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CN106596400B - A kind of evaluating apparatus and experimental method of second contact surface bonding quality of cementing the well - Google Patents

A kind of evaluating apparatus and experimental method of second contact surface bonding quality of cementing the well Download PDF

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CN106596400B
CN106596400B CN201611247445.5A CN201611247445A CN106596400B CN 106596400 B CN106596400 B CN 106596400B CN 201611247445 A CN201611247445 A CN 201611247445A CN 106596400 B CN106596400 B CN 106596400B
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杨浩
吴少诚
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China University of Geosciences Beijing
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    • G01N19/04Measuring adhesive force between materials, e.g. of sealing tape, of coating
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    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
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Abstract

本发明公开了一种固井第二界面胶结质量的评价装置及实验方法,第二界面即水泥‑地层界面,由于井下隔层和水泥的低渗特性对地层中的流体起到了关键的封隔作用,因而第二界面窜流的根本原因是地层隔层与水泥的胶结质量差,所以固井第二界面胶结质量的评价主要考虑地层隔层与水泥的胶结。该装置在于解决此问题,但同时也可以评价水泥与其他地层的胶结情况。本发明一般采用钻井现场所采集的真实岩心进行实验,最大限度模拟现场界面胶结情况,实验原理可靠,实验结果与分析可为固井水泥第二界面胶结质量的评价提供重要参考,为工程设计提供重要的依据。

The invention discloses an evaluation device and an experimental method for the cementation quality of the second interface of well cementing. The second interface is the cement-formation interface. Due to the low-permeability characteristics of the downhole interlayer and cement, the fluid in the formation plays a key role in sealing Therefore, the root cause of channeling at the second interface is the poor bonding quality between the formation interlayer and cement, so the evaluation of the cementation quality at the second interface of cementing mainly considers the bonding between the formation interlayer and cement. This device aims to solve this problem, but at the same time it can also evaluate the bonding of cement to other formations. The present invention generally adopts the real rock core collected at the drilling site to carry out experiments to simulate the site interface cementation to the greatest extent. The experimental principle is reliable, and the experimental results and analysis can provide important references for the evaluation of the cementing quality of the second interface of the cementing cement and provide engineering design. important basis.

Description

一种固井第二界面胶结质量的评价装置及实验方法An evaluation device and experimental method for the cementation quality of the second interface of well cementing

技术领域technical field

本发明属于油气井固井第二胶结界面即地层与水泥环界面的评价技术领域,具体涉及一种固井第二界面胶结质量的评价装置及实验方法。The invention belongs to the technical field of evaluation of the second cementing interface of oil and gas well cementing, that is, the interface between the formation and the cement sheath, and in particular relates to an evaluation device and an experimental method for the cementing quality of the second cementing interface of well cementing.

背景技术Background technique

固井质量的好坏影响着后期安全稳定生产的进行和各个增产措施的可行性。固井第二界面,即地层与水泥环的胶结界面,由于存在较为松散的泥饼以及地层流体,使水泥环凝固后易被剥落,胶结强度下降,相比第一界面更容易发生窜层。因而,第二界面的抗气窜能力是更需要重视的一个问题。The quality of cementing affects the safe and stable production in the later stage and the feasibility of various stimulation measures. The second interface of cementing, that is, the cemented interface between the formation and the cement sheath, due to the presence of relatively loose mud cake and formation fluid, makes the cement sheath easy to peel off after solidification, and the cementation strength decreases. Compared with the first interface, layer channeling is more likely to occur. Therefore, the anti-gas channeling ability of the second interface is a problem that needs more attention.

对于第二界面胶结状况的评价是固井质量评价中一直存在的亟待解决的问题,常用的测井技术也难以给出具体的评价结果。而目前室内实验评价主要由两方面来确定,一是采用剪切胶结强度,二是水力胶结强度。前者目前有较多的研究,如杨振杰(杨振杰,梁红军,李锋,等.固井界面胶结强度试验仪:CN202381076U[P].2012.)、程荣超(程荣超,步玉环,王瑞和.高炉矿渣改善固井水泥界面胶结性能研究[J].天然气工业,2007,27(2):63-66.)等都采用该原理进行了第二界面胶结评价的研究,但采用该原理进行测试所得到的结果无法直接给出胶结面可以承受的地层窜流压力,同时胶结强度的大小与防窜能力无法建立关系,如胶结面存在裂缝,实际地层已经发生窜流,但是测试显示的剪切胶结强度仍可能很大。可见,该种评价方法存在问题。后者采用水力胶结强度评价,实质是评价界面的抗窜能力,以窜流压力作为评价固井二界面防窜能力指标。与井下情况符合,评价方法和得出的参数具有直接的指导意义。顾军(顾军,杨卫华,秦文政,等.固井二界面封隔能力评价方法研究[J].石油学报,2008,29(3):451-454.)提出了一种评价第二界面封固能力的方法,但该方法采用的是人造岩心,而且未能充分模拟泥饼形成与冲洗,模型过于理想化。郭小阳提出了一种高温高压下一、二两个胶结界面的胶结能力评价装置(郭小阳,张凯,李早元,等.高温高压固井一、二界面封固能力测试装置及方法[P].四川:CN104406910A,2015-03-11.),该装置虽可对固井第二胶结界面进行,但其采用的是人造岩心模拟地层,其胶结状况与井下第二界面的真实情况存在较大差异;同时该装置可测量一、二两个胶结界面,可能会导致流体在两个界面的互窜,如本是测量第一界面的气体由于第一界面的胶结强度远大于第二界面,使得气体窜至第二界面等现象,影响实验结果,尤其是第二胶结界面的窜流通道有多个,如岩心本身、岩心与水泥环的胶结面等,该装置无法区分气窜的气体来源于哪条通道,故该仪器存在较多不合理之处。The evaluation of the cementation status of the second interface is an urgent problem to be solved in the evaluation of cementing quality, and it is difficult to give specific evaluation results by common logging techniques. At present, the indoor experimental evaluation is mainly determined by two aspects, one is the shear bond strength, and the other is the hydraulic bond strength. There are many studies on the former, such as Yang Zhenjie (Yang Zhenjie, Liang Hongjun, Li Feng, etc. Cementing Interface Bond Strength Tester: CN202381076U[P].2012.), Cheng Rongchao (Cheng Rongchao, Bu Yuhuan, Wang Ruihe. BF Research on cementing performance of slag improving cement interface[J]. Natural Gas Industry, 2007, 27 (2): 63-66.) etc. have used this principle to carry out the research on the second interface cementation evaluation, but using this principle to test The results obtained cannot directly give the formation channeling pressure that the cemented surface can bear, and the relationship between the cementation strength and the anti-channeling ability cannot be established. Intensity can still be great. It can be seen that there are problems in this evaluation method. The latter uses hydraulic cement strength evaluation, which essentially evaluates the anti-channeling ability of the interface, and uses the channeling pressure as an index to evaluate the anti-channeling ability of the cementing interface. In line with the downhole situation, the evaluation method and the obtained parameters have direct guiding significance. Gu Jun (Gu Jun, Yang Weihua, Qin Wenzheng, et al. Research on the evaluation method of the sealing ability of the second interface of cementing[J]. Acta Petroleum Sinica, 2008,29(3):451-454.) proposed a method for evaluating the second interface However, this method uses artificial cores and cannot fully simulate the formation and flushing of mud cakes, and the model is too ideal. Guo Xiaoyang proposed a high-temperature and high-pressure cementing ability evaluation device for the first and second cementing interfaces (Guo Xiaoyang, Zhang Kai, Li Zaoyuan, et al. Device and method for testing the sealing capacity of the first and second interfaces of high-temperature and high-pressure well cementing[P].Sichuan : CN104406910A, 2015-03-11.), although this device can carry out to the cementing second cementing interface, what it adopts is artificial rock core simulation stratum, and there is big difference between its cementing state and the real situation of the downhole second interface; At the same time, the device can measure the first and second cemented interfaces, which may cause the fluid to cross between the two interfaces. For example, the gas at the first interface is measured because the cementation strength of the first interface is much greater than that of the second interface. Phenomena such as the second interface, etc., affect the experimental results, especially the channeling of the second cemented interface has multiple channels, such as the core itself, the cemented surface of the core and the cement sheath, etc., the device cannot distinguish which channel the gas channeling comes from Channel, so there are many unreasonable things in this instrument.

