of rhenium, 2 parts of hafnium, 6 parts of glycerol, 2 parts of binding agent.
Example IV：
A kind of industrial titanium alloy, is made up of following mass fraction formula components：42 parts of titanium, 12 parts of aluminum, 7 parts of ferrum, molybdenum 7
Part, 5 parts of niobium, 4 parts of tantalum, 3 parts of vanadium, 1 part of chromium, 2 parts of zirconium, 1 part of rhenium, 2 parts of hafnium, 5 parts of glycerol, 2 parts of binding agent.
Embodiment five：
A kind of industrial titanium alloy its preparation method comprises the steps：
Titanium, ferrum are melted and are made intermediate alloy 1 by step one, and aluminum, molybdenum are melted and intermediate alloy 2 is made, then refine
Intermediate alloy 1 and 2 makes intermediate alloy 3；
Step 2, niobium, tantalum, vanadium, chromium, zirconium, rhenium, hafnium is melted and adds that intermediate alloy 3 mixes and melting is made from power consumption
Pole；
The consutrodes are carried out cogging casting by step 3, and temperature is 1000～1200 DEG C, makes middle base 1；
Step 4, middle base 1 is forged, and forging temperature is 700～750 DEG C, makes middle base 2；
Middle base 2 is carried out cured, makes middle base 3 by step 5.
Step 6, middle base 3 is added in container 1, adds glycerol and binding agent, is subsequently adding distilled water and was not had powder
Till, stirred 2 hours using motor stirrer, after stirring, add heating in baking oven, 1 hour heat time heating time of 100 DEG C of heating-up temperature,
Obtain middle base 4；
Step 7, by middle base 4 dry-mixed 5～6 hours, makes middle base 5；
Step 8, middle base 5 is poured into a mould, and pouring temperature is 1250 DEG C, makes finished product.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of description is only that those skilled in the art should for clarity
Using description as an entirety, the technical scheme in each embodiment can also Jing it is appropriately combined, form those skilled in the art
Understandable other embodiment.
Claims (5)
1. a kind of industrial titanium alloy, it is characterised in that：It is made up of following mass fraction formula components：
40～45 parts of titanium, 10～15 parts of aluminum, 5～10 parts of ferrum, 5～8 parts of molybdenum, 5～6 parts of niobium, 3～5 parts of tantalum, 3～4 parts of vanadium, chromium 1～
2 parts, 1～2 part of zirconium, 1～2 part of rhenium, 1～2 part of hafnium, 5～6 parts of glycerol, 1～2 part of binding agent.
2. a kind of industrial titanium alloy according to claim 1, it is characterised in that：By following mass fraction formula components group
Into：
40 parts of titanium, 10 parts of aluminum, 5 parts of ferrum, 5 parts of molybdenum, 5 parts of niobium, 3 parts of tantalum, 3 parts of vanadium, 1 part of chromium, 1 part of zirconium, 1 part of rhenium, 1 part of hafnium, glycerol 5
Part, 1 part of binding agent.
3. a kind of industrial titanium alloy according to claim 1, it is characterised in that：By following mass fraction formula components group
Into：
45 parts of titanium, 15 parts of aluminum, 10 parts of ferrum, 8 parts of molybdenum, 6 parts of niobium, 5 parts of tantalum, 4 parts of vanadium, 2 parts of chromium, 2 parts of zirconium, 2 parts of rhenium, 2 parts of hafnium, glycerol
6 parts, 2 parts of binding agent.
4. a kind of industrial titanium alloy according to claim 1, it is characterised in that：By following mass fraction formula components group
Into：
42 parts of titanium, 12 parts of aluminum, 7 parts of ferrum, 7 parts of molybdenum, 5 parts of niobium, 4 parts of tantalum, 3 parts of vanadium, 1 part of chromium, 2 parts of zirconium, 1 part of rhenium, 2 parts of hafnium, glycerol 5
Part, 2 parts of binding agent.