目前的研究中,模拟地层有些采用没有渗透性的金属薄片,使固井第二界面的胶结质量评价不具有参考价值。也有采用人造岩心模拟地层,但是未说明人造岩心对实际地层的模拟方法和是否达到现场地层物性参数,不符合现场情况,同时人造岩心根据井下要求实际尺寸很大,压制困难,成本高,实验周期长,采用的人造岩心制造不符合现场情况,模拟结果参考价值低,基本不具有实际参考价值。In the current research, some non-permeable metal sheets are used in the simulated formations, so the evaluation of the cementation quality of the second cementing interface has no reference value. There are also artificial cores used to simulate strata, but it does not explain how the artificial core simulates the actual stratum and whether it meets the physical parameters of the on-site stratum. Long, the man-made core used does not conform to the site conditions, the reference value of the simulation results is low, and basically has no actual reference value.

发明内容Contents of the invention

为了克服背景技术所述的不足,本发明提供了一种固井第二界面胶结质量的评价装置及实验方法,该装置使用的岩心尺寸小,克服了对岩心需求过大的问题,且能形成泥饼,可以直接用现场岩心,也可以用人造岩心,根据地层岩石全岩、粘土成分、粒度分布、渗透率、孔隙度、油气水饱和度等资料,人工压制模拟地层的人造岩心。此外,该装置对岩心采用了岩心帽处理,将第一界面、第二界面以及岩心本身渗透三条可能发生气窜的通道分离开,能准确地获得第二界面气窜的压力及流量。In order to overcome the deficiencies described in the background technology, the present invention provides an evaluation device and an experimental method for the cementing quality of the second cementing interface. Mud cakes can be directly used on-site cores or artificial cores. According to the data of the whole rock, clay composition, particle size distribution, permeability, porosity, oil-gas-water saturation and other data of the formation rocks, the artificial cores of the simulated formations are artificially pressed. In addition, the device adopts a core cap treatment for the core, which separates the first interface, the second interface and the core itself from the three channels where gas channeling may occur, and can accurately obtain the pressure and flow rate of the second interface gas channeling.

本发明解决其技术问题所采用的技术方案是:The technical solution adopted by the present invention to solve its technical problems is:

一种固井第二界面胶结质量的评价装置,包括釜体,釜体内部设置有岩心,岩心与釜体之间设置有水泥环;岩心顶部套有岩心帽,岩心帽下缘与水泥环之间设置有间隙;岩心底部设置有羊毛垫,羊毛垫居中可固定岩心,并防止水泥浆流入下堵头上的高压气体管道;水泥环外侧面与釜体内侧面紧密组成第一界面气窜通道,岩心外侧面与水泥环内侧面紧密组成第二界面气窜通道。An evaluation device for the cementing quality of the second interface of well cementing, comprising a kettle body, a core is arranged inside the kettle body, a cement sheath is arranged between the core and the kettle body; There is a gap between them; there is a wool pad at the bottom of the core, and the wool pad is in the middle to fix the core and prevent the cement slurry from flowing into the high-pressure gas pipeline on the lower plug; the outer side of the cement ring and the inner side of the kettle body closely form the first interface gas channel, The outer surface of the core and the inner surface of the cement sheath closely constitute the second interface gas channeling channel.

所述岩心为真实岩心,岩心直径在25mm到50mm之间,高度50mm,如没有地下实际地层钻取的岩心,可以采用钻屑压制,或根据地层岩石全岩、粘土成分、粒度分布、渗透率、孔隙度、油气水饱和度等资料,人工压制模拟地层的人造岩心。The core is a real core with a diameter between 25mm and 50mm and a height of 50mm. If there is no core drilled from the actual underground strata, it can be pressed with cuttings, or according to the whole rock, clay composition, particle size distribution, and permeability of the stratum. , porosity, oil-gas-water saturation and other data, and artificially suppress the artificial core of the simulated formation.

所述的间隙使第二界面气窜气体逸出,岩心帽中心有孔和管线与岩心体渗透气体通道相连,即可分离开第二界面气窜的气体和从岩心本身渗透过的气体。The gap allows gas channeling from the second interface to escape, and the hole in the center of the core cap and the pipeline are connected to the permeable gas channel of the core body, so that the gas channeling from the second interface can be separated from the gas permeating through the core itself.

所述的釜体外侧面紧密设置有加热套,加热套内部设置有热电偶,用于加热使用,加热套外侧面紧密设置有保温层,用于保温。A heating jacket is closely arranged on the outer surface of the kettle body, a thermocouple is arranged inside the heating jacket for heating, and an insulation layer is arranged closely on the outer surface of the heating jacket for heat preservation.

所述的釜体上部分连接上端盖,上端盖下部设置有上陶瓷垫圈和上堵头,上陶瓷垫圈用于用以隔热,上堵头上设置有密封圈、第一界面气窜气体收集口、岩心体渗透气体收集口和第二界面气窜气体收集口,密封圈用以分隔开第一、第二界面发生气窜时的气体,第一界面气窜气体收集口用于收集水泥环与釜体内表面形成的第一胶结界面发生气窜时逸出的气体,岩心体渗透气体收集口用于收集岩心本身渗透过的气体,第二界面气窜气体收集口用于收集岩心与水泥环形成的第二界胶结面发生气窜时逸出的气体,该装置中,第一界面、第二界面和岩心本身渗透过的气窜气体均被单独分离开,可准确获知第二界面发生气窜时的压力和流量。The upper part of the kettle body is connected to the upper end cover, and the lower part of the upper end cover is provided with an upper ceramic gasket and an upper plug. port, core body infiltration gas collection port and second interface gas channeling gas collection port, the sealing ring is used to separate the gas when gas channeling occurs at the first and second interfaces, and the first interface gas channeling gas collection port is used to collect cement The first cemented interface formed by the ring and the inner surface of the kettle is the gas that escapes when gas channeling occurs. The core body infiltration gas collection port is used to collect the gas permeated by the core itself, and the second interface gas channeling gas collection port is used to collect the core and cement. The gas that escapes when gas channeling occurs on the cemented surface of the second interface formed by the ring, in this device, the gas channeling gas permeated through the first interface, the second interface and the core itself are all separated separately, and the occurrence of the second interface can be accurately known. Pressure and flow during gas blow-by.

所述的釜体下部分连接下端盖,下端盖上表面依次紧密设置有下陶瓷垫圈、下封头和下堵头,下堵头与釜体的间隙处设置有石墨填料,石墨填料保证密封性能,下陶瓷垫圈用以隔热,下堵头中轴线方向设置有高压气体管道,通过高压气体管道向该装置输入高压空气或高压流体;下堵头与水泥环之间设置有过气槽,通过高压气体管道输入的高压气体经过羊毛垫和过气槽流至岩心、水泥环下部,模拟井下气窜。The lower part of the kettle body is connected to the lower end cover, and the upper surface of the lower end cover is closely arranged with a lower ceramic gasket, a lower head and a lower plug in sequence, and a graphite filler is arranged at the gap between the lower plug and the kettle body, and the graphite filler ensures the sealing performance , the lower ceramic gasket is used for heat insulation, and a high-pressure gas pipeline is arranged in the direction of the central axis of the lower plug, and high-pressure air or high-pressure fluid is input to the device through the high-pressure gas pipeline; there is an air passage between the lower plug and the cement ring, through The high-pressure gas input by the high-pressure gas pipeline flows through the wool pad and the gas channel to the core and the lower part of the cement sheath to simulate downhole gas channeling.

所述的高压气体管道连接两条管线:一是通过特殊单向阀连接气体压力表、气体稳压阀和氮气源,二是通过第一控制阀连接第一液压压力表和第一液压泵;第一条管路用于对该装置充入带有一定压力的氮气,模拟气窜以测试各个界面的胶结质量;第二条管路用于对该装置充入具有一定压力的流体,以清洗装置内部或在水泥环形成过程中形成养护压力。所述的特殊单向阀,只有在氮气源所释放出的压力大于釜体内液压的压力时才能被打开,并且流体只能进入釜体,不能返回氮气源,若氮气源释放气压小于釜体内液压时,氮气源释放的气体不能通过该阀门。The high-pressure gas pipeline is connected to two pipelines: one is to connect the gas pressure gauge, the gas regulator valve and the nitrogen source through a special one-way valve, and the other is to connect the first hydraulic pressure gauge and the first hydraulic pump through the first control valve; The first pipeline is used to fill the device with nitrogen with a certain pressure to simulate gas channeling to test the bonding quality of each interface; the second pipeline is used to fill the device with a certain pressure of fluid for cleaning Curing pressure builds up inside the unit or during cement sheath formation. The special one-way valve can only be opened when the pressure released by the nitrogen source is greater than the hydraulic pressure in the kettle body, and the fluid can only enter the kettle body and cannot return to the nitrogen source. If the pressure released by the nitrogen source is lower than the hydraulic pressure in the kettle body , the gas released from the nitrogen source cannot pass through the valve.

所述的第一界面气窜气体收集口、岩心体渗透气体收集口和第二界面气窜气体收集口分别通过管道连接第一界面气窜气体集气瓶、岩心体渗透气体集气瓶和第二界面气窜气体集气瓶;沿气体流动方向,每个管道上依次设置有回压阀、压力表和流量计;当气体发生气窜时,气体上逸并从最近的气体收集口逸出,通过相应的回压阀,经流量计记录流量大小并由各个集气瓶收集气体。由于各个界面通过的气体量较小,通过产生气泡即可观察是否有气体进入到集气瓶中,即可知各个界面的是否被击穿,界面发生气窜时气压大小可表征该界面的胶结质量。The first interface gas channeling gas collection port, the core body permeated gas collection port and the second interface gas channeling gas collection port are respectively connected to the first interface gas channeling gas collection bottle, the core body permeated gas gas collection bottle and the second interface gas channeling gas collection port through pipelines. Two-interface gas channeling gas collection cylinder; along the gas flow direction, each pipeline is provided with a back pressure valve, pressure gauge and flow meter in sequence; when gas channeling occurs, the gas escapes upward and escapes from the nearest gas collection port , through the corresponding back pressure valve, the flow rate is recorded by the flow meter and the gas is collected by each gas collection bottle. Since the amount of gas passing through each interface is small, you can observe whether there is gas entering the gas collecting bottle by generating bubbles, and you can know whether each interface is broken down. When gas channeling occurs at the interface, the air pressure can represent the cementation quality of the interface. .