5. a kind of a kind of preparation method of industrial titanium alloy according to claim 1, it is characterised in that：Including following step
Suddenly：
Titanium, ferrum are melted and are made intermediate alloy 1 by step one, aluminum, molybdenum are melted and intermediate alloy 2 is made, then in the middle of refine
Alloy 1 and 2 makes intermediate alloy 3；
Step 2, niobium, tantalum, vanadium, chromium, zirconium, rhenium, hafnium is melted and adds that intermediate alloy 3 mixes and consutrodes are made in melting；
The consutrodes are carried out cogging casting by step 3, and temperature is 1000～1200 DEG C, makes middle base 1；
Step 4, middle base 1 is forged, and forging temperature is 700～750 DEG C, makes middle base 2；
Middle base 2 is carried out cured, makes middle base 3 by step 5.
Step 6, middle base 3 is added in container 1, adds glycerol and binding agent, is subsequently adding distilled water and was not had the powder to be
Only, stirred 2 hours using motor stirrer, heating, 1 hour heat time heating time of 100 DEG C of heating-up temperature in baking oven are added after stirring, is obtained
To middle base 4；
Step 7, by middle base 4 dry-mixed 5～6 hours, makes middle base 5；
Step 8, middle base 5 is poured into a mould, and pouring temperature is 1250 DEG C, makes finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611157725.7A CN106609333A (en) | 2016-12-15 | 2016-12-15 | Industrial titanium alloy and preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611157725.7A CN106609333A (en) | 2016-12-15 | 2016-12-15 | Industrial titanium alloy and preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106609333A true CN106609333A (en) | 2017-05-03 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611157725.7A Pending CN106609333A (en) | 2016-12-15 | 2016-12-15 | Industrial titanium alloy and preparation method |
Country Status (1)
| Country | Link |
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| CN (1) | CN106609333A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107775287A (en) * | 2017-10-24 | 2018-03-09 | 宝鸡金恒瑞金属科技有限公司 | A kind of preparation method of titanium alloy bicycle frame |
| CN109338158A (en) * | 2018-12-24 | 2019-02-15 | 南通金源智能技术有限公司 | 3D printing titanium alloy powder and its atomization production |
| CN115652141A (en) * | 2022-11-18 | 2023-01-31 | 厦门九牧研发有限公司 | Low-cost free-cutting antibacterial titanium alloy and preparation method of titanium alloy faucet |
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| CN101921930A (en) * | 2010-09-16 | 2010-12-22 | 上海交通大学 | Multi-component microalloyed titanium alloy and preparation method thereof |
| CN102936673A (en) * | 2012-12-04 | 2013-02-20 | 西北有色金属研究院 | Titanium alloy for spring parts and preparation method of alloy |
| CN105925845A (en) * | 2016-07-11 | 2016-09-07 | 东北大学 | High-strength, high-plasticity and corrosion-resistant titanium alloy, preparation method thereof and application thereof |
-
2016
- 2016-12-15 CN CN201611157725.7A patent/CN106609333A/en active Pending
Patent Citations (3)
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|---|---|---|---|---|
| CN101921930A (en) * | 2010-09-16 | 2010-12-22 | 上海交通大学 | Multi-component microalloyed titanium alloy and preparation method thereof |
| CN102936673A (en) * | 2012-12-04 | 2013-02-20 | 西北有色金属研究院 | Titanium alloy for spring parts and preparation method of alloy |
| CN105925845A (en) * | 2016-07-11 | 2016-09-07 | 东北大学 | High-strength, high-plasticity and corrosion-resistant titanium alloy, preparation method thereof and application thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107775287A (en) * | 2017-10-24 | 2018-03-09 | 宝鸡金恒瑞金属科技有限公司 | A kind of preparation method of titanium alloy bicycle frame |
| CN109338158A (en) * | 2018-12-24 | 2019-02-15 | 南通金源智能技术有限公司 | 3D printing titanium alloy powder and its atomization production |
| CN115652141A (en) * | 2022-11-18 | 2023-01-31 | 厦门九牧研发有限公司 | Low-cost free-cutting antibacterial titanium alloy and preparation method of titanium alloy faucet |
| CN115652141B (en) * | 2022-11-18 | 2023-09-01 | 厦门九牧研发有限公司 | Preparation method of low-cost free-cutting antibacterial titanium alloy and titanium alloy faucet |
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