所述的第一界面气窜气体收集口还通过管道连接第二控制阀、第三控制阀、第二液压压力表和第二液压泵,第二界面气窜气体收集口还通过管道连接至第二控制阀和第三控制阀之间的管道上,方便通过第一界面气窜气体收集口和第二界面气窜气体收集口向该装置中输入一定压力的液体,同时高压气体管道连通液压泵,可在水泥环下部注入一定压力的液体,上下挤压水泥环(上下的压力是相等的,否则水泥环可能发生位移),来模拟井下水泥环是受到的地层压力,以及本身自重或者上覆地层压力。The gas blow-by gas collection port of the first interface is also connected to the second control valve, the third control valve, the second hydraulic pressure gauge and the second hydraulic pump through pipelines, and the gas blow-by gas collection port of the second interface is also connected to the second control valve through pipelines. On the pipeline between the second control valve and the third control valve, it is convenient to input a certain pressure liquid into the device through the gas channeling gas collection port of the first interface and the gas channeling gas collection port of the second interface, and at the same time, the high pressure gas pipeline is connected with the hydraulic pump , a certain pressure liquid can be injected into the lower part of the cement sheath, and the cement sheath can be squeezed up and down (the upper and lower pressures are equal, otherwise the cement sheath may be displaced) to simulate the formation pressure of the downhole cement sheath, as well as its own weight or overlying formation pressure.

优选的,所述的热电偶、压力表、第二液压压力表、气体压力表、第一液压压力表和流量计分别电连接计算机,由计算机记录和分析数据。Preferably, the thermocouple, pressure gauge, second hydraulic pressure gauge, gas pressure gauge, first hydraulic pressure gauge and flowmeter are respectively electrically connected to a computer, and the data is recorded and analyzed by the computer.

一种固井第二界面胶结质量的评价装置的实验方法,包括如下步骤:An experimental method of an evaluation device for the cementing quality of the second interface of well cementing, comprising the following steps:

1)制备泥饼:将岩心烘干,放入岩心真空饱和装置中,抽真空处理,在抽真空环境下饱和地层钻井液,在岩心外表面形成泥饼,模拟地层泥饼的形成;1) Preparation of mud cake: drying the core, putting it into a core vacuum saturation device, vacuuming, saturating the formation drilling fluid in a vacuum environment, forming a mud cake on the outer surface of the core, and simulating the formation of the formation mud cake;

2)冲洗:泥饼形成后,将岩心放入该装置中并固定住,由高压气体管道泵入固井常用的冲洗液,由第一界面气窜气体收集口、第二界面气窜气体收集口以及岩心体渗透气体收集口流出,并持续一段时间,之后放掉冲洗液,换成隔离液根据实验需要循环一定时间后将装置内的液体全释放掉,模拟后续施工中冲洗液和隔离液对地层界面的作用;此处的冲洗液和隔离液根据具体的实验要求或者井下情况来确定选择何种冲洗液或隔离液;2) Flushing: After the mud cake is formed, the core is put into the device and fixed, and the flushing fluid commonly used in cementing is pumped into the high-pressure gas pipeline, and the gas channeling gas collection port of the first interface and the gas channeling gas of the second interface are collected After a period of time, the flushing fluid is released and replaced with an isolating fluid. After a certain period of circulation according to the experiment, all the liquid in the device is released to simulate the flushing fluid and isolating fluid in the subsequent construction. The effect on the formation interface; the flushing fluid and spacer fluid here are determined according to the specific experimental requirements or downhole conditions; which flushing fluid or spacer fluid to choose;

3)制备水泥环:取出岩心在岩心上套上岩心帽,在釜体中放入羊毛垫,之后将岩心放入釜体中的羊毛垫上并固定住,向岩心和釜体之间的环空处注入水泥浆,待注入水泥浆完毕后,盖上堵头、上陶瓷垫圈和上端盖,在第一液压泵和第二液压泵的作用下,通过高压气体管道、第一界面气窜气体收集口和第二界面气窜气体收集口注入水泥养护时所需压力的压力流体,模拟井下水泥环所受压力情况,压力流体可直接使用水或者中性的液压油;压力流体经过第一液压泵泵出,流经第一液压压力表,第一控制阀门进入水泥环下方;压力流体还经过第二液压泵泵出,流经第二液压压力表、第三控制阀门和第二界面气窜气体收集口以及流经第二液压压力表、第三控制阀门、第二控制阀门和第一界面气窜气体收集口两条途径进入水泥环上方;注入压力流体的目的:因为井下水泥环是受到地层压力的,同时本身自重或者上覆地层压力,因而为模拟这种压力,在这个装置中通过第一和第二液压泵向水泥环的上下面注入具有一定压力(该压力根据地层压力调整)的流体,上下挤压水泥环(上下的压力是相等的,否则水泥环可能发生位移),来模拟井下水泥环受到的压力情况;同时打开加热带加热至设定温度,根据实验以及实际需要,在一定的温度条件下养护,该温度由实验所模拟的地层温度决定,养护时间根据水泥浆的特性以及模拟的地层环境等因素决定,或者根据具体模拟的实验要求设定;3) Prepare the cement sheath: take out the rock core, put a core cap on the rock core, put a wool pad in the kettle body, then put the rock core on the wool pad in the kettle body and fix it, and move to the annulus between the rock core and the kettle body After the cement slurry is injected, cover the plug, the upper ceramic gasket and the upper end cover. Under the action of the first hydraulic pump and the second hydraulic pump, the gas channeling gas is collected through the high-pressure gas pipeline and the first interface. The pressure fluid required for cement curing is injected into the gas channeling port of the second interface and the gas channeling gas collection port of the second interface to simulate the pressure of the downhole cement sheath. The pressure fluid can directly use water or neutral hydraulic oil; the pressure fluid passes through the first hydraulic pump Pumped out, flows through the first hydraulic pressure gauge, and the first control valve enters under the cement sheath; the pressure fluid is also pumped out through the second hydraulic pump, flows through the second hydraulic pressure gauge, the third control valve and the gas channeling gas at the second interface The collection port and the second hydraulic pressure gauge, the third control valve, the second control valve and the first interface gas channeling gas collection port enter into the top of the cement sheath; the purpose of injecting pressure fluid: because the downhole cement sheath is affected by the formation pressure, and at the same time its own weight or the pressure of the overlying formation, so in order to simulate this pressure, in this device, the first and second hydraulic pumps are injected into the upper and lower sides of the cement sheath with a certain pressure (the pressure is adjusted according to the formation pressure). Fluid, squeeze the cement sheath up and down (the upper and lower pressures are equal, otherwise the cement sheath may be displaced) to simulate the pressure of the downhole cement sheath; at the same time, turn on the heating belt to heat to the set temperature, according to the experiment and actual needs, in the Curing under certain temperature conditions, the temperature is determined by the stratum temperature simulated by the experiment, and the curing time is determined according to the characteristics of the cement slurry and the simulated stratum environment and other factors, or set according to the specific simulated experimental requirements;

4)高压气体管道换接特殊单向阀,第一界面气窜气体收集口和第二界面气窜气体收集口换接回压阀,调整回压阀直到的釜体内部压力为水泥养护所需压力,因为釜体内部是存在压力流体的(之前注入用以模拟水泥环养护压力),所以回压阀即背压阀所承受的压力就设置为养护压力,而发生气窜时,下部高压气体窜至上部,使上部的压力升高,此时上部的压力便大于回压阀的压力,气体就会从回压阀流出,釜体内部压力降低,直到等于设定的水泥环养护压力值;4) The high-pressure gas pipeline is replaced with a special one-way valve, the gas channeling gas collection port of the first interface and the gas channeling gas collection port of the second interface are replaced with a back pressure valve, and the back pressure valve is adjusted until the internal pressure of the kettle body is required for cement maintenance Pressure, because there is pressure fluid inside the kettle body (previously injected to simulate the curing pressure of the cement ring), so the pressure on the back pressure valve, that is, the back pressure valve, is set as the curing pressure, and when gas channeling occurs, the lower high-pressure gas Go to the upper part to increase the pressure of the upper part. At this time, the pressure of the upper part will be greater than the pressure of the back pressure valve, the gas will flow out from the back pressure valve, and the internal pressure of the kettle body will decrease until it is equal to the set cement ring curing pressure value;

5)通入高压气体,逐渐增大气压,观察第二界面气窜气体集气瓶是否有气泡产生和气体气压表的压力变化,若出现气泡或气体气压表出现显著变化,则表明第二胶结界面处已窜通,此时气体气压表所得气压为第二胶结界面的抗窜压力大小,可表征第二胶结界面的胶结质量。5) Introduce high-pressure gas, gradually increase the air pressure, and observe whether there are bubbles in the second interface gas channeling gas collection bottle and the pressure change of the gas barometer. If there are bubbles or a significant change in the gas barometer, it indicates the second cemented interface At this time, the air pressure obtained by the gas barometer is the anti-channeling pressure of the second cemented interface, which can characterize the cementation quality of the second cemented interface.

优选的,在步骤1)中,岩心烘干的时间为45-50h,抽真空的时间为6-10h,岩心真空饱和装置中真空度不小于0.1MPa,饱和地层钻井液的时间为6-10h。Preferably, in step 1), the time for drying the core is 45-50h, the time for vacuuming is 6-10h, the vacuum degree in the core vacuum saturation device is not less than 0.1MPa, and the time for saturated formation drilling fluid is 6-10h .

本发明的优点是:The advantages of the present invention are:

1)本发明采用的岩心为真实岩心,且体积较小,克服了对岩心需求过大的问题,且能形成泥饼;1) the rock core that the present invention adopts is real rock core, and volume is less, overcomes the problem that the demand for rock core is too large, and can form mud cake;

2)本发明分离开了岩心在压力作用下可能出现的三条气体窜通通道(第一界面、第二界面、岩心本身),能准确地获得第二界面气窜的压力及流量,达到对第二界面胶接质量的准确表征;2) The present invention separates three gas channeling passages (the first interface, the second interface, and the core itself) that may occur in the core under pressure, and can accurately obtain the pressure and flow rate of the gas channeling at the second interface to achieve the goal of controlling the gas channeling of the second interface. Accurate characterization of the bonding quality of the two interfaces;

3)本发明还可可将养护水泥所用的压力流体改为腐蚀性流体,利用该装置可研究流体腐蚀性对水泥环防窜能力的影响;3) The present invention can also change the pressure fluid used for curing the cement into a corrosive fluid, and the device can be used to study the influence of fluid corrosiveness on the anti-channeling ability of the cement sheath;

4)本发明可以模拟高温高压下水泥环的抗气窜实验。4) The present invention can simulate the anti-gas channeling experiment of the cement sheath under high temperature and high pressure.

附图说明Description of drawings

图1为本发明结构示意图;Fig. 1 is a structural representation of the present invention;

图2为本发明岩心帽处的结构示意图。Fig. 2 is a schematic diagram of the structure at the core cap of the present invention.

具体实施方式Detailed ways

下面将结合附图对本发明作进一步的说明:The present invention will be further described below in conjunction with accompanying drawing:

实施例1:Example 1:

一种固井第二界面胶结质量的评价装置,包括釜体10,釜体10内部设置有岩心11,岩心11与釜体10之间设置有水泥环12;岩心11顶部套有岩心帽13,岩心帽13下缘与水泥环12之间设置有间隙14;岩心11底部设置有羊毛垫15;水泥环12与釜体10形成第一胶结界面16,岩心11与水泥环12形成第二胶结界面17。间隙14使第二界面气窜气体逸出,岩心帽13中心有孔和管线与岩心体渗透气体通道相连,即可分离开第二界面气窜的气体和从岩心11本身渗透过的气体。An evaluation device for cementing quality of the second interface of well cementing, comprising a kettle body 10, a rock core 11 is arranged inside the kettle body 10, a cement sheath 12 is arranged between the rock core 11 and the kettle body 10; a core cap 13 is set on the top of the rock core 11, A gap 14 is provided between the lower edge of the core cap 13 and the cement sheath 12; a wool pad 15 is provided at the bottom of the rock core 11; the cement sheath 12 and the kettle body 10 form a first cemented interface 16, and the rock core 11 and the cement sheath 12 form a second cemented interface 17. The gap 14 allows the second interface gas channeling gas to escape, and the center of the core cap 13 has holes and pipelines connected with the core body permeating gas channel, so that the gas channeling through the second interface can be separated from the gas permeating from the core 11 itself.

为了模拟地层温度对水泥环12胶结强度的影响,所述的釜体10外侧面紧密设置有加热套18,加热套18内部设置有热电偶,加热套18外侧面紧密设置有保温层19。In order to simulate the influence of formation temperature on the cement sheath 12 bonding strength, a heating jacket 18 is closely arranged on the outer surface of the kettle body 10, a thermocouple is arranged inside the heating jacket 18, and an insulating layer 19 is arranged closely on the outer surface of the heating jacket 18.

所述的釜体10上部分连接上端盖20,上端盖20下部设置有上陶瓷垫圈50和上堵头22,上堵头22上设置有密封圈23、第一界面气窜气体收集口24、岩心体渗透气体收集口25和第二界面气窜气体收集口26;密封圈23用以分隔开第一、第二界面发生气窜时的气体,第一界面气窜气体收集口24用于收集水泥环12与釜体10形成的第一胶结界面16发生气窜时逸出的气体,岩心体渗透气体收集口25用于收集岩心本身渗透过的气体,第二界面气窜气体收集口26用于收集岩心11与水泥环12形成的第二胶结界面17发生气窜时逸出的气体,该装置中,第一界面16、第二界面17和岩心11本身渗透过的气体均被单独分离开,可准确获知第二界面发生气窜时的压力和流量。The upper part of the kettle body 10 is connected to the upper end cover 20, and the lower part of the upper end cover 20 is provided with an upper ceramic gasket 50 and an upper plug 22, and the upper plug 22 is provided with a sealing ring 23, a first interface gas channeling gas collection port 24, The core body infiltration gas collection port 25 and the second interface gas channeling gas collection port 26; the sealing ring 23 is used to separate the gas when gas channeling occurs at the first and second interfaces, and the first interface gas channeling gas collection port 24 is used for Collect the escaped gas when the first cemented interface 16 formed by the cement sheath 12 and the kettle body 10 undergoes gas channeling. The core body infiltration gas collection port 25 is used to collect the gas permeated by the core itself. The second interface gas channeling gas collection port 26 It is used to collect the escaped gas when the second cemented interface 17 formed by the core 11 and the cement sheath 12 undergoes gas channeling. In this device, the gas permeated by the first interface 16, the second interface 17 and the core 11 itself are all separated separately The pressure and flow rate when gas channeling occurs at the second interface can be accurately known.

所述的釜体10下部分连接下端盖27,下端盖27上表面依次紧密设置有下陶瓷垫圈28、下封头29和下堵头30,下堵头30与釜体10的间隙处设置有石墨填料31,石墨填料31保证密封性能,下陶瓷垫圈28用以隔热,下堵头30中轴线方向设置有高压气体管道32,通过高压气体管道32向该装置输入高压空气或高压流体;下堵头30与水泥环12之间设置有过气槽33,通过高压气体管道32输入的高压气体经过羊毛垫15和过气槽33均分到岩心11、水泥环12的下部,模拟井下气窜条件。The lower part of the kettle body 10 is connected to the lower end cover 27, and the upper surface of the lower end cover 27 is closely arranged with a lower ceramic gasket 28, a lower sealing head 29 and a lower plug 30, and the gap between the lower plug 30 and the kettle body 10 is provided with a Graphite packing 31, graphite packing 31 guarantees the sealing performance, the lower ceramic gasket 28 is used for heat insulation, and the central axis direction of the lower plug 30 is provided with a high-pressure gas pipeline 32, and high-pressure air or high-pressure fluid is input to the device through the high-pressure gas pipeline 32; A gas passage 33 is provided between the plug 30 and the cement sheath 12, and the high-pressure gas input through the high-pressure gas pipeline 32 is evenly distributed to the lower part of the core 11 and the cement sheath 12 through the wool pad 15 and the gas passage 33, simulating downhole gas channeling condition.

所述的高压气体管道32连接两条管线:一是通过特殊单向阀34连接气体压力表35、气体稳压阀36和氮气源37,二是通过第一控制阀38连接第一液压压力表39和第一液压泵40;第一条管路用于对该装置充入带有一定压力的氮气,用于测试各个界面的胶结质量;第二条管路用于对该装置充入具有一定压力的流体,作为清洗装置内部和水泥环12形成过程中养护使用。The high-pressure gas pipeline 32 is connected to two pipelines: one is to connect the gas pressure gauge 35, the gas regulator valve 36 and the nitrogen source 37 through a special one-way valve 34; the other is to connect the first hydraulic pressure gauge through the first control valve 38 39 and the first hydraulic pump 40; the first pipeline is used to charge nitrogen with a certain pressure to the device, and is used to test the bonding quality of each interface; the second pipeline is used to charge the device with a certain pressure. The pressurized fluid is used for cleaning the interior of the device and for maintenance during the formation of the cement sheath 12 .

所述的第一界面气窜气体收集口24、岩心体渗透气体收集口25和第二界面气窜气体收集口26分别通过管道连接第一界面气窜气体集气瓶41、岩心体渗透气体集气瓶42和第二界面气窜气体集气瓶43;沿气体流动方向,每个管道上依次设置有回压阀44、压力表45和流量计46;当气体发生气窜时,气体上逸并从最近的气体收集口逸出,通过相应的回压阀44,经流量计46记录流量大小并由各个集气瓶收集气体。The first interface gas channeling gas collection port 24, the core body infiltration gas collection port 25 and the second interface gas channeling gas collection port 26 are respectively connected to the first interface gas channeling gas collection bottle 41 and the core body infiltration gas collection port 26 through pipelines. Gas cylinder 42 and second interface gas channeling gas collecting bottle 43; along the gas flow direction, each pipeline is provided with a back pressure valve 44, a pressure gauge 45 and a flow meter 46 in sequence; And escape from the nearest gas collection port, pass through the corresponding back pressure valve 44, record the flow size through the flow meter 46 and collect the gas by each gas collection bottle.

为了方便通过第一界面气窜气体收集口24和第二界面气窜气体收集口26向该装置中输入一定压力的液体,所述的第一界面气窜气体收集口24还通过管道连接第二控制阀47、第三控制阀48、第二液压压力表49和第二液压泵51,第二界面气窜气体收集口26还通过管道连接至第二控制阀47和第三控制阀48之间的管道上。In order to facilitate the input of a certain pressure liquid into the device through the first interface gas channeling gas collection port 24 and the second interface gas channeling gas collection port 26, the first interface gas channeling gas collection port 24 is also connected to the second interface gas channeling port through a pipeline. The control valve 47, the third control valve 48, the second hydraulic pressure gauge 49 and the second hydraulic pump 51, and the second interface blow-by gas collection port 26 are also connected between the second control valve 47 and the third control valve 48 through pipelines on the pipeline.

为了提高表征精度,本发明采用计算机记录和分析数据,热电偶、压力表45、第二液压压力表49、气体压力表35、第一液压压力表39和流量计46分别电连接计算机。In order to improve the characterization accuracy, the present invention uses a computer to record and analyze data, and the thermocouple, pressure gauge 45, second hydraulic pressure gauge 49, gas pressure gauge 35, first hydraulic pressure gauge 39 and flowmeter 46 are electrically connected to the computer respectively.

实施例2:Example 2:

采用实施例1所述的一种固井第二界面胶结质量的评价装置的实验方法,包括如下步骤:Adopt the experimental method of the evaluation device of a kind of cementing second interface cementing quality described in embodiment 1, comprise the steps:

1)制备泥饼:将岩心11烘干,放入岩心真空饱和装置中,抽真空处理,在抽真空环境下饱和地层钻井液,在岩心外表面模拟地层泥饼的形成;1) Preparation of mud cake: drying the core 11, putting it into a core vacuum saturation device, vacuuming, saturating the formation drilling fluid in a vacuum environment, and simulating the formation of formation mud cake on the outer surface of the core;

2)冲洗:泥饼形成后,将岩心11放入该装置中并固定住,由高压气体管道32泵入固井常用的冲洗液,由第一界面气窜气体收集口24、第二界面气窜气体收集口26以及岩心体渗透气体收集口25流出,并持续一段时间,之后放掉冲洗液,换成隔离液根据实验需要循环一定时间后将装置内的液体全释放掉,模拟后续施工中冲洗液和隔离液对地层界面的作用;2) Flushing: After the mud cake is formed, the rock core 11 is put into the device and fixed, and the flushing fluid commonly used in cementing is pumped in from the high-pressure gas pipeline 32, and the gas channeling from the first interface to the gas collection port 24, the second interface gas The channeling gas collection port 26 and the core body infiltration gas collection port 25 flow out, and last for a period of time, then release the flushing fluid and replace it with the spacer fluid, and release all the liquid in the device after circulating for a certain period of time according to the experimental requirements, simulating the subsequent construction The effect of flushing fluid and spacer fluid on the formation interface;

3)制备水泥环12:取出岩心11在岩心11上套上岩心帽13,在釜体10中放入羊毛垫15,之后将岩心11放入釜体10中的羊毛垫15上并固定住,向岩心11和釜体10之间的环空处注入水泥浆(水泥浆高度恰好淹没密封圈2~4cm),待注入水泥浆完毕后,盖上堵头20、上陶瓷垫圈50和上端盖22,在第一液压泵40和第二液压泵51的作用下,通过高压气体管道32、第一界面气窜气体收集口24和第二界面气窜气体收集口26注入水泥养护时所需压力的压力流体,同时打开加热带18加热至设定温度,根据实验以及实际需要,在一定的温度条件下养护;3) Prepare the cement sheath 12: take out the rock core 11, put a rock core cap 13 on the rock core 11, put a wool pad 15 in the kettle body 10, then put the rock core 11 into the wool pad 15 in the kettle body 10 and fix it, Inject cement slurry into the annular space between the rock core 11 and the kettle body 10 (the height of the cement slurry just submerges the sealing ring by 2 to 4 cm), and after the injection of the cement slurry is completed, cover the plug 20, the upper ceramic gasket 50 and the upper end cover 22 , under the action of the first hydraulic pump 40 and the second hydraulic pump 51, through the high-pressure gas pipeline 32, the first interface gas channeling gas collection port 24 and the second interface gas channeling gas collection port 26, the pressure required for cement curing Pressurized fluid, simultaneously turn on the heating belt 18 to heat to the set temperature, and maintain under certain temperature conditions according to the experiment and actual needs;

4)高压气体管道32换接特殊单向阀34,第一界面气窜气体收集口24和第二界面气窜气体收集口26换接回压阀44,调整回压阀44直到的釜体10内部压力为水泥养护所需压力;4) The high-pressure gas pipeline 32 is replaced with a special one-way valve 34, the first interface gas channeling gas collection port 24 and the second interface gas channeling gas collection port 26 are replaced with a back pressure valve 44, and the back pressure valve 44 is adjusted until the kettle body 10 The internal pressure is the pressure required for cement curing;

5)通入高压气体,逐渐增大气压,观察第二界面气窜气体集气瓶43是否有气泡产生和气体气压表的压力变化,若出现气泡或气体气压表35出现显著变化,则表明第二胶结界面处已窜通,此时气体气压表35所得气压为第二胶结界面的抗窜压力大小,可表征第二胶结界面的胶结质量。5) Feed high-pressure gas, gradually increase the air pressure, observe whether there are bubbles in the second interface gas channeling gas collecting bottle 43 and the pressure change of the gas barometer, if there are bubbles or significant changes in the gas barometer 35, it indicates that the second interface The cemented interface has channeled through. At this time, the air pressure obtained by the gas pressure gauge 35 is the anti-channeling pressure of the second cemented interface, which can represent the cemented quality of the second cemented interface.

其中,在步骤1)中,岩心烘干的时间为48h,抽真空的时间为24h,岩心真空饱和装置中真空度不小于0.1MPa,饱和地层钻井液的时间为24h。Wherein, in step 1), the time for drying the core is 48 hours, the time for vacuuming is 24 hours, the vacuum degree in the core vacuum saturation device is not less than 0.1 MPa, and the time for saturating the formation drilling fluid is 24 hours.

最后应说明的是:显然,上述实施例仅仅是为清楚地说明本发明所作的举例,而并非对实施方式的限定。对于所属领域的普通技术人员来说,在上述说明的基础上还可以做出其它不同形式的变化或变动。这里无需也无法对所有的实施方式予以穷举。而由此所引申出的显而易见的变化或变动仍处于本发明的保护范围之中。Finally, it should be noted that: obviously, the above-mentioned embodiments are only examples for clearly illustrating the present invention, rather than limiting the implementation. For those of ordinary skill in the art, on the basis of the above description, other changes or changes in different forms can also be made. It is not necessary and impossible to exhaustively list all the implementation manners here. However, obvious changes or modifications derived therefrom are still within the protection scope of the present invention.

Claims (4)

1. a kind of evaluating apparatus for second contact surface bonding quality of cementing the well, which is characterized in that including autoclave body, autoclave body is internally provided with rock The heart is provided with cement sheath between rock core and autoclave body;It is cased with rock core cap at the top of rock core, is provided between rock core cap lower edge and cement sheath Gap;Rock core bottom is provided with wool pad;Cement sheath lateral surface and autoclave body medial surface closely form the first interface has channeling channel, rock Facies lateralis cordis and cement sheath medial surface closely form second contact surface has channeling channel;
The autoclave body lateral surface is closely provided with heating mantle, and heating mantle is internally provided with thermocouple, and heating mantle lateral surface is close It is provided with insulating layer;
Upper end cover is partially connected on the autoclave body, upper end cover lower part is provided with upper plug head and upper ceramic washer, sets on upper plug head It is equipped with sealing ring, the first interface has channeling gas collection mouth, rock core body infiltration gas collection mouth and second contact surface has channeling gas collection Mouthful;
Partially connect lower cover under the autoclave body, lower end cap upper surface be successively closely provided with lower ceramic washer, lower head and The gap location of lower end cap, lower end cap and autoclave body is provided with graphite packing, and lower end cap central axes direction is provided with high-pressure gas pipelines, Air drain was provided between lower end cap and cement sheath;
The high-pressure gas pipelines connect two pipelines:First is that connecting gas gauge, gas pressure stabilizing by special check valve Valve and source nitrogen, second is that connecting the first hydraulic gage and the first hydraulic pump by the first control valve;
First interface has channeling gas collection mouth, rock core body infiltration gas collection mouth and the second contact surface has channeling gas collection mouth The first interface has channeling gas collection bottle is connected by pipeline respectively, rock core body permeates gas collection bottle and second contact surface has channeling gas Gas bottle;Along gas flow direction, back-pressure valve, pressure gauge and flowmeter are disposed on each pipeline;
The first interface has channeling gas collection mouth also connects the second control valve, third control valve, second hydraulic by pipeline Pressure gauge and the second hydraulic pump, second contact surface has channeling gas collection mouth also pass through pipeline and are connected to the second control valve and third control On pipeline between valve.
2. a kind of evaluating apparatus of second contact surface bonding quality of cementing the well as described in claim 1, which is characterized in that the heat Galvanic couple, pressure gauge, the second hydraulic gage, gas gauge, the first hydraulic gage and flowmeter are electrically connected computer.
3. a kind of experimental method of the evaluating apparatus using well cementation second contact surface bonding quality as claimed in claim 1 or 2, It is characterized in that, described method includes following steps:
1) mud cake is prepared:Rock core is dried, is put into rock core vacuum saturation device, vacuumize process, is satisfied in the case where vacuumizing environment With strata drilling liquid, in the formation of core outside surface simulated formation mud cake;
2) it rinses:After mud cake is formed, rock core is put into the device and is fixed, it is common to be pumped into well cementation by high-pressure gas pipelines Flushing liquor permeates gas collection by the first interface has channeling gas collection mouth, second contact surface has channeling gas collection mouth and rock core body Mouth outflow, and continue for some time, flushing liquor is bled off later, is changed insulating liquid into and is needed to recycle after a certain period of time according to experiment by dress Liquid in setting discharges entirely, simulates the effect of flushing liquor and insulating liquid to bed boundary in subsequent construction;
3) cement sheath is prepared:Removal of core covers rock core cap on rock core, and wool pad is put into autoclave body, is later put into rock core On wool pad in autoclave body and fix, to the annular space between rock core and autoclave body at inject cement slurry, cement slurry to be implanted finishes Afterwards, plug, upper ceramic washer and upper end cover are covered and passes through high pressure gas under the action of the first hydraulic pump and the second hydraulic pump The pressure of required pressure when pipeline, the first interface has channeling gas collection mouth and second contact surface has channeling gas collection mouth injection cement conservation Force flow body opens simultaneously heating tape and is heated to set temperature, according to experiment and actual needs, supports in a certain temperature conditions Protect appropriate time;
4) the special check valve of high-pressure gas pipelines changing-over, the first interface has channeling gas collection mouth and second contact surface has channeling gas collection Mouthful changing-over back-pressure valve adjusts back-pressure valve, sets the pressure of back-pressure valve as autoclave body internal pressure, i.e. pressure needed for cement conservation;
5) it is passed through high pressure gas by high-pressure gas pipelines, is gradually increased air pressure, whether is observation second contact surface has channeling gas collection bottle There is bubble to generate and the barometric pressure change of gas, if there is bubble or significant changes occurs in gas atmosphere table, shows the Alter logical at two cementation interfaces, air pressure obtained by gas atmosphere table at this time is that the anti-of the second cementation interface alters pressure size, can be characterized The bonding quality of second cementation interface.
4. experimental method as claimed in claim 3, which is characterized in that in step 1)In, the time of rock core drying is 45-50h, The time vacuumized is 6-10h, and vacuum degree is not less than 0.1MPa in rock core vacuum saturation device, is saturated the time of strata drilling liquid For 6-10h.
